CN110105864A - Boost metabolism, improve the pyramid craftwork of cell viability - Google Patents
Boost metabolism, improve the pyramid craftwork of cell viability Download PDFInfo
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- CN110105864A CN110105864A CN201910292797.XA CN201910292797A CN110105864A CN 110105864 A CN110105864 A CN 110105864A CN 201910292797 A CN201910292797 A CN 201910292797A CN 110105864 A CN110105864 A CN 110105864A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D175/00—Coating compositions based on polyureas or polyurethanes; Coating compositions based on derivatives of such polymers
- C09D175/04—Polyurethanes
- C09D175/14—Polyurethanes having carbon-to-carbon unsaturated bonds
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
- C09D7/62—Additives non-macromolecular inorganic modified by treatment with other compounds
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/63—Additives non-macromolecular organic
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/70—Additives characterised by shape, e.g. fibres, flakes or microspheres
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/24—Acids; Salts thereof
- C08K3/26—Carbonates; Bicarbonates
- C08K2003/265—Calcium, strontium or barium carbonate
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/014—Additives containing two or more different additives of the same subgroup in C08K
Abstract
The invention discloses a kind of pyramid craftwork far-infrared negative-ion coating and the pyramid craftwork for the cell viability that boosts metabolism, improves, the pyramid craftwork to be prepared with far-infrared negative-ion coating by following raw materials: polyurethane resin, modified six ring stones, modification infusorial earth, modified verdelite, levelling agent, dispersing agent, anti skinning agent, drier, functional additive, solvent naphtha.The present invention boosts metabolism, improves the pyramid craftwork of cell viability, the handicraft surface is coated with pyramid craftwork far-infrared negative-ion coating, interior is carried or be put in the craftwork, anion and far infrared can be released effectively, to accelerate blood circulation, promote human metabolism, activation histocyte, improve the immunity of the human body.The technique also has certain anti-radiation effect, can reduce radiation of the electronic equipment to human body.
Description
Technical field
The present invention relates to a kind of pyramid craftworks for boosting metabolism, improving cell viability, belong to craftwork technology
Field.
Background technique
Craftwork is manual manufacture or the product that reprocessing obtains, and traditional arts and crafts can decorate room, beautify the environment, existing
Having the craftwork in technology substantially is decoration, beautification household or office space, and purposes is single, without actual health-care efficacy.
With the development of the society, people increasingly pay close attention to the health of itself, the requirement to craftwork is not only to pursue vision
Aesthetic feeling, enhancing is decorative, also requires craftwork itself material to human body and environmentally friendly, and require craftwork that can purify
Air has health-care efficacy to human body.
Negative aeroion is also negative oxygen ion, refers to and obtains extra paired electrons and negatively charged oxygen ion.Bear from
Son can facilitate human body synthesize and vitamin storage, strengthen and human activin physiological activity, therefore it be otherwise known as " air dimension life
Element ".Anion can neutralize free radical and be allowed to lose activity, no longer plunder electronics, or dead by aging after plunder electronics
It dies cell and electronics is provided, be allowed to restore normal activity.It is anti-that this journey inherently inhibits substance to lose the electronics i.e. oxidation of substance
It answers, therefore anion actually plays the role of " anti-oxidant " in human body.Anion can significantly improve body's immunity, living
Change reticuloendothelial system, the i.e. phagocytic function of mononuclear macrophage, improve reactivity of organism, enhance body resistance against diseases, is promoted
Human body vis medicatrix naturae.
Far infrared has stronger penetration and radiant force, has significant temperature control effect and resonance effects, far infrared
After being absorbed by the body, resonance effects, caused hot deep layer effect in vivo, energy activating cell, raising group can be generated with biological cell
Power of regeneration is knitted, promotes cell growth, and make telangiectasis, promotes blood circulation, boost metabolism, body Gao Renti
Immunity.
The demand of the present inventors's most craftwork provides a kind of pyramid work for boosting metabolism, improving cell viability
Skill product reach health-care efficacy by release far infrared and anion.
Summary of the invention
The problem to be solved by the invention is to provide a kind of pyramid craftwork far-infrared negative-ion coating and promotions
Metabolism, the pyramid craftwork for improving cell viability, it is negative that the handicraft surface is coated with pyramid craftwork far infrared
The craftwork is carried or is put in interior, can be released effectively anion and far infrared, to accelerate blood by ion coating
Liquid circulation promotes human metabolism, activation histocyte, improves the immunity of the human body.The technique also has certain radiation protection
Effect can reduce radiation of the electronic equipment to human body.
The present invention provides a kind of pyramid craftwork far-infrared negative-ion coating, the pyramid craftwork is used remote red
Outer negative ion paint is prepared by the raw material of following weight parts: 65-75 parts of polyurethane resin, is modified modified 3-8 parts of six ring stone
1-2 parts of diatomite, 1-2 parts of modified verdelite, 0.1-0.5 parts of levelling agent, 0.1-0.5 parts of dispersing agent, anti skinning agent 0.1-0.5
Part, 0.5-1 parts of drier, 0.5-1 parts of functional additive, 35-45 parts of solvent naphtha.
Preferably, the functional additive is cobalt titanate and/or cadmium ferrite.
It is further preferred that the functional additive be cobalt titanate and cadmium ferrite mixture, wherein the cobalt titanate and
The mass ratio of cadmium ferrite is 1:(1-5).
