CN110261313A - A kind of distributed optical fiber acoustic sensor-based system for monitoring coke drum operation conditions on-line - Google Patents

A kind of distributed optical fiber acoustic sensor-based system for monitoring coke drum operation conditions on-line Download PDF

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Publication number
CN110261313A
CN110261313A CN201910370907.XA CN201910370907A CN110261313A CN 110261313 A CN110261313 A CN 110261313A CN 201910370907 A CN201910370907 A CN 201910370907A CN 110261313 A CN110261313 A CN 110261313A
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CN
China
Prior art keywords
coke drum
optical fiber
chirp grating
operation conditions
based system
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Pending
Application number
CN201910370907.XA
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Chinese (zh)
Inventor
童杏林
潘旭
邓承伟
张翠
冒燕
殷仁杰
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Beijing University of Chemical Technology
Wuhan University of Technology WUT
Sinopec Luoyang Guangzhou Engineering Co Ltd
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Wuhan University of Technology WUT
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Application filed by Wuhan University of Technology WUT filed Critical Wuhan University of Technology WUT
Priority to CN201910370907.XA priority Critical patent/CN110261313A/en
Publication of CN110261313A publication Critical patent/CN110261313A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10GCRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G55/00Treatment of hydrocarbon oils, in the absence of hydrogen, by at least one refining process and at least one cracking process
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/17Systems in which incident light is modified in accordance with the properties of the material investigated
    • G01N21/1702Systems in which incident light is modified in accordance with the properties of the material investigated with opto-acoustic detection, e.g. for gases or analysing solids
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N29/00Investigating or analysing materials by the use of ultrasonic, sonic or infrasonic waves; Visualisation of the interior of objects by transmitting ultrasonic or sonic waves through the object
    • G01N29/22Details, e.g. general constructional or apparatus details
    • G01N29/24Probes
    • G01N29/2418Probes using optoacoustic interaction with the material, e.g. laser radiation, photoacoustics
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/17Systems in which incident light is modified in accordance with the properties of the material investigated
    • G01N21/1702Systems in which incident light is modified in accordance with the properties of the material investigated with opto-acoustic detection, e.g. for gases or analysing solids
    • G01N2021/1704Systems in which incident light is modified in accordance with the properties of the material investigated with opto-acoustic detection, e.g. for gases or analysing solids in gases
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2291/00Indexing codes associated with group G01N29/00
    • G01N2291/02Indexing codes associated with the analysed material
    • G01N2291/023Solids
    • G01N2291/0234Metals, e.g. steel
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2291/00Indexing codes associated with group G01N29/00
    • G01N2291/02Indexing codes associated with the analysed material
    • G01N2291/025Change of phase or condition
    • G01N2291/0258Structural degradation, e.g. fatigue of composites, ageing of oils
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2291/00Indexing codes associated with group G01N29/00
    • G01N2291/10Number of transducers
    • G01N2291/106Number of transducers one or more transducer arrays
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2291/00Indexing codes associated with group G01N29/00
    • G01N2291/26Scanned objects
    • G01N2291/269Various geometry objects
    • G01N2291/2698Other discrete objects, e.g. bricks

Abstract

The invention discloses a kind of distributed optical fiber acoustic sensor-based systems for monitoring coke drum operation conditions on-line, including sequentially connected laser light source (1), isolator (2), optical circulator (3), multiple chirp grating acoustics sensor arrays (4), the output end of optical circulator (3) is also successively connect with signal processing unit (5), computer (6), and multiple chirp grating acoustics sensor arrays (3) are distributed in coke drum metal outer wall surface from top to bottom.The present invention realizes the on-line monitoring of STRENGTH ON COKE tower green coke and decoking process state, improves the degree of automation when measurement, eliminates security risk when manual work, improves work efficiency, reduce the labor intensity of worker.

