CN110129117A - Lifetime lubrication agent and preparation method thereof for Internet of Things artificial intelligence equipment - Google Patents

Lifetime lubrication agent and preparation method thereof for Internet of Things artificial intelligence equipment Download PDF

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Publication number
CN110129117A
CN110129117A CN201910551092.5A CN201910551092A CN110129117A CN 110129117 A CN110129117 A CN 110129117A CN 201910551092 A CN201910551092 A CN 201910551092A CN 110129117 A CN110129117 A CN 110129117A
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parts
internet
artificial intelligence
pao
poly alpha
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CN201910551092.5A
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Chinese (zh)
Inventor
吴鹏
赵天祥
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HUBEI CHENGXIANG TECHNOLOGY Co Ltd
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HUBEI CHENGXIANG TECHNOLOGY Co Ltd
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Priority to CN201910551092.5A priority Critical patent/CN110129117A/en
Publication of CN110129117A publication Critical patent/CN110129117A/en
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    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M169/00Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
    • C10M169/04Mixtures of base-materials and additives
    • C10M169/048Mixtures of base-materials and additives the additives being a mixture of compounds of unknown or incompletely defined constitution, non-macromolecular and macromolecular compounds
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/04Elements
    • C10M2201/041Carbon; Graphite; Carbon black
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/10Compounds containing silicon
    • C10M2201/105Silica
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2203/00Organic non-macromolecular hydrocarbon compounds and hydrocarbon fractions as ingredients in lubricant compositions
    • C10M2203/06Well-defined aromatic compounds
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2205/00Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
    • C10M2205/02Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers
    • C10M2205/0206Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers used as base material
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2205/00Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
    • C10M2205/02Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers
    • C10M2205/026Butene
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2219/00Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
    • C10M2219/04Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions containing sulfur-to-oxygen bonds, i.e. sulfones, sulfoxides
    • C10M2219/044Sulfonic acids, Derivatives thereof, e.g. neutral salts
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2223/00Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
    • C10M2223/02Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having no phosphorus-to-carbon bonds
    • C10M2223/04Phosphate esters
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10NINDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/06Oiliness; Film-strength; Anti-wear; Resistance to extreme pressure

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Lubricants (AREA)

Abstract

The invention discloses a kind of lifetime lubrication agent for Internet of Things artificial intelligence equipment, and raw material includes following components by weight: 50-88 parts of Poly alpha Olefins (PAO), 10-25 parts of polyisobutene, 0.2-2 parts of graphene, 5-10 parts of calcium mahogany sulfonate, 0.5-10 parts of detersive, Ans5-15 parts of alkylnaphthalene .2-1.5 parts of phosphoesterase 30,1-15 parts of fumed silica;Using specific raw material, reasonable proportion, the chemical balance for forming lubricating oil each component is stablized, the properties of lubricant are more stable, suitable for lubrication of the Internet of Things artificial intelligence equipment under wide warm operating condition (- 30 DEG C of -300 DEG C of working environments), complicated adverse circumstances, the lubrication interval of lubricant is long, equipment service free and maintenance in use, it does not need more to change lubricant, reaches the requirement of lifetime lubrication.

Description

Lifetime lubrication agent and preparation method thereof for Internet of Things artificial intelligence equipment
Technical field
The present invention relates to lubricating oil field, in particular to a kind of lifetime lubrication agent for Internet of Things artificial intelligence equipment And preparation method thereof.
Background technique
The AI equipment that the arriving in 5G epoch, all things on earth interconnect continues to bring out, and all kinds of intelligence AI equipment are various severe Working environment application, such as answering for the big bad working environments of high-low temperature difference (such as in -30 DEG C of -300 DEG C of working environments), high-altitude or difficult maintenance Miscellaneous position.Therefore, requirement of the AI equipment to lubricant is also constantly being promoted, and in the prior art, AI equipment is to lubricant also from one Class base oil turns to the even more high level four classes oil of two classes, three classes, GTL base oil, such as newest metallocene poly alpha olefin PAOs.But these high-end base oil polarity are all very low, it is poor with the dissolubility of additive, and existing lubricating oil needs periodically Maintenance, maintenance and replacement, cause equipment to be also required to periodic maintenance, therefore, existing AI equipment lubrication oil is difficult to meet extreme work Lubricating requirement under the conditions of condition, there is also very big problems for the maintenance and replacement of lubricating oil.
Summary of the invention
In view of this, the purpose of the present invention is to provide a kind of lifetime lubrication agent for Internet of Things artificial intelligence equipment And preparation method thereof, it is severe in wide warm operating condition (- 30 DEG C of -300 DEG C of working environments), complexity to be suitable for Internet of Things artificial intelligence equipment The lubrication interval of lubrication under environment, lubricant is long, and equipment service free and maintenance in use does not need more to change lubrication Agent reaches the requirement of lifetime lubrication.
Lifetime lubrication agent for Internet of Things artificial intelligence equipment of the invention, raw material includes with the following group by weight Point: 50-88 parts of Poly alpha Olefins (PAO), 10-25 parts of polyisobutene, 0.2-2 parts of graphene, 5-10 parts of calcium mahogany sulfonate, detersive 0.5- 10 parts, Ans5-15 parts of alkylnaphthalene .2-1.5 parts of phosphoesterase 30,1-15 parts of fumed silica;
Further, raw material includes following components by weight: 70 parts of Poly alpha Olefins (PAO), 18 parts of polyisobutene, 1 part of graphene, 7 parts of calcium mahogany sulfonate, 6 parts of detersive, Ans10 parts of alkylnaphthalene, 1 part of phosphate, 8 parts of fumed silica;
Further, the detersive is T154;
Further, the polyisobutene molecular weight is 1300.
The preparation method of lifetime lubrication agent for Internet of Things artificial intelligence equipment of the invention, comprising the following steps:
It is warming up to 40-60 DEG C after graphene, fumed silica and Poly alpha Olefins (PAO) are mixed evenly, is then added surplus Excess material is stirred to react 2 hours or more at being 40-60 DEG C in temperature;
Further, premix is formed after dispersing graphene and fumed silica in the Poly alpha Olefins (PAO) of part respectively, Two kinds of premixs are added into remaining Poly alpha Olefins (PAO) after mixing.
Beneficial effects of the present invention: the lifetime lubrication agent and its preparation for Internet of Things artificial intelligence equipment of the invention Method, reasonable to match using specific raw material, the chemical balance for forming lubricating oil each component is stablized, the items of lubricant Performance is more stable, is suitable for Internet of Things artificial intelligence equipment in wide warm operating condition (- 30 DEG C of -300 DEG C of working environments), complicated severe ring The lubrication interval of lubrication under border, lubricant is long, and equipment service free and maintenance in use does not need more to change lubrication Agent reaches the requirement of lifetime lubrication.
Specific embodiment
The lifetime lubrication agent for Internet of Things artificial intelligence equipment of the present embodiment, raw material includes with the following group by weight Point: 50-88 parts of Poly alpha Olefins (PAO), 10-25 parts of polyisobutene, 0.2-2 parts of graphene, 5-10 parts of calcium mahogany sulfonate, detersive 0.5- 10 parts, Ans5-15 parts of alkylnaphthalene .2-1.5 parts of phosphoesterase 30,1-15 parts of fumed silica;Using Poly alpha Olefins (PAO) PAO and gather different Butylene alternative ore oil lubrication, wide warm nature is good, friction high temperature is reduced using graphene, and generate high tough film, using petroleum sulphur In sour calcium and oil product when used for a long time aging generate acid, extend Oil life, and detersive dispersion oil product deterioration greasy filth, stone Oily sulfoacid calcium and detersive synergistic effect extend the service life of oil product, cooperate with work with poly alpha olefin PAOs using alkylnaphthalene Ans With heat resistance, thermo oxidative stability, dissolubility, the dispersibility for improving oil product, additive response, paint film control, rubber compatibility Property, volatility and hydrolytic stability, to extend the service life of these high performance lubricants, using phosphate improve emulsification, Extreme pressure and greasy property, and there is good aluminium alloy corrosion inhibition.
In the present embodiment, raw material includes following components by weight: 70 parts of Poly alpha Olefins (PAO), 18 parts of polyisobutene, graphene 1 Part, 7 parts of calcium mahogany sulfonate, 6 parts of detersive, Ans10 parts of alkylnaphthalene, 1 part of phosphate, 8 parts of fumed silica;To be preferably implemented Example.
In the present embodiment, the detersive is T154;T154 is derivatives of poly (iso) butene, and increasing is cooperateed with calcium mahogany sulfonate Effect effect.
In the present embodiment, the polyisobutene molecular weight is 1300.
The preparation method of lifetime lubrication agent for Internet of Things artificial intelligence equipment of the invention, comprising the following steps:
It is warming up to 40-60 DEG C after graphene, fumed silica and Poly alpha Olefins (PAO) are mixed evenly, is then added surplus Excess material is stirred to react 2 hours or more at being 40-60 DEG C in temperature;
In the present embodiment, premixing is formed after dispersing graphene and fumed silica in the Poly alpha Olefins (PAO) of part respectively Two kinds of premixs are added remaining Poly alpha Olefins (PAO) by material after mixing;Simple process is easily operated, and each raw material passes through physics The chemical balance that reaction, microneutralization reaction are formed by lubricant is stablized.
Embodiment one
The lifetime lubrication agent for Internet of Things artificial intelligence equipment of the present embodiment, raw material includes with the following group by weight Point: 50 parts of Poly alpha Olefins (PAO), 10 parts of polyisobutene, 0.2 part of graphene, 5 parts of calcium mahogany sulfonate, 0.5 part of detersive, alkylnaphthalene Ans5 Part .2 parts of phosphoesterase 30,1 part of fumed silica;Preparation method includes the following steps:
Premix is formed after dispersing graphene and fumed silica in the Poly alpha Olefins (PAO) of part respectively, it is pre- by two kinds Mixture adds remaining Poly alpha Olefins (PAO) after mixing;It is warming up to 40 DEG C after mixing evenly, surplus material is then added in temperature Degree is to be stirred to react 2 hours or more at 40 DEG C.
Embodiment two
The lifetime lubrication agent for Internet of Things artificial intelligence equipment of the present embodiment, raw material includes with the following group by weight Point: 88 parts of Poly alpha Olefins (PAO), 25 parts of polyisobutene, 2 parts of graphene, 10 parts of calcium mahogany sulfonate, 10 parts of detersive, alkylnaphthalene Ans15 Part, 1.5 parts of phosphate, 15 parts of fumed silica;Preparation method includes the following steps:
Premix is formed after dispersing graphene and fumed silica in the Poly alpha Olefins (PAO) of part respectively, it is pre- by two kinds Mixture adds remaining Poly alpha Olefins (PAO) after mixing;It is warming up to 60 DEG C after mixing evenly, surplus material is then added in temperature Degree is to be stirred to react 2 hours at 60 DEG C.
Embodiment three
The lifetime lubrication agent for Internet of Things artificial intelligence equipment of the present embodiment, raw material includes with the following group by weight Point: 50 parts of Poly alpha Olefins (PAO), 25 parts of polyisobutene, 0.2 part of graphene, 10 parts of calcium mahogany sulfonate, 0.5 part of detersive, alkylnaphthalene Ans15 parts .2 parts of phosphoesterase 30,15 parts of fumed silica;Preparation method includes the following steps:
Premix is formed after dispersing graphene and fumed silica in the Poly alpha Olefins (PAO) of part respectively, it is pre- by two kinds Mixture adds remaining Poly alpha Olefins (PAO) after mixing;It is warming up to 45 DEG C after mixing evenly, surplus material is then added in temperature Degree is to be stirred to react 2 hours or more at 45 DEG C.
Example IV
The lifetime lubrication agent for Internet of Things artificial intelligence equipment of the present embodiment, raw material includes with the following group by weight Point: 88 parts of Poly alpha Olefins (PAO), 10 parts of polyisobutene, 2 parts of graphene, 5 parts of calcium mahogany sulfonate, 10 parts of detersive, Ans5 parts of alkylnaphthalene, 1.5 parts of phosphate, 1 part of fumed silica;Preparation method includes the following steps:
Premix is formed after dispersing graphene and fumed silica in the Poly alpha Olefins (PAO) of part respectively, it is pre- by two kinds Mixture adds remaining Poly alpha Olefins (PAO) after mixing;It is warming up to 42 DEG C after mixing evenly, surplus material is then added in temperature Degree is to be stirred to react 2 hours or more at 42 DEG C.
Embodiment five
The lifetime lubrication agent for Internet of Things artificial intelligence equipment of the present embodiment, raw material includes with the following group by weight Point: 65 parts of Poly alpha Olefins (PAO), 10 parts of polyisobutene, 2 parts of graphene, 7 parts of calcium mahogany sulfonate, 0.5 part of detersive, alkylnaphthalene Ans15 Part, 1 part of phosphate, 10 parts of fumed silica;Preparation method includes the following steps:
Premix is formed after dispersing graphene and fumed silica in the Poly alpha Olefins (PAO) of part respectively, it is pre- by two kinds Mixture adds remaining Poly alpha Olefins (PAO) after mixing;It is warming up to 55 DEG C after mixing evenly, surplus material is then added in temperature Degree is to be stirred to react 2 hours at 55 DEG C.
Embodiment six
The lifetime lubrication agent for Internet of Things artificial intelligence equipment of the present embodiment, raw material includes with the following group by weight Point: 70 parts of Poly alpha Olefins (PAO), 18 parts of polyisobutene, 1 part of graphene, 7 parts of calcium mahogany sulfonate, 6 parts of detersive, Ans10 parts of alkylnaphthalene, 1 part of phosphate, 8 parts of fumed silica;Preparation method includes the following steps:
Premix is formed after dispersing graphene and fumed silica in the Poly alpha Olefins (PAO) of part respectively, it is pre- by two kinds Mixture adds remaining Poly alpha Olefins (PAO) after mixing;It is warming up to 50 DEG C after mixing evenly, surplus material is then added in temperature Degree is to be stirred to react 2 hours or more at 50 DEG C.
Lubricant of the invention is compared with conventional lubrication material property:
Project Acid value Rotary oxygen bomb It is recommended to use the period
I class oil type 0.6 150min 1 year
II class oil type 0.1 230min 2 years
III class oil type 0.03 350min 3 years
Poly alpha Olefins (PAO) PAO 0.01 500min 5 years
The present invention 0.003 800min Life-cycle
The technical indicator of the lubricant of the embodiment of the present invention one and mineral type and synthesis type lubriation material is compared and is as follows:
Finally, it is stated that the above examples are only used to illustrate the technical scheme of the present invention and are not limiting, although referring to compared with Good embodiment describes the invention in detail, those skilled in the art should understand that, it can be to skill of the invention Art scheme is modified or replaced equivalently, and without departing from the objective and range of technical solution of the present invention, should all be covered at this In the scope of the claims of invention.