Preferably, the drier is at least one of zinc Isoocatanoate, cobalt iso-octoate.
Preferably, the anti skinning agent is methyl ethyl ketoxime.
Preferably, the levelling agent is Silicone modified acryl's ester levelling agent.
Preferably, the six ring stone of modification is prepared using following methods:
(1) six ring stone 25-35g are added in 90-110mL water, with 100-300 revs/min stirring 10-20 minutes, obtain
Six ring stone dispersion liquids；
(2) cerous sulfate 0.01-1mol is added in 90-110mL water, with 100-300 revs/min stirring 20-30 minutes, obtain
To cerous sulfate solution；
(3) titanium sulfate 0.05-0.15mol is added in 90-110mL water, is stirred at 90-95 DEG C with 100-300 revs/min
After 20-30 minutes, adjusting pH with 8-12wt% sodium hydroxide is 8-9, six ring stone dispersion liquids is added, at 90-95 DEG C with 100-300
Revs/min stirring 8-12 minutes, add cerous sulfate solution, 90-95 DEG C with 100-300 revs/min stirring 2-4 hours, with 4000-
8000 revs/min centrifugation 10-20 minutes, lower sediment be washed with water to washing lotion pH for neutrality, it is small in 90-100 DEG C of dry 2-4
When, then 300-500 DEG C heat preservation 1-3 hours, obtain six metal oxide-loaded ring stones；
(4) after diluting titanate coupling agent TC114 0.5-1g with solvent naphtha 8-12g, dilution is obtained, by 25-35g
Six metal oxide-loaded ring stones are added in 90-110mL ethyl alcohol, at 70-80 DEG C with 100-300 revs/min of stirring 10-20 points
Clock, be added dilution, 70-80 DEG C with 100-300 revs/min stirring 60-90 minutes, with 4000-8000 revs/min of centrifugation 10-20
Minute, lower sediment is 6-10 hours dry at 90-100 DEG C, obtains modified six ring stones.
Preferably, the modification infusorial earth is prepared using following methods: by titanate coupling agent TC114 0.5-1g
With solvent naphtha 8-12g dilution after, obtain dilution, 25-35g diatomite be added in 90-110mL ethyl alcohol, 70-80 DEG C with
100-300 revs/min stirring 10-20 minutes, be added dilution, 70-80 DEG C with 100-300 revs/min stirring 60-90 minutes, with
4000-8000 revs/min centrifugation 10-20 minutes, lower sediment is 6-10 hours dry at 90-100 DEG C, obtains modification infusorial earth.
Preferably, the solvent naphtha is No. 200 solvent naphthas.
The pyramid craftwork is prepared with far-infrared negative-ion coating using following methods: by polyurethane resin,
It is modified six ring stones, modification infusorial earth, modified verdelite, levelling agent, dispersing agent, anti skinning agent, drier, functional additive, molten
The mixing of agent oil, with 400-800 revs/min of stirring 10-20 minutes to get.
The present invention also provides a kind of pyramid craftwork for boosting metabolism, improving cell viability, including tower body, institutes
The outer surface for stating tower body, which is uniformly brushed, pyramid craftwork far-infrared negative-ion coating
Preferably, any one of the tower body material in iron, stainless steel, titanium, magnetite, metal alloy.
Preferably, the pyramid craftwork is 0.02-0.2mm with the coating layer thickness of far-infrared negative-ion coating.
Six ring stones integrate multiple kinds of energy, can discharge the far infrared of anion and 8-15 μm.Anion in air
Be conducive to the conveying of human body blood oxygen, absorb and utilize, promotes human metabolism, improve the immunity of the human body；Far infrared can cause people
The human body and molecular resonance of body cell accelerate blood circulation, to activate histocyte, body immune system.The present invention
It is middle to be modified six ring stones, it is metal oxide-loaded in six ring stones, further promote the release of anion and far infrared,
To make the coating of preparation that there is significant health-care efficacy.
Tourmaline has the characteristic permanently discharged, and can discharge the electric current of 0.06mA, promote blood circulation, and it is living to improve cell
Power, can also be release far infrared and anion, the anion discharged can neutralize the cation released by radiation,
Electromagnetic wave propagation is resisted, thus has the function of significantly being electromagnetically shielded.
Diatomite is added in coating, can improve the wearability of film, while also having purification air, removes in environment
Formaldehyde energy harmful substance.
The present invention boosts metabolism, improves the pyramid craftwork of cell viability, and the handicraft surface is coated with golden word
Interior is carried or be put in the craftwork by tower process product far-infrared negative-ion coating, can be released effectively anion and
Far infrared improves the immunity of the human body to accelerate blood circulation, promote human metabolism, activation histocyte.The technique
Also there is certain anti-radiation effect, radiation of the electronic equipment to human body can be reduced.
Specific embodiment
Below with reference to specific embodiment, the present invention is further explained.It should be appreciated, however, that these embodiments are only used for
It is bright the present invention and be not meant to limit the scope of the invention.The test method of actual conditions is not specified in the following example, usually
According to normal conditions, or according to the normal condition proposed by manufacturer.
Levelling agent is Silicone modified acryl's ester levelling agent, specific using application No. is the inventions of 201510515339.X
The method of embodiment 1 is prepared in patent.
Polyurethane resin, referring to application No. is in 201410852824 patent of invention the step of embodiment 1 (1) method
It is prepared.
