CN110201626A - A kind of vulcanizing agent synthesis technology - Google Patents
A kind of vulcanizing agent synthesis technology Download PDFInfo
- Publication number
- CN110201626A CN110201626A CN201910390520.0A CN201910390520A CN110201626A CN 110201626 A CN110201626 A CN 110201626A CN 201910390520 A CN201910390520 A CN 201910390520A CN 110201626 A CN110201626 A CN 110201626A
- Authority
- CN
- China
- Prior art keywords
- reaction kettle
- fixedly connected
- water tank
- vulcanizing agent
- water
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
- B01D53/04—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/14—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by absorption
- B01D53/18—Absorbing units; Liquid distributors therefor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/28—Moving reactors, e.g. rotary drums
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J4/00—Feed or outlet devices; Feed or outlet control devices
- B01J4/001—Feed or outlet devices as such, e.g. feeding tubes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B08—CLEANING
- B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
- B08B9/00—Cleaning hollow articles by methods or apparatus specially adapted thereto
- B08B9/08—Cleaning containers, e.g. tanks
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C35/00—Heating, cooling or curing, e.g. crosslinking or vulcanising; Apparatus therefor
- B29C35/02—Heating or curing, e.g. crosslinking or vulcanizing during moulding, e.g. in a mould
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C319/00—Preparation of thiols, sulfides, hydropolysulfides or polysulfides
- C07C319/22—Preparation of thiols, sulfides, hydropolysulfides or polysulfides of hydropolysulfides or polysulfides
- C07C319/24—Preparation of thiols, sulfides, hydropolysulfides or polysulfides of hydropolysulfides or polysulfides by reactions involving the formation of sulfur-to-sulfur bonds
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2252/00—Absorbents, i.e. solvents and liquid materials for gas absorption
- B01D2252/10—Inorganic absorbents
- B01D2252/103—Water
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2253/00—Adsorbents used in seperation treatment of gases and vapours
- B01D2253/10—Inorganic adsorbents
- B01D2253/102—Carbon
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Analytical Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Thermal Sciences (AREA)
- Oral & Maxillofacial Surgery (AREA)
- Health & Medical Sciences (AREA)
- Mechanical Engineering (AREA)
- Physics & Mathematics (AREA)
- Mixers Of The Rotary Stirring Type (AREA)
- Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
Abstract
The invention discloses a kind of vulcanizing agent synthesis technologies, including synthesizer, the synthesizer includes fixing seat, the upper center of fixing seat is equipped with groove, the interior lower end of groove is fixedly connected with rotating disc, the upper end of rotating disc is rotatably connected to shaft, the upper end of shaft is fixedly connected with reaction kettle, the front upper portion of reaction kettle is fixedly connected with material injecting mechanism, the lower end of reaction kettle is arranged with ring gear, ring gear is fixedly connected on reaction kettle, the two sides upper end of reaction kettle is fixedly connected to filter mechanism, the inner upper end of reaction kettle is connected with cover board, the inside of cover board is fixedly connected with ball bearing, when work, the water stored in filter mechanism water tank of the present invention can carry out preliminary treatment to the gas with foreign flavor fallen in vulcanizing agent production process, and the activated charcoal strainer of filter mechanism is again filtered gas with foreign flavor, it solves at present, vulcanizing agent exists The offensive gases generated in production process cause certain pollution to environment, and on the influential problem of the health of staff.
Description
Technical field:
The invention belongs to synthesis technology field, in particular to a kind of vulcanizing agent synthesis technology.
Background technique:
Currently, vulcanizing agent is in process of production, many unpleasant gases can be generated, certain pollution is caused to environment,
Have an impact to the health of staff, when throwing raw materials, raw material is easy to be sprinkled upon the periphery of equipment, causes the waste of material.
Summary of the invention:
The object of the invention is that providing a kind of vulcanizing agent synthesis technology to solve the above-mentioned problems, solves mesh
Before, vulcanizing agent in process of production, can generate many unpleasant gases, certain pollution be caused to environment, to staff
Health have an impact, when throwing raw materials, raw material is easy the shortcomings that being sprinkled upon the periphery of equipment, causing the waste of material.
