CN110231204A - For extracting the acidolysis device of kerogen and cryptogam in rock - Google Patents

For extracting the acidolysis device of kerogen and cryptogam in rock Download PDF

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Publication number
CN110231204A
CN110231204A CN201910602397.4A CN201910602397A CN110231204A CN 110231204 A CN110231204 A CN 110231204A CN 201910602397 A CN201910602397 A CN 201910602397A CN 110231204 A CN110231204 A CN 110231204A
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CN
China
Prior art keywords
rock
pipe
fluid reservoir
liquid
kerogen
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201910602397.4A
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Chinese (zh)
Inventor
惠书梅
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
KUNSHAN HRHA ELECTRONIC TECHNOLOGY Co Ltd
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KUNSHAN HRHA ELECTRONIC TECHNOLOGY Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by KUNSHAN HRHA ELECTRONIC TECHNOLOGY Co Ltd filed Critical KUNSHAN HRHA ELECTRONIC TECHNOLOGY Co Ltd
Priority to CN201910602397.4A priority Critical patent/CN110231204A/en
Publication of CN110231204A publication Critical patent/CN110231204A/en
Pending legal-status Critical Current

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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/28Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q

Abstract

The invention discloses a kind of for extracting the acidolysis device of kerogen and cryptogam in rock, including filling mechanism, devil liquor recovery mechanism and several beakers equipped with rock, several described beakers are placed in heating tank, the lower section of the heating tank is equipped with the lift drive mechanism for driving the heating tank oscilaltion, the filling mechanism includes hydrofluoric acid fluid reservoir, hydrochloric acid fluid reservoir, crosses drainage fluid reservoir, metering pump and feed liquor house steward, the feed liquor house steward is the snake pipe turned back back and forth, and the devil liquor recovery mechanism includes air inlet pipe, waste discharge liquid pipe and the cup lid.Present invention ensures that accurate liquid feeding and quick drain, high degree of automation reduce labour, avoid manually-operated unstability, guarantee the safety of operator.

