CN110117836A - The preparation method of precursor containing jade powder and bedclothes fabric containing the precursor - Google Patents
The preparation method of precursor containing jade powder and bedclothes fabric containing the precursor Download PDFInfo
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- CN110117836A CN110117836A CN201811383669.8A CN201811383669A CN110117836A CN 110117836 A CN110117836 A CN 110117836A CN 201811383669 A CN201811383669 A CN 201811383669A CN 110117836 A CN110117836 A CN 110117836A
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- A—HUMAN NECESSITIES
- A47—FURNITURE; DOMESTIC ARTICLES OR APPLIANCES; COFFEE MILLS; SPICE MILLS; SUCTION CLEANERS IN GENERAL
- A47C—CHAIRS; SOFAS; BEDS
- A47C27/00—Spring, stuffed or fluid mattresses or cushions specially adapted for chairs, beds or sofas
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- A—HUMAN NECESSITIES
- A47—FURNITURE; DOMESTIC ARTICLES OR APPLIANCES; COFFEE MILLS; SPICE MILLS; SUCTION CLEANERS IN GENERAL
- A47G—HOUSEHOLD OR TABLE EQUIPMENT
- A47G9/00—Bed-covers; Counterpanes; Travelling rugs; Sleeping rugs; Sleeping bags; Pillows
- A47G9/02—Bed linen; Blankets; Counterpanes
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J3/00—Processes of treating or compounding macromolecular substances
- C08J3/20—Compounding polymers with additives, e.g. colouring
- C08J3/22—Compounding polymers with additives, e.g. colouring using masterbatch techniques
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
- D01D13/00—Complete machines for producing artificial threads
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
- D01D5/00—Formation of filaments, threads, or the like
- D01D5/08—Melt spinning methods
- D01D5/098—Melt spinning methods with simultaneous stretching
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F6/00—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof
- D01F6/88—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polycondensation products as major constituent with other polymers or low-molecular-weight compounds
- D01F6/92—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polycondensation products as major constituent with other polymers or low-molecular-weight compounds of polyesters
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- D—TEXTILES; PAPER
- D03—WEAVING
- D03D—WOVEN FABRICS; METHODS OF WEAVING; LOOMS
- D03D1/00—Woven fabrics designed to make specified articles
-
- D—TEXTILES; PAPER
- D03—WEAVING
- D03D—WOVEN FABRICS; METHODS OF WEAVING; LOOMS
- D03D15/00—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used
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- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2503/00—Domestic or personal
- D10B2503/06—Bed linen
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacturing & Machinery (AREA)
- Mechanical Engineering (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Artificial Filaments (AREA)
Abstract
The present invention relates to the preparation method of the precursor containing jade powder and contain the bedclothes fabric of the precursor.Provided method according to the present invention, masterbatch is prepared by using 0.5~1 μm of uniform jade powder and according to stable mixed proportion mixing masterbatch and polyester raw material, thus spinning is carried out in specific Denier range, is not damaged spinning properties to can provide and is made the far infrared radiation excellent of prepared fiber and the durability also beautiful fiber of outstanding functionality of fiber.
Description
Technical field
The present invention relates to the preparation method of the precursor containing jade powder and using prepared precursor bedclothes fabric,
More particularly, to preparing masterbatch with subtle jade powder and by (poly- with the macromolecule resin that forms function with fiber
Ester) raw material mix and spinning is to prepare the precursor with function far infrared radiation function, and the fabric prepared by the precursor is used
Articles in bed.
In particular, the content of jade powder contained in the size and masterbatch of the stable jade powder to be mixed before spinning,
The fiber number condition of the content, prepared most filum terminale that are blended in the masterbatch of spinning resin is characteristic point therein.
Background technique
The ore of jade, germanium, tourmaline etc. is the outstanding natural minerals of far infrared radiation, wherein jade be since ancient times mostly with
Ornament come using the familiar minerals of people, the far infrared given off from jade has warm-heat effect, ripe to human body
At effect, self purification, dry and wet effect, neutralization, sympathetic response effect etc., in industry and medical field, widely with therapeutic purposes
It uses.
