CN110102580A - It is a kind of for processing the 1100-H14 state aluminium alloy band production method of high-end bottle lid of cosmetics - Google Patents

It is a kind of for processing the 1100-H14 state aluminium alloy band production method of high-end bottle lid of cosmetics Download PDF

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CN110102580A
CN110102580A CN201910292736.3A CN201910292736A CN110102580A CN 110102580 A CN110102580 A CN 110102580A CN 201910292736 A CN201910292736 A CN 201910292736A CN 110102580 A CN110102580 A CN 110102580A
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aluminium alloy
temperature
rolling
production method
bottle lid
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CN110102580B (en
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宋喜波
柴明科
李克振
李坤朋
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Henan Mingsheng New Material Technology Co.,Ltd.
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ZHENGZHOU MINGTAI ENGINEERING Co Ltd
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21BROLLING OF METAL
    • B21B15/00Arrangements for performing additional metal-working operations specially combined with or arranged in, or specially adapted for use in connection with, metal-rolling mills
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21BROLLING OF METAL
    • B21B37/00Control devices or methods specially adapted for metal-rolling mills or the work produced thereby
    • B21B37/28Control of flatness or profile during rolling of strip, sheets or plates
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21BROLLING OF METAL
    • B21B37/00Control devices or methods specially adapted for metal-rolling mills or the work produced thereby
    • B21B37/28Control of flatness or profile during rolling of strip, sheets or plates
    • B21B37/44Control of flatness or profile during rolling of strip, sheets or plates using heating, lubricating or water-spray cooling of the product
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C21/00Alloys based on aluminium
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22FCHANGING THE PHYSICAL STRUCTURE OF NON-FERROUS METALS AND NON-FERROUS ALLOYS
    • C22F1/00Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working
    • C22F1/04Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working of aluminium or alloys based thereon
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21BROLLING OF METAL
    • B21B15/00Arrangements for performing additional metal-working operations specially combined with or arranged in, or specially adapted for use in connection with, metal-rolling mills
    • B21B2015/0064Uncoiling the rolled product

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  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Cosmetics (AREA)
  • Metal Rolling (AREA)

Abstract

The invention belongs to aluminum alloy processing technology fields, disclose a kind of for processing the 1100-H14 state aluminium alloy band production method of high-end bottle lid of cosmetics, comprising the following steps: melting, using semi-continuous process ingot casting, homogenization heat treatment, cutting head, back-end crop mill face, hot rolling, once cold rolling, an intermediate annealing, secondary cold-rolling, secondary intermediate annealing, it is cold-rolled to 0.7mm finished product thickness below three times, cleans, straightening.The present invention is by optimizing hot rolling and cold-rolling process, balance heat treating regime and the deformed rolling texture of final cold rolling and annealing texture, make mill product thickness in 1mm or less, the earing rate after material punching is reduced simultaneously, it ensure that high surface characteristic of the material after anodic oxidation and coloring, uniform color is consistent after oxidation and coloring, and appearance metal-like is strong, is satisfied with the requirement of high-end cosmetic cap material substrate.