Claims (6)

1. a kind of lifetime lubrication agent for Internet of Things artificial intelligence equipment, it is characterised in that: raw material include by weight with Lower component: 50-88 parts of Poly alpha Olefins (PAO), 10-25 parts of polyisobutene, 0.2-2 parts of graphene, 5-10 parts of calcium mahogany sulfonate, detersive 0.5-10 parts, Ans5-15 parts of alkylnaphthalene .2-1.5 parts of phosphoesterase 30,1-15 parts of fumed silica.
2. the lifetime lubrication agent according to claim 1 for Internet of Things artificial intelligence equipment, it is characterised in that: raw material It by weight include following components: 70 parts of Poly alpha Olefins (PAO), 18 parts of polyisobutene, 1 part of graphene, 7 parts of calcium mahogany sulfonate, detersive 6 parts, Ans10 parts of alkylnaphthalene, 1 part of phosphate, 8 parts of fumed silica.
3. the lifetime lubrication agent according to claim 1 for Internet of Things artificial intelligence equipment, it is characterised in that: described Detersive is T154.
4. the lifetime lubrication agent according to claim 3 for Internet of Things artificial intelligence equipment, it is characterised in that: described Polyisobutene molecular weight is 1300.
5. the preparation method of the lifetime lubrication agent according to claim 1 for Internet of Things artificial intelligence equipment, special Sign is: the following steps are included:
It is warming up to 40-60 DEG C after graphene, fumed silica and Poly alpha Olefins (PAO) are mixed evenly, residue is then added Material is stirred to react 2 hours or more at being 40-60 DEG C in temperature.
6. the preparation method of the lifetime lubrication agent according to claim 5 for Internet of Things artificial intelligence equipment, special Sign is: premix is formed after dispersing graphene and fumed silica in the Poly alpha Olefins (PAO) of part respectively, it is pre- by two kinds Mixture adds remaining Poly alpha Olefins (PAO) after mixing.
CN201910551092.5A 2019-06-24 2019-06-24 Lifetime lubrication agent and preparation method thereof for Internet of Things artificial intelligence equipment Pending CN110129117A (en)

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Cited By (1)

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CN115895760A (en) * 2022-12-18 2023-04-04 云南光电辅料有限公司 Small-gap precision instrument lubricating grease and preparation method thereof

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