It is well known that far infrared has the electricity of very big heat effect as because wavelength is longer than the red light region of visible light
Magnetic wave is invisible to the naked eye, and is easily absorbed by object, resonance and sympathetic response powerful to organic compound molecule, therefore, when by people
It is 80 times stronger than general heat radiation when body absorbs, it may penetrate into deep skin and treat bacterium, cancer cell.
Also, far infrared is by moisture to group adult somatic cells and protein molecule irradiation come by per minute about
2000 microseismic activities generate resonance, and thus cellular activity becomes active.During cellular activity, thermal energy can be generated, will be made
Body temperature increases, and the raising of body temperature will be such that fine vascular expands and accelerate blood circulation, reinforces metabolism, improves regeneration
Ability decomposes endovascular thrombus and promotes blood circulation.Due to making blood become limpid, thus can be by improving hydrogen ion
Acidic constitution is changed to the ability of alkalescent constitution to strengthen by concentration pH, by facilitating the relaxation effect of mental health, is eliminated
The pressure of one of the principal element of adult diseases.
There are many kinds of the technologies using jade powder with this characteristic, wherein in Korean Patent Laid 10-
It is described in 2010-0131639, Korean Patent Laid 10-2009-0006307 and jade powder is applied (coating) in original
Silk table face contains Yu Yuansi.
It is well known that it is used as modular flooring plate for building also by adhesive of the exploitation containing jade powder, or
By developing there is the precursor of far-infrared functional and antibacterial, deodorant function to be used as the example (KR published patent of garment material
Bulletin 10-2000-0065341).
Also, other than jade, also describes and cut by crushing rub root stone, tourmaline, titanium and medical stone to produce anion
Piece is simultaneously mixed with cotton yarn, polyester, nylon, propylene, polypropylene etc. to produce precursor technology (Korea Spro of radiation anion and far infrared
State publication bulletin 10-2009-0093507) and by mixing thin fine jade powder and spinning material come spinning
And the technology (Korean Patent Laid 10-2000-0065341) of beautiful silk is prepared, but be difficult to confirm specific preparation section
With the durability of far-infrared effect, precursor.
Also, the shortcomings that prior art, is as follows, that is, since jade powder is attached to fiber surface using binder, because
This is difficult even application, falls off because of washing etc. and causes to lose far infrared function.
Summary of the invention
The object of the present invention is to provide the beautiful fibers of following functionality, that is, according to the present invention, by using 0.5~1 μ
The uniform jade powder of m is to prepare masterbatch and according to stable mixed proportion mixing masterbatch and polyester raw material, thus specific
Spinning is carried out in Denier range, is not damaged spinning properties to can provide and is kept the far infrared radiation effect of prepared fiber excellent
Elegant and fiber the durability also outstanding beautiful fiber of functionality.
Also, it is an object of the present invention to prepare bedclothes fabric using beautiful precursor.
To achieve the above object, preparation method of the invention offer prepares 40~85 fibres by being stretched after spinning
The method containing beautiful drawn yarn of degree and 36~204 filament counts.It is a feature of the present invention that including: 0.5~1 μm of preparation thin
The step of micro- jade powder;The content for preparing above-mentioned jade powder reaches 10~20 weight percent of total weight and surplus is polyester
Masterbatch the step of;Above-mentioned masterbatch and polyester are mixed according to the weight ratio of 4:96 to 10:90 come the step of preparing spinning material;With
Above-mentioned spinning material carries out the step of melt spinning;And 40~85 are prepared by being stretched to the precursor through above-mentioned spinning
The step of fiber number and the drawn yarn of 36~204 filament counts.
In order to make to reach maximizations from the far-infrared effect for kindly helping secure the success of point radiation, it is necessary to which addition is to greatest extent in the fibre
It kindly helps secure the success of point.But this has negative effect for the radiativity of macromolecule resin, the physical property (intensity) of fiber.Also, in fabric system
After the completion of standby, it is natural for also generating baneful influence for precursor durability.Therefore, select content ratio appropriate very heavy
It wants, and it is a feature of the present invention that making final drawn yarn by the size and content of the jade powder for adjusting beautiful fibrous inside
Thickness is in 40~85 fiber numbers, 36~204 filament count ranges.That is, it is a feature of the present invention that thickness is up to 40~85 in order to obtain
Fiber number, the final drawn yarn of 36~204 filament counts, so that the mixing between the size and jade powder and polyester of jade powder particle
Being optimal of ratio.