Description

For extracting the acidolysis device of kerogen and cryptogam in rock
Technical field
The invention belongs to oil exploration analysis technical fields, more particularly to one kind for extracting kerogen and spore in rock The acidolysis device of powder.
Background technique
Kerogen is the dispersed organic matter in sedimentary rock insoluble in alkali, non-oxidizing acid and organic solvent, is appropriate Temperature and pressure under be formed by condensation polymer, account for about 90% of organic matter in sedimentary rock, kerogen is considered as oil generation Hyle.
The acidolysis analysis of kerogen and cryptogam sample is according to " GB- sedimentary rock kerogen maceration side in traditional oil exploration Method " and " SY/T 5915-2000 spore-pollen analysis identification ", which is all made of by hand and semi-automatic operation, deposits In following disadvantage: one, whole process labor intensity is big, needs to waste a large amount of manpowers, and affected unstable by hand, to rear Continuous test data causes a degree of influence;Two, volatile hydrofluoric acid, hydrochloric acid are volatile, cause centainly to operator Injury.
Summary of the invention
The acidolysis dress that the invention mainly solves the technical problem of providing a kind of for extracting kerogen and cryptogam in rock It sets, it is ensured that accurate liquid feeding and quick drain, high degree of automation reduce labour, avoid manually-operated unstability, Guarantee the safety of operator.
In order to solve the above technical problems, one technical scheme adopted by the invention is that: one kind is for extracting cheese in rock The acidolysis device of root and cryptogam, including filling mechanism, devil liquor recovery mechanism and several beakers equipped with rock, described in several Beaker is placed in heating tank, and the lower section of the heating tank is equipped with the lift drive mechanism for driving the heating tank oscilaltion;
The filling mechanism includes that hydrofluoric acid fluid reservoir, hydrochloric acid fluid reservoir, mistake drainage fluid reservoir, metering pump and feed liquor are total Pipe, the hydrofluoric acid fluid reservoir are connected to hydrofluoric acid solenoid valve, and the hydrochloric acid fluid reservoir is connected to hydrochloric acid solenoid valve, the filtering Water fluid reservoir is connected to filtering water solenoid valve, the hydrofluoric acid solenoid valve, the hydrochloric acid solenoid valve and the filtering water solenoid valve It is all connected to the metering pump, the metering pump is connected to the feed liquor house steward, and the feed liquor house steward goes out liquid with several and is in charge of Connection, the liquid out, which is in charge of, to be connected to across cup lid with the beaker, and liquid is in charge of equipped with liquid outlet electromagnetic valve out;
The devil liquor recovery mechanism includes air inlet pipe, waste discharge liquid pipe and the cup lid, and the air inlet pipe and the feed liquor are total Pipe connection, the inlet of the waste discharge liquid pipe pass through the bottom that the cup lid is placed in beaker, the end of the waste discharge liquid pipe and useless Liquid collects tank connection, and the waste liquid collects tank and is connected to sewer pipe, and the sewer pipe is equipped with pH meter, several described cups Lid is located at the top of the beaker, and several cup lids are fixed on mounting plate, and the mounting plate is fixed on rack, the lifting Driving mechanism drives several described beakers to rise with cup lid sealing to carry out aerating drain to beaker;
The feed liquor house steward is the snake pipe turned back back and forth.
It further include control cabinet, the metering pump, the hydrofluoric acid solenoid valve, the hydrochloric acid solenoid valve, the filtering water power Magnet valve, the liquid outlet electromagnetic valve, the pH meter and the lift drive mechanism are all electrically connected with the control cabinet.
It further says, the lift drive mechanism includes fixed plate, lifter plate and the driving lifter plate oscilaltion Lifting drive electric cylinders, the heating tank is located at the top of the lifter plate, and the lifter plate and the lifting drive electric cylinders Push rod connection, the lifting driving electric cylinders are fixed on the fixed plate, and the fixed plate is fixed on the rack.
It further says, further includes several guide rods, the upper end of the guide rod is fixed with the lifter plate, the liter The lower section for dropping plate passes through the fixed plate.
It further says, the push rod of the guide rod and the lifting driving electric cylinders is all cased with ripple protection pipe sleeve, several A ripple protection pipe sleeve is between the fixed plate and the lifter plate.
It further says, the inside of the heating tank is equipped with heating tube and the support frame for positioning the beaker, described Heating tube is located at the lower section of support frame as described above, and the side wall of the heating tank is equipped with liquid level sensor and outlet pipe, the outlet pipe It is connected to the heating tank, the outlet pipe is equipped with outlet valve.
It further says, further includes ventilation duct, the mounting plate, and the ventilation duct are fixed in the lower end of the ventilation duct It is connected to the heating tank.