To solve the above-mentioned problems, the present invention provides a kind of technical solutions:
A kind of vulcanizing agent synthesis technology, including synthesizer, the synthesizer include fixing seat, the fixing seat it is upper
End middle part is equipped with groove, and the interior lower end of the groove is fixedly connected with rotating disc, and the upper end of the rotating disc is rotatably connected to
Shaft, the upper end of the shaft are fixedly connected with reaction kettle, and the front upper portion of the reaction kettle is fixedly connected with material injecting mechanism, institute
The lower end for stating reaction kettle is arranged with ring gear, and the ring gear is fixedly connected on reaction kettle, and the two sides upper end of the reaction kettle is solid
Surely it is connected with filter mechanism, the inner upper end of the reaction kettle is connected with cover board, and the inside of the cover board is fixedly connected with ball
Bearing, the side lower end of the reaction kettle are inserted with outlet pipe, and the upper end two sides of the fixing seat are fixedly connected to vertical plate, institute
It states vertical plate and is equipped with first sliding groove close to the side upper end of reaction kettle, the vertical plate is equipped with logical far from the side upper end of reaction kettle
Slot, the first sliding groove that the through slot and on the vertical plate of place is arranged are located in approximately the same plane, the interior subordinate of the first sliding groove
End slidably connects the first sliding block, and transverse slat is fixedly connected between first sliding block, is fixed in the middle part of the lower end of the transverse slat
It is connected with agitating shaft, the lower end ball bearing of the agitating shaft and the inside for extending to reaction kettle, the agitating shaft is fixedly connected
On ball bearing, the lower end two sides of the agitating shaft are fixedly connected to paddle, fixed company between the upper end of the vertical plate
It is connected to top plate.
Preferably, the material injecting mechanism includes filling tube, the filling tube passes through the outside of reaction kettle and extends to anti-
The inside of kettle is answered, the upper end of the filling tube is fixedly connected with transverse tube, and the transverse tube passes through the inside phase of filling tube and reaction kettle
Logical, the upper end of the transverse tube is fixedly connected there are two standpipe, and two standpipes are located at the upper end two sides of transverse tube, two institutes
The upper end for stating standpipe is fixedly connected to funnel, and the upper end diameter of the funnel is bigger than the diameter of place standpipe, the funnel
It is communicated by the inside of place standpipe and transverse tube, the upper end of the transverse tube is fixedly connected with water-supply-pipe, and the water-supply-pipe is located at
Between two standpipes, the upper end of the water-supply-pipe is fixedly connected with mounting flange, than two standpipes of diameter of the mounting flange
The distance between it is small.
Preferably, the filter mechanism includes water tank, the side inside the water tank close to reaction kettle is inserted with logical
Tracheae, the inside of water tank where the snorkel both passes through and the inside for all extending to reaction kettle, the water tank pass through ventilation
The inside of pipe and reaction kettle communicates, and one end that the snorkel is located at place water tank is fixedly connected to connecting tube, the water tank
The internal side upper end far from reaction kettle is inserted with escape pipe, and the escape pipe both passes through the inside of place water tank and extends
To the outside of place water tank, the inside of the escape pipe is fixedly connected to activated charcoal strainer, and the water tank outside is far from anti-
A middle side part of kettle is answered to be inserted with water inlet pipe, water tank where the water inlet pipe both passes through the outside of place water tank and all extends to
Inside, height of the water inlet pipe apart from place water tank lower end is than ipsilateral connecting tube lower end apart from the high of place water tank lower end
Degree is high.
Preferably, the upper end side of the fixing seat is fixedly connected with motor, the motor is positioned at cant board and instead
It answers between kettle, the output end of the motor is fixedly connected with rotation axis, and the upper end of the rotation axis is fixedly connected with gear.
Preferably, the gear and ring gear are located on same horizontal line, the gear and ring gear engagement connection.
Preferably, the lower end of the transverse slat is equipped with second sliding slot, the second sliding slot is in ring type structure, and described second is sliding
The inside two sides of slot slidably connect the second sliding block, and the lower end of second sliding block is fixedly connected to fixed link, described solid
The lower end of fixed pole is fixedly connected in the upper end of cover board.
Preferably, first sliding block is fixedly connected to supporting plate far from the side of transverse slat, the supporting plate is far from place
The side of first sliding block both passes through the through slot being arranged on same cant board and all extends to the outside of same cant board.