Dispersing agent, using German Bi Ke dispersant B YK-163.
Six ring stones are bought from hundred Feng Kuangchanpinjiagongchang of Lingshou County, granularity: 2000 mesh.
Diatomite is bought from hundred Feng Kuangchanpinjiagongchang of Lingshou County, granularity: 2000 mesh.
Tourmaline buys the crystal tourmaline from mineral products processing factory, Lingshou County Hengchang, granularity: 2000 mesh.
Cobalt titanate, referring to application No. is the methods of embodiment 6 in 201710110262.7 patent of invention to be prepared.
Cadmium ferrite, referring to application No. is the methods of embodiment 1 in 201110239123.7 patent of invention to be prepared.
No. 200 solvent naphthas are bought from this Science and Technology Ltd. of Wuhan Kano.
Cerous sulfate, uses four cerium sulfate hydrates in embodiment, and purchase is from cruel scientific and technological (Beijing) Co., Ltd of your chemistry.
Titanium sulfate is bought from Shanghai Mike's woods biochemical technology Co., Ltd.
Titanate coupling agent TC114, the production of Tiancheng Chemical Co., Ltd., Tianzhang City.
Embodiment 1
A kind of pyramid craftwork for boosting metabolism, improving cell viability, including tower body, the outer surface of the tower body
Pyramid craftwork far-infrared negative-ion coating, the painting of pyramid craftwork far-infrared negative-ion coating are uniformly sprayed
Layer is with a thickness of 0.1mm.
The tower body material is stainless steel.
The tower body is conventional Pyramid, and inside is cavity, the high 80cm of tower body, tower body bottom side length 120cm, tower body thickness
Spend 1.5cm.
The pyramid craftwork is with far-infrared negative-ion coating raw material (parts by weight): 70 parts of polyurethane resin is modified six
5 parts of ring stone, 1.5 parts of modification infusorial earth, 1.5 parts of modified verdelite, 0.2 part of levelling agent, 0.2 part of dispersing agent, anti skinning agent 0.2
Part, 0.8 part of drier, 40 parts of solvent naphtha.
The drier is zinc Isoocatanoate.
The anti skinning agent is methyl ethyl ketoxime.
The levelling agent is Silicone modified acryl's ester levelling agent.
The solvent naphtha is No. 200 solvent naphthas.
The six ring stone of modification is prepared using following methods: by titanate coupling agent TC114 0.6g solvent naphtha
After 10g dilution, dilution is obtained, six ring stone of 30g is added in 100mL ethyl alcohol, stirred 15 minutes at 75 DEG C with 200 revs/min,
Dilution is added, is stirred 80 minutes at 75 DEG C with 200 revs/min, is centrifuged 15 minutes with 6000 revs/min, lower sediment is dry at 95 DEG C
Dry 8 hours, obtain modified six ring stones.
The modification infusorial earth is prepared using following methods: after TC114 0.6g is diluted with solvent naphtha 10g, being obtained
30g diatomite is added in 100mL ethyl alcohol by dilution, is stirred 15 minutes at 75 DEG C with 200 revs/min, dilution is added,
75 DEG C are stirred 80 minutes with 200 revs/min, are centrifuged 15 minutes with 6000 revs/min, and lower sediment is 8 hours dry at 95 DEG C, are changed
Property diatomite.
The modified verdelite is prepared using following methods: after TC114 0.6g is diluted with solvent naphtha 10g, being obtained
30g tourmaline is added in 100mL ethyl alcohol by dilution, is stirred 15 minutes at 75 DEG C with 200 revs/min, dilution is added,
75 DEG C are stirred 80 minutes with 200 revs/min, are centrifuged 15 minutes with 6000 revs/min, and lower sediment is 8 hours dry at 95 DEG C, are changed
Property tourmaline.
The solvent naphtha is No. 200 solvent naphthas.
The pyramid craftwork is prepared with far-infrared negative-ion coating using following methods: by polyurethane resin,
Modified six ring stones, modification infusorial earth, modified verdelite, levelling agent, dispersing agent, anti skinning agent, drier, solvent naphtha mixing, with
500 revs/min stirring 15 minutes to get.
Embodiment 2
Substantially the same manner as Example 1, difference is only that:
The pyramid craftwork is with far-infrared negative-ion coating raw material (parts by weight): 70 parts of polyurethane resin is modified six
5 parts of ring stone, 1.5 parts of modification infusorial earth, 1.5 parts of modified verdelite, 0.2 part of levelling agent, 0.2 part of dispersing agent, anti skinning agent 0.2
Part, 0.8 part of drier, 40 parts of solvent naphtha.
The drier is zinc Isoocatanoate.
The anti skinning agent is methyl ethyl ketoxime.
The levelling agent is Silicone modified acryl's ester levelling agent.
The solvent naphtha is No. 200 solvent naphthas.