It further says, the inside of the beaker is equipped with stirring blade, the stirring blade and stirring axis connection, described to stir The output axis connection of axis and stirring motor is mixed, the stirring motor is fixed by the bracket in mounting plate.
It further says, the liquid outlet of the sewer pipe is connected to waste liquid pool.
It further says, the air inlet pipe is connected to gas source.
It further says, the hydrofluoric acid fluid reservoir, hydrochloric acid fluid reservoir, drainage fluid reservoir excessively are all located at the interior of vent cabinet Portion.
Beneficial effects of the present invention at least have the following:
The present invention includes filling mechanism and devil liquor recovery mechanism, it is ensured that accurate liquid feeding and quick drain automate journey Degree is high, reduces labour, avoids manually-operated unstability;
Lift drive mechanism of the invention drives several beakers to rise and seals with cup lid, is sent by air inlet pipe into beaker Gas pressurization, so that the liquid in beaker is carried out drain by waste discharge liquid pipe and sewer pipe;
The lower section of heating tank of the invention is equipped with the lift drive mechanism that driving heating tank rises, to make heating tank and peace An apertured cavity is collectively formed in loading board, is exhausted using ventilation duct, prevents the gas diffusion of reaction to interior, guarantees The safety of operator;
The push rod of guide rod and lifting driving electric cylinders of the invention is all cased with ripple protection pipe sleeve, prevents guide rod and lifting Driving electric cylinders are corroded, and guarantee its physical life, it is worth mentioning at this point that, the outer surface of heating tube is cased with acid-proof pipe sleeve, anti-acid tube Set is Teflon pipe sleeve, effectively prevent heating tube to be corroded by strong acid, guarantees its service life;
The inside of beaker of the invention is equipped with stirring blade, reacts the rock sample in liquid and beaker sufficiently, also sharp Rock sample is sufficiently filtered in drainage excessively, is cleaned, the extraction time of kerogen and cryptogam is shortened;
Hydrofluoric acid fluid reservoir of the invention, hydrochloric acid fluid reservoir cross the inside that drainage fluid reservoir is all located at vent cabinet, volatility The sour gas such as hydrofluoric acid, hydrochloric acid diffuse to interior, guarantee the safety of operator.
Detailed description of the invention
Fig. 1 is one of structural schematic diagram of the invention (no vent cabinet, without control cabinet);
Fig. 2 is the structural schematic diagram of filling mechanism and devil liquor recovery mechanism of the invention;
Fig. 3 is the structural schematic diagram of stirring blade of the invention, stirring motor and cup lid;
Fig. 4 is the structural schematic diagram of heating tank of the invention;
Fig. 5 is second structural representation of the invention (containing vent cabinet, control cabinet);
Fig. 6 is the liquid flow graph of filling mechanism and devil liquor recovery mechanism of the invention;
Fig. 7 is control principle drawing of the invention;
Each section label is as follows in attached drawing:
Filling mechanism 1, hydrofluoric acid fluid reservoir 11, hydrochloric acid fluid reservoir 12, drainage fluid reservoir 13, metering pump 14, feed liquor excessively are total Pipe 15, hydrofluoric acid solenoid valve 16, hydrochloric acid solenoid valve 17, filtering water solenoid valve 18, liquid is in charge of 19, liquid outlet electromagnetic valve 20, air inlet out Pipe 21, check valve 211, waste discharge liquid pipe 22, cup lid 23, waste liquid collect tank 24, pH meter 25, sewer pipe 26, devil liquor recovery machine Structure 2, beaker 3, heating tank 4, heating tube 41, support frame 42, liquid level sensor 43, outlet pipe 44, outlet valve 441, lifting driving Mechanism 5, fixed plate 51, lifter plate 52, lifting driving electric cylinders 53, guide rod 54, ripple protect pipe sleeve 55, mounting plate 6, paddle Piece 61, agitating shaft 62, stirring motor 63, bracket 64, rack 7, control cabinet 8, ventilation duct 9, waste liquid pool 10, gas source 100 and ventilation Cabinet 200.
Specific embodiment
The preferred embodiments of the present invention will be described in detail with reference to the accompanying drawing, so that advantages and features of the invention energy It is easier to be readily appreciated by one skilled in the art, so as to make a clearer definition of the protection scope of the present invention.
Embodiment: it is a kind of for extracting the acidolysis device of kerogen and cryptogam in rock, as shown in Fig. 1-Fig. 7, including add Liquid mechanism 1, devil liquor recovery mechanism 2 and several beakers 3 equipped with rock, several described beakers 3 are placed in heating tank 4, institute The lower section for stating heating tank 4 is equipped with the lift drive mechanism 5 for driving 4 oscilaltion of heating tank;
The filling mechanism 1 includes hydrofluoric acid fluid reservoir 11, hydrochloric acid fluid reservoir 12, crosses drainage fluid reservoir 13, metering pump 14 With feed liquor house steward 15, the hydrofluoric acid fluid reservoir 11 is connected to hydrofluoric acid solenoid valve 16, the hydrochloric acid fluid reservoir 12 and hydrochloric acid electricity Magnet valve 17 is connected to, and the drainage fluid reservoir 13 of crossing is connected to filtering water solenoid valve 18, the hydrofluoric acid solenoid valve 16, the hydrochloric acid Solenoid valve 17 and the filtering water solenoid valve 18 are all connected to the metering pump 14, the metering pump 14 and the feed liquor house steward 15 Connection, the feed liquor house steward 15 go out liquid with several and are in charge of 19 and are connected to, it is described go out liquid be in charge of 19 and pass through cup lid 23 and the beaker 3 Connection, and liquid is in charge of 19 equipped with liquid outlet electromagnetic valve 20 out;