A kind of vulcanizing agent synthesis technology, which is characterized in that specific steps are as follows:
The first step, the inside that raw material are put into reaction kettle, i.e., by the mixture and basic catalyst of mercaptan and elemental sulfur
Put into the inside of reaction kettle；
Second step, starting motor, rotate reaction kettle in fixing seat, stir raw material by agitating shaft and paddle,
The gas generated in reaction process is discharged to the inside of water tank, and the activated charcoal strainer inside water and escape pipe in water tank can be to gas
Body is handled；
Third step opens outlet pipe, collects the reactant inside reaction kettle, and reactant is put into degassing equipment and is carried out
Vulcanizing agent can be obtained in degassing process；
Drainage equipment is mounted on water-supply-pipe by the 4th step, the internal water flooding to reaction kettle, starts motor, cleaning reaction
Residue on kettle inner wall.
Beneficial effects of the present invention:
1, when working, the water stored in filter mechanism water tank of the present invention can be to the gas with foreign flavor fallen in vulcanizing agent production process
Preliminary treatment is carried out, and the activated charcoal strainer of filter mechanism is again filtered gas with foreign flavor, solves currently, vulcanizing agent exists
The offensive gases generated in production process cause certain pollution to environment, and have an impact to the health of staff
The problem of.
2, it is provided with funnel on the standpipe of material injecting mechanism of the present invention, can be convenient for launching raw material when work, solves throwing
When putting raw material, raw material is easy the problem of being sprinkled upon the periphery of equipment, causing the waste of material.
Detailed description of the invention:
Detailed description will be given by the following detailed implementation and drawings by the present invention for ease of explanation,.
Fig. 1 is cut away view of the invention；
Fig. 2 is external structure schematic diagram of the invention；
Fig. 3 is enlarged structure schematic diagram at A in Fig. 2；
Fig. 4 is the structural schematic diagram of vertical plate of the present invention；
Fig. 5 is the structural schematic diagram of transverse slat of the present invention.
In figure: 1, fixing seat；2, groove；3, rotating disc；4, shaft；5, reaction kettle；6, material injecting mechanism；61, filling tube；
62, transverse tube；63, standpipe；64, funnel；65, water-supply-pipe；66, mounting flange；7, filter mechanism；71, water tank；72, snorkel；
73, connecting tube；74, escape pipe；75, activated charcoal strainer；76, water inlet pipe；8, ring gear；9, cover board；10, ball bearing；11, it stands
Plate；12, first sliding groove；13, through slot；14, the first sliding block；15, transverse slat；16, supporting plate；17, second sliding slot；18, the second sliding block；
19, fixed link；20, agitating shaft；21, paddle；22, motor；23, rotation axis；24, gear；25, outlet pipe；26, top plate.
Specific embodiment:
As shown in Figs. 1-5, present embodiment uses a kind of following technical scheme: vulcanizing agent synthesis technology, including closes
At device, the synthesizer includes fixing seat 1, and the upper center of the fixing seat 1 is equipped with groove 2, the inside of the groove 2
Lower end is fixedly connected with rotating disc 3, and the upper end of the rotating disc 3 is rotatably connected to shaft 4, and the upper end of the shaft 4 is fixed to be connected
It is connected to reaction kettle 5, the front upper portion of the reaction kettle 5 is fixedly connected with material injecting mechanism 6, and the lower end of the reaction kettle 5 is arranged with
Ring gear 8, the ring gear 8 are fixedly connected on reaction kettle 5, and the two sides upper end of the reaction kettle 5 is fixedly connected to filter mechanism
7, the inner upper end of the reaction kettle 5 is connected with cover board 9, and the inside of the cover board 9 is fixedly connected with ball bearing 10, described anti-
The side lower end of kettle 5 is answered to be inserted with outlet pipe 25, the upper end two sides of the fixing seat 1 are fixedly connected to vertical plate 11, described vertical
Plate 11 is equipped with first sliding groove 12 close to the side upper end of reaction kettle 5, and the vertical plate 11 is all provided with far from the side upper end of reaction kettle 5
There is through slot 13, the first sliding groove 12 that the through slot 13 and on place vertical plate 11 is arranged is located in approximately the same plane, and described first
The interior lower end of sliding slot 12 slidably connects the first sliding block 14, and transverse slat 15, institute are fixedly connected between first sliding block 14
It states and is fixedly connected with agitating shaft 20 in the middle part of the lower end of transverse slat 15, the lower end ball bearing 10 of the agitating shaft 20 and extend to reaction
The inside of kettle 5, the agitating shaft 20 are fixedly connected on ball bearing 10, and the lower end two sides of the agitating shaft 20 are fixedly connected with
There is paddle 21, is fixedly connected with top plate 26 between the upper end of the vertical plate 11.