Description

A kind of distributed optical fiber acoustic sensor-based system for monitoring coke drum operation conditions on-line
Technical field
The present invention relates to delayed coking unit detection technique fields, more specifically to a kind of on-line monitoring coke drum The distributed optical fiber acoustic sensor-based system of operation conditions.
Background technique
Delayed coking is very important process procedure in current petroleum refining production process, and removes in coke drum and produce Coke method be hydraulic decoking, its working principle is that being washed away using the impact force constant impingement coke inner wall of tower of high pressure water Coke simultaneously makes it fall off, and the coke to fall off clears out of tower from the chute of bottom.Currently, in the production process of petrochemical industry, The sound for listening water slug coke and tower wall by human ear by operator mostly, in conjunction with the coke in chute in observation tower bottom Charcoal water judges whether coke is removed completely, this results in operator that the position for needing to devoke can not be accurately positioned, so that weight It is high that burnt operating frequency is cut again, and working efficiency is relatively low.
External hydraulic decoking detection technique, which mainly has using tools such as tuning forks, at present is monitored, such monitoring technology May determine that whether coke is cleared, but there is also certain difficulties for the measurement for layer thickness variation of focusing, since such technology belongs to Electricity sensing measurement technology could be transmitted since the ultra-weak electronic signal that sensing generates has to pass through enhanced processing, it is necessary to from tower The corresponding processing circuit of installation is immediated vicinity, and takes technological processing for explosion protection feature, not only cost is excessively high, and because of the harsh ring on tower The long-term working stability in border, circuit system is poor, and accuracy of measurement is lower, limits technology oil refining enterprise at home It promotes and applies.
In recent years, domestic Liang Jia enterprise also had developed the real-time monitoring system of decoking, their system passes through centainly Mechanical structure and cooling method by tower wall vibration transmit and act on be evenly arranged on coking tower tower wall piezoelectric acceleration sense Device, to obtain the vibration signal of tower wall during hydraulic decoking, the situation devoked during monitoring hydraulic decoking.Such sensor It is lower to the sensitivity vibrated during hydraulic decoking, be typically only capable to monitor during hydraulic decoking coke it is whether cleared this One switching value of sample, that is, monitor decoking it is clean whether, during cutting coke thickness of coke layer change measurement in terms of exist be stranded It is difficult.
Currently, being applied in the industrial productions such as petrochemical industry, supervised using the artificial intelligence system of distributing optical fiber sensing The process for surveying hydraulic decoking has not been reported at home, not only to consider measurement accuracy and measurement efficiency problem, while also to overcome The problem of leading to security risk because of the system and device of installation at the scene.
Summary of the invention
To overcome defect of the existing technology, the present invention provides a kind of distribution for monitoring coke drum operation conditions on-line Optical fiber acoustic sensor-based system.
The purpose of the present invention is achieved through the following technical solutions:
The present invention designs a kind of distributed optical fiber acoustic sensor-based system for monitoring coke drum operation conditions on-line, including is sequentially connected Laser light source, isolator, optical circulator, multiple chirp grating acoustics sensor arrays, the output end of optical circulator also successively with Signal processing unit, computer connection, multiple chirp grating acoustics sensor arrays are distributed in coke drum metal outer wall from top to bottom Surface.
In the above scheme, the chirp grating acoustics sensor array is ultra-low reflectance chirp grating acoustics sensor battle array Column, reflectivity are lower than 0.4%.
In the above scheme, the surface of the chirp grating acoustics sensor array is coated with gold of the heatproof at 500 °C or more Belong to layer.
In the above scheme, the length of the chirp grating acoustics sensor array is higher by 5 ± 0.5 than the froth bed limit for height of setting Rice.
In the above scheme, the length of the chirp grating acoustics sensor array is 40 ± 1 meters.
In the above scheme, the spacing between adjacent chirp grating acoustics sensor array is 10 centimetres.
In the above scheme, the chirp grating that the chirp grating acoustics sensor array selects three dB bandwidth to be greater than 2nm.
In the above scheme, multiple chirp grating acoustics sensor arrays are fixed from top to bottom by high-temperature resistance adhesive In coke drum outer wall.