The devil liquor recovery mechanism 2 includes air inlet pipe 21, waste discharge liquid pipe 22 and the cup lid 23, the air inlet pipe 21 and institute The connection of feed liquor house steward 15 is stated, the inlet of the waste discharge liquid pipe passes through the bottom that the cup lid 23 is placed in beaker 3, the removal waste fluid The end of pipe 22 is collected tank 24 with waste liquid and is connected to, and the waste liquid collects tank 24 and is connected to sewer pipe 26, sets on the sewer pipe 26 There is pH meter 25, several described cup lids 23 are located at the top of the beaker 3, and several cup lids 23 are fixed on mounting plate 6, the mounting plate 6 is fixed on rack 7, and the lift drive mechanism 5 drives several described beakers 3 to rise and seals with cup lid 23 To carry out aerating drain to beaker 3;
The feed liquor house steward 15 is the snake pipe turned back back and forth.
It further include control cabinet 8, the metering pump 14, the hydrofluoric acid solenoid valve 16, the hydrochloric acid solenoid valve 17, the mistake Drainage solenoid valve 18, the liquid outlet electromagnetic valve 20, the pH meter 25 and the lift drive mechanism 5 all with the control cabinet 8 electrical connections.
The lift drive mechanism 5 includes the liter of fixed plate 51, lifter plate 52 and driving 52 oscilaltion of lifter plate Drop driving electric cylinders 53, the heating tank 4 are located at the top of the lifter plate 52, and the lifter plate 52 drives electric cylinders with the lifting 53 push rod connection, the lifting driving electric cylinders 53 are fixed on the fixed plate 51, and the fixed plate 51 is fixed on the rack 7。
When it is implemented, the lifting driving electric cylinders 53 are electrically connected with the control cabinet 8.
It further include several guide rods 54, the upper end of the guide rod 54 and the lifter plate 52 are fixed, the lifter plate 52 lower section passes through the fixed plate 51.
The guide rod 54 and the push rod of the lifting driving electric cylinders 53 are all cased with ripple protection pipe sleeve 55, described in several Ripple protects pipe sleeve 55 between the fixed plate 51 and the lifter plate 52.
The inside of the heating tank 4 is equipped with heating tube 41 and the support frame 42 for positioning the beaker 3, the heating tube 41 are located at the lower section of support frame as described above 42, and the side wall of the heating tank 4 is equipped with liquid level sensor 43 and outlet pipe 44, the water outlet Pipe 44 is connected to the heating tank 4, and the outlet pipe is equipped with outlet valve 441.
When it is implemented, the inside of the heating tank 4 is equipped with water for heating.
The outer surface of the heating tube 41 is cased with acid-proof pipe sleeve, and the acid-proof pipe sleeve is Teflon pipe sleeve, the heating tube 41 and the liquid level sensor 43 be all electrically connected with the control cabinet 8.
Further include ventilation duct 9, the mounting plate 6 is fixed in the lower end of the ventilation duct 9, and the ventilation duct 9 with it is described Heating tank 4 is connected to.
The inside of the beaker 3 is equipped with stirring blade 61, and the stirring blade 61 is connect with agitating shaft 62, the agitating shaft 62 are fixed on mounting plate 6 by bracket 64 with the output axis connection of stirring motor 63, the stirring motor 63.
When it is implemented, the stirring motor 63 is electrically connected with the control cabinet 8.
The liquid outlet of the sewer pipe 26 is connected to waste liquid pool 10.
The air inlet pipe 21 is connected to gas source 100.
When it is implemented, air inlet pipe 21 is equipped with check valve 211.
The gas source 100 is air pump, and the air pump is electrically connected with the control cabinet 8.
The hydrofluoric acid fluid reservoir 11, hydrochloric acid fluid reservoir 12 cross the inside that drainage fluid reservoir 13 is all located at vent cabinet 200.
Working principle of the present invention is as follows: suitable rock sample is put into beaker, beaker is placed by support frame In heating tank, heating tank is warming up to 70 DEG C, and suitable water is added, and lift drive mechanism drives beaker to rise and seals with cup lid, then Hydrochloric acid solenoid valve is opened, suitable hydrochloric acid successively is added into 24 beakers, hydrochloride waste is discharged after being stirred to react precipitating, Hydrofluoric acid solenoid valve is opened again, suitable hydrofluoric acid successively is added into 24 beakers, is stirred to react hydrofluoric acid after precipitating Waste liquid is discharged, then drainage neutralization was added into beaker, and drainage is discharged after stirring precipitating, adds in drainage stirring repeatedly With until the pH value that measures of pH meter is greater than 6.
The above description is only an embodiment of the present invention, is not intended to limit the scope of the invention, all to utilize this hair Equivalent structure transformation made by bright specification and accompanying drawing content is applied directly or indirectly in other relevant technical fields, Similarly it is included within the scope of the present invention.