The six ring stone of modification is prepared using following methods:
(1) six ring stone 30g are added in 100mL water, are stirred 15 minutes with 200 revs/min, obtains six ring stone dispersion liquids；
(2) cerous sulfate 20.2g (0.05mol) is added in 100mL water, is stirred 20 minutes with 200 revs/min, obtains sulphur
Sour cerium solution；
(3) titanium sulfate 24g (0.1mol) is added in 100mL water, is stirred after twenty minutes, is used with 200 revs/min at 92 DEG C
It is 8.5 that 10wt% sodium hydroxide, which adjusts pH, and six ring stone dispersion liquids are added, and is stirred 10 minutes, is added with 200 revs/min at 92 DEG C
Cerous sulfate solution, 92 DEG C are stirred 3 hours with 200 revs/min, are centrifuged 15 minutes with 6000 revs/min, are washed with water in lower sediment
Washing lotion pH is neutrality, 3 hours dry at 95 DEG C, then keeps the temperature 2 hours at 400 DEG C, obtains six metal oxide-loaded ring stones；
(4) after diluting titanate coupling agent TC114 0.6g with solvent naphtha 10g, dilution is obtained, by 30g carried metal
Six ring stones of oxide are added in 100mL ethyl alcohol, are stirred 15 minutes at 75 DEG C with 200 revs/min, dilution are added, at 75 DEG C
It is stirred 80 minutes with 200 revs/min, is centrifuged 15 minutes with 6000 revs/min, lower sediment is 8 hours dry at 95 DEG C, obtains modified six
Ring stone.
The modification infusorial earth is prepared using following methods: after TC114 0.6g is diluted with solvent naphtha 10g, being obtained
30g diatomite is added in 100mL ethyl alcohol by dilution, is stirred 15 minutes at 75 DEG C with 200 revs/min, dilution is added,
75 DEG C are stirred 80 minutes with 200 revs/min, are centrifuged 15 minutes with 6000 revs/min, and lower sediment is 8 hours dry at 95 DEG C, are changed
Property diatomite.
The modified verdelite is prepared using following methods: after TC114 0.6g is diluted with solvent naphtha 10g, being obtained
30g tourmaline is added in 100mL ethyl alcohol by dilution, is stirred 15 minutes at 75 DEG C with 200 revs/min, dilution is added,
75 DEG C are stirred 80 minutes with 200 revs/min, are centrifuged 15 minutes with 6000 revs/min, and lower sediment is 8 hours dry at 95 DEG C, are changed
Property tourmaline.
The solvent naphtha is No. 200 solvent naphthas.
The pyramid craftwork is prepared with far-infrared negative-ion coating using following methods: by polyurethane resin,
Modified six ring stones, modification infusorial earth, modified verdelite, levelling agent, dispersing agent, anti skinning agent, drier, solvent naphtha mixing, with
500 revs/min stirring 15 minutes to get.
Embodiment 3
Substantially the same manner as Example 1, difference is only that:
The pyramid craftwork is with far-infrared negative-ion coating raw material (parts by weight): 70 parts of polyurethane resin is modified six
5 parts of ring stone, 1.5 parts of modification infusorial earth, 1.5 parts of modified verdelite, 0.2 part of levelling agent, 0.2 part of dispersing agent, anti skinning agent 0.2
Part, 0.8 part of drier, 40 parts of solvent naphtha.
The drier is zinc Isoocatanoate.
The anti skinning agent is methyl ethyl ketoxime.
The levelling agent is Silicone modified acryl's ester levelling agent.
The solvent naphtha is No. 200 solvent naphthas.
The six ring stone of modification is prepared using following methods:
(1) six ring stone 30g are added in 100mL water, are stirred 15 minutes with 200 revs/min, obtains six ring stone dispersion liquids；
(2) titanium sulfate 26g (0.15mol) is added in 100mL water, is stirred after twenty minutes at 92 DEG C with 200 revs/min,
Adjusting pH with 10wt% sodium hydroxide is 8.5, and six ring stone dispersion liquids are added, and 92 DEG C are stirred 3 hours with 200 revs/min, with 6000
Revs/min centrifugation 15 minutes, it is washed with water to washing lotion pH in lower sediment as neutrality, it is 3 hours dry at 95 DEG C, then protected at 400 DEG C
Temperature 2 hours, obtains six metal oxide-loaded ring stones；
(3) after diluting titanate coupling agent TC114 0.6g with solvent naphtha 10g, dilution is obtained, by 30g carried metal
Six ring stones of oxide are added in 100mL ethyl alcohol, are stirred 15 minutes at 75 DEG C with 200 revs/min, dilution are added, at 75 DEG C
It is stirred 80 minutes with 200 revs/min, is centrifuged 15 minutes with 6000 revs/min, lower sediment is 8 hours dry at 95 DEG C, obtains modified six
Ring stone.
The modification infusorial earth is prepared using following methods: after TC114 0.6g is diluted with solvent naphtha 10g, being obtained
30g diatomite is added in 100mL ethyl alcohol by dilution, is stirred 15 minutes at 75 DEG C with 200 revs/min, dilution is added,
75 DEG C are stirred 80 minutes with 200 revs/min, are centrifuged 15 minutes with 6000 revs/min, and lower sediment is 8 hours dry at 95 DEG C, are changed
Property diatomite.
The modified verdelite is prepared using following methods: after TC114 0.6g is diluted with solvent naphtha 10g, being obtained
30g tourmaline is added in 100mL ethyl alcohol by dilution, is stirred 15 minutes at 75 DEG C with 200 revs/min, dilution is added,
75 DEG C are stirred 80 minutes with 200 revs/min, are centrifuged 15 minutes with 6000 revs/min, and lower sediment is 8 hours dry at 95 DEG C, are changed
Property tourmaline.
The solvent naphtha is No. 200 solvent naphthas.