In the above scheme, the chirp grating acoustics sensor array passes through optical fiber and the laser light being arranged in Master Control Room Source is connected with signal processing unit.
Compared with prior art, the invention has the following advantages:
The present invention realizes the on-line monitoring of STRENGTH ON COKE tower green coke and decoking process state, improves the degree of automation when measurement, disappears Security risk when except manual work, improves work efficiency, and reduces the labor intensity of worker.
Detailed description of the invention
Present invention will be further explained below with reference to the attached drawings and examples, in attached drawing:
Fig. 1 is a kind of structural schematic diagram of distributed optical fiber acoustic sensor-based system for monitoring coke drum operation conditions on-line.
In figure: light source 1, optical circulator 3, chirp grating acoustics sensor array 4, signal processing unit 5, calculates isolator 2 Machine 6.
Specific embodiment
In order to make the objectives, technical solutions, and advantages of the present invention clearer, with reference to the accompanying drawings and embodiments, right The present invention is further elaborated.
As shown in Figure 1, the present invention provides a kind of distributed optical fiber acoustic sensing system for monitoring coke drum operation conditions on-line System, which can monitor the height of coke and froth bed during coke drum green coke, coke becomes in tower in water conservancy decoking process Change and cleared degree, the operation conditions of decoking device and fault condition, obtain the operation conditions of coke drum.
The system includes sequentially connected laser light source 1, isolator 2, optical circulator 3, multiple chirp grating acoustics sensors Array 4, the output end of optical circulator 3 are also successively connect with signal processing unit 5, computer 6, multiple chirp grating acoustics sensors Array 4 is distributed in coke drum metal outer wall surface.Light source 1, for issuing optical signal;Optical circulator 3, for transmitting optical signal To chirp grating acoustics sensor array 4.
Chirp grating acoustics sensor array 4 has ultra-low reflectance;To guarantee that chirp grating acoustics sensor array 4 can be (500 °C or more) normal use, surface metallization layer under high temperature;The length of chirp grating acoustics sensor array 4 compares coking The froth bed limit for height of enterprise's setting is 5 ± 0.5 meters high, and most preferred length is 40 ± 1 meters.Adjacent chirp grating acoustics sensor array Spacing between 4 is 10 centimetres, selects three dB bandwidth to be greater than the chirp grating of 2nm, to prevent grating to be adapted to;Multiple chirp gratings Acoustics sensor array 4 is arranged in coke drum outer wall by high-temp glue from top to bottom;Chirp grating acoustics sensor array 4 passes through optical fiber Be connected to the Master Control Room of enterprise, in Master Control Room laser light source and signal processing unit 5 be connected.
The light that laser light source 1 issues is by being distributed in multiple chirp grating acoustics sensor battle arrays on coke drum metal outer wall surface Column 4 can pass through signal processing unit with the acoustic signal of inner wall different parts in real-time detection coke drum green coke and decoking process The acoustical signal being collected into is changed into electric signal by 5, finally by artificial intelligence technology (chemical industry pipe of the building based on MLP neural network Road monitoring model and chemical pipeline corrosion condition monitoring model based on LSTM neural network) detectable signal of acquisition (is instructed Practice sample) it is analyzed, green coke coke in the process is obtained by being evenly arranged on the frequency signature signal of grating array of coke column overhead The height of coke and froth bed in charcoal tower, the frequency of the grating array by being evenly arranged on coke drum waist, amplitude Characteristics signal obtain The progress and cleared degree of coke in tower in water conservancy decoking process, supervised by the anomalous variation and disturbance of detectable signal frequency Survey coke collapse the decoking devices failure such as burnt burying occur before characteristic parameter, the extent of corrosion of coke inner wall of tower etc., and with enterprise Automatic control unit and administrative unit linkage, provide comprehensive technical parameter for the safety in production of coke drum and automation control.
The embodiment of the present invention is described in attached drawing, but the invention is not limited to above-mentioned specific embodiment parties Formula, the above mentioned embodiment is only schematical, rather than restrictive, and those skilled in the art are in this hair Under bright enlightenment, without breaking away from the scope protected by the purposes and claims of the present invention, many forms can be also made, this It is belonged within protection of the invention a bit.