Description

A kind of 1100-H14 state aluminium alloy band for processing high-end bottle lid of cosmetics is raw Production method
Technical field
The invention belongs to aluminum alloy processing technology fields, and in particular to a kind of for processing high-end bottle lid of cosmetics 1100-H14 state aluminium alloy band production method.
Background technique
Aluminum alloy bottle cap material is widely used in bottle, can, medicine bottle, cosmetics as novel bottle cap joint filling material In the outer sealing packaging of lid, punch forming is mostly processed in the higher production line of the degree of automation, performance, ruler to material The requirements such as very little deviation, earing rate size are all very stringent, otherwise can generate rupture, folding line etc. and seriously affect and rush Gai Xiaoguo and become a useful person Rate.
With the increasingly raising of people's living standard, the production of cosmetics capping is more and more high-grade, in the market high-grade makeup Product bottle cap material is made from the japanning of traditional handicraft to be developed in terms of anodic oxidation, electrolytic coloring/dyeing.Because of bottle cap material Fine and close oxidation film layer is formed in aluminium surface after anodic oxidation, its corrosion resistance, wearability and decorative performance can be significantly changed;Electricity Appearance luster is abundant after solution coloring, and metal sense is strong, therefore current cosmetics of super quality bottle cap, high-grade IT product shell are all made of anode Oxidation after stain or dyeing are decorative to improve its.
The requirement of cosmetics of super quality bottle cap material Surface Quality has nearly reached the quality standard of " zero-fault ", i.e. material Surface is not allow for bright line, striped, black-white point etc defect.Aluminium and aluminium alloy anode oxide Shi Yaojing alkali cleaning and pickling, oxidation Substrate surface and superficial layer tiny defect can be exposed or be amplified in the process, and influence the mass effect of oxidized surface, such as surface Slight strip defect, viscous hurt point, mark etc. and will be appeared undoubtedly after anodic oxidation at secret note.Currently, doing the normal of bottle cap in the market See that aluminium alloy and state have: 8011-H14/H16 or 3003-H16 etc., but the cosmetics of super quality bottle made by both aluminium alloys The anodic oxidation effect of cover material is not satisfactory.
The aluminum alloy sheets and strips of traditional 1100-H14 production technology production, surface quality are unable to satisfy advanced oxidation appearance The surface demand of material, and aluminum alloy sheets and strips thickness is in 1.0mm or more.Authorization Notice No. is the invention of 103009010 B of CN Patent discloses a kind of 1100-H14 aluminum alloy sheets and strips and its production method, production procedure include: founding, sawing, milling face, Heating, hot rolling and cold rolling are cold-rolled to finished product thickness still in 1mm or more although improving hot rolling technology, and for processing height Can earing rate size when shelves bottle for cosmetics cover material, which meet the requirements, does not also know.
Summary of the invention
It should guarantee that there is good punching performance and lower earing rate the purpose of the present invention is to provide one kind, again Meet material has aesthetic surface, the 1100-H14 state aluminium alloy band for producing high-grade bottle lid of cosmetics after anodic oxidation Material production method.
To achieve the above object, the invention adopts the following technical scheme:
The present invention provide it is a kind of for processing the 1100-H14 state aluminium alloy band production method of high-end bottle lid of cosmetics, including Following steps:
Step a: melting, smelting temperature are 700 DEG C ~ 750 DEG C;Each composition quality percentage in the aluminium alloy of the melting are as follows: 0.05%≤Si≤0.15%、0.35%≤Fe≤0.55%、0.10%≤Cu≤0.20%、Mn≤0.02%、Mg≤0.05%、Ti≤ 0.04%, other impurities total≤0.05%, remaining is Al;
Step b: semi-continuous process ingot casting is used;
Step c: ingot casting carries out homogenization heat treatment in 600 ± 15 DEG C of 12 ~ 16h of heat preservation, and cutting head, back-end crop mill face;
Step d: being hot-rolled down to the hot rolling blank of 8.0mm or more, and finishing temperature is greater than 300 DEG C;
Step e: through 2 passes, once cold rolling is to a thickness of 3.5 ~ 4.5mm;
Step f: by blank heating to 200 ~ 220 DEG C and keep the temperature 4 ~ 5h carry out an oil removing, an intermediate annealing;It is described it is primary in Between annealing temperature be 360 ~ 450 DEG C, heat preservation 20 ~ for 24 hours;
Step g: through 2 ~ 4 passes, 38 ~ 42% processing capacity, secondary cold-rolling are reserved according to finished product thickness;
Step h: blank heating to 200 ~ 220 DEG C and is kept the temperature 4 ~ 5h and carries out secondary oil removing, secondary intermediate annealing;It is described it is secondary in Between annealing temperature be 320 ~ 360 DEG C, heat preservation 20 ~ for 24 hours;
Step i: through 1 ~ 2 passes, it is cold-rolled to 0.7mm finished product thickness below three times;
Step j: cleaning, straightening.
Preferably, the casting temperature of semi-continuous process ingot casting described in step b be 690 ~ 730 DEG C, casting speed be 50 ~ 65mm/min。
Preferably, hot rolling described in step d is that ingot casting is heated to 450 ~ 530 DEG C, keeps the temperature 3h or more, first hot roughing, after Hot finishing to 8.0mm or more hot rolling blank.
Preferably, lotion parameter in the hot roughing are as follows: concentration 4.0 ~ 6.0%, 45 ~ 60 DEG C of temperature, pH value 7.5 ~ 8.5, ash Divide and is less than 800PPm, 500 μ s/cm of conductivity <.
Preferably, lotion parameter in the hot finishing are as follows: concentration 7.0 ~ 8.0%, 45 ~ 65 DEG C of temperature, pH value 7.5 ~ 8.5, ash Divide and is less than 1000