The pyramid craftwork is prepared with far-infrared negative-ion coating using following methods: by polyurethane resin,
Modified six ring stones, modification infusorial earth, modified verdelite, levelling agent, dispersing agent, anti skinning agent, drier, solvent naphtha mixing, with
500 revs/min stirring 15 minutes to get.
Embodiment 4
Substantially the same manner as Example 1, difference is only that:
The pyramid craftwork is with far-infrared negative-ion coating raw material (parts by weight): 70 parts of polyurethane resin is modified six
5 parts of ring stone, 1.5 parts of modification infusorial earth, 1.5 parts of modified verdelite, 0.2 part of levelling agent, 0.2 part of dispersing agent, anti skinning agent 0.2
Part, 0.8 part of drier, 40 parts of solvent naphtha.
The drier is zinc Isoocatanoate.
The anti skinning agent is methyl ethyl ketoxime.
The levelling agent is Silicone modified acryl's ester levelling agent.
The solvent naphtha is No. 200 solvent naphthas.
The six ring stone of modification is prepared using following methods:
(1) six ring stone 30g are added in 100mL water, are stirred 15 minutes with 200 revs/min, obtains six ring stone dispersion liquids；
(2) cerous sulfate 60.6g (0.05mol) is added in 100mL water, is stirred 20 minutes with 200 revs/min, used
It is 8.5 that 10wt% sodium hydroxide, which adjusts pH, and six ring stone dispersion liquids are added, and is stirred 3 hours at 92 DEG C with 200 revs/min, with 6000
Revs/min centrifugation 15 minutes, it is washed with water to washing lotion pH in lower sediment as neutrality, it is 3 hours dry at 95 DEG C, then protected at 400 DEG C
Temperature 2 hours, obtains six metal oxide-loaded ring stones；
(3) after diluting titanate coupling agent TC114 0.6g with solvent naphtha 10g, dilution is obtained, by 30g carried metal
Six ring stones of oxide are added in 100mL ethyl alcohol, are stirred 15 minutes at 75 DEG C with 200 revs/min, dilution are added, at 75 DEG C
It is stirred 80 minutes with 200 revs/min, is centrifuged 15 minutes with 6000 revs/min, lower sediment is 8 hours dry at 95 DEG C, obtains modified six
Ring stone.
The modification infusorial earth is prepared using following methods: after TC114 0.6g is diluted with solvent naphtha 10g, being obtained
30g diatomite is added in 100mL ethyl alcohol by dilution, is stirred 15 minutes at 75 DEG C with 200 revs/min, dilution is added,
75 DEG C are stirred 80 minutes with 200 revs/min, are centrifuged 15 minutes with 6000 revs/min, and lower sediment is 8 hours dry at 95 DEG C, are changed
Property diatomite.
The modified verdelite is prepared using following methods: after TC114 0.6g is diluted with solvent naphtha 10g, being obtained
30g tourmaline is added in 100mL ethyl alcohol by dilution, is stirred 15 minutes at 75 DEG C with 200 revs/min, dilution is added,
75 DEG C are stirred 80 minutes with 200 revs/min, are centrifuged 15 minutes with 6000 revs/min, and lower sediment is 8 hours dry at 95 DEG C, are changed
Property tourmaline.
The solvent naphtha is No. 200 solvent naphthas.
The pyramid craftwork is prepared with far-infrared negative-ion coating using following methods: by polyurethane resin,
Modified six ring stones, modification infusorial earth, modified verdelite, levelling agent, dispersing agent, anti skinning agent, drier, solvent naphtha mixing, with
500 revs/min stirring 15 minutes to get.
Embodiment 5
Substantially the same manner as Example 1, difference is only that:
The pyramid craftwork is with far-infrared negative-ion coating raw material (parts by weight): 70 parts of polyurethane resin is modified six
5 parts of ring stone, 1.5 parts of modification infusorial earth, 1.5 parts of modified verdelite, 0.2 part of levelling agent, 0.2 part of dispersing agent, anti skinning agent 0.2
Part, 0.8 part of drier, 0.8 part of functional additive, 40 parts of solvent naphtha.
The functional additive is cobalt titanate.
The drier is zinc Isoocatanoate.
The anti skinning agent is methyl ethyl ketoxime.
The levelling agent is Silicone modified acryl's ester levelling agent.
The solvent naphtha is No. 200 solvent naphthas.
The six ring stone of modification is prepared using following methods:
(1) six ring stone 30g are added in 100mL water, are stirred 15 minutes with 200 revs/min, obtains six ring stone dispersion liquids；
(2) cerous sulfate 20.2g (0.05mol) is added in 100mL water, is stirred 20 minutes with 200 revs/min, obtains sulphur
Sour cerium solution；
(3) titanium sulfate 24g (0.1mol) is added in 100mL water, is stirred after twenty minutes, is used with 200 revs/min at 92 DEG C
It is 8.5 that 10wt% sodium hydroxide, which adjusts pH, and six ring stone dispersion liquids are added, and is stirred 10 minutes, is added with 200 revs/min at 92 DEG C
Cerous sulfate solution, 92 DEG C are stirred 3 hours with 200 revs/min, are centrifuged 15 minutes with 6000 revs/min, are washed with water in lower sediment
Washing lotion pH is neutrality, 3 hours dry at 95 DEG C, then keeps the temperature 2 hours at 400 DEG C, obtains six metal oxide-loaded ring stones；
(4) after diluting titanate coupling agent TC114 0.6g with solvent naphtha 10g, dilution is obtained, by 30g carried metal
Six ring stones of oxide are added in 100mL ethyl alcohol, are stirred 15 minutes at 75 DEG C with 200 revs/min, dilution are added, at 75 DEG C
It is stirred 80 minutes with 200 revs/min, is centrifuged 15 minutes with 6000 revs/min, lower sediment is 8 hours dry at 95 DEG C, obtains modified six
Ring stone.