Claims (9)

1. a kind of distributed optical fiber acoustic sensor-based system for monitoring coke drum operation conditions on-line, which is characterized in that including successively The laser light source (1) of connection, isolator (2), optical circulator (3), multiple chirp grating acoustics sensor arrays (4), optical circulator (3) output end is also successively connect with signal processing unit (5), computer (6), multiple chirp grating acoustics sensor arrays (3) It is distributed in coke drum metal outer wall surface.
2. the distributed optical fiber acoustic sensor-based system of on-line monitoring coke drum operation conditions according to claim 1, special Sign is that the chirp grating acoustics sensor array (4) is ultra-low reflectance chirp grating acoustics sensor array (4), reflection Rate is lower than 0.4%.
3. the distributed optical fiber acoustic sensor-based system of on-line monitoring coke drum operation conditions according to claim 1, special Sign is that the surface of the chirp grating acoustics sensor array (4) is coated with metal layer of the heatproof at 500 °C or more.
4. the distributed optical fiber acoustic sensor-based system of on-line monitoring coke drum operation conditions according to claim 1, special Sign is that the length of the chirp grating acoustics sensor array (4) is 5 ± 0.5 meters higher than the froth bed limit for height of setting.
5. the distributed optical fiber acoustic sensor-based system of on-line monitoring coke drum operation conditions according to claim 1, special Sign is that the length of the chirp grating acoustics sensor array (4) is 40 ± 1 meters.
6. the distributed optical fiber acoustic sensor-based system of on-line monitoring coke drum operation conditions according to claim 1, special Sign is that the spacing between adjacent chirp grating acoustics sensor array (4) is 10 centimetres.
7. the distributed optical fiber acoustic sensor-based system of on-line monitoring coke drum operation conditions according to claim 1, special Sign is that the chirp grating acoustics sensor array (4) selects chirp grating of the three dB bandwidth greater than 2nm.
8. the distributed optical fiber acoustic sensor-based system of on-line monitoring coke drum operation conditions according to claim 1, special Sign is that multiple chirp grating acoustics sensor arrays (4) are fixed on outside coke drum from top to bottom by high-temperature resistance adhesive Wall.
9. the distributed optical fiber acoustic sensor-based system of on-line monitoring coke drum operation conditions according to claim 1, special Sign is that the chirp grating acoustics sensor array (4) passes through at optical fiber and the laser light source and signal that are arranged in Master Control Room Unit (5) are managed to be connected.
CN201910370907.XA 2019-05-06 2019-05-06 A kind of distributed optical fiber acoustic sensor-based system for monitoring coke drum operation conditions on-line Pending CN110261313A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2021147216A1 (en) * 2020-01-21 2021-07-29 中国科学院上海光学精密机械研究所 Distributed optical fiber acoustic sensing system and signal processing method

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103256897A (en) * 2013-04-19 2013-08-21 武汉理工大学 Optical fiber sensing on-line monitoring system and method for hydraulic decoking operating state of petrochemical coking tower
CN106153482A (en) * 2016-07-13 2016-11-23 武汉理工大学 In a kind of hydraulic decoking process coke drum, focus layer hardness is distributed in provision of on-line analysis methodology
CN108775955A (en) * 2018-07-18 2018-11-09 武汉理工大学 A kind of petrochemical industry oil-gas pipeline corrosion state Fibre Optical Sensor on-line monitoring system

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103256897A (en) * 2013-04-19 2013-08-21 武汉理工大学 Optical fiber sensing on-line monitoring system and method for hydraulic decoking operating state of petrochemical coking tower
CN106153482A (en) * 2016-07-13 2016-11-23 武汉理工大学 In a kind of hydraulic decoking process coke drum, focus layer hardness is distributed in provision of on-line analysis methodology
CN108775955A (en) * 2018-07-18 2018-11-09 武汉理工大学 A kind of petrochemical industry oil-gas pipeline corrosion state Fibre Optical Sensor on-line monitoring system

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2021147216A1 (en) * 2020-01-21 2021-07-29 中国科学院上海光学精密机械研究所 Distributed optical fiber acoustic sensing system and signal processing method
US11946799B2 (en) 2020-01-21 2024-04-02 Shanghai Institute Of Optics And Fine Mechanics, Chinese Academy Of Sciences Distributed fiber-optic acoustic sensing system and signal processing method using the same

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Inventor after: Tong Xinglin

Inventor after: Pan Xu

Inventor after: Deng Chengwei

Inventor after: Zhang Cui

Inventor after: Mao Yan

Inventor after: Yin Renjie

Inventor after: Jin Qibing

Inventor after: Pei Bingan

Inventor before: Tong Xinglin

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Inventor before: Deng Chengwei

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Applicant after: WUHAN University OF TECHNOLOGY

Applicant after: BEIJING University OF CHEMICAL TECHNOLOGY

Applicant after: LUOYANG PETROCHEMICAL ENGINEERING CORPORATION, SINOPEC

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