Claims (10)

1. a kind of for extracting the acidolysis device of kerogen and cryptogam in rock, it is characterised in that: including filling mechanism (1), give up Liquid recovering mechanism (2) and several beakers (3) equipped with rock, several described beakers are placed in heating tank (4), the heating The lower section of slot is equipped with the lift drive mechanism (5) for driving the heating tank oscilaltion;
The filling mechanism includes hydrofluoric acid fluid reservoir (11), hydrochloric acid fluid reservoir (12), crosses drainage fluid reservoir (13), metering pump (14) it is connected to feed liquor house steward (15), the hydrofluoric acid fluid reservoir with hydrofluoric acid solenoid valve (16), the hydrochloric acid fluid reservoir and salt The connection of sour solenoid valve (17), it is described cross drainage fluid reservoir and filter water solenoid valve (18) be connected to, it is the hydrofluoric acid solenoid valve, described Hydrochloric acid solenoid valve and the filtering water solenoid valve are all connected to the metering pump, and the metering pump is connected to the feed liquor house steward, The feed liquor house steward goes out liquid with several and is in charge of (19) and be connected to, and the liquid out, which is in charge of, to be connected to across cup lid (23) with the beaker, And liquid is in charge of equipped with liquid outlet electromagnetic valve (20) out;
The devil liquor recovery mechanism includes air inlet pipe (21), waste discharge liquid pipe (22) and the cup lid, the air inlet pipe and it is described into Liquid general pipeline connection, the inlet of the waste discharge liquid pipe pass through the bottom that the cup lid is placed in beaker, the end of the waste discharge liquid pipe Collect tank (24) with waste liquid to be connected to, the waste liquid collects tank and is connected to sewer pipe (26), and the sewer pipe is equipped with pH meter (25), several described cup lids are located at the top of the beaker, and several cup lids are fixed on mounting plate (6), the installation Plate is fixed on rack (7), the lift drive mechanism drive several described beakers rise with cup lid sealing to beaker into Row aerating drain;
The feed liquor house steward is the snake pipe turned back back and forth.
It further include control cabinet (8), the metering pump, the hydrofluoric acid solenoid valve, the hydrochloric acid solenoid valve, the filtering water power magnetic Valve, the liquid outlet electromagnetic valve, the pH meter and the lift drive mechanism are all electrically connected with the control cabinet.
2. according to claim 1 for extracting the acidolysis device of kerogen and cryptogam in rock, it is characterised in that: described Lift drive mechanism includes the lifting driving electric cylinders of fixed plate (51), lifter plate (52) and the driving lifter plate oscilaltion (53), the heating tank is located at the top of the lifter plate, and the lifter plate is connect with the push rod of the lifting driving electric cylinders, institute It states lifting driving electric cylinders and is fixed on the fixed plate, the fixed plate is fixed on the rack.
3. according to claim 2 for extracting the acidolysis device of kerogen and cryptogam in rock, it is characterised in that: also wrap Several guide rods (54) are included, the upper end of the guide rod is fixed with the lifter plate, and the lower section of the lifter plate passes through described Fixed plate.
4. according to claim 3 for extracting the acidolysis device of kerogen and cryptogam in rock, it is characterised in that: described Guide rod and the push rod of the lifting driving electric cylinders are all cased with ripple protection pipe sleeve (55), several described ripples protect pipe sleeve position Between the fixed plate and the lifter plate.
5. according to claim 1 for extracting the acidolysis device of kerogen and cryptogam in rock, it is characterised in that: described The inside of heating tank is equipped with heating tube (41) and the support frame (42) for positioning the beaker, and the heating tube is located at the branch The lower section of support, the side wall of the heating tank are equipped with liquid level sensor (43) and outlet pipe (44), and the outlet pipe adds with described Heat channel connection, the outlet pipe are equipped with outlet valve (441).
6. according to claim 1 for extracting the acidolysis device of kerogen and cryptogam in rock, it is characterised in that: also wrap It includes ventilation duct (9), the mounting plate is fixed in the lower end of the ventilation duct, and the ventilation duct is connected to the heating tank.
7. according to claim 1 for extracting the acidolysis device of kerogen and cryptogam in rock, it is characterised in that: described The inside of beaker is equipped with stirring blade (61), and the stirring blade is connect with agitating shaft (62), the agitating shaft and stirring motor (63) output axis connection, the stirring motor are fixed on mounting plate by bracket (64).
8. according to claim 1 for extracting the acidolysis device of kerogen and cryptogam in rock, it is characterised in that: described The liquid outlet of sewer pipe is connected to waste liquid pool (10).
9. according to claim 1 for extracting the acidolysis device of kerogen and cryptogam in rock, it is characterised in that: described Air inlet pipe is connected to gas source (100).
10. according to claim 1 for extracting the acidolysis device of kerogen and cryptogam in rock, it is characterised in that: institute It states hydrofluoric acid fluid reservoir, hydrochloric acid fluid reservoir, cross the inside that drainage fluid reservoir is all located at vent cabinet (200).
CN201910602397.4A 2019-07-05 2019-07-05 For extracting the acidolysis device of kerogen and cryptogam in rock Pending CN110231204A (en)