Wherein, the material injecting mechanism 6 includes filling tube 61, and the filling tube 61 passes through the outside of reaction kettle 5 and extends to
The inside of reaction kettle 5, the upper end of the filling tube 61 are fixedly connected with transverse tube 62, and the transverse tube 62 passes through filling tube 61 and reaction
The inside of kettle 5 communicates, and the upper end of the transverse tube 62 is fixedly connected there are two standpipe 63, and two standpipes 63 are located at transverse tube
62 upper end two sides, the upper end of two standpipes 63 are fixedly connected to funnel 64, and the upper end diameter of the funnel 64 compares
The diameter of place standpipe 63 is big, and the funnel 64 is communicated by the inside of place standpipe 63 and transverse tube 62, the transverse tube 62
Upper end is fixedly connected with water-supply-pipe 65, and the water-supply-pipe 65 is located between two standpipes 63, and the upper end of the water-supply-pipe 65 is fixed
It is connected with mounting flange 66, the diameter of the mounting flange 66 is smaller than the distance between two standpipes 63.
Wherein, the filter mechanism 7 includes water tank 71, and 71 inside of water tank is inserted with close to the side of reaction kettle 5
Snorkel 72, the inside of water tank 71 where the snorkel 72 both passes through and the inside for all extending to reaction kettle 5, the water tank 71
It is communicated by the inside of snorkel 72 and reaction kettle 5, one end that the snorkel 72 is located at place water tank 71 is fixedly connected with
There is connecting tube 73,71 inside of water tank is inserted with escape pipe 74 far from the side upper end of reaction kettle 5, and the escape pipe 74 is
Across the inside of place water tank 71 and the outside of water tank 71 where all extending to, the inside of the escape pipe 74 is fixedly connected to
Activated charcoal strainer 75,71 outside of water tank are inserted with water inlet pipe 76, the water inlet pipe far from a middle side part of reaction kettle 5
76 both pass through the outside of place water tank 71 and all extend to the inside of place water tank 71, and the water inlet pipe 76 is apart from place water tank 71
Height of the height of lower end than ipsilateral 73 lower end of connecting tube apart from 71 lower end of place water tank is high.
Wherein, the upper end side of the fixing seat 1 is fixedly connected with motor 22, and the motor 22 is located at 11 He of cant board
Between reaction kettle 5, the output end of the motor 22 is fixedly connected with rotation axis 23, and the upper end of the rotation axis 23 is fixedly connected with
Gear 24.
Wherein, the gear 24 and ring gear 8 are located on same horizontal line, the gear 24 and the engagement connection of ring gear 8.
Wherein, the lower end of the transverse slat 15 be equipped with second sliding slot 17, the second sliding slot 17 be in ring type structure, described second
The inside two sides of sliding slot 17 slidably connect the second sliding block 18, and the lower end of second sliding block 18 is fixedly connected to fixed link
19, the lower end of the fixed link 19 is fixedly connected in the upper end of cover board 9.
Wherein, first sliding block 14 is fixedly connected to supporting plate 16 far from the side of transverse slat 15, and the supporting plate 16 is separate
The side of the first sliding block of place 14 both passes through the through slot 13 being arranged on same cant board 11 and all extends to the outside of same cant board 11.
A kind of vulcanizing agent synthesis technology, which is characterized in that specific steps are as follows:
The first step, the inside that raw material are put into reaction kettle 5, i.e., by the mixture and basic catalyst of mercaptan and elemental sulfur
Put into the inside of reaction kettle 5；
Second step, starting motor 22, rotate reaction kettle 5 in fixing seat 1, are stirred by agitating shaft 20 and paddle 21
Raw material, the gas generated in reaction process are discharged to the inside of water tank 71, the activity inside water and escape pipe 74 in water tank 71
Charcoal filter screen 75 can be handled gas；
Third step opens outlet pipe 25, collects the reactant inside reaction kettle 5, and reactant is put into degassing equipment
It is de-gassed, vulcanizing agent can be obtained；
Drainage equipment is mounted on water-supply-pipe 65 by the 4th step, the internal water flooding to reaction kettle 5, starts motor 22, cleaning
Residue on 5 inner wall of reaction kettle.