Also, it is a feature of the present invention that in a manner of making to kindly help secure the success of point beautiful fiber for being contained uniformly in institute's spinning not
Beautiful powder directly is mixed to polyester resin, but utilizes masterbatch, and the beautiful content in masterbatch is made to reach 10~20 weight percent.
Above-mentioned masterbatch is squeezed out by the screw extruder of high temperature, in the jade powder and 80 for mixing 10~20 weight percent
The screw extruder that the backward temperature of the polyester slice of~90 weight percent is 240~280 DEG C is put into, and is extracted out by spray head
And it is cooled down.
Also, high-temperature spiral extruder preferably gradually rises temperature, and it is a feature of the present invention that with initial section
Temperature be 240~250 DEG C, the temperature in intermediate section is 250~260 DEG C, the side that the temperature in final section is 260~280 DEG C
Formula is come that temperature is arranged to above-mentioned screw extruder by section.
According to the present invention, the beautiful fiber for including beautiful powder in the resin of institute's spinning and making spinning properties outstanding is provided
Preparation method.Also, the outstanding beautiful fiber of the physical property and far-infrared radiated property for the beautiful fiber that present invention offer finally stretches
Preparation method.The beautiful fiber prepared through the invention can it is woven, be woven into bedclothes fabric, to be used in quilt, cushion
Equal bedding.
Detailed description of the invention
Fig. 1 shows the character photo of the preparation process point by jade powder.
Fig. 2 shows the sections and surface picture of the beautiful fiber prepared through the invention.
Fig. 3 is shown to be become by using the quilt of beautiful fiber preparation prepared by the present invention and the testee body temperature of common quilt
Change curve graph.
Fig. 4 is shown by using beautiful fiber prepared by the present invention come the quilt prepared and the testee toe of common quilt
Blood flow change curve.
Fig. 5 is shown by using beautiful fiber prepared by the present invention come the quilt prepared and the testee finger of common quilt
Refer to blood flow change curve.
Fig. 6 show by using beautiful fiber prepared by the present invention the infrared heat of the quilt and common quilt surface that prepare at
As figure.
Fig. 7 show by using beautiful fiber prepared by the present invention the infrared heat of the cushion and common mat surface that prepare at
As figure.
Specific embodiment
Hereinafter, the present invention will be described in detail.
The preparation of jade powder
Although nephrite, jadeite, serpentine can be used, the jade used in embodiments of the present invention is as in nephrite
Spring river it is beautiful.By the uniform fine-powdered for crushing 0.5~1 μm of spring river Yu Yuanshi, Lai Shixian.The size of jade powder is according to original
The thickness of silk determines, if precursor thickness is big, the big powder of size can be used, it is contemplated that final drawn yarn is strong
Degree, far-infrared radiation rate, spinnability etc. are, it is specified that particle size appropriate is critically important.The present invention is prepared by finally stretching
40~85 fiber numbers, the drawn yarn containing jade of 36~204 filament counts confirm the particle size of jade powder no more than 1 μm.
Size of powder particles and spinnability
(1) jade powder size is 500~700nm
Convenient for spinning, because powder is well dispersed in precursor, the durability of precursor, far infrared emissivity can be maintained
Also very outstanding.
(2) jade powder size is less than 1 μm
Can spinning because powder is well dispersed in precursor can maintain the durability of precursor, far infrared emissivity
It is very outstanding.
(3) jade powder size is greater than 1 μm and less than 5 μm
The thickness of drawn yarn be greater than 85 fiber number in the case where can spinning, but so that the scope of the present invention 36~204
In the case that the mode that the thickness containing beautiful drawn yarn of filament count reaches 40~85 fiber numbers prepares most filum terminale, it can not be melted
Spinning.
(4) jade powder size is greater than 5 μm
Can not spinning, the reason of powder interferes the binding force in precursor between molecule, becomes fracture of wire.
The quantity of the silk of institute's spinning can be adjusted by replacing the type of spinneret orifice, in the present invention, by the silk of institute's spinning
Quantity be limited to the ranges of 36~204 filament counts, reach the thickness of final drawn yarn by stretching these tow
To 40~85 fiber numbers.
The preparation of masterbatch
0.5~1 μm, especially 500nm~700nm nanosized particle are because of the electrostatic repulsion and Fan De between particle
Wals force and make cohesive force very strong, thus have and be difficult to control, the very low feature of dispersibility.Therefore, if by above-mentioned size
Particle be mixed directly into polyester to carry out spinning, then jade powder cannot be uniformly dispersed, not only make spinnability bad, but also will
Adverse effect is brought to the physical property of most filum terminale.That is, the dispersibility of jade powder determines in fusing spinning step in masterbatch preparation
The physical property of fiber needs jade powder size and content appropriate, fills to be uniformly dispersed jade powder in screw extruder
Point mixing, temperature condition.
Therefore, it is a feature of the present invention that make jade powder be evenly distributed on the beautiful fibrous inside of institute's spinning, not directly to
Polyester resin mixes jade powder, but utilizes masterbatch, and the beautiful content in masterbatch reaches 10~20 weight percent.
That is, mixing the jade powder of 10~20 weight percent to the polyester slice of 80~90 weight percent to prepare mother
Material, to temperature be 240~280 DEG C screw extruder investment be completely dried under vacuum conditions and dewatered jade powder and
Polyester slice.It has confirmed that and is conducive to mixture homogeneity, mechanical load etc. by the temperature of section setting screw extruder.Thus,
The temperature in initial section is 240~250 DEG C, the temperature in intermediate section is 250~260 DEG C, the temperature in final section be 260~
280℃.It is extracted and is cooled by spray head as the resin of liquid condition at high operating temperatures, it is long according to the regulation of 2 × 3mm
Continuous cutting-off is spent to be prepared into masterbatch.
Wherein, being distinguished the temperature of screw extruder by section and be gradually warmed up is melting and powder for the ease of resin
Mixing.
It is advantageous to dispersibility if making the content of jade powder lower than 10 weight percent when preparing masterbatch, but can not be
Reach the highest content that may include, and far infrared radiation in the Denier range for the final drawn yarn to be obtained through the invention
It measures small, if jade powder content is made to be more than 20 weight percent, masterbatch can not be prepared at all, because of the jade powder in resin point
Scattered property is low and causes to agglomerate, and machine will generate failure due to by load.It therefore, should include 10~20 weights when preparing masterbatch
Measure the jade powder of percentage.
Melt spinning
The masterbatch prepared is mixed with polyester, fibre is prepared by common melt spinning (Melt Spinnning)
Dimension.Temperature of the common melt spinning more than fusing point squeeze out by spinneret orifice, be cooling, attachment finish step come prepare not only it is thin but also
It is wound after long Filamentous line.At this moment, the orientation of precursor changes according to spinning speed, and spinning speed is in 500~1500m/min
Lower spun silk has the very low degree of orientation and is called low-oriented yarn (LOY;Low oriented spun yarn).Spinning speed
The precursor spun in 1500~2500m/min is called half preoriented yarn (MOY; medium oriented spun yarn),
The precursor that spinning speed is spun in 2500~4000m/min is called preoriented yarn (POY;partially oriented
Yarn), the precursor that spinning speed is spun in 4000~6000m/min is called high oriented yarn (HOY;highly oriented
Yarn), the precursor that spinning speed is spun in 6000m/min is called fully drawn yarn (FOY;fully oriented yarn).
The filamentary fibers of such spinning belong to the undrawn yarn (Undrawn yarn) for not having sufficient physical property also, lead to
The false twisting that overstretching is allowed to become more elongated is called drawn yarn (Drawn yarn) to be orientated spinneret chain and do crystallization.The weight of false twisting
Wanting condition is to twist (Twist), temperature (temperature), tension (Tension), time (Time), the feelings of adjusted temperature and humidity
Under condition, is passing through roller and extending the fixed device of point, after heating plate and work beam etc., twisted with spindle, with 1000m/min speed
It is wound on spool.
The present invention extends the beam of 36~204 filament counts, and the final fiber number for preparing is 40~85 fiber number jade fibers.
In the final precursor for extending preparation, spring river jade content of powder is had confirmed that as 0.4~2 weight percent.If adjusting
The amount of polyester mixed before masterbatch preparation step or spinning is come so that the beautiful content in final drawn yarn can then go out greater than 2%
When existing spinning the problem of precursor fracture of wire, this is because jade powder can not be evenly dispersed in precursor, and there is coacervation, thus
Reduce the binding force in precursor between molecular structure.Also, in economic aspect, more than above range and bad.Another party
Face is come if adjusting the amount of polyester mixed before masterbatch preparation step or spinning so that the beautiful content in final drawn yarn is less than
0.4%, the jade powder content in precursor reduces, and causes far-infrared radiated property faint.
Embodiment
The preparation of masterbatch
By being completely dried under vacuum conditions and dewatered 20 weight to the mixing of the polyester slice of 80 weight percent
It measures the jade powder of percentage and puts into and maintain 250 DEG C, 260 DEG C, 270 DEG C respectively by initial section, intermediate section, final section
Temperature screw extruder.It is extracted and is cooled down by spray head as the resin of liquid at high operating temperatures, according to 2 ×
The specific length continuous cutting-off of 3mm is prepared into masterbatch.
Melt spinning
The masterbatch for 7 weight percent for preparing and drying through the above steps to the mixing of the polyester raw material of 93 weight percent
And melt spinning is carried out, 75 fiber numbers, 36 drawn yarns (DTY) are prepared for by false twisting and extension.Pass through micro- sem observation
The result of practical filament surfaces and section, it is thus identified that spring river jade powder is located at filament surfaces and inside (referring to Fig. 2).
The preparation of beautiful fabric lining
Fabric is prepared for using the beautiful fiber prepared through the above steps come plain weave.Organizine has used common polyester precursor
(50 fiber number/144 thread), dimension silk have used the beautiful fiber precursor (75 fiber number/36 thread) prepared in the above-described embodiments.Pass through South Korea
Far infrared association has detected far infrared radiation rate to the fabric prepared in the manner, and confirmed far infrared radiation
Rate is 89.3% or more, has outstanding performance.
The infrared ray checking of bedding
Understood using the above-mentioned quilt for preparing fabric preparation and cushion (hereinafter referred to as spring river jade quilt, spring river jade mattress)
The practical influence to human body of far infrared, and assessed by Inha University, South Korea Leisure Sport fiber research center.
Testee is three healthy adult females, identical environment (23 ± 0.5 DEG C of temperature, humidity 50 ±
10%) under, on the different dates, at the same time tested, have detected skin temperature (chest, upper arm, thigh, shank) with
Blood flow (left hand middle finger, left foot thumb), comparative group used 100% polyester common quilt and common cushion (referring to table 1,
Table 2).
Table 1
Table 2
Experimental sequence
1. confirming the physical condition on the day of testee, rest 20 minutes after wearing shorts in waiting room.
2. attaching the related electrode of detection project in waiting room (23 ± 0.5 DEG C of temperature, humidity 50 ± 10%).
3. the detection position of detection project is respectively chest, upper arm, thigh, the skin temperature of shank and left hand middle finger, left foot
The blood flow of thumb.
4. entering phjytotron (23 ± 0.5 DEG C of temperature, humidity 50 ± 10%).
5. lying 60 minutes under conditions of spring river jade quilt/cushion and common quilt/cushion and detecting stable and physiology letter
Number.
6. detecting chest with thermal infrared imager under conditions of using spring river jade quilt/cushion and common quilt/cushion respectively
The quilt surface at portion position.
7. spring river jade quilt/cushion and common quilt/cushion are the implementation of section at the same time in not same date, and in perseverance
12 hours of constant temperature and humidity room use after being stablized.
Experimental result
Experimental result, skin surface temperature divide human body and different, pass through La Manatanshi (Ramananthan) and count
Comfortable human body mean skin temperature is 33 ± 1 DEG C when the sleep of calculation.As time go on, under the conditions of two kinds of samples, skin
Temperature averagely rises 7% respectively, but generally speaking, does not occur significant gap in each condition (referring to Fig. 3).
Blood flow (in the body tissue of 100g, the amount of the hemoglobin flowed in one minute) is to compare toe and finger,
As time go on, confirm the blood flow of toe within 40%, finger changes within 5% (referring to Fig. 4, Fig. 5)
As a result.Also, when comparing two kinds of samples on the basis of toe blood flow, beautiful (experimental subjects) the quilt comparison in display spring river is common
(comparison other) quilt is big (referring to Fig. 4, Fig. 5).
Also, confirm infrared thermal imaging figure as a result, comparing quilt surface temperature after sixty minutes, spring river jade quilt after experiment
Son rises 0.9 DEG C, and common quilt rises 1.1 DEG C, the mat surface temperature before testing after comparative experiments, on spring river jade mattress
8.1 DEG C are risen, common cushion rises 7.7 DEG C (referring to Fig. 6, Fig. 7).
Finally, when using spring river jade quilt, compared with common quilt, toe blood flow increases 40%, before cushion use
Surface temperature afterwards rises 0.4 DEG C (spring river jade mattress rises 8.1 DEG C, and common pad rises 7.7 DEG C), therefore the effect confirmed exists
In, use when jade powder improve heat insulation effect and improve blood circulation.
According to the present invention, beautiful precursor is available in multiple product, such as diaper, female article, mask, underwear, socks, fortune
Dynamic clothes etc., but far-infrared effect is faint, when being used in bedding, due to wrapping up whole body, it is thus regarded that far infrared can be made to imitate
Fruit maximizes.
Claims (4)
1. a kind of preparation method of the precursor comprising the jade powder with function far infrared radiation function, by being stretched after spinning
To prepare 40~85 fiber numbers i.e. drawn yarn of 36~204 filament counts characterized by comprising
The step of subtle jade powder of 0.5~1 μm of preparation;
Prepare above-mentioned jade powder content reach total weight 10~20 weight percent and surplus be polyester masterbatch the step of;
Above-mentioned masterbatch and polyester are mixed according to the weight ratio of 4:96 to 10:90 come the step of preparing spinning material;
The step of carrying out melt spinning with above-mentioned spinning material;And
The i.e. drawn yarn of 36~204 filament counts of 40~85 fiber numbers is prepared by being stretched to the precursor through above-mentioned spinning
Step.
2. the preparation method of the precursor according to claim 1 comprising the jade powder with function far infrared radiation function, special
Sign is, in the step of preparing above-mentioned masterbatch, mixes the above-mentioned jade powder and 80~90 weight hundred of 10~20 weight percent
Divide the polyester slice of ratio, and put into the screw extruder that temperature is 240~280 DEG C, is extracted out and cooled down by spray head.
3. the precursor preparation method according to claim 2 comprising the jade powder with function far infrared radiation function, feature
It is, the temperature with initial section is 240~250 DEG C, the temperature in intermediate section is 250~260 DEG C, the temperature in final section is
260~280 DEG C of mode is come that temperature is arranged to above-mentioned screw extruder by section.
4. a kind of bedclothes fabric, which is characterized in that comprising passing through the packet described in any one of described in claims 1 to 3
Precursor preparation method containing the jade powder with function far infrared radiation function is come the fiber for preparing.
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KR1020180015054A KR101904105B1 (en) | 2018-02-07 | 2018-02-07 | Method of manufacturing yarn containing jade powder with far infrared ray activity and bedding product using yarn produced thereby |
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KR102409236B1 (en) * | 2021-12-21 | 2022-06-16 | 대구경북침구류협동조합 | Manufacturing method of yarn for bedding containing functional material |
KR20230163162A (en) | 2022-05-23 | 2023-11-30 | 박주현 | Manufacturing Method of Composite Infrared Emission Filament Yarn with Far Infrared and Near Infrared Emission Functions, and its Composite Infrared Emission Filament Yarn |
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CN110685031A (en) * | 2019-10-31 | 2020-01-14 | 宁波瑞凌新能源科技有限公司 | Radiation refrigeration fiber and preparation method and application thereof |
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