CN110229711A - The high-accuracy Metalworking fluid of mirror surface grade and preparation method thereof suitable for bloom processing technology - Google Patents
The high-accuracy Metalworking fluid of mirror surface grade and preparation method thereof suitable for bloom processing technology Download PDFInfo
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- CN110229711A CN110229711A CN201910551093.XA CN201910551093A CN110229711A CN 110229711 A CN110229711 A CN 110229711A CN 201910551093 A CN201910551093 A CN 201910551093A CN 110229711 A CN110229711 A CN 110229711A
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
- C10M169/04—Mixtures of base-materials and additives
- C10M169/044—Mixtures of base-materials and additives the additives being a mixture of non-macromolecular and macromolecular compounds
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
- C10M2201/04—Elements
- C10M2201/041—Carbon; Graphite; Carbon black
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
- C10M2205/02—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers
- C10M2205/026—Butene
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
- C10M2209/10—Macromolecular compoundss obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- C10M2209/103—Polyethers, i.e. containing di- or higher polyoxyalkylene groups
- C10M2209/104—Polyethers, i.e. containing di- or higher polyoxyalkylene groups of alkylene oxides containing two carbon atoms only
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
- C10M2219/04—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions containing sulfur-to-oxygen bonds, i.e. sulfones, sulfoxides
- C10M2219/044—Sulfonic acids, Derivatives thereof, e.g. neutral salts
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2223/00—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
- C10M2223/02—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having no phosphorus-to-carbon bonds
- C10M2223/04—Phosphate esters
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2040/00—Specified use or application for which the lubricating composition is intended
- C10N2040/20—Metal working
- C10N2040/22—Metal working with essential removal of material, e.g. cutting, grinding or drilling
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Lubricants (AREA)
Abstract
The invention discloses a kind of high-accuracy Metalworking fluids of mirror surface grade suitable for bloom processing technology, it is characterised in that: raw material includes following components by weight: 80-90 parts of electric spark machine oil, 0.3-2 parts of polyisobutene, 0.2-5 parts of graphene, 0.5-3 parts of detergent-dispersant additive, 0.5-3 parts of alkali retention agent .2-1.5 parts of phosphoesterase 30,6.2-13 parts of surfactant；Raw material are easy to get, and preparation process is simple to operation, and each component acts synergistically to form stable chemical balance, keep the performance of processing oil more stable.The processing oil can reduce the activation energy of material surface, reduce surface tension, reduce the suspension of the fine dusts shape chip generated in process of metal working, and accelerate the sedimentation of fine dusts shape chip, the filterability of working fluid is improved simultaneously, guarantees the cleaning of oil product, it is therefore prevented that chatter mark when bloom is processed and is scratched, the brightness for improving bloom converted products, substantially improves mirror effect.
Description
Technical field
The present invention relates to a kind of Metalworking fluid, in particular to a kind of mirror surface grade suitable for bloom processing technology is high-accuracy
Metalworking fluid and preparation method thereof.
Background technique
, surface roughness, brightness to product higher and higher to the requirement of intermetallic composite coating in modern mechanical manufacturing industry
There is very high requirement, more and more mirror finish effects need to meet, and therefore, high light technology is widely used in mirror surface and adds
Work.And bloom processing procedure simplicity of explanation is to be processed using the cutters such as diamond (having high hardness and wearability) in fast state
The beautiful chamfering of product (its effect is bright such as mirror).Especially in terms of electronic product, it is outer that high light technology is applied to label, knob etc.
It sees on component, substantially increases product appearance decorative effect.CNC bloom processing technology is applied to the works such as milling, turnery processing
In industry industry, and suitable bloom processing technology is the basis of mirror finish with the high-accuracy Metalworking fluid of mirror surface grade, existing
The processing effect that industrial lubricants are not able to satisfy the long period is constant, occur as soon as within general one week or so product scratch, scratch, influence
The quality and manufacturing schedule of product, and conventional lubrication oil seldom considers the fine dusts shape chip produced in process of metal working
Surface activation energy, and process in fine dusts shape chip suspension exactly influence mirror effect key, it is therefore, existing
Lubricating oil is difficult to promote the mirror effect of bloom processing.
Summary of the invention
In view of this, the purpose of the present invention is to provide a kind of high-accuracy metals of mirror surface grade suitable for bloom processing technology
Processing oil and preparation method thereof improves bloom processing performance, greatly promotes bloom processing mirror effect.
The high-accuracy Metalworking fluid of mirror surface grade suitable for bloom processing technology of the invention, raw material include by weight with
Lower component: 80-90 parts of electric spark machine oil, 0.3-2 parts of polyisobutene, 0.2-5 parts of graphene, 0.5-3 parts of detergent-dispersant additive, alkali are protected
Hold 0.5-3 parts of agent .2-1.5 parts of phosphoesterase 30,6.2-13 parts of surfactant；
Further, raw material includes following components by weight: 85 parts of electric spark machine oil, 1 part of polyisobutene, 3 parts of graphene,
1.5 parts of detergent-dispersant additive, 1.5 parts of alkali retention agent .8 parts of phosphoesterase 30,10 parts of surfactant；
Further, the surfactant is the compounding of sorbester p17 and Tween 80；
Further, the weight ratio of the Tween 80 and sorbester p17 is 1:12-30；
Further, the detergent-dispersant additive is T154；
Further, the alkali retention agent is calcium mahogany sulfonate；
Further, the flash-point of the electric spark machine oil be 110 DEG C, viscosity 2cst；
Further, the molecular weight of the polyisobutene is 1300；
Invention additionally discloses a kind of preparation method of high-accuracy Metalworking fluid of mirror surface grade suitable for bloom processing technology,
The following steps are included:
A. respectively by sorbester p17 and graphene it is pre-dispersed in the electric spark machine oil of part after again with remaining electric spark machine oil
It is mixed evenly；
B. surplus material is added after the mixture in step a being warming up to 40-60 DEG C, and temperature is continuously to stir at 40-60 DEG C again
It mixes reaction 2 hours or more；
Further, in step a, sorbester p17 and alkali retention agent are mixed evenly with part electric spark machine oil；By graphite
Alkene is mixed evenly with part electric spark machine oil；Finally the above two material being pre-mixed is added in stirring remaining
It is stirred evenly in electric spark machine oil.
Beneficial effects of the present invention: the high-accuracy Metalworking fluid of mirror surface grade suitable for bloom processing technology of the invention,
Raw material are easy to get, and preparation process is simple to operation, and each component acts synergistically to form stable chemical balance, make the performance of processing oil
It is more stable.In bloom process, which can reduce the activation energy of material surface, reduce surface tension, reduce metal
The suspension of the fine dusts shape chip generated in process, and accelerate the sedimentation of fine dusts shape chip, while improving processing
The filterability of liquid guarantees the cleaning of oil product, it is therefore prevented that bloom process when chatter mark and scratch, improve bloom converted products light
Brightness substantially improves mirror effect.It is good that the processing oil processes fines settleability when in use, and filterability is high, without changing oil, has
There is long-term effectiveness.
Specific embodiment
The high-accuracy Metalworking fluid of mirror surface grade suitable for bloom processing technology of the present embodiment, raw material include by weight
Following components: 80-90 parts of electric spark machine oil, 0.3-2 parts of polyisobutene, 0.2-5 parts of graphene, 0.5-3 parts of detergent-dispersant additive, alkali
0.5-3 parts of retention agent .2-1.5 parts of phosphoesterase 30,6.2-13 parts of surfactant；Moistened using electric spark machine oil substitute mineral oil
Sliding, settleability is good, easily excludes carbon slag, and the flash-point of electric spark machine oil is 110 DEG C, viscosity 2cst；Reach anti-using polyisobutene
The purpose of mist of oil, wherein the molecular weight of polyisobutene is 1300；Friction high temperature is reduced using graphene, and is assisted with other components
Same-action forms high tough film, and the cleanliness and filterability of oil product are promoted by detergent-dispersant additive, using alkali retention agent and clearly
Net dispersing agent synergistic effect improves the service life and long-term effectiveness of oil product, achievees the purpose that without changing oil；Using phosphate
Acting synergistically with graphene enhances lubricity；Surface tension of liquid is reduced using surfactant, helps sedimentation.
In the present embodiment, raw material includes following components by weight: 85 parts of electric spark machine oil, 1 part of polyisobutene, graphene
3 parts, 1.5 parts of detergent-dispersant additive, 1.5 parts of alkali retention agent .8 parts of phosphoesterase 30,10 parts of surfactant；For preferred embodiment.
In the present embodiment, the surfactant is the compounding of sorbester p17 and Tween 80, the Tween 80 and sorbester p17
Weight ratio is 1:12-30；The two synergistic effect, enhances effect of settling.
In the present embodiment, the detergent-dispersant additive is T154 (derivatives of poly (iso) butene)；The alkali retention agent is petroleum sulphur
Sour calcium；The two synergistic effect reaches the long-term cleannes for keeping oil product, extends the purpose of oil product service life.
A kind of preparation side of high-accuracy Metalworking fluid of mirror surface grade suitable for bloom processing technology is also disclosed in the present embodiment
Method, comprising the following steps:
A. respectively by sorbester p17 and graphene it is pre-dispersed in the electric spark machine oil of part after again with remaining electric spark machine oil
It is mixed evenly；Preferably graphene is carried out to disperse to stir evenly in advance in 5 times (weight) of electric spark machine oil；It will department
Disk 80 and calcium mahogany sulfonate T106 carry out dispersing to stir evenly in advance in 3 times (weight) of electric spark machine oil.
B. surplus material is added after the mixture in step a being warming up to 40-60 DEG C, and temperature is continuously to stir at 40-60 DEG C again
It mixes reaction 2 hours or more；
Further, in step a, sorbester p17 and alkali retention agent are mixed evenly with part electric spark machine oil；By graphite
Alkene is mixed evenly with part electric spark machine oil；Finally the above two material being pre-mixed is added in stirring remaining
It is stirred evenly in electric spark machine oil.
Embodiment one
The high-accuracy Metalworking fluid of mirror surface grade suitable for bloom processing technology of the present embodiment, raw material include by weight
Following components: 80 parts of electric spark machine oil, 0.3 part of polyisobutene, 0.2 part, 0.5 part T154 of graphene, 0.5 part of calcium mahogany sulfonate,
.2 parts, 6 parts sorbester p17s of phosphoesterase 30,0.2 part of Tween 80；Preparation method includes the following steps: a. is by sorbester p17 and mahogany acid
Calcium is mixed evenly with part electric spark machine oil；Graphene and part electric spark machine oil are mixed evenly；It finally will be upper
It states the material that two kinds are pre-mixed and is added in stirring in remaining electric spark machine oil and stirred evenly；
B. it is added after the mixture in step a being warming up to 40 DEG C at surplus material is 40 DEG C in temperature and continuously stirs reaction
2 hours.
Embodiment two
The high-accuracy Metalworking fluid of mirror surface grade suitable for bloom processing technology of the present embodiment, raw material include by weight
Following components: 90 parts of electric spark machine oil, 2 parts of polyisobutene, 5 parts, 3 parts T154 of graphene, 3 parts of calcium mahogany sulfonate, phosphate 1.5
Part, 12 parts of sorbester p17s, 1 part of Tween 80；Preparation method includes the following steps: a. is electric by sorbester p17 and calcium mahogany sulfonate and part
Spark machine oil is mixed evenly；Graphene and part electric spark machine oil are mixed evenly；It finally will be above two preparatory
Mixed material is added in remaining electric spark machine oil in stirring and stirs evenly；
B. it is added after the mixture in step a being warming up to 60 DEG C at surplus material is 60 DEG C in temperature and continuously stirs reaction
2 hours.
Embodiment three
The high-accuracy Metalworking fluid of mirror surface grade suitable for bloom processing technology of the present embodiment, raw material include by weight
Following components: 80 parts of electric spark machine oil, 2 parts of polyisobutene, 0.2 part, 3 parts T154 of graphene, 0.5 part of calcium mahogany sulfonate, phosphoric acid
1.5 parts, 6 parts sorbester p17s of ester, 1 part of Tween 80；Preparation method includes the following steps: a. is by sorbester p17 and calcium mahogany sulfonate and portion
Electric spark machine oil is divided to be mixed evenly；Graphene and part electric spark machine oil are mixed evenly；It finally will be above two
The material being pre-mixed is added in remaining electric spark machine oil in stirring and stirs evenly；
B. it is added after the mixture in step a being warming up to 40 DEG C at surplus material is 40 DEG C in temperature and continuously stirs reaction
2 hours or more.
Example IV
The high-accuracy Metalworking fluid of mirror surface grade suitable for bloom processing technology of the present embodiment, raw material include by weight
Following components: 85 parts of electric spark machine oil, 0.3 part of polyisobutene, 5 parts, 2 parts T154 of graphene, 0.5 part of calcium mahogany sulfonate, phosphoric acid
1.5 parts, 10 parts sorbester p17s of ester, 0.2 part of Tween 80；Preparation method includes the following steps: a. is by sorbester p17 and calcium mahogany sulfonate
It is mixed evenly with part electric spark machine oil；Graphene and part electric spark machine oil are mixed evenly；It finally will be above-mentioned
Two kinds of materials being pre-mixed are added in remaining electric spark machine oil in stirring and stir evenly；
B. it is added after the mixture in step a being warming up to 45 DEG C at surplus material is 45 DEG C in temperature and continuously stirs reaction
2 hours or more.
Embodiment five
The high-accuracy Metalworking fluid of mirror surface grade suitable for bloom processing technology of the present embodiment, raw material include by weight
Following components: 90 parts of electric spark machine oil, 0.5 part of polyisobutene, 0.7 part, 0.5 part T154 of graphene, 3 parts of calcium mahogany sulfonate, phosphorus
0.8 part, 7 parts sorbester p17s of acid esters, 0.8 part of Tween 80；Preparation method includes the following steps: a. is by sorbester p17 and calcium mahogany sulfonate
It is mixed evenly with part electric spark machine oil；Graphene and part electric spark machine oil are mixed evenly；It finally will be above-mentioned
Two kinds of materials being pre-mixed are added in remaining electric spark machine oil in stirring and stir evenly；
B. it is added after the mixture in step a being warming up to 55 DEG C at surplus material is 55 DEG C in temperature and continuously stirs reaction
2 hours.
Embodiment six
The high-accuracy Metalworking fluid of mirror surface grade suitable for bloom processing technology of the present embodiment, raw material include by weight
Following components: 85 parts of electric spark machine oil, 1 part of polyisobutene, 3 parts, 1.5 parts T154 of graphene, 1.5 parts of calcium mahogany sulfonate, phosphoric acid
0.8 part, 9 parts sorbester p17s of ester, 1 part of Tween 80；Preparation method includes the following steps: a. is by sorbester p17 and calcium mahogany sulfonate and portion
Electric spark machine oil is divided to be mixed evenly；Graphene and part electric spark machine oil are mixed evenly；It finally will be above two
The material being pre-mixed is added in remaining electric spark machine oil in stirring and stirs evenly；B. the mixture in step a is heated up
It is added at surplus material is 42 DEG C in temperature and continuously stirs reaction 2 hours or more after to 42 DEG C.
By the processing oil of the embodiment of the present invention one and several mineral types in the prior art and the technology of synthesis lubriation material
Index comparison result such as following table.
Finally, it is stated that the above examples are only used to illustrate the technical scheme of the present invention and are not limiting, although referring to compared with
Good embodiment describes the invention in detail, those skilled in the art should understand that, it can be to skill of the invention
Art scheme is modified or replaced equivalently, and without departing from the objective and range of technical solution of the present invention, should all be covered at this
In the scope of the claims of invention.
Claims (10)
1. a kind of high-accuracy Metalworking fluid of mirror surface grade suitable for bloom processing technology, it is characterised in that: raw material is by weight
Including following components: 80-90 parts of electric spark machine oil, 0.3-2 parts of polyisobutene, 0.2-5 parts of graphene, detergent-dispersant additive 0.5-3
Part, 0.5-3 parts of alkali retention agent .2-1.5 parts of phosphoesterase 30,6.2-13 parts of surfactant.
2. the mirror surface grade high-accuracy Metalworking fluid according to claim 1 suitable for bloom processing technology, feature exist
In: raw material includes following components by weight: 85 parts of electric spark machine oil, 1 part of polyisobutene, 3 parts of graphene, detergent-dispersant additive
1.5 parts, 1.5 parts of alkali retention agent .8 parts of phosphoesterase 30,10 parts of surfactant.
3. the mirror surface grade high-accuracy Metalworking fluid according to claim 1 suitable for bloom processing technology, feature exist
In: the surfactant is the compounding of sorbester p17 and Tween 80.
4. the mirror surface grade high-accuracy Metalworking fluid according to claim 3 suitable for bloom processing technology, feature exist
In: the weight ratio of the Tween 80 and sorbester p17 is 1:12-30.
5. the mirror surface grade high-accuracy Metalworking fluid according to claim 3 suitable for bloom processing technology, feature exist
In: the detergent-dispersant additive is T154.
6. the mirror surface grade high-accuracy Metalworking fluid according to claim 5 suitable for bloom processing technology, feature exist
In: the alkali retention agent is calcium mahogany sulfonate.
7. the mirror surface grade high-accuracy Metalworking fluid according to claim 6 suitable for bloom processing technology, feature exist
In: the flash-point of the electric spark machine oil be 110 DEG C, viscosity 2cst.
8. the mirror surface grade high-accuracy Metalworking fluid according to claim 7 suitable for bloom processing technology, feature exist
In: the molecular weight of the polyisobutene is 1300.
9. the preparation side of the mirror surface grade high-accuracy Metalworking fluid according to claim 1 suitable for bloom processing technology
Method, it is characterised in that: the following steps are included:
A. respectively by sorbester p17 and graphene it is pre-dispersed in the electric spark machine oil of part after mixed again with remaining electric spark machine oil
It stirs evenly；
B. surplus material is added after the mixture in step a being warming up to 40-60 DEG C, and temperature is to continuously stir at 40-60 DEG C instead again
It answers 2 hours or more.
10. the preparation side of the mirror surface grade high-accuracy Metalworking fluid according to claim 9 suitable for bloom processing technology
Method, it is characterised in that: in step a, sorbester p17 and alkali retention agent are mixed evenly with part electric spark machine oil；By graphene
It is mixed evenly with part electric spark machine oil；Remaining electricity is finally added in the above two material being pre-mixed in stirring
It is stirred evenly in spark machine oil.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| WO2023024367A1 (en) * | 2021-08-26 | 2023-03-02 | 安美科技股份有限公司 | Mirror discharge machining oil and preparation method therefor |
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