Specific: a kind of vulcanizing agent synthesis technology connects charged before use, the present invention to be moved to the place of work,
In use, raw material are put into funnel 64, raw material pass sequentially through standpipe 63, transverse tube 62 and filling tube 61 and inject reaction kettle 5
Funnel 64 and water-supply-pipe 65 are blocked in inside, then by internal water flooding of the water inlet pipe 76 to water tank 71, and the water surface are made to be located at water inlet
The lower end of pipe 76, then water inlet pipe 76 is blocked, then start motor 22, motor 22 passes through 23 rotate gear 24 of rotation axis, gear 24
Rotate reaction kettle 5 in fixing seat 1 by ring gear 8, since agitating shaft 20 is fixed on the ball bearing 10 being arranged inside cover board 9
On, so agitating shaft 20 and paddle 21 not can rotate when reaction kettle 5 rotates, to carry out to the raw material inside reaction kettle 5
Stirring, during raw material react, the gas of generation can be discharged into the inside of water tank 71, water by snorkel 72 and connecting tube 73
Water in case 71 can carry out preliminary treatment to gas, and then water tank 71 is being discharged by escape pipe 74 in gas, during this, outlet
The activated charcoal strainer 75 being arranged inside pipe 74 can remove the bad smell in gas, and staff can be by reaction kettle 5
Observation panel observing response the case where, after a period of time, close motor 22, open outlet pipe 25, the product after collecting reaction, and
Reactant is put into degassing equipment, is de-gassed, vulcanizing agent can be obtained, after work, drainage equipment can be consolidated
It is scheduled on water-supply-pipe 65, water is discharged into the inside of reaction kettle 5, start motor 22, water is stirred, clear up 5 inner wall of reaction kettle
Residue.
The above shows and describes the basic principles and main features of the present invention and the advantages of the present invention, the technology of the industry
Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the above embodiments and description only describe this
The principle of invention, without departing from the spirit and scope of the present invention, various changes and improvements may be made to the invention, these changes
Change and improvement all fall within the protetion scope of the claimed invention, the claimed scope of the invention by appended claims and its
Equivalent thereof.
Claims (8)
1. a kind of vulcanizing agent synthesis technology, which is characterized in that including synthesizer, the synthesizer includes fixing seat (1), institute
The upper center for stating fixing seat (1) is equipped with groove (2), and the interior lower end of the groove (2) is fixedly connected with rotating disc (3), institute
The upper end for stating rotating disc (3) is rotatably connected to shaft (4), and the upper end of the shaft (4) is fixedly connected with reaction kettle (5), described
The front upper portion of reaction kettle (5) is fixedly connected with material injecting mechanism (6), and the lower end of the reaction kettle (5) is arranged with ring gear (8), institute
It states ring gear (8) to be fixedly connected on reaction kettle (5), the two sides upper end of the reaction kettle (5) is fixedly connected to filter mechanism
(7), the inner upper end of the reaction kettle (5) is connected with cover board (9), and the inside of the cover board (9) is fixedly connected with ball bearing
(10), the side lower end of the reaction kettle (5) is inserted with outlet pipe (25), and the upper end two sides of the fixing seat (1) are fixed to be connected
It is connected to vertical plate (11), the vertical plate (11) is equipped with first sliding groove (12), the vertical plate close to the side upper end of reaction kettle (5)
(11) the side upper end far from reaction kettle (5) is equipped with through slot (13), and the through slot (13) and on place vertical plate (11) is arranged
First sliding groove (12) be located in approximately the same plane, the interior lower end of the first sliding groove (12) slidably connects the first sliding block
(14), it is fixedly connected with transverse slat (15) between first sliding block (14), is fixedly connected in the middle part of the lower end of the transverse slat (15)
Agitating shaft (20), the lower end ball bearing (10) of the agitating shaft (20) and the inside for extending to reaction kettle (5), the agitating shaft
(20) it being fixedly connected on ball bearing (10), the lower end two sides of the agitating shaft (20) are fixedly connected to paddle (21),
Top plate (26) are fixedly connected between the upper end of the vertical plate (11).
