CN110124459A - Methanol air water cleaning of evaporator - Google Patents

Methanol air water cleaning of evaporator Download PDF

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Publication number
CN110124459A
CN110124459A CN201810130930.7A CN201810130930A CN110124459A CN 110124459 A CN110124459 A CN 110124459A CN 201810130930 A CN201810130930 A CN 201810130930A CN 110124459 A CN110124459 A CN 110124459A
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CN
China
Prior art keywords
methanol
methanol gas
gas
water
tank body
Prior art date
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Pending
Application number
CN201810130930.7A
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Chinese (zh)
Inventor
王以斌
豆宝宜
程继元
丁梅峰
姚建军
王文昊
郭维军
李战杰
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Sinopec Engineering Group Co Ltd
Sinopec Guangzhou Engineering Co Ltd
Original Assignee
Sinopec Engineering Group Co Ltd
Sinopec Guangzhou Engineering Co Ltd
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Application filed by Sinopec Engineering Group Co Ltd, Sinopec Guangzhou Engineering Co Ltd filed Critical Sinopec Engineering Group Co Ltd
Priority to CN201810130930.7A priority Critical patent/CN110124459A/en
Publication of CN110124459A publication Critical patent/CN110124459A/en
Pending legal-status Critical Current

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/14Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by absorption
    • B01D53/1487Removing organic compounds
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/14Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by absorption
    • B01D53/18Absorbing units; Liquid distributors therefor

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Analytical Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Cleaning By Liquid Or Steam (AREA)

Abstract

The invention discloses a kind of methanol air water cleaning of evaporators, including horizontal tank body, horizontal top of the tank is equipped with the import of methanol gas and the first clean gas outlet, bottom is equipped with washing water inlet and water supplement port, first clean gas outlet is between the import of methanol gas and one end end socket, the end seal head is equipped with overflow water out, water supplement port is between washing water inlet and other end end socket, the end seal head is equipped with the second clean gas outlet, overflow baffle is arranged in horizontal tank inner chamber middle position, horizontal tank inner chamber middle and upper part is equipped with the methanol gas cushion chamber of rectangular shape above overflow baffle, methanol gas inlet communication methanol gas cushion chamber, methanol gas down-comer is set below the bottom plate of methanol gas cushion chamber, methanol gas down-comer passes through rectangle liquid reducing hole and extends downwardly into liquid level or less, each rectangle liquid reducing hole and each row's methanol gas down-comer cooperate.Incoming flow methanol gas can sufficiently be buffered using the present invention, by bath wash with elution be combined with each other in the way of, promote the high-efficient contact of methanol gas and washing water, reaching the washing of methanol gas, flowing is steady, good absorption effect.

Description

Methanol air water cleaning of evaporator
Technical field
The invention belongs to the methanol gas disposal technology in gas purification technique field, in particular to a kind of methanol air water is washed Tank.
Background technique
Methanol has a wide range of applications in petrochemical industry, is not only important industrial chemicals, but also is that performance is excellent The good energy and vehicle fuel.With the rise of coal chemical industry, methanol more highlights its important value as intermediate raw material.Methanol has The toxicity of toxicity, methanol influences maximum to the nervous system of human body and hematological system, it takes in through alimentary canal, respiratory tract or skin Toxic reaction will be generated, the respiratory mucosa and eyesight that methanol vapor energy loss victimizes.It must be worn in the work on the spot for having methanol gas Breathing mask.
The storage tank that petrochemical industry is used to store methanol is passed through frequently with nitrogen-sealed, and storage tank can be discharged when superpressure is discharged Harmful gas containing methanol (mixed gas of methanol gas and nitrogen) out, it is necessary to can just be discharged into atmosphere by purified treatment.Currently, often Method that the characteristics of being dissolved each other completely using methanol and water is washed with water handles gas containing methanol (and methanol gas).Chinese patent CN104275073A discloses a kind of methanol aspiration method and device, has been horizontally disposed in horizontal water washing tank used with sieve The methanol tracheae in hole and fresh water pipe with sieve pore.Methanol tracheae with sieve pore be located at water-bath water in water washing tank surface it Under, the fresh water pipe with sieve pore is arranged in water-bath water surface.Fresh length of pipe with sieve pore, which is greater than, has sieve pore Methanol tracheae length, with sieve pore fresh water pipe sieve pore spray radiation areas envelope methanol air sifter bore region.Normally In the case of, methanol gas is absorbed by water-bath;Methanol gas is eluted when saturation state needs to replace when methanol aqueous solution reaches Washing.When water-bath absorbs, methanol gas is entered in water-bath water by the methanol tracheae with sieve pore to be absorbed.When elution washing, methanol Gas from sieve pore methanol tracheae enter water-bath water and from water-bath water evolution flow up, with sieve pore fresh water pipe to Fresh water (washing water) counter current contacting of lower spray is absorbed.But there are the following problems for the technology: (1) gas containing methanol enters and has There is no enough spaces to be buffered after the methanol tracheae of sieve pore, the pressure oscillation in pipe everywhere is larger;(2) when gas containing methanol from Air-flow is unstable, uneven when sieve pore flows out, and is easy to escape and the sieve pore airless of distant place from sieve pore nearby, flow disorderly Disorderly, poor with the contact condition of water-bath water;(3) when above-mentioned gas containing methanol is flowed up from water-bath water evolution and with sieve pore The washing water counter current contacting that sprays downwards of fresh water pipe when carrying out elution washing, it is uneven due to gas overflowing, with elution The contact condition of water is also poor.This will affect absorption of the water to methanol gas, keep water washing effect poor;(4) with sieve pore The washing water that fresh water pipe sprays downwards be difficult the gas containing methanol that will flow up always completely effectively covering and high-efficient contact, Some gas containing methanol have when elution washing without washing i.e. discharge water washing tank, water washing effect is difficult to reliably be guaranteed.
Summary of the invention
The object of the present invention is to provide a kind of methanol air water cleaning of evaporators, sufficiently buffer to incoming flow methanol gas, are washed and overflow using bath The mode that stream be combined with each other promotes the high-efficient contact of methanol gas and washing water, can solve prior art gas-liquid using the present invention and connect The problem that touching is uneven, fluctuation is violent, water washing effect is poor.
The present invention provides a kind of methanol air water cleaning of evaporator, and specific technical solution is as follows:
A kind of methanol air water cleaning of evaporator, including horizontal tank body, horizontal tank body is by horizontal cylindrical shape cylinder and positioned at the end socket at its both ends Composition, it is characterised in that: the horizontal top of the tank is equipped with the import of methanol gas and the first clean gas outlet, and the import of methanol gas is sleeping Formula top of the tank center, horizontal tank base are equipped with washing water inlet and water supplement port, wash water inlet in horizontal tank base Center, for the first clean gas outlet between the import of methanol gas and one end end socket, which is equipped with overflow water out, moisturizing Mouthful between washing water inlet and other end end socket, which is equipped with the second clean gas outlet, among horizontal tank inner chamber Overflow baffle is arranged in position, and overflow baffle is horizontally disposed plate, and edge is connected with the inner wall of horizontal tank body, under overflow baffle Side is washing space, and the liquid level for washing space is located at central axes on horizontal length of tank direction hereinafter, in horizontal tank inner chamber Top is equipped with methanol gas cushion chamber, methanol gas inlet communication methanol gas cushion chamber above overflow baffle, and methanol gas cushion chamber is The cushion space of rectangular shape opens up the mounting hole of methanol gas down-comer on the bottom plate of methanol gas cushion chamber, for installing Methanol gas down-comer, overflow baffle are equipped with rectangle liquid reducing hole, are arranged symmetrically in the two sides of washing water inlet, the decline of methanol gas Pipe extends downwardly into liquid level hereinafter, each rectangle liquid reducing hole and each row's methanol gas down-comer phase interworking across rectangle liquid reducing hole It closes, washing water inlet connects overflow water tedge, and overflow water tedge is connected to overflow baffle upper space straight up.
The present invention be further technically characterized in that rectangle liquid reducing hole upper surface be higher by overflow baffle upper surface 50~ 80mm, the low 50~80mm of overflow baffle lower surface out in rectangle liquid reducing hole lower surface, rectangle liquid reducing hole are each washing water inlet Side is in a row to be evenly arranged.
The present invention be further technically characterized in that the methanol gas down-comer outside wall surface and rectangle liquid reducing hole inner wall it Between distance should be in 10~30mm.
The present invention is further technically characterized in that the methanol gas cushion chamber is fixed in horizontal tank body by fixed floor On wall.
The present invention is further technically characterized in that the mounting hole on the methanol gas cushion chamber bottom plate is circular hole, mounting hole Diameter be about 20~50mm, the square arrangement of mounting hole, which is covered with, fills a bottom plate for methanol gas cushion chamber, two neighboring installation The installation bore dia that spacing between hole is 2~5 times.
The present invention is further technically characterized in that the length of the methanol gas cushion chamber and the horizontal cylindrical shape of horizontal tank body Barrel lenght is suitable, and the two of methanol gas cushion chamber end face is concordant with head bend line in the longitudinal direction, methanol gas cushion chamber Width is 0.6~0.8 times of horizontal tank diameter, the bottom surface of methanol gas cushion chamber apart from overflow baffle upper surface 150~ 200mm。
The present invention is further technically characterized in that the methanol gas down-comer is short straight tube structure, and entrance is installed on methanol Mounting hole arranged in square on gas cushion chamber bottom plate exports and protrudes into water seal water liquid level or less about 50~100mm, under methanol gas Pipe setting tens to several hundred is dropped, controls the air velocity in methanol gas down-comer in the range of 0.2~0.5m/s.
During the present invention is further technically characterized in that the liquid level in the washing space is located on horizontal length of tank direction 100~150mm below axis.
The present invention is further technically characterized in that the water supplement port and the first clean gas outlet distance adjacent to head bend line Distance is 0.2~0.5 times of horizontal tank diameter, and overflow water out vertical position is in 50~100mm of water seal water liquid level or less, Second clean gas outlet is in the lower section of overflow baffle in vertical position.
The present invention is further technically characterized in that position occupied by methanol gas inlet pipe is not on the methanol gas cushion chamber Carry out the arrangement of methanol gas down-comer.
A kind of method that methanol air water cleaning of evaporator washes methanol gas of the present invention are as follows:
(1) bath is used only when methanol stream amount is smaller to wash, at this time: (content is 20% hereinafter, remaining is nitrogen etc. for methanol gas first Inert gas) from methanol gas import enter methanol gas cushion space;After buffering, methanol gas is downward along methanol gas down-comer It flows into washing water level or less and carries out washing operation;Fresh water enters washing space through water supplement port, and wastewater containing methanol is through overflowing Flowing water exports outflow water cleaning of evaporator;Outside wall surface and rectangle liquid reducing hole inner wall of the purified gas through methanol gas down-comer after washing Being spatially advanced into overflow down-flow plate upper space and being discharged into atmosphere through the first clean gas outlet between face.
(2) methanol stream amount increase when bath wash with overflow washing is used in combination: first methanol gas (content 20% hereinafter, Remaining is the inert gases such as nitrogen) enter methanol gas cushion space from methanol gas import;After buffering, methanol gas is along methanol Gas down-comer flow downward into washing water level below carry out bath wash operation;Overflow water is from overflow water inlet through overflow water inlet Pipe enters above overflow baffle, and then the wall surface from rectangle liquid reducing hole along methanol gas down-comer drops to water seal water level and methanol The methanol vapor phase that the outlet of gas down-comer rises after washing carries out methanol absorption to contact;Fresh water enters water through water supplement port Space is washed, wastewater containing methanol exports outflow water cleaning of evaporator through overflow water;Purified gas after washing through the second purified gas through going out Mouth is discharged into atmosphere.
Present invention is mainly used for the gas containing methanol to industries such as petrochemical industries to wash.It is also applied for liquid ammonia storage tank discharge The washing process of gas (ammonia level is below 20%) etc..
Using the invention has the following advantages: (1) methanol gas has enough spaces in the cushion space being specially arranged It is buffered with the residence time, methanol stream is dynamic steady after buffering, be evenly distributed, pressure oscillation everywhere is little, energy It is enough it is steady from methanol gas down-comer with certain speed, evenly into carrying out first time water in the washing water in washing space It washes, it is preferable with the contact condition of washing water, washing water will not be made biggish irregular fluctuation occur, reach and improve water washing effect Purpose.Gas containing methanol after first wash also can more smoothly escape into washing water surface, and under methanol gas The wall surface of drop pipe drops to water seal aqueous water phase and carries out methanol absorption to contact, and adverse current docks good absorption effect.(2) under methanol gas Drop Guan Chengzheng square is intensively covered with entire washing water ullage, is that a kind of methanol gas of high efficiency smooth enters water mode, promotes The absorption efficiency and absorptivity of methanol gas.(3) gas containing methanol is washed and is eluted by bath in water washing tank of the invention and washes twice Operation, effect are preferable.
Invention is further described in detail with reference to the accompanying drawings and detailed description, but is not intended to limit of the invention Range.
Detailed description of the invention
Fig. 1 is a kind of the main to topology view of methanol air water cleaning of evaporator of the present invention.
Fig. 2 is the present invention a kind of the methanol gas cushion chamber and methanol gas down-comer 3-D view of methanol air water cleaning of evaporator.
Fig. 3 is the present invention a kind of the methanol gas cushion chamber and methanol gas downcomer structure view of methanol air water cleaning of evaporator.
Fig. 4 is a kind of overflow water tedge 3-D view of methanol air water cleaning of evaporator of the present invention.
Fig. 5 is a kind of overflow water tedge top view of methanol air water cleaning of evaporator of the present invention.
Fig. 6 is that a kind of methanol air water cleaning of evaporator overflow water tedge rectangle liquid reducing hole of the present invention is locally matched with methanol gas down-comer Close view.
Appended drawing reference as shown in the figure are as follows:
The horizontal tank body of 1-, 2- methanol gas import, 3- methanol gas cushion chamber, 4- wash water inlet, 5- overflow water out, 6- moisturizing Mouthful, the first clean gas outlet of 7-, 8- rectangle liquid reducing hole, 9- overflow baffle, 10- overflow water tedge, 11- methanol gas inlet pipe, 12- methanol gas down-comer, the second clean gas outlet of 13-, 14- end socket, 15- wash space.
Specific embodiment
Referring to Fig. 1~6.A kind of methanol air water cleaning of evaporator of the present invention, including horizontal tank body 1, horizontal tank body 1 is by horizontal cylindrical shape Cylinder and end socket 14 positioned at its both ends form, and the import 2 of methanol gas and the first clean gas outlet 7, first are equipped at the top of horizontal tank body 1 In horizontal 1 top center of tank body, horizontal 1 bottom of tank body is equipped with washing water inlet 4 and water supplement port 6 for alcohol gas import 2, washing water into Mouth 4 is in horizontal 1 bottom center of tank body, and the first clean gas outlet 7 is between methanol gas import 2 and one end end socket 14, the end seal First 14 are equipped with overflow water out 5, and between washing water inlet 4 and other end end socket 14, which is equipped with water supplement port 6 Overflow baffle 9 is arranged in second clean gas outlet 13, horizontal 1 inner cavity middle position of tank body, and overflow baffle 9 is horizontally disposed flat Plate, edge are connected with the inner wall of horizontal tank body 1, are washing space 15 below overflow baffle 9, the liquid level 16 in washing space 15 is located at Central axes on horizontal 1 length direction of tank body are hereinafter, 1 inner cavity middle and upper part of horizontal tank body is equipped with methanol gas above overflow baffle 9 Cushion chamber 3, methanol gas import 2 are connected to methanol gas cushion chamber 3, and methanol gas cushion chamber 3 is the cushion space of rectangular shape, methanol Gas cushion chamber 3 is fixed on horizontal 2 inner wall of tank body by modes such as fixed floors, is opened on the bottom plate of methanol gas cushion chamber 3 If the mounting hole of methanol gas down-comer 12, for installing methanol gas down-comer 12, overflow baffle 9 is equipped with rectangle liquid reducing hole 8, Washing water inlet 4 two sides be arranged symmetrically, methanol gas down-comer 12 pass through rectangle liquid reducing hole 8 extend downwardly into liquid level 16 hereinafter, Each rectangle liquid reducing hole 8 and each row's methanol gas down-comer 12 cooperate.
8 upper surface of rectangle liquid reducing hole is higher by 9 50~80mm of upper surface of overflow baffle, and 8 lower surface of rectangle liquid reducing hole is low 9 50~80mm of lower surface of overflow baffle out.Rectangle liquid reducing hole 8 washing water inlet 4 every side it is in a row be evenly arranged, through square The overflow water that 8 upper edge of shape liquid reducing hole enters is directly along the outside wall surface of methanol gas down-comer 12 and 8 inner wall of rectangle liquid reducing hole Between space flow downward.The distance between the outside wall surface of methanol gas down-comer 12 and 8 inner wall of rectangle liquid reducing hole should be kept In 10~30mm, to form the overflow water stablized at the uniform velocity.
Mounting hole on 3 bottom plate of methanol gas cushion chamber is circular hole, and the diameter of mounting hole is about 20~50mm, mounting hole Square arrangement, which is covered with, fills a bottom plate for methanol gas cushion chamber 3, the installation for being spaced about 2~5 times between adjacent mounting hole Bore dia.
The length of the methanol gas cushion chamber 3 is suitable with the horizontal cylindrical shape barrel lenght of horizontal tank body 1, in length direction Two end faces of upper methanol gas cushion chamber 3 are concordant with 15 tangent line of end socket, and the width of methanol gas cushion chamber 3 is about that horizontal tank body 1 is straight 0.6~0.8 times of diameter, the bottom surface of methanol gas cushion chamber 3 is apart from 9 upper surface of overflow baffle about 150~200mm.
Methanol gas down-comer 12 is short straight tube structure, and entrance is installed on square arrangement on 3 bottom plate of methanol gas cushion chamber Mounting hole, outlet protrude into 16 or less about 50~100mm of water seal water liquid level.The air-flow in methanol gas down-comer 12 should generally be controlled Speed is in the range of 0.2~0.5m/s, in order to avoid big impact is caused to washing water and guarantees contact of the methanol gas with washing water Time.Methanol gas down-comer 12 can be set tens to several hundred as needed.
The liquid level 16 in the washing space 15 is located at 100~150mm of the central axes on horizontal 1 length direction of tank body or less.
Methanol gas import 2 connects methanol gas inlet pipe 11, is normally at horizontal 1 top center of tank body, methanol gas inlet pipe 11 straight down across the end face center of the through methanol gas cushion chamber 3 of the top center of horizontal tank body 1.First clean gas outlet 3 It is installed straight up positioned at horizontal 1 top side of tank body, water supplement port 6 is located at horizontal 1 bottom of tank body and installs straight up, horizontal Water supplement port 6 and the first clean gas outlet 7 are located at the two sides of methanol gas import 2, and close end socket 14 on 1 length direction of tank body, away from 1 diameter of horizontal tank body from neighbouring 14 tangent line of end socket about 0.2~0.5 or so.Overflow water out 5 is located remotely from the envelope of water supplement port 6 It is horizontally mounted on head, vertical position is in 16 or less 50~100mm of water seal water liquid level, overflow water out installation control water washing tank The small water seal of liquid level.It washes water inlet 4 and connects overflow water tedge 10, overflow water tedge 10 is connected to overflow baffle straight up 9 upper spaces.Second clean gas outlet 13 is installed on the side end socket of horizontal tank body 2, is vertically located at overflow baffle 9 Lower section.
Arrangement of the position occupied by methanol gas inlet pipe 11 without methanol gas down-comer 12 on methanol gas cushion chamber 3. Methanol gas cushion chamber 3 will have sufficiently large volume, after buffering, should flow it is steady, be evenly distributed, pressure oscillation everywhere Less, washing liquid level smoothly can be stably entered through methanol gas down-comer 12 hereinafter, not making liquid level appearance is biggish not advise It then fluctuates, achievees the purpose that improve water washing effect.
Methanol gas after 3 buffering of methanol gas cushion chamber through methanol gas down-comer enter washing space 15 liquid level 16 with Under washed, this process be bath wash;Fresh water is through washing water inlet 4 into 9 upper space of overflow baffle and along methanol Space between 8 inner wall of outside wall surface and rectangle liquid reducing hole of gas down-comer 12 flows downward to form extraction effect, overflow water edge Methanol gas down-comer 12 outer wall flow downward with after washing the gas phase that rises under buoyancy directly countercurrently connect Touching is washed, this process is overflow washing, and the direct counter current contacting of overflow water-washing process gas-liquid can increase water, gas contact Time and contact area improve the absorption efficiency to methanol gas.
The material of each component of the present invention is generally stainless steel (such as 304 stainless steels), and the connection between component generally uses Welding.
It is as follows using a kind of simple procedure that methanol air water cleaning of evaporator washes methanol gas of the present invention:
(1) methanol stream amount it is smaller (with methanol tank total measurement (volume) at 20000 cubic metres or less) when washed using bath, at this time second Clean gas outlet 13 blocks, and methanol gas (content is 20% hereinafter, remaining is the inert gases such as nitrogen) first is from methanol gas import 2 Enter the space of methanol gas cushion chamber 3 with methanol gas inlet pipe 11;By buffering after, methanol gas along methanol gas down-comer 12 to Under flow into washing water level below carry out washing operation;Fresh water enters washing space, wastewater containing methanol warp through water supplement port 6 Overflow water out 5 flows out water washing tank;Outside wall surface and rectangle descending liquid of the purified gas through methanol gas down-comer 12 after washing Being spatially advanced into 9 upper space of overflow down-flow plate and being discharged into atmosphere through the first clean gas outlet 7 between 8 inner wall of hole.
(2) when methanol stream amount increases (with methanol tank total measurement (volume) at 20000 cubic metres or more), bath is washed and overflow water It washes and is used in combination, the first clean gas outlet 7 blocks at this time, and (content is 20% hereinafter, remaining is lazy for nitrogen etc. for methanol gas first Property gas) from methanol gas import 2 enter methanol gas cushion space 3;By buffering after, methanol gas along methanol gas down-comer 12 to Under flow into washing water level below carry out bath wash operation;Overflow water enters from overflow water inlet 4 through overflow water inlet tube 10 9 top of overflow baffle, then the wall surface from rectangle liquid reducing hole 8 along methanol gas down-comer 12 drops to water seal water level and methanol gas The methanol vapor phase that the outlet of down-comer 12 rises after washing carries out methanol absorption to contact;Fresh water enters through water supplement port 6 Space is washed, wastewater containing methanol flows out water washing tank through overflow water out 5;Purified gas after washing is through through the second purified gas Outlet 13 is discharged into atmosphere.

Claims (10)

1. a kind of methanol air water cleaning of evaporator, including horizontal tank body (1), horizontal tank body (1) by horizontal cylindrical shape cylinder and be located at its two The end socket (14) at end forms, it is characterised in that: is equipped with methanol gas import (2) and the first purified gas at the top of the horizontal tank body (1) It exports (7), methanol gas import (2) center at the top of horizontal tank body (1), horizontal tank body (1) bottom is equipped with washing water inlet (4) With water supplement port (6), wash water inlet (4) in horizontal tank body (1) bottom center, the first clean gas outlet (7) methanol gas into Between mouth (2) and one end end socket (14), which is equipped with overflow water out (5), and water supplement port (6) is in washing water inlet (4) between other end end socket (14), which is equipped with the second clean gas outlet (13), horizontal tank body (1) inner cavity Overflow baffle (9) are arranged in middle position, and overflow baffle (9) is horizontally disposed plate, the inner wall phase at edge and horizontal tank body (1) It even, is washing space (15) below overflow baffle (9), the liquid level (16) of washing space (15) is located at horizontal tank body (1) length side Upward central axes are hereinafter, horizontal tank body (1) inner cavity middle and upper part is equipped with methanol gas cushion chamber (3), first above overflow baffle (9) Alcohol gas import (2) is connected to methanol gas cushion chamber (3), and methanol gas cushion chamber (3) is the cushion space of rectangular shape, and methanol gas is slow The mounting hole that methanol gas down-comer (12) is opened up on the bottom plate of chamber (3) is rushed, for installing methanol gas down-comer (12), overflow gear Plate (9) is equipped with rectangle liquid reducing hole (8), is arranged symmetrically in the two sides of washing water inlet (4), methanol gas down-comer (12) passes through Rectangle liquid reducing hole (8) extends downwardly into liquid level (16) hereinafter, each rectangle liquid reducing hole (8) and each row's methanol gas down-comer (12) It cooperates, washing water inlet (4) connection overflow water tedge (10), overflow water tedge (10) is connected to overflow gear straight up Plate (9) upper space.
2. a kind of methanol air water cleaning of evaporator according to claim 1, it is characterised in that: rectangle liquid reducing hole (8) upper surface Be higher by overflow baffle (9) 50~80mm of upper surface, rectangle liquid reducing hole (8) lower surface it is low go out overflow baffle (9) lower surface 50~ 80mm, rectangle liquid reducing hole (8) in a row are evenly arranged in every side of washing water inlet (4).
3. a kind of methanol air water cleaning of evaporator according to claim 1, it is characterised in that: outside the methanol gas down-comer (12) The distance between wall surface and rectangle liquid reducing hole (8) inner wall should be in 10~30mm.
4. a kind of methanol air water cleaning of evaporator according to claim 1, it is characterised in that: the methanol gas cushion chamber (3) passes through Fixed floor is fixed on horizontal tank body (2) inner wall.
5. a kind of methanol air water cleaning of evaporator according to claim 1, it is characterised in that: methanol gas cushion chamber (3) bottom plate On mounting hole be circular hole, the diameter of mounting hole is about 20~50mm, and it is slow that the square arrangement of mounting hole is covered with dress methanol gas The bottom plate of chamber (3) is rushed, the installation bore dia that the spacing between two neighboring mounting hole is 2~5 times.
6. a kind of methanol air water cleaning of evaporator according to claim 1 or 5, it is characterised in that: the methanol gas cushion chamber (3) Length is suitable with the horizontal cylindrical shape barrel lenght of horizontal tank body (1), in the longitudinal direction two ends of methanol gas cushion chamber (3) Face is concordant with end socket (15) tangent line, and the width of methanol gas cushion chamber (3) is 0.6~0.8 times of horizontal tank body (1) diameter, methanol The bottom surface of gas cushion chamber (3) is apart from overflow baffle (9) 150~200mm of upper surface.
7. a kind of methanol air water cleaning of evaporator according to claim 1, it is characterised in that: the methanol gas down-comer (12) is short Straight tube structure, entrance are installed on mounting hole arranged in square on methanol gas cushion chamber (3) bottom plate, and water seal aqueous is protruded into outlet About 50~100mm, methanol gas down-comer (12) setting tens to several hundred control in methanol gas down-comer (12) below for position (16) Air velocity in the range of 0.2~0.5m/s.
8. a kind of methanol air water cleaning of evaporator according to claim 1, it is characterised in that: the liquid level of washing space (15) (16) it is located at 100~150mm of the central axes on horizontal tank body (1) length direction or less.
9. a kind of methanol air water cleaning of evaporator according to claim 1, it is characterised in that: the water supplement port (6) and the first purification Gas exports 0.2~0.5 times of the distance of neighbouring end socket (14) tangent line of (7) distance for horizontal tank body (1) diameter, overflow water out (5) vertical position is in water seal water liquid level (16) 50~100mm below, and the second clean gas outlet (13) is in vertical position to overflow Flow the lower section of baffle (9).
10. a kind of methanol air water cleaning of evaporator according to claim 1, it is characterised in that: first on the methanol gas cushion chamber (3) Arrangement of the position occupied by alcohol gas inlet pipe (11) without methanol gas down-comer (12).
CN201810130930.7A 2018-02-09 2018-02-09 Methanol air water cleaning of evaporator Pending CN110124459A (en)

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Application publication date: 20190816