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CN201910602397.4A CN110231204A (en) 2019-07-05 2019-07-05 For extracting the acidolysis device of kerogen and cryptogam in rock

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CN201910602397.4A CN110231204A (en) 2019-07-05 2019-07-05 For extracting the acidolysis device of kerogen and cryptogam in rock

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112021836A (en) * 2020-09-23 2020-12-04 深圳市吖咕智能科技有限公司 Electric drawer
CN114177646A (en) * 2021-12-07 2022-03-15 常州市易用科技有限公司 Kerogen acidizing treatment device

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN201773023U (en) * 2010-04-09 2011-03-23 谢家骆 Kerogen automatic extraction device
CN107132366A (en) * 2017-06-28 2017-09-05 中国海洋石油总公司 A kind of kerogen automatic analytical instrument
CN108287098A (en) * 2017-12-21 2018-07-17 中国地质大学(武汉) A kind of microfossil steeps sampling device automatically
CN210198824U (en) * 2019-07-05 2020-03-27 昆山和润华电子科技有限公司 Acidolysis device for extracting kerogen and sporopollen in rock

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN201773023U (en) * 2010-04-09 2011-03-23 谢家骆 Kerogen automatic extraction device
CN107132366A (en) * 2017-06-28 2017-09-05 中国海洋石油总公司 A kind of kerogen automatic analytical instrument
CN108287098A (en) * 2017-12-21 2018-07-17 中国地质大学(武汉) A kind of microfossil steeps sampling device automatically
CN210198824U (en) * 2019-07-05 2020-03-27 昆山和润华电子科技有限公司 Acidolysis device for extracting kerogen and sporopollen in rock

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112021836A (en) * 2020-09-23 2020-12-04 深圳市吖咕智能科技有限公司 Electric drawer
CN114177646A (en) * 2021-12-07 2022-03-15 常州市易用科技有限公司 Kerogen acidizing treatment device

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