2. a kind of vulcanizing agent synthesis technology according to claim 1, it is characterised in that: the material injecting mechanism (6) includes note
Expects pipe (61), the filling tube (61) pass through the outside of reaction kettle (5) and extend to the inside of reaction kettle (5), the filling tube
(61) upper end is fixedly connected with transverse tube (62), and the transverse tube (62) is communicated by the inside of filling tube (61) and reaction kettle (5),
The upper end of the transverse tube (62) is fixedly connected there are two standpipe (63), and two standpipes (63) are located at the upper of transverse tube (62)
Two sides are held, the upper end of two standpipes (63) is fixedly connected to funnel (64), and the upper end diameter of the funnel (64) compares
The diameter of place standpipe (63) is big, and the funnel (64) is communicated by the inside of place standpipe (63) and transverse tube (62), described
The upper end of transverse tube (62) is fixedly connected with water-supply-pipe (65), and the water-supply-pipe (65) is located between two standpipes (63), described defeated
The upper end of water pipe (65) is fixedly connected with mounting flange (66), between than two standpipes (63) of diameter of the mounting flange (66)
Distance it is small.
3. a kind of vulcanizing agent synthesis technology according to claim 1, it is characterised in that: the filter mechanism (7) includes water
Case (71), the internal side close to reaction kettle (5) of the water tank (71) are inserted with snorkel (72), and the snorkel (72) is equal
Across place water tank (71) inside and all extend to the inside of reaction kettle (5), the water tank (71) passes through snorkel (72)
It is communicated with the inside of reaction kettle (5), one end that the snorkel (72) is located at place water tank (71) is fixedly connected to connecting tube
(73), the internal side upper end far from reaction kettle (5) of the water tank (71) is inserted with escape pipe (74), the escape pipe (74)
The inside of water tank (71) where both passing through and the outside for all extending to place water tank (71), the inside of the escape pipe (74) are solid
Surely it is connected with activated charcoal strainer (75), the external middle side part far from reaction kettle (5) of the water tank (71) is inserted with into water
It manages (76), the outside of water tank (71) where the water inlet pipe (76) both passes through and the inside for all extending to place water tank (71), institute
Height of the water inlet pipe (76) apart from place water tank (71) lower end is stated than ipsilateral connecting tube (73) lower end apart from place water tank (71)
The height of lower end is high.
4. a kind of vulcanizing agent synthesis technology according to claim 1, it is characterised in that: the upper end one of the fixing seat (1)
Side is fixedly connected with motor (22), and the motor (22) is between same cant board (11) and reaction kettle (5), the motor (22)
Output end be fixedly connected with rotation axis (23), the upper end of the rotation axis (23) is fixedly connected with gear (24).
5. a kind of vulcanizing agent synthesis technology according to claim 4, it is characterised in that: the gear (24) and ring gear (8)
On same horizontal line, the gear (24) and ring gear (8) engagement connection.
6. a kind of vulcanizing agent synthesis technology according to claim 1, it is characterised in that: the lower end of the transverse slat (15) is equipped with
Second sliding slot (17), the second sliding slot (17) are in ring type structure, and the inside two sides of the second sliding slot (17) are slidably connected
Have the second sliding block (18), the lower end of second sliding block (18) is fixedly connected to fixed link (19), the fixed link (19)
Lower end is fixedly connected with the upper end in cover board (9).
7. a kind of vulcanizing agent synthesis technology according to claim 1, it is characterised in that: first sliding block (14) is far from horizontal
The side of plate (15) is fixedly connected to supporting plate (16), and the supporting plate (16) both passes through far from the side of the first sliding block of place (14)
The through slot (13) that is arranged on same cant board (11) and the outside for all extending to same cant board (11).
