CN110142193A - A kind of high intensity solid-state superslide moves the preparation method of coating - Google Patents
A kind of high intensity solid-state superslide moves the preparation method of coating Download PDFInfo
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- CN110142193A CN110142193A CN201910389375.4A CN201910389375A CN110142193A CN 110142193 A CN110142193 A CN 110142193A CN 201910389375 A CN201910389375 A CN 201910389375A CN 110142193 A CN110142193 A CN 110142193A
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05D—PROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05D5/00—Processes for applying liquids or other fluent materials to surfaces to obtain special surface effects, finishes or structures
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05D—PROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05D5/00—Processes for applying liquids or other fluent materials to surfaces to obtain special surface effects, finishes or structures
- B05D5/08—Processes for applying liquids or other fluent materials to surfaces to obtain special surface effects, finishes or structures to obtain an anti-friction or anti-adhesive surface
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05D—PROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05D7/00—Processes, other than flocking, specially adapted for applying liquids or other fluent materials to particular surfaces or for applying particular liquids or other fluent materials
- B05D7/24—Processes, other than flocking, specially adapted for applying liquids or other fluent materials to particular surfaces or for applying particular liquids or other fluent materials for applying particular liquids or other fluent materials
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D183/00—Coating compositions based on macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon, with or without sulfur, nitrogen, oxygen, or carbon only; Coating compositions based on derivatives of such polymers
- C09D183/04—Polysiloxanes
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/08—Anti-corrosive paints
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/16—Antifouling paints; Underwater paints
- C09D5/1687—Use of special additives
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/18—Fireproof paints including high temperature resistant paints
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05D—PROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05D2601/00—Inorganic fillers
- B05D2601/20—Inorganic fillers used for non-pigmentation effect
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05D—PROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05D2602/00—Organic fillers
Abstract
The present invention provides the preparation method that a kind of high-intensitive solid-state superslide moves coating, which can effectively prevent basis material to be sticked by water, grease, blood, ice and biomembrane etc., belong to material surface modifying technology field.The substrate can with and be not limited to the surfaces of solids such as metal, plastics, glass, timber, concrete, leather, paper.Above-mentioned substrate is handled first with the solution impregnation of the filtered masking liquid containing nano-ceramic particle and lubricant after evenly mixing；Finally infiltration treated solid substrate is taken out, it is allowed to do solid work naturally or quick 1~2 hour completion coating ceramic of room temperature after surface drying.Coating prepared by the present invention is well combined with matrix, has many advantages, such as lyophobicity, the high grade of transparency, high temperature resistant and compression resistance, self-cleaning property, good antisticking polishing machine.Preparation process of the present invention is simple, environmentally protective, at low cost, has broad application prospects in self-cleaning coating, marine anti-pollution, bio-medical field.
Description
Technical field
The present invention relates to a kind of to obtain the preparation method that high-intensitive solid-state superslide moves coating on solid material, belongs to material
Process for modifying surface field.
Background technique
Slip surface can reach the smooth of molecular scale, can be substantially reduced drop in the slide angle and angle of lag on its surface,
Have comprehensive lyophobicity, can selfreparing, the high grade of transparency, high temperature resistant and many advantages, such as compression resistance, matrix can be effectively prevent
Material is sticked by grease, blood, ice and biomembrane etc., therefore slip surface is in self-cleaning coating, marine anti-pollution, bio-medical neck
Domain etc. has broad application prospects.
Currently, having much in the method for preparing slip surface.CN103966641A discloses a kind of utilize and manually imitates boar cage
The method that careless slip surface prevents metal atmospheric corrosion, specifically, constructed using microstructure-lubricating oil injection two-step method is in aluminium
Common nepenthes slip surface is manually imitated in surface preparation, however, it is liquid slip surface that this method, which is formed by slip surface, in metal
One layer of oil film of upper covering reaches superslide effect, and oil film is lower intolerant to abrasion, intensity, after metal comes into operation, surface
The oil film highly volatile of upper covering is even worn, once oil film is worn, metal is still by atmospheric corrosion.CN107130223A is announced
A kind of preparation method of novel super lubricating solid coating, this method use metal vacuum steam plasma source (MEVVA) first,
Substrate surface injects one layer of metal ＂ pinning layer that can improve film-substrate cohesion ", on the ＂ pinning layer ＂, using Magnetic filter
Cathode vacuum arc deposition method (FCVA) deposit alloy stress release layer, and then using FCVA method and MEVVA while work
Make, the multiphase hybrid solid lubricant coating for being 1~10 micron in substrate surface deposition overall thickness, however, this method complex process,
Stringent, not applicable large scale preparation slip surface is required basis material and microstructural shape.CN109127330A is disclosed
A kind of preparation method of super-hydrophobic coat, polyvinyl alcohol-polyacrylic acid of this method to metal surface nano-silica-containing
After aqueous solution dip-coating, then carries out two step of vacuum reaction and the preparation of super-hydrophobic coat can be completed.However, super hydrophobic surface machinery is resistance to
Long property, wear resistance are poor, are highly prone to physical abrasion and even fail by destroying.And in 2017, the World Health Organization
In the carcinogenic substance that international cancer research institution announces, polyvinyl alcohol has certain poison to human body in 3 class carcinogenic substance inventories
Property, acid solution will also result in the pollution of environment.Therefore, it is badly in need of proposing a kind of environmentally friendly, simple, safe and efficient and nontoxic method
Coating is moved to prepare high-intensitive solid-state superslide, can be applied in surfaces of solids such as metal, plastics, glass, leather, paper.
Summary of the invention
The technical problem to be solved by the present invention is to propose a kind of environmentally friendly, simple, safe and efficient method in the surface of solids
The method that high-intensitive solid-state superslide moves coating is obtained, drips can fast ski-running on the solid material surface for smearing the coating
It falls.The solid material substrate can with and the solids table such as be not limited to metal, plastics, glass, timber, concrete, leather, paper
Face.
Technical solution of the present invention:
By the masking liquid filter screen filtration containing nano-ceramic particle, and it is mixed in a certain ratio with lubricant and is newly applied
Material, substrate is dipped in completely in coating material and is taken out after a certain period of time, and the substrate after taking-up does solid work naturally or quickly after surface drying, that is, is existed
Solid substrate surface can obtain high-intensitive solid-state superslide and move coating.
A kind of high intensity solid-state superslide moves the preparation method of coating, and steps are as follows:
(1) coating prepare: by after the masking liquid filter screen filtration containing nano-ceramic particle with lubricant in mass ratio not
The uniformly mixing less than 1, for use；
The nano-ceramic particle diameter is between 10nm~100nm；The nano-ceramic particle is aluminium oxide pottery
The mixing of one or more of porcelain particle, silicon nitride ceramic particles, silicon carbide ceramics particle；The filter screen specification is
It is more than 400 mesh；
The lubricant solution is perfluoro polyether oil, silicone oil, Du Pont krytox or perfluor triamylamine；
(2) infiltration is handled: coating obtained in step (1) is coated in solid substrate；The base obtained after infiltration processing
Slanted floor is stood, its surface is made to form one layer of uniform coating, and the tilt angle is 15 °~50 °；
The coating method be spraying, brushing, roller coating, dip-coating, spreading implement need it is clean and dry, can not speckle with water or
Other substances.
The solid substrate is metal, plastics, glass, timber, concrete, leather, paper.
(3) coating is dried: infiltration treated substrate obtained in step (2) is taken out, allow its do solid work naturally or
Quick surface drying；Described do solid work naturally refers to coating is allowed to be maintained under 25 DEG C of temperature 12~24 hours；The quick surface drying is
Coating is allowed to dry 30~50 minutes at a temperature of 100 DEG C；After coating does solid work cooling, 1~2 hour completion coating ceramic of room temperature
Change.
In step (2), spreading implement cleaning: after washes of absolute alcohol, clear water is cleaned up, and is deposited after compressed air drying
It puts；
In step (2), coating method, spraying: conventional spray guns spraying, sprayable one time；Brush: soft or hard medium hairbrush is equal
Even coating can brush one time；Roller coating: uniform roller coating coating, it can be roller coating one time；Dip-coating: dip-coating one time.
Coating is coated with the cleaning that environment is kept in work progress, so as not to dust or impurity reduce coating superslide characteristic and from
Spatter property.
Coating is only coated with one time, and otherwise the coating of subsequent coating and non-cohesive or adhesive force for the first time are bad.
Beneficial effects of the present invention:
(1) operation is simple for preparation method of the present invention, prepares low-cost, not need valuableness equipment, agents useful for same
Without environmental hazard, there is significant practicability.
(2) the super slip surface of solid-state prepared by the present invention, can be by preventing the modes such as rainwater sedimentation, salt grain deliquescence from leading
The presence of the water droplet of cause on the surface of the material, can be effectively suppressed corrosion of metal when applied to metal surface.
(3) the super slip surface of solid-state is not more than 5 ° to the roll angle of drop in the solid substrate prepared by the present invention, surface
With good self-cleaning property.
(4) coating compactness prepared by the present invention is preferable, has good antisticking polishing machine.
(5) the solid-state high intensity superslide coating prepared by the present invention is well combined with matrix, can improve matrix surface
Tribological property improves matrix wear resistant friction reducing performance.
(6) present invention prepared by solid-state high intensity superslide coating have comprehensive lyophobicity, the high grade of transparency, high temperature resistant and
Compression resistance.
Detailed description of the invention
Fig. 1 is the experimental provision schematic diagram of embodiment 1.
Fig. 2 is the dynamic behaviour for the stainless steel surface that water droplet is obtained in inclined embodiment 1 (inclination angle is less than 5 °).
In figure: 1 silicon nitride ceramics coating；2400 mesh filter screens；Ceramic coating after 3 filterings；Ceramic coating and profit after 4 filterings
Lubrication prescription 1:1 mixed solution；5 coating treatment metal process；6 anti-adherency, automatically cleaning metallic substrates.
Specific embodiment
Below in conjunction with attached drawing and technical solution, a specific embodiment of the invention is further illustrated.
The present invention relates to a kind of method for preparing high-intensitive solid-state superslide coating in solid material surface, prepared coatings
Compactness is preferable, has good antisticking polishing machine.Basis material can be effectively prevent by grease, blood, ice and biology
Film etc. sticks, and has broad application prospects in self-cleaning coating, marine anti-pollution, bio-medical field.
Embodiment 1:
(1) pretreatment of metallic substrates:
It will first be used respectively after drying having a size of 20mm × 20mm × 2mm metal stainless steel plate washes of absolute alcohol oil removing
The sand paper polishing removal surface oxide layer of 800# and 1500#, then the stainless steel plate after polishing is cleaned with a large amount of deionized waters, then
It is dried up using ultrasonic cleaning 5min, and with hair dryer.
(2) coating prepares:
By the 400 mesh filter screen filtrations of masking liquid containing the silicon nitride ceramic particles that nano-particle diameter is 100nm, and will
It is mixed with the dimethicone 1:1 in mass ratio that kinematic viscosity is 10cs, and uniform stirring.
(3) infiltration is handled:
Pretreated metal obtained in step (1) is immersed in step (2) coating, sufficiently infiltrates, then tilts quiet
It sets, so that its surface is formed one layer of uniform coating, and it is quiet to 30min with 20 ° of inclination angle, 30 ° of inclination makes extra painting
Expect flux surface, obtains stable coating.
(4) coating is dried:
Infiltration treated metallic substrates obtained in step (3) are taken out, 40min are dried at 100 DEG C, coating is done solid work
After cooling, 2 hours completion coating ceramics of room temperature.
Embodiment 2:
(1) pretreatment of substrate of glass:
First ultrasonic wave will be used again after drying having a size of the washes of absolute alcohol oil removing of 75mm × 25mm × 1mm glass slide
5min is cleaned, and is dried up with hair dryer.
(2) coating prepares:
By the 400 mesh filter screen filtrations of masking liquid containing the silicon carbide ceramics particle that nano-particle diameter is 100nm, and will
It is mixed with perfluoro polyether oil 2:1 in mass ratio, and uniform stirring.
(3) infiltration is handled
Pretreated glass slide obtained in step (1) is immersed in step (2) coating, sufficiently infiltrates, then tilts
It stands, so that its surface is formed one layer of uniform coating, and it is quiet to 30min with 20 ° of inclination angle, it is extra that 20 ° of inclination makes
Coating flux surface obtains stable coating.
(4) coating is dried:
Infiltration treated glass slide obtained in step (3) is taken out, 30min is dried at 100 DEG C, coating is done solid work cold
But after, 1 hour completion coating ceramic of room temperature.
Embodiment 3:
(1) pretreatment of plastic-substrates:
First it is clear will to reuse ultrasonic wave having a size of the washes of absolute alcohol oil removing of 50mm × 50mm × 5mm polyethylene board
5min is washed, and is dried up with hair dryer.
(2) coating prepares:
By the 400 mesh filter screen filtrations of masking liquid containing the alumina ceramic grain that nano-particle diameter is 70nm, and will
It is mixed with perfluor triamylamine 1:1 in mass ratio, and uniform stirring.
(3) infiltration is handled
Pretreated polyethylene obtained in step (1) is immersed in step (2) coating, sufficiently infiltrates, then tilts
It stands, so that its surface is formed one layer of uniform coating, and it is quiet to 30min with 50 ° of inclination angle, it is extra that 20 ° of inclination makes
Coating flux surface obtains stable coating.
(4) coating is dried:
Infiltration treated polyvinyl bottom obtained in step (3) is taken out, 50min is dried at 100 DEG C, coating is real
It is dry and cold but after, 1.5 hours completion coating ceramics of room temperature.
Embodiment 4:
(1) coating prepares:
By the 400 mesh filter screen filtrations of masking liquid containing the silicon nitride ceramic particles that nano-particle diameter is 100nm, and will
It is mixed with the dimethicone 5:1 in mass ratio that kinematic viscosity is 10cs, and uniform stirring.
(2) infiltration is handled
95mm × 50mm × 5mm timber is immersed in step (1) coating, is sufficiently infiltrated, then inclination is stood, and makes its surface
One layer of uniform coating being formed, and it is quiet to 30min with 20 ° of inclination angle, 20 ° of inclination makes extra coating flux surface,
Obtain stable coating.
(3) coating is dried:
Infiltration treated wood substrate obtained in step (3) is taken out, 40min is dried at 100 DEG C, coating is done solid work
After cooling, 1 hour completion coating ceramic of room temperature.
Claims (8)
1. the preparation method that a kind of high intensity solid-state superslide moves coating, which is characterized in that steps are as follows:
(1) coating prepares: will be not less than in mass ratio 1 with lubricant after the masking liquid filter screen filtration containing nano-ceramic particle
Uniformly mixing, for use；
The lubricant solution is one or more of perfluoro polyether oil, silicone oil, Du Pont krytox, perfluor triamylamine
Mixing；
(2) infiltration is handled: coating obtained in step (1) is coated in solid substrate；The substrate obtained after infiltration processing is inclined
It tiltedly stands, its surface is made to form one layer of uniform coating, the tilt angle is 15 °~50 °；
(3) coating is dried: infiltration treated substrate obtained in step (2) being taken out, it is allowed to do solid work naturally or quickly
Surface drying；After coating does solid work cooling, 1~2 hour completion coating ceramic of room temperature.
2. preparation method according to claim 1, which is characterized in that the nano-ceramic particle diameter be 10nm~
Between 100nm；The nano-ceramic particle is alumina ceramic grain, in silicon nitride ceramic particles, silicon carbide ceramics particle
One or more kinds of mixing；The filter screen specification is 400 mesh or more.
3. preparation method according to claim 1 or 2, which is characterized in that described doing solid work naturally, which refers to, allows coating to keep
12~24 hours under 25 DEG C of temperature；The quick surface drying is that coating is allowed to dry 30~50 minutes at a temperature of 100 DEG C.
4. preparation method according to claim 1 or 2, which is characterized in that in step (2), coating method, spraying: common
Spray gun spraying sprays one time；Brush: soft or hard medium hairbrush even spread is brushed one time；Roller coating: uniform roller coating coating
, roller coating one time；Dip-coating: dip-coating one time；Spreading implement cleaning: after washes of absolute alcohol, clear water is cleaned up, pressure
It is stored after contracting air blow drying.
5. preparation method according to claim 3, which is characterized in that in step (2), coating method, spraying: conventional spray guns
Spraying sprays one time；Brush: soft or hard medium hairbrush even spread is brushed one time；Roller coating: uniform roller coating coating,
Roller coating one time；Dip-coating: dip-coating one time；Spreading implement cleaning: after washes of absolute alcohol, clear water is cleaned up, and compression is empty
It is stored after air-blowing is dry.
6. according to claim 1, preparation method described in 2 or 5, which is characterized in that the solid substrate be metal, plastics,
Glass, timber, concrete, leather, paper.
7. preparation method according to claim 3, which is characterized in that the solid substrate be metal, plastics, glass,
Timber, concrete, leather, paper.
8. the preparation method according to claim 4, which is characterized in that the solid substrate be metal, plastics, glass,
Timber, concrete, leather, paper.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910389375.4A CN110142193A (en) | 2019-05-10 | 2019-05-10 | A kind of high intensity solid-state superslide moves the preparation method of coating |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201910389375.4A CN110142193A (en) | 2019-05-10 | 2019-05-10 | A kind of high intensity solid-state superslide moves the preparation method of coating |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110903845A (en) * | 2019-11-28 | 2020-03-24 | 刘鹏 | Method for solving corrosion of fractionating tower top pipeline and equipment of oil refining device by using coating |
| CN113801535A (en) * | 2021-08-30 | 2021-12-17 | 大连理工大学 | Paint for preparing super-slip coating and application thereof |
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| CN113801535A (en) * | 2021-08-30 | 2021-12-17 | 大连理工大学 | Paint for preparing super-slip coating and application thereof |
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Application publication date: 20190820 |