The modification infusorial earth is prepared using following methods: after TC114 0.6g is diluted with solvent naphtha 10g, being obtained
30g diatomite is added in 100mL ethyl alcohol by dilution, is stirred 15 minutes at 75 DEG C with 200 revs/min, dilution is added,
75 DEG C are stirred 80 minutes with 200 revs/min, are centrifuged 15 minutes with 6000 revs/min, and lower sediment is 8 hours dry at 95 DEG C, are changed
Property diatomite.
The modified verdelite is prepared using following methods: after TC114 0.6g is diluted with solvent naphtha 10g, being obtained
30g tourmaline is added in 100mL ethyl alcohol by dilution, is stirred 15 minutes at 75 DEG C with 200 revs/min, dilution is added,
75 DEG C are stirred 80 minutes with 200 revs/min, are centrifuged 15 minutes with 6000 revs/min, and lower sediment is 8 hours dry at 95 DEG C, are changed
Property tourmaline.
The solvent naphtha is No. 200 solvent naphthas.
The pyramid craftwork is prepared with far-infrared negative-ion coating using following methods: by polyurethane resin,
It is modified six ring stones, modification infusorial earth, modified verdelite, levelling agent, dispersing agent, anti skinning agent, drier, functional additive, molten
Agent oil mixing, with 500 revs/min stir 15 minutes to get.
Embodiment 6
Substantially the same manner as Example 1, difference is only that:
The pyramid craftwork is with far-infrared negative-ion coating raw material (parts by weight): 70 parts of polyurethane resin is modified six
5 parts of ring stone, 1.5 parts of modification infusorial earth, 1.5 parts of modified verdelite, 0.2 part of levelling agent, 0.2 part of dispersing agent, anti skinning agent 0.2
Part, 0.8 part of drier, 0.8 part of functional additive, 40 parts of solvent naphtha.
The functional additive is cadmium ferrite.
The drier is zinc Isoocatanoate.
The anti skinning agent is methyl ethyl ketoxime.
The levelling agent is Silicone modified acryl's ester levelling agent.
The solvent naphtha is No. 200 solvent naphthas.
The six ring stone of modification is prepared using following methods:
(1) six ring stone 30g are added in 100mL water, are stirred 15 minutes with 200 revs/min, obtains six ring stone dispersion liquids；
(2) cerous sulfate 20.2g (0.05mol) is added in 100mL water, is stirred 20 minutes with 200 revs/min, obtains sulphur
Sour cerium solution；
(3) titanium sulfate 24g (0.1mol) is added in 100mL water, is stirred after twenty minutes, is used with 200 revs/min at 92 DEG C
It is 8.5 that 10wt% sodium hydroxide, which adjusts pH, and six ring stone dispersion liquids are added, and is stirred 10 minutes, is added with 200 revs/min at 92 DEG C
Cerous sulfate solution, 92 DEG C are stirred 3 hours with 200 revs/min, are centrifuged 15 minutes with 6000 revs/min, are washed with water in lower sediment
Washing lotion pH is neutrality, 3 hours dry at 95 DEG C, then keeps the temperature 2 hours at 400 DEG C, obtains six metal oxide-loaded ring stones；
(4) after diluting titanate coupling agent TC114 0.6g with solvent naphtha 10g, dilution is obtained, by 30g carried metal
Six ring stones of oxide are added in 100mL ethyl alcohol, are stirred 15 minutes at 75 DEG C with 200 revs/min, dilution are added, at 75 DEG C
It is stirred 80 minutes with 200 revs/min, is centrifuged 15 minutes with 6000 revs/min, lower sediment is 8 hours dry at 95 DEG C, obtains modified six
Ring stone.
The modification infusorial earth is prepared using following methods: after TC114 0.6g is diluted with solvent naphtha 10g, being obtained
30g diatomite is added in 100mL ethyl alcohol by dilution, is stirred 15 minutes at 75 DEG C with 200 revs/min, dilution is added,
75 DEG C are stirred 80 minutes with 200 revs/min, are centrifuged 15 minutes with 6000 revs/min, and lower sediment is 8 hours dry at 95 DEG C, are changed
Property diatomite.
The modified verdelite is prepared using following methods: after TC114 0.6g is diluted with solvent naphtha 10g, being obtained
30g tourmaline is added in 100mL ethyl alcohol by dilution, is stirred 15 minutes at 75 DEG C with 200 revs/min, dilution is added,
75 DEG C are stirred 80 minutes with 200 revs/min, are centrifuged 15 minutes with 6000 revs/min, and lower sediment is 8 hours dry at 95 DEG C, are changed
Property tourmaline.
The solvent naphtha is No. 200 solvent naphthas.
The pyramid craftwork is prepared with far-infrared negative-ion coating using following methods: by polyurethane resin,
It is modified six ring stones, modification infusorial earth, modified verdelite, levelling agent, dispersing agent, anti skinning agent, drier, functional additive, molten
Agent oil mixing, with 500 revs/min stir 15 minutes to get.