8. a kind of vulcanizing agent synthesis technology according to claim 1, which is characterized in that specific steps are as follows:
The first step, the inside that raw material are put into reaction kettle (5), i.e., throw the mixture and basic catalyst of mercaptan and elemental sulfur
Enter the inside of reaction kettle (5)；
Second step, starting motor (22), rotate reaction kettle (5) on fixing seat (1), pass through agitating shaft (20) and paddle
(21) raw material are stirred, the gas generated in reaction process is discharged to the inside of water tank (71), water and escape pipe in water tank (71)
(74) internal activated charcoal strainer (75) can be handled gas；
Third step opens outlet pipe (25), collects reaction kettle (5) internal reactant, and reactant is put into degassing equipment
It is de-gassed, vulcanizing agent can be obtained；
Drainage equipment is mounted on water-supply-pipe (65) by the 4th step, the water filling to the inside of reaction kettle (5), is started motor (22),
Clear up the residue on reaction kettle (5) inner wall.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910390520.0A CN110201626B (en) | 2019-05-10 | 2019-05-10 | Vulcanizing agent synthesizing device and synthesizing process thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910390520.0A CN110201626B (en) | 2019-05-10 | 2019-05-10 | Vulcanizing agent synthesizing device and synthesizing process thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN110201626A true CN110201626A (en) | 2019-09-06 |
| CN110201626B CN110201626B (en) | 2021-04-02 |
Family
ID=67785798
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201910390520.0A Active CN110201626B (en) | 2019-05-10 | 2019-05-10 | Vulcanizing agent synthesizing device and synthesizing process thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN110201626B (en) |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5068445A (en) * | 1988-04-14 | 1991-11-26 | Societe Nationale Elf Aquitaine (Production) | Process for the preparation of organic disulphides and polysulphides |
| CN106582395A (en) * | 2016-12-18 | 2017-04-26 | 南昌叁润科技有限公司 | Remaining material scraping device of stirring bar for rare earth recycling and stirring |
| CN108211936A (en) * | 2018-01-25 | 2018-06-29 | 毛孝人 | A kind of agricultural liquids fertilizer stirs and evenly mixs equipment |
| CN208612416U (en) * | 2018-07-18 | 2019-03-19 | 东莞金派工贸有限公司 | It is a kind of for heating the thermal energy collecting structure of reaction kettle |
| CN208727260U (en) * | 2018-07-10 | 2019-04-12 | 烟台只楚化学新材料股份有限公司 | A kind of chemical solution mixing arrangement stirred evenly |
-
2019
- 2019-05-10 CN CN201910390520.0A patent/CN110201626B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5068445A (en) * | 1988-04-14 | 1991-11-26 | Societe Nationale Elf Aquitaine (Production) | Process for the preparation of organic disulphides and polysulphides |
| CN106582395A (en) * | 2016-12-18 | 2017-04-26 | 南昌叁润科技有限公司 | Remaining material scraping device of stirring bar for rare earth recycling and stirring |
| CN108211936A (en) * | 2018-01-25 | 2018-06-29 | 毛孝人 | A kind of agricultural liquids fertilizer stirs and evenly mixs equipment |
| CN208727260U (en) * | 2018-07-10 | 2019-04-12 | 烟台只楚化学新材料股份有限公司 | A kind of chemical solution mixing arrangement stirred evenly |
| CN208612416U (en) * | 2018-07-18 | 2019-03-19 | 东莞金派工贸有限公司 | It is a kind of for heating the thermal energy collecting structure of reaction kettle |
Also Published As
| Publication number | Publication date |
|---|---|
| CN110201626B (en) | 2021-04-02 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN107998761A (en) | A kind of marine exhaust desulfurizer and method | |
| US3909291A (en) | Comestible cleaning apparatus | |
| CN208727266U (en) | A kind of environmental protecting device for collecting chemical industry solid liquid waste | |
| CN110201626A (en) | A kind of vulcanizing agent synthesis technology | |
| CN219186375U (en) | Environment-friendly engineering waste gas purification device | |
| CN210251692U (en) | Dust absorption system for crushing chemical raw materials | |
| CN114604997B (en) | Desulfurization waste water integrated treatment's device | |
| CN109289287A (en) | A kind of spent acid filtering recovering device | |
| CN210065223U (en) | Sewage treatment equipment | |
| CN112126558A (en) | Automatic filtering device for red date fruit wine brewing residues | |
| CN208151096U (en) | Tub oil water separator | |
| CN208193843U (en) | A kind of vacuum filter being separated by solid-liquid separation for insoluble sulfur | |
| CN209076171U (en) | A kind of garbage separator | |
| CN209034200U (en) | A kind of agitating device of dairy produce | |
| CN218529908U (en) | Turnover type medium filter | |
| CN112011440B (en) | Biogas fermentation tank | |
| CN220723729U (en) | Purifying and filtering device for animal drinking water | |
| CN217696230U (en) | ICU nursing patient food treatment facility | |
| CN213623621U (en) | Fruit vegetables juice waste water flocculation treatment device | |
| CN115152826B (en) | Device for rinsing minced fillet by mixing filtered water and ozone water | |
| CN216538037U (en) | Stirring machine with dust removal effect for production of knife scraping cloth | |
| CN109316815A (en) | Pressurize disc stack filter | |
| CN212441417U (en) | Pulp stirring device | |
| CN217377472U (en) | Activated carbon tank of water inlet softening treatment device | |
| CN221246270U (en) | Washing kettle for sodium carboxymethyl cellulose production |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |