CN110214884A - Application of the black ginger as preservative - Google Patents
Application of the black ginger as preservative Download PDFInfo
- Publication number
- CN110214884A CN110214884A CN201910532874.4A CN201910532874A CN110214884A CN 110214884 A CN110214884 A CN 110214884A CN 201910532874 A CN201910532874 A CN 201910532874A CN 110214884 A CN110214884 A CN 110214884A
- Authority
- CN
- China
- Prior art keywords
- black ginger
- handled
- humidity
- ginger
- black
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 241000234314 Zingiber Species 0.000 title claims abstract description 121
- 235000006886 Zingiber officinale Nutrition 0.000 title claims abstract description 120
- 235000008397 ginger Nutrition 0.000 title claims abstract description 120
- 239000003755 preservative agent Substances 0.000 title claims abstract description 22
- 230000002335 preservative effect Effects 0.000 title claims abstract description 20
- 239000000843 powder Substances 0.000 claims abstract description 57
- 238000012545 processing Methods 0.000 claims abstract description 32
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 10
- 239000005452 food preservative Substances 0.000 claims abstract description 5
- 235000019249 food preservative Nutrition 0.000 claims abstract description 5
- 238000002360 preparation method Methods 0.000 claims description 18
- 239000000284 extract Substances 0.000 claims description 10
- 206010027146 Melanoderma Diseases 0.000 claims description 8
- 238000004806 packaging method and process Methods 0.000 claims description 8
- 229910001220 stainless steel Inorganic materials 0.000 claims description 7
- 239000010935 stainless steel Substances 0.000 claims description 7
- 238000010992 reflux Methods 0.000 claims description 6
- 238000000605 extraction Methods 0.000 claims description 5
- 239000007921 spray Substances 0.000 claims description 5
- 239000006228 supernatant Substances 0.000 claims description 5
- 239000000463 material Substances 0.000 claims description 4
- 239000003595 mist Substances 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 8
- 239000004615 ingredient Substances 0.000 abstract description 7
- 235000013305 food Nutrition 0.000 abstract description 5
- 238000005516 engineering process Methods 0.000 abstract description 4
- 238000005260 corrosion Methods 0.000 abstract description 3
- 235000016709 nutrition Nutrition 0.000 abstract description 3
- 206010059866 Drug resistance Diseases 0.000 abstract description 2
- 239000003963 antioxidant agent Substances 0.000 abstract description 2
- 230000003078 antioxidant effect Effects 0.000 abstract description 2
- 235000006708 antioxidants Nutrition 0.000 abstract description 2
- 230000003115 biocidal effect Effects 0.000 abstract description 2
- 239000008845 cholagoga Substances 0.000 abstract description 2
- 229940124571 cholagogue Drugs 0.000 abstract description 2
- 230000002349 favourable effect Effects 0.000 abstract description 2
- 230000002443 hepatoprotective effect Effects 0.000 abstract description 2
- 231100000331 toxic Toxicity 0.000 abstract description 2
- 230000002588 toxic effect Effects 0.000 abstract description 2
- 238000000034 method Methods 0.000 description 12
- 241000894006 Bacteria Species 0.000 description 11
- ZMQAAUBTXCXRIC-UHFFFAOYSA-N safrole Chemical compound C=CCC1=CC=C2OCOC2=C1 ZMQAAUBTXCXRIC-UHFFFAOYSA-N 0.000 description 8
- 238000012360 testing method Methods 0.000 description 7
- 235000008429 bread Nutrition 0.000 description 6
- 239000000126 substance Substances 0.000 description 6
- 241000588724 Escherichia coli Species 0.000 description 5
- 230000003385 bacteriostatic effect Effects 0.000 description 5
- 230000002829 reductive effect Effects 0.000 description 5
- CHHHXKFHOYLYRE-UHFFFAOYSA-M 2,4-Hexadienoic acid, potassium salt (1:1), (2E,4E)- Chemical compound [K+].CC=CC=CC([O-])=O CHHHXKFHOYLYRE-UHFFFAOYSA-M 0.000 description 4
- 239000004599 antimicrobial Substances 0.000 description 4
- 230000002401 inhibitory effect Effects 0.000 description 4
- 239000007788 liquid Substances 0.000 description 4
- 238000002156 mixing Methods 0.000 description 4
- 235000010241 potassium sorbate Nutrition 0.000 description 4
- 239000004302 potassium sorbate Substances 0.000 description 4
- 229940069338 potassium sorbate Drugs 0.000 description 4
- 241000589517 Pseudomonas aeruginosa Species 0.000 description 3
- 241000293869 Salmonella enterica subsp. enterica serovar Typhimurium Species 0.000 description 3
- 238000004500 asepsis Methods 0.000 description 3
- 238000005119 centrifugation Methods 0.000 description 3
- 239000003814 drug Substances 0.000 description 3
- 238000011156 evaluation Methods 0.000 description 3
- 238000002474 experimental method Methods 0.000 description 3
- 230000001953 sensory effect Effects 0.000 description 3
- 239000000243 solution Substances 0.000 description 3
- 239000000725 suspension Substances 0.000 description 3
- FFRBMBIXVSCUFS-UHFFFAOYSA-N 2,4-dinitro-1-naphthol Chemical compound C1=CC=C2C(O)=C([N+]([O-])=O)C=C([N+]([O-])=O)C2=C1 FFRBMBIXVSCUFS-UHFFFAOYSA-N 0.000 description 2
- 241001478240 Coccus Species 0.000 description 2
- 241000191967 Staphylococcus aureus Species 0.000 description 2
- 235000009754 Vitis X bourquina Nutrition 0.000 description 2
- 235000012333 Vitis X labruscana Nutrition 0.000 description 2
- 240000006365 Vitis vinifera Species 0.000 description 2
- 235000014787 Vitis vinifera Nutrition 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 244000052616 bacterial pathogen Species 0.000 description 2
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 description 2
- 235000014121 butter Nutrition 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 238000001514 detection method Methods 0.000 description 2
- 229940079593 drug Drugs 0.000 description 2
- 230000002255 enzymatic effect Effects 0.000 description 2
- 235000013312 flour Nutrition 0.000 description 2
- 244000078673 foodborn pathogen Species 0.000 description 2
- 238000007710 freezing Methods 0.000 description 2
- 230000008014 freezing Effects 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 239000011785 micronutrient Substances 0.000 description 2
- 235000013369 micronutrients Nutrition 0.000 description 2
- 235000013336 milk Nutrition 0.000 description 2
- 239000008267 milk Substances 0.000 description 2
- 210000004080 milk Anatomy 0.000 description 2
- 150000002989 phenols Chemical class 0.000 description 2
- 238000004321 preservation Methods 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 230000001681 protective effect Effects 0.000 description 2
- 238000011084 recovery Methods 0.000 description 2
- 239000000758 substrate Substances 0.000 description 2
- 239000005711 Benzoic acid Substances 0.000 description 1
- 241000407170 Curcuma Species 0.000 description 1
- 235000014375 Curcuma Nutrition 0.000 description 1
- 241000388070 Curcuma caesia Species 0.000 description 1
- 235000008359 Curcuma caesia Nutrition 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- 102000004190 Enzymes Human genes 0.000 description 1
- 108010068370 Glutens Proteins 0.000 description 1
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 229930182555 Penicillin Natural products 0.000 description 1
- JGSARLDLIJGVTE-MBNYWOFBSA-N Penicillin G Chemical compound N([C@H]1[C@H]2SC([C@@H](N2C1=O)C(O)=O)(C)C)C(=O)CC1=CC=CC=C1 JGSARLDLIJGVTE-MBNYWOFBSA-N 0.000 description 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
- 241000235342 Saccharomycetes Species 0.000 description 1
- 241000607142 Salmonella Species 0.000 description 1
- 244000269722 Thea sinensis Species 0.000 description 1
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 235000010233 benzoic acid Nutrition 0.000 description 1
- 235000021028 berry Nutrition 0.000 description 1
- 238000002815 broth microdilution Methods 0.000 description 1
- 230000000711 cancerogenic effect Effects 0.000 description 1
- 125000000837 carbohydrate group Chemical group 0.000 description 1
- 235000014633 carbohydrates Nutrition 0.000 description 1
- 231100000357 carcinogen Toxicity 0.000 description 1
- 239000003183 carcinogenic agent Substances 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 239000003610 charcoal Substances 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 230000008878 coupling Effects 0.000 description 1
- 238000010168 coupling process Methods 0.000 description 1
- 238000005859 coupling reaction Methods 0.000 description 1
- VFLDPWHFBUODDF-FCXRPNKRSA-N curcumin Chemical compound C1=C(O)C(OC)=CC(\C=C\C(=O)CC(=O)\C=C\C=2C=C(OC)C(O)=CC=2)=C1 VFLDPWHFBUODDF-FCXRPNKRSA-N 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 238000004043 dyeing Methods 0.000 description 1
- 230000001408 fungistatic effect Effects 0.000 description 1
- 235000021312 gluten Nutrition 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 230000001939 inductive effect Effects 0.000 description 1
- 238000001095 inductively coupled plasma mass spectrometry Methods 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 239000013642 negative control Substances 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 244000144985 peep Species 0.000 description 1
- 229940049954 penicillin Drugs 0.000 description 1
- 239000013641 positive control Substances 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 238000012113 quantitative test Methods 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- 239000008223 sterile water Substances 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 230000001629 suppression Effects 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 239000011573 trace mineral Substances 0.000 description 1
- 235000013619 trace mineral Nutrition 0.000 description 1
- 238000004879 turbidimetry Methods 0.000 description 1
- 108010078692 yeast proteinase B Proteins 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L3/00—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
- A23L3/34—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals
- A23L3/3454—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals in the form of liquids or solids
- A23L3/3463—Organic compounds; Microorganisms; Enzymes
- A23L3/3472—Compounds of undetermined constitution obtained from animals or plants
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L5/00—Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Abstract
The invention belongs to preservative technology fields, and in particular to application of the black ginger as preservative.Manufactured black ginger after the processing of fresh ginger high temperature and humidity is used as preservative by the present invention.The black ginger powder of the present invention is as aseptic applications, and ingredient is simple, and favorable anti-corrosion effect has no toxic side effect.Black ginger nutritional ingredient improves simultaneously, improves smell, making an addition to has the effects of Hepatoprotective cholagogue, anti-oxidant in food;Black ginger powder is a kind of pure natural food preservative, and water solubility is good, antibiotic property is good and is not likely to produce drug resistance.
Description
Technical field
The invention belongs to preservative technology fields, and in particular to application of the black ginger as preservative.
Background technique
Ginger is long in China's usage history, can be dish, can be flavouring, can more be used as medicine.But ginger is due to spicy
Groups of people can be brought with the feeling detested or some adverse effects can be generated to human body.
Black ginger, there are two types of understanding for ordinary circumstance: one kind referring to baked ginger or ginger charcoal, i.e., fries after rhizoma zingiberis being made in fresh ginger to outer black
Interior is in strong yellow.The key point of the processing procedure is the grasp of the duration and degree of heating and time.Another kind refers to Zingiber curcuma evil mind
Ginger (Curcuma caesiaRoxb.).Black ginger of the present invention, is different from the above two, be after being handled with fresh ginger made of,
Its micronutrient levels is higher, and nonirritant acid, treated, and nutriment is easier to be absorbed by the human body, and is health care
Ultimate food.
Existing preservative is classified by composed structure, there is chemical preservation and natural anticorrosion two major classes.For a long time, benzoic acid
The synthetic preservatives such as sodium, potassium sorbate, parabens are widely used in food industry.Due to most of chemical preservations
Agent has certain toxicity, and people urgently want to find the substitute of chemical preservative.In recent years, natural type food preservative
Research becomes the emphasis studied both at home and abroad.Natural antiseptic agent is not only nontoxic, harmless, also has certain nutriture value
Value is generally welcome and is paid attention to by people.Therefore, safety and stability, environmentally protective, superior performance efficient, wide spectrum is developed
Natural antiseptic agent has huge practical significance.
Summary of the invention
Obtained black ginger is as natural antiseptic agent after the present invention handles ginger high temperature and humidity, the preservative safety and stability,
Environmentally protective, superior performance has certain inhibiting effect to common food source pathogenic bacteria.
To achieve the above object, the present invention takes following technical scheme:
The present invention provides application of the black ginger as preservative, and the black ginger is that fresh ginger is made after high temperature and humidity is handled
At.
Further, the preparation of the black ginger of processing specifically includes the following contents:
(1) color just, without blackspot, without mildew and rot ginger is cleaned, dries, is then freezed under the conditions of -15 DEG C~-25 DEG C
12~for 24 hours;
Cryogenic freezing processing can destroy Ginger Tissue cell interior structure, enhance cell leakage, make its Dissolve things inside stream
Out, the compartmentalization distribution for having broken enzyme, browning substrates and oxygen, comes into full contact with it, enzymatic browning is caused to be accelerated, and is non-enzymatic
A large amount of browning substrates are laid in brown stain, accelerate the nonenzymatic browning reaction process after heating, shorten the reaction time.It is pre- due to freezing
Processing accelerates the reflection process of brown stain, and the content of reduced sugar and total phenol is largely accumulated, and is not only advantageous to the shape of black ginger melanoidin
At, and greatly increase the nutritional ingredient and functional component of black ginger.
(2) high temperature and humidity is handled: the ginger freezed is packed into high-temp resisting high-humidity resisting packaging bag or stainless steel box, then
Packaging bag or stainless steel box are placed in closed container and are handled,
First processing stage: 30~45 DEG C of set temperature, humidity 75~85% is handled 36~72 hours;
Second processing stage: 50~70 DEG C of set temperature, humidity 80~90% is handled 100~144 hours;
Third processing stage: 75~85 DEG C of set temperature, humidity 90~95% is handled 120~168 hours;Pass through setting
Different temperature accelerates the decomposition of carbohydrate, accelerates the accumulation of the substances such as reduced sugar, soluble sugar, phenols.
Further, black ginger powder is made in black ginger, is then added in raw-food material and is used as food preservative.
Further, the mass percent that the black ginger powder adds in raw-food material is 0.025%~0.1%.
Further, the preparation of the black ginger powder specifically: by mixing according to mass ratio 1:5 for Hei Jiang and water, reflux is mentioned
It takes twice, each 2h, combined extract, centrifuging and taking supernatant, is concentrated into medicinal extract, subsequent spray is dry, obtains black ginger powder.
Further, the preparation of the black ginger powder specifically: black ginger is dried, is then crushed, 100 mesh are crossed
Sieve.
The invention has the following advantages:
(1) the black ginger powder of the present invention is as aseptic applications, and ingredient is simple, and favorable anti-corrosion effect has no toxic side effect.Existing anti-corrosion
Agent mostly uses mixed species preservative, and ingredient is miscellaneous, and majority contains chemical synthesis substance, can generate side effect;
(2) the black ginger nutritional ingredient that high temperature and humidity is handled improves, and improves the original smell of ginger, makes an addition to food
In have the effects of Hepatoprotective cholagogue, anti-oxidant;
(3) black ginger powder is a kind of pure natural food preservative, and water solubility is good, antibiotic property is good and is not likely to produce drug resistance
Property.
(4) the safrole content in ginger is high, and black ginger prepared by the present invention safrole content compared with ginger significantly drops
It is low.
Specific embodiment
Following embodiment is technical solution in order to better illustrate the present invention, rather than limits guarantor of the invention with this
Protect range.
Ginger used is the same a collection of ginger purchased from market in embodiment.
Embodiment 1
The preparation (method one) of black ginger powder:
(1) color just, without blackspot, without mildew and rot ginger 1500g is cleaned, 12h is then freezed under the conditions of -20 DEG C;
(2) high temperature and humidity is handled: the ginger freezed being packed into PVC packaging bag, every packet 500g fills 3 packets, then it
It is placed in closed container and is handled,
First processing stage: 30 DEG C of set temperature, humidity 75% is handled 36 hours;
Second processing stage: 50 DEG C of set temperature, humidity 80% is handled 100 hours;
Third processing stage: 75 DEG C of set temperature, humidity 90% is handled 120 hours;
(3) mixing according to mass ratio 1:5 by Hei Jiang and water, 100 DEG C of refluxing extractions twice, each 2h, combined extract,
Centrifugation (5000rpm, 10min) takes supernatant, and 60~70 DEG C are concentrated under reduced pressure into medicinal extract, the dry (intake air temperature of subsequent spray
200 DEG C, 80 DEG C of air outlet temperature), black ginger powder 27g is obtained, the moisture content of black ginger powder is 9% or so.
Embodiment 2
The preparation (method one) of black ginger powder:
(1) color just, without blackspot, without mildew and rot ginger 1500g is cleaned, 16h is then freezed under the conditions of -20 DEG C;
(2) high temperature and humidity is handled: the ginger freezed being packed into PVC packaging bag, every packet 500g fills 3 packets, then it
It is placed in closed container and is handled,
First processing stage: 40 DEG C of set temperature, humidity 80% is handled 48 hours;
Second processing stage: 60 DEG C of set temperature, humidity 85% is handled 120 hours;
Third processing stage: 80 DEG C of set temperature, humidity 92% is handled 140 hours;
(3) mixing according to mass ratio 1:5 by Hei Jiang and water, 100 DEG C of refluxing extractions twice, each 2h, combined extract,
Centrifugation (5000rpm, 10min) takes supernatant, and 60~70 DEG C are concentrated under reduced pressure into medicinal extract, the dry (intake air temperature 200 of subsequent spray
DEG C, 80 DEG C of air outlet temperature), black ginger powder 32.4g is obtained, the moisture content of black ginger powder is 9% or so.
Embodiment 3
The preparation (method one) of black ginger powder:
(1) color just, without blackspot, without mildew and rot ginger 2400g is cleaned, is then freezed for 24 hours under the conditions of -20 DEG C;
(2) high temperature and humidity is handled: the ginger of cold mistake being packed into PVC packaging bag, every packet 800g fills 3 packets, then it is put
It sets and is handled in closed container,
First processing stage: 45 DEG C of set temperature, humidity 85% is handled 72 hours;
Second processing stage: 70 DEG C of set temperature, humidity 90% is handled 144 hours;
Third processing stage: 85 DEG C of set temperature, humidity 95% is handled 168 hours;
(3) mixing according to mass ratio 1:5 by Hei Jiang and water, 100 DEG C of refluxing extractions twice, each 2h, combined extract,
Centrifugation (5000rpm, 10min) takes supernatant, and 60~70 DEG C are concentrated under reduced pressure into medicinal extract, the dry (intake air temperature 200 of subsequent spray
DEG C, 80 DEG C of air outlet temperature), black ginger powder 43.2g is obtained, the moisture content of black ginger powder is 9% or so.
Embodiment 4
The preparation (method two) of black ginger powder:
(1) color just, without blackspot, without mildew and rot ginger 600g is cleaned, 12h is then freezed under the conditions of -20 DEG C;
(2) high temperature and humidity is handled: the ginger freezed being packed into stainless steel box, every box 300g fills 2 boxes, then it
It is placed in closed container and is handled,
First processing stage: 30 DEG C of set temperature, humidity 75% is handled 36 hours;
Second processing stage: 50 DEG C of set temperature, humidity 80% is handled 100 hours;
Third processing stage: 75 DEG C of set temperature, humidity 90% is handled 120 hours;
(3) 3h is dried under the conditions of 65 DEG C, obtains black ginger of the moisture content 7.5%~11%;Use pulverizer
Black ginger powder is broken, it sieves with 100 mesh sieve, obtains black ginger powder 54g.
Embodiment 5
The preparation (method two) of black ginger powder:
(1) color just, without blackspot, without mildew and rot ginger 800g is cleaned, 12h is then freezed under the conditions of -20 DEG C;
(2) high temperature and humidity is handled: the ginger freezed being packed into stainless steel box, every box 400g fills 2 boxes, then it
It is placed in closed container and is handled,
First processing stage: 40 DEG C of set temperature, humidity 80% is handled 48 hours;
Second processing stage: 60 DEG C of set temperature, humidity 85% is handled 120 hours;
Third processing stage: 80 DEG C of set temperature, humidity 92% is handled 140 hours;
(3) 3h is dried under the conditions of 65 DEG C, obtains black ginger of the moisture content 7.5%~11%;Use pulverizer
Black ginger powder is broken, it sieves with 100 mesh sieve, obtains black ginger powder 72g.
Embodiment 6
The preparation (method two) of black ginger powder:
(1) color just, without blackspot, without mildew and rot ginger 1000g is cleaned, is then freezed for 24 hours under the conditions of -20 DEG C;
(2) high temperature and humidity is handled: the ginger freezed being packed into stainless steel box, every box 500g fills 2 boxes, then it
It is placed in closed container and is handled,
First processing stage: 45 DEG C of set temperature, humidity 85% is handled 72 hours;
Second processing stage: 70 DEG C of set temperature, humidity 90% is handled 144 hours;
Third processing stage: 85 DEG C of set temperature, humidity 95% is handled 168 hours;
(3) 3h is dried under the conditions of 65 DEG C, obtains black ginger of the moisture content 7.5%~11%;Use pulverizer
Black ginger powder is broken, it sieves with 100 mesh sieve, obtains black ginger powder 90g.
Embodiment 7
Using mass spectrograph, with ICP-MS plasma inductive coupling mass spectrography to black ginger made from ginger, Examples 1 to 3
Black ginger powder made from powder and embodiment 4~6 carries out trace element detection, and safrole, phenols etc. are examined using high performance liquid chromatograph
It surveys, as a result as shown in the table.
Each Indexs measure value in 1 ginger of table and black ginger powder
Note: data are mean+/-standard error in table.
The result shows that: the micronutrient levels in black ginger is higher than ginger, and nonirritant acid, obtains after processing
The nutriment of black ginger is easier to be absorbed by the human body, while carcinogen safrole content reduces.In addition, refluxing extraction obtains
Black ginger powder in microelement slightly above crush obtained black ginger powder.
Embodiment 8
Bacteriostatic experiment
Black ginger powder prepared by embodiment 1 and the black ginger powder of 4 preparations carry out bacteriostatic experiment, specific as follows:
(1) 4 kinds of food-borne pathogens Escherichia coli (E.coli), staphylococcus aureus (S.aureus), mouse wound are selected
The black ginger powder suppression that cold salmonella (S.typhimurium), Pseudomonas aeruginosa (P.Aeruginosa) prepare as embodiment 1 and 4
The test sample of bacterium experiment, its minimal inhibitory concentration MIC value of quantitative test.Using doubling dilution prepared by embodiment 1 and 4
Black ginger powder is diluted, and concentration is successively set as 2mg/ml, 1mg/ml, 0.5mg/ml, 0.25mg/ml, 0.125mg/ml.
(2) Luria-Bertani (LB) liquid and solid medium are prepared.
(3) activated spawn dips bacterium solution scribing line coated plate with collarium is chosen.
(4) 37 DEG C of insulating box cultures of picking single bacterium colony on the plate from length after good.
(5) bacteria suspension after recovery culture is diluted to 1 × 10 with Maxwell turbidimetry6~1 × 108CFU/ml is separately added into
Into 96 porocyte culture plates, test sample is then added, each sample concentration in triplicate, is put into 37 DEG C of insulating box cultures.
Negative control (only culture solution) and positive control (penicillin concn is 1 μ g/ml) are set.
(6) whether liquid is muddy in peep hole after culture 16~for 24 hours, record.
(7) the black ginger powder that as the result is shown prepared by embodiment 1 and 4 has bacteriostasis to 4 kinds of bacterium.The black ginger powder of embodiment 1
To Escherichia coli, staphylococcus aureus, salmonella typhimurium MIC value in 0.25mg/ml or so, the MIC of Pseudomonas aeruginosa
Value is in 0.5mg/ml or so.The black ginger powder of embodiment 4 to the MIC value of Escherichia coli in 0.5mg/ml or so, to golden yellow grape
Coccus, salmonella typhimurium MIC value in 0.25mg/ml or so, to the MIC value of Pseudomonas aeruginosa in 1mg/ml or so.
The bacteriostatic test result of the black ginger powder of 2 embodiment 1 of table preparation
Note: "-" indicates asepsis growth, and "+" indicates bacterium growth
The bacteriostatic test result of the black ginger powder of 3 embodiment 4 of table preparation
Note: "-" indicates asepsis growth, and "+" indicates bacterium growth
Embodiment 9
Antibacterial comparative example
In order to compare natural antiseptic agent and chemical classes preservative to 2 kinds of food-borne pathogens (Escherichia coli and golden yellow Portugal
Grape coccus) fungistatic effect, now by etc. two kinds of preservatives of mass concentrations the inhibiting rate of pathogenic bacteria is summarized as follows.
(1) take on the market common potassium sorbate preservative be prepared into mass percent be 1.2%, 0.6%, 0.3%,
0.15%, 0.075% preservative 1.
(2) take black ginger powder (preparation of embodiment 3) be configured to mass percent be 1.2%, 0.6%, 0.3%, 0.15%,
0.075% preservative 2.
(3) minimal inhibitory concentration measurement uses standard broth dilution method: by the bacteria suspension Maxwell after recovery culture than turbid
Method is diluted to 1 × 106CFU/mL takes bacteria suspension and each 100 μ L of preservative to be separately added into 96 orifice plates respectively with pipettor.37℃
After culture for 24 hours, living cells dyeing is carried out with MTT, the drug concentration for visually observing the minimum drug concentration hole of no chromogenic reaction is sentenced
Break as MIC value.
(4) test result discovery potassium sorbate has apparent bacteriostasis when mass concentration percentage is 0.3%, and black
Ginger powder just has good bacteriostasis at 0.075%.
The comparison of the bacteriostatic test of the black ginger powder of table 4 and potassium sorbate
Note: "-" indicates asepsis growth, and "+" indicates bacterium growth
Embodiment 10
Application of the black ginger powder as preservative in bread
Ingredient: Strong flour 100g, one, egg, milk powder 15g, butter 8g, cerevisin 1g, berry sugar 12g, salt
0.6g, water 72g, black ginger powder 0.1g, black ginger powder used in the present embodiment are black ginger powder prepared by embodiment 4.
Bread preparation process:
(1) by load weighted flour, milk powder, sugar, saccharomycete, black ginger powder etc. is mixed.
(2) egg and water accomplished fluently are poured into after a hole is dug in centre, slowly stirred agglomerating.
(3) dough is rubbed to gluten and is preliminarily formed, butter is added, continues to rub.
(4) dough mixed is kneaded into circle, it is seamless, it applies and oils in dough bottom, cover preservative film, be placed at room temperature
Stand 15 minutes.
(5) dough stood is taken out, pressing exhaust, and divides and plucks into uniform small group, carry out integer.Integer is good
The oiling of dough bottom, is placed on the baking tray for being placed with tinfoil.It is 35~40 DEG C that baking tray, which is placed on processing the temperature inside the box, and processing one is small
When.Handling to the volume of dough becomes 2 times to 2.5 times.
(6) dough handled well is put into oven, 180 DEG C of temperature, baked 20 minutes.Baked bread is taken out, is placed
It is cooled to room temperature that it can be served in the cool.
(7) bread is sealed in packaging bag and is placed at room temperature for observation color, smell, mouthfeel variation, placement 2, discovery bread
The moon is still intact.Sensory evaluation index: referring to People's Republic of China's required standard GB7100, sensory evaluation be see the table below.
5 bread sensory evaluation of table
Embodiment 11
The preparation of black ginger tea
(1) it is spare that vial is cleaned to horizontal high voltage sterilizing of going forward side by side, respectively label 15 days, 1 month, 2 months, 3 months, 5
Month.Black ginger powder 1g is accurately weighed, is averagely put into 5 not in the bottle of isolabeling.
(2) it jiggles uniformly, places to injection sterile water 500ml in every bottle respectively.
(3) it was taken out respectively at step (2) 15 days afterwards, 1 month, 2 months, 3 months, 5 months and is marked with 15 days, 1 month, 2
A month, 3 months, 5 months vials, observe color, smell, mouthfeel, the situation of change of clump count.Bacterium colony detection method can join
It is carried out according to GB/T 4789.24 and GB 29921.When 5 months, liquid is still clear in vial for test result discovery
Clear transparence has normal color, smell and mouthfeel, free from extraneous odour, the impurity such as floccule being visible by naked eyes.
The embodiment of the above is only used to explain the present invention, the scope of the present invention is not limited, for this technology
It, certainly can be according to technology contents disclosed in this specification, by way of replacing or changing for the technical staff in field
Other embodiments are made easily, therefore all changes and improvements etc. done in the principle of the present invention and process conditions, it should all wrap
It includes in scope of the present invention patent.
Claims (6)
1. application of the black ginger as preservative, which is characterized in that the black ginger is that fresh ginger is made after high temperature and humidity is handled
At.
2. application according to claim 1, which is characterized in that the preparation of the black ginger specifically includes the following contents:
(1) color just, without blackspot, without mildew and rot ginger is cleaned, dries, then freezes 12 under the conditions of -15 DEG C ~ -25 DEG C
~24 h;
(2) high temperature and humidity is handled: the ginger freezed being packed into high-temp resisting high-humidity resisting packaging bag or stainless steel box, then packaging
Bag or stainless steel box are placed in closed container and are handled:
First processing stage: 30~45 DEG C of set temperature, humidity 75~85% is handled 36~72 hours;
Second processing stage: 50~70 DEG C of set temperature, humidity 80~90% is handled 100~144 hours;
Third processing stage: 75~85 DEG C of set temperature, humidity 90~95% is handled 120~168 hours.
3. application according to claim 1, which is characterized in that black ginger powder is made in black ginger, is then added in raw-food material
As food preservative.
4. application according to claim 3, which is characterized in that the quality percentage that the black ginger powder adds in raw-food material
Than being 0.025%~0.1%.
5. application according to claim 3, which is characterized in that the preparation of the black ginger powder specifically: press Hei Jiang and water
It is mixed according to mass ratio 1:5, twice, 2 h, combined extract, centrifuging and taking supernatant are concentrated into medicinal extract to refluxing extraction every time, then spray
Mist is dry, obtains black ginger powder.
6. application according to claim 3, which is characterized in that the preparation of the black ginger powder specifically: do black ginger
It is dry, it is then crushed, is sieved with 100 mesh sieve.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201910532874.4A CN110214884A (en) | 2019-06-19 | 2019-06-19 | Application of the black ginger as preservative |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201910532874.4A CN110214884A (en) | 2019-06-19 | 2019-06-19 | Application of the black ginger as preservative |
Publications (1)
Publication Number | Publication Date |
---|---|
CN110214884A true CN110214884A (en) | 2019-09-10 |
Family
ID=67814001
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201910532874.4A Pending CN110214884A (en) | 2019-06-19 | 2019-06-19 | Application of the black ginger as preservative |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN110214884A (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN115176990A (en) * | 2022-08-19 | 2022-10-14 | 闽南师范大学 | Ginger sauce and preparation method thereof |
Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103564374A (en) * | 2013-10-28 | 2014-02-12 | 青岛农业大学 | Black garlic as well as fermentation process thereof |
CN103892220A (en) * | 2014-03-12 | 2014-07-02 | 菏泽天鸿果蔬有限公司 | Preparation technology of black garlic |
CN104783096A (en) * | 2014-01-17 | 2015-07-22 | 河南省淼雨饮品股份有限公司 | Quick fermentation method of black garlic by enzymatic reaction |
CN106962850A (en) * | 2017-03-29 | 2017-07-21 | 安徽农业大学 | A kind of preparation method of two-part black garlic |
KR20180110921A (en) * | 2017-03-30 | 2018-10-11 | 주식회사 건강다모아 | Manufacturing method of black ginger juice and black ginger juice using this method |
KR101932941B1 (en) * | 2018-07-06 | 2018-12-27 | 유시호 | A manufacturing method of functional black ginger having magnesium |
-
2019
- 2019-06-19 CN CN201910532874.4A patent/CN110214884A/en active Pending
Patent Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103564374A (en) * | 2013-10-28 | 2014-02-12 | 青岛农业大学 | Black garlic as well as fermentation process thereof |
CN104783096A (en) * | 2014-01-17 | 2015-07-22 | 河南省淼雨饮品股份有限公司 | Quick fermentation method of black garlic by enzymatic reaction |
CN103892220A (en) * | 2014-03-12 | 2014-07-02 | 菏泽天鸿果蔬有限公司 | Preparation technology of black garlic |
CN106962850A (en) * | 2017-03-29 | 2017-07-21 | 安徽农业大学 | A kind of preparation method of two-part black garlic |
KR20180110921A (en) * | 2017-03-30 | 2018-10-11 | 주식회사 건강다모아 | Manufacturing method of black ginger juice and black ginger juice using this method |
KR101932941B1 (en) * | 2018-07-06 | 2018-12-27 | 유시호 | A manufacturing method of functional black ginger having magnesium |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN115176990A (en) * | 2022-08-19 | 2022-10-14 | 闽南师范大学 | Ginger sauce and preparation method thereof |
CN115176990B (en) * | 2022-08-19 | 2023-11-14 | 闽南师范大学 | Ginger sauce and preparation method thereof |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
Shao et al. | Preparation, antioxidant and antimicrobial evaluation of hydroxamated degraded polysaccharides from Enteromorpha prolifera | |
Ye et al. | Antimicrobial and antioxidant activities of the essential oil from onion (Allium cepa L.) | |
Meot-Duros et al. | Radical scavenging, antioxidant and antimicrobial activities of halophytic species | |
Pundir et al. | Comparative studies on the antimicrobial activity of black pepper (Piper nigrum) and turmeric (Curcuma longa) extracts | |
Norziah et al. | Effect of extraction solvents on antioxidant and antimicrobial properties of fenugreek seeds (Trigonella foenum-graecum L.). | |
Abdeldaiem | Use of yellow pigment extracted from turmeric (Curcuma longa) rhizomes powder as natural food preservative | |
Yang et al. | Evaluation of chitosan coatings enriched with turmeric and green tea extracts on postharvest preservation of strawberries | |
Vidović et al. | Screening of changes in content of health benefit compounds, antioxidant activity and microbiological status of medicinal plants during the production of herbal filter tea | |
Akbar et al. | Functional, antioxidant, antimicrobial potential and food safety applications of curcuma longa and cuminum cyminum | |
Chang et al. | Antioxidant and antimicrobial activities of commercial rice wine extracts of Taiwanese Allium fistulosum | |
Asker Mohsen et al. | A. Active Constituents of Kiwi (Actinidia Deliciosa Planch) Peels and Their Biological Activities as Antioxidant, Antimicrobial and Anticancer | |
Xedzro et al. | Antibacterial efficacies and time-kill kinetics of indigenous Ghanaian spice extracts against Listeria monocytogenes and some other food-borne pathogenic bacteria | |
Adera et al. | Physicochemical properties and biological activities of garden cress (Lepidium sativum L.) seed and leaf oil extracts | |
CN110214884A (en) | Application of the black ginger as preservative | |
Romson et al. | Stability of antioxidant and antibacterial properties in heated turmeric-chili paste and its ingredients. | |
Gumus | Determination of the changes of antifungal properties of Satureja hortensis, Thymus vulgaris and Thymbra spicata exposed to gamma irradiation | |
Mazumder et al. | Evaluation of synergistic antimicrobial activity and antioxidant activity of blend of essential oil contains fennel, coriander, ajowan and caraway | |
Elakremi et al. | Chemical composition and biological activity of pistacia vera l. Leaves: beneficial effects of female leaves extract on food products | |
Jabin et al. | Effect of gamma irradiation on chemical composition, antioxidant activity, antibacterial activity, shelf life, and cytotoxicity in the peels of two mango varieties grown in Bangladesh | |
Park et al. | Decontamination of chokeberries (Aronia melanocarpa L.) by cold plasma treatment and its effects on biochemical composition and storage quality of their corresponding juices | |
Saber | Utilization of Cinnamon in Preparation and Preservation of Food Products from Microbial Contamination | |
Saddiq et al. | Assessment of phenolic content, free radical-scavenging capacity and antimicrobial activities of Truffle claveryi | |
Francilia et al. | Physicochemical properties and inhibitory effects of essential oils from selected local Spices | |
Cheng et al. | Antibacterial activities and mechanism of action of acetone extracts from Rabdosia rubescens | |
Mathur et al. | Pectin content as an index for screening different varieties of Apple (Pyrusmalus L.) of Kashmir (J&K) on the basis of antimicrobial activity |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
PB01 | Publication | ||
PB01 | Publication | ||
SE01 | Entry into force of request for substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
TA01 | Transfer of patent application right |
Effective date of registration: 20210427 Address after: 450002 No. 58 Hongdi Road, Jinshui District, Zhengzhou City, Henan Province Applicant after: Henan Napu Biotechnology Co.,Ltd. Applicant after: HENAN ACADEMY OF SCIENCES Address before: 450002 No. 58 Hongdi Road, Jinshui District, Zhengzhou City, Henan Province Applicant before: HENAN ACADEMY OF SCIENCES |
|
TA01 | Transfer of patent application right | ||
RJ01 | Rejection of invention patent application after publication |
Application publication date: 20190910 |
|
RJ01 | Rejection of invention patent application after publication |