Embodiment 7
Substantially the same manner as Example 1, difference is only that:
The pyramid craftwork is with far-infrared negative-ion coating raw material (parts by weight): 70 parts of polyurethane resin is modified six
5 parts of ring stone, 1.5 parts of modification infusorial earth, 1.5 parts of modified verdelite, 0.2 part of levelling agent, 0.2 part of dispersing agent, anti skinning agent 0.2
Part, 0.8 part of drier, 0.8 part of functional additive, 40 parts of solvent naphtha.
The functional additive is the mixture of cobalt titanate and cadmium ferrite, wherein the mass ratio of the cobalt titanate and cadmium ferrite
For 1:3.
The drier is zinc Isoocatanoate.
The anti skinning agent is methyl ethyl ketoxime.
The levelling agent is Silicone modified acryl's ester levelling agent.
The solvent naphtha is No. 200 solvent naphthas.
The six ring stone of modification is prepared using following methods:
(1) six ring stone 30g are added in 100mL water, are stirred 15 minutes with 200 revs/min, obtains six ring stone dispersion liquids；
(2) cerous sulfate 20.2g (0.05mol) is added in 100mL water, is stirred 20 minutes with 200 revs/min, obtains sulphur
Sour cerium solution；
(3) titanium sulfate 24g (0.1mol) is added in 100mL water, is stirred after twenty minutes, is used with 200 revs/min at 92 DEG C
It is 8.5 that 10wt% sodium hydroxide, which adjusts pH, and six ring stone dispersion liquids are added, and is stirred 10 minutes, is added with 200 revs/min at 92 DEG C
Cerous sulfate solution, 92 DEG C are stirred 3 hours with 200 revs/min, are centrifuged 15 minutes with 6000 revs/min, are washed with water in lower sediment
Washing lotion pH is neutrality, 3 hours dry at 95 DEG C, then keeps the temperature 2 hours at 400 DEG C, obtains six metal oxide-loaded ring stones；
(4) after diluting titanate coupling agent TC114 0.6g with solvent naphtha 10g, dilution is obtained, by 30g carried metal
Six ring stones of oxide are added in 100mL ethyl alcohol, are stirred 15 minutes at 75 DEG C with 200 revs/min, dilution are added, at 75 DEG C
It is stirred 80 minutes with 200 revs/min, is centrifuged 15 minutes with 6000 revs/min, lower sediment is 8 hours dry at 95 DEG C, obtains modified six
Ring stone.
The modification infusorial earth is prepared using following methods: after TC114 0.6g is diluted with solvent naphtha 10g, being obtained
30g diatomite is added in 100mL ethyl alcohol by dilution, is stirred 15 minutes at 75 DEG C with 200 revs/min, dilution is added,
75 DEG C are stirred 80 minutes with 200 revs/min, are centrifuged 15 minutes with 6000 revs/min, and lower sediment is 8 hours dry at 95 DEG C, are changed
Property diatomite.
The modified verdelite is prepared using following methods: after TC114 0.6g is diluted with solvent naphtha 10g, being obtained
30g tourmaline is added in 100mL ethyl alcohol by dilution, is stirred 15 minutes at 75 DEG C with 200 revs/min, dilution is added,
75 DEG C are stirred 80 minutes with 200 revs/min, are centrifuged 15 minutes with 6000 revs/min, and lower sediment is 8 hours dry at 95 DEG C, are changed
Property tourmaline.
The solvent naphtha is No. 200 solvent naphthas.
The pyramid craftwork is prepared with far-infrared negative-ion coating using following methods: by polyurethane resin,
It is modified six ring stones, modification infusorial earth, modified verdelite, levelling agent, dispersing agent, anti skinning agent, drier, functional additive, molten
Agent oil mixing, with 500 revs/min stir 15 minutes to get.
Test case 1
The pyramid craftwork that embodiment obtains is tested with the Negative ion disengagement of far-infrared negative-ion coating
Tested: it is 200mm × 200mm × 0.5mm sample that size, which is made, in 304 stainless steels, pyramid craftwork is used remote red
Outer negative ion paint is coated on six surfaces of sample, coating layer thickness 0.1mm, obtains test raw material；Take one piece of test former
Material is placed on 0.1m3Seal box in, 25 DEG C of experimental temperature, relative humidity 40%, closed 1 hour, with U.S. Alphalab
The AIC-1000 anionic textiles instrument of company's production detects anion-generating capacity, and test result is shown in Table 1.
1 anion releasing effect test result table of table
| Anion discharges number, a/cm3 | |
| Embodiment 1 | 647 |
| Embodiment 2 | 976 |
| Embodiment 3 | 812 |
| Embodiment 4 | 754 |
| Embodiment 5 | 1245 |
| Embodiment 6 | 1304 |
| Embodiment 7 | 1663 |
Test case 2
The far infrared transmission performance for the pyramid craftwork far-infrared negative-ion coating that embodiment obtains is tested:
It is 200mm × 200mm × 0.5mm sample that size, which is made, in 304 stainless steels, and pyramid craftwork is applied with far-infrared negative-ion
Material is coated in six surfaces of sample, coating weight 150g/m2, obtain test raw material.Raw material at 25 DEG C of specific test
Normal direction Vertical Launch rate, test scope are 4-14 μm, and test result is shown in Table 2.
2 far infrared transmission the performance test results table of table
| Normal direction total radiation emissivity | |
| Embodiment 1 | 0.826 |
| Embodiment 2 | 0.892 |
| Embodiment 3 | 0.847 |
| Embodiment 4 | 0.841 |
| Embodiment 5 | 0.914 |
| Embodiment 6 | 0.920 |
| Embodiment 7 | 0.946 |
Test case 3
Test can be carried out with the anti-radiation performance of far-infrared negative-ion coating to the pyramid craftwork that embodiment obtains: will
It is 200mm × 200mm × 0.5mm sample that size, which is made, in 304 stainless steels, by pyramid craftwork far-infrared negative-ion coating
It is coated on six surfaces of sample, coating weight 150g/m2, test raw material are obtained, using HP-8720B Network Analyzer in nothing
It is required in echo darkroom according to national standard GJB2038-1994, using the absorbing property of arched reflective method test raw material.Test frequency
Section is 2-18GHz, and test result is shown in Table 3.
3 shielding property test result table of table
| Maximum absorption peak, dB | |
| Embodiment 2 | -11.316 |
| Embodiment 5 | -12.015 |
| Embodiment 6 | -12.673 |
| Embodiment 7 | -13.845 |
Claims (9)
1. a kind of pyramid craftwork far-infrared negative-ion coating, which is characterized in that by the raw material preparation of following weight parts
At: 65-75 parts of polyurethane resin, modified 3-8 parts of six ring stone, 1-2 parts of modification infusorial earth, 1-2 parts of modified verdelite, levelling agent
0.1-0.5 parts, 0.1-0.5 parts of dispersing agent, 0.1-0.5 parts of anti skinning agent, 0.5-1 parts of drier, 0.5-1 parts of functional additive,
35-45 parts of solvent naphtha.
2. pyramid craftwork far-infrared negative-ion coating as described in claim 1, which is characterized in that the functional additive
For cobalt titanate and/or cadmium ferrite.
3. pyramid craftwork far-infrared negative-ion coating as described in claim 1, which is characterized in that the drier is different
At least one of zinc octoate, cobalt iso-octoate；The anti skinning agent is methyl ethyl ketoxime；The levelling agent is silicone-modified propylene
Acid esters levelling agent；The solvent naphtha is No. 200 solvent naphthas.
4. pyramid craftwork far-infrared negative-ion coating as described in claim 1, which is characterized in that the six ring stone of modification
It is prepared using following methods:
(1) six ring stone 25-35g are added in 90-110mL water, stir 10-20 minutes, obtains six ring stone dispersion liquids；
(2) cerous sulfate 0.01-1mol is added in 90-110mL water, stirs 20-30 minutes, obtains cerous sulfate solution；
(3) titanium sulfate 0.05-0.15mol is added in 90-110mL water, after stirring 20-30 minutes, uses 8- at 90-95 DEG C
12wt% sodium hydroxide adjust pH be 8-9, be added six ring stone dispersion liquids, 90-95 DEG C stirring 8-12 minutes, add cerous sulfate
Solution, 90-95 DEG C stirring 2-4 hours, be centrifuged 10-20 minute, lower sediment be washed with water to washing lotion pH be it is neutral, in 90-
100 DEG C are 2-4 hours dry, then 300-500 DEG C heat preservation 1-3 hours, obtain six metal oxide-loaded ring stones；
(4) after diluting titanate coupling agent TC114 0.5-1g with solvent naphtha 8-12g, dilution is obtained, 25-35g is loaded
Six ring stones of metal oxide are added in 90-110mL ethyl alcohol, 70-80 DEG C stirring 10-20 minutes, be added dilution,
70-80 DEG C stirring 60-90 minutes, be centrifuged 10-20 minute, lower sediment is 6-10 hours dry at 90-100 DEG C, obtain modification six
Ring stone.
5. pyramid craftwork far-infrared negative-ion coating as described in claim 1, which is characterized in that the modification infusorial earth
It is prepared using following methods: after titanate coupling agent TC114 0.5-1g is diluted with solvent naphtha 8-12g, being diluted
25-35g diatomite is added in 90-110mL ethyl alcohol by liquid, 70-80 DEG C stirring 10-20 minutes, be added dilution, in 70-
80 DEG C stirring 60-90 minutes, be centrifuged 10-20 minute, lower sediment is 6-10 hours dry at 90-100 DEG C, obtain be modified diatom
Soil.
6. pyramid craftwork far-infrared negative-ion coating as described in claim 1, which is characterized in that use following methods system
It is standby to obtain: by polyurethane resin, modified six ring stones, modification infusorial earth, modified verdelite, levelling agent, dispersing agent, anti skinning agent,
Drier, functional additive, solvent naphtha mixing, with 400-800 revs/min of stirring 10-20 minutes to get.
7. a kind of pyramid craftwork for boosting metabolism, improving cell viability, which is characterized in that including tower body, the tower
The outer surface of body, which is uniformly brushed, has the right to require the described in any item pyramid craftwork far-infrared negative-ion coating of 1-6.
8. the pyramid craftwork for the cell viability that boosts metabolism, improves as claimed in claim 7, which is characterized in that described
Any one of tower body material in iron, stainless steel, titanium, magnetite, metal alloy.
9. the pyramid craftwork for the cell viability that boosts metabolism, improves as claimed in claim 7, which is characterized in that described
Pyramid craftwork is 0.02-0.2mm with the coating layer thickness of far-infrared negative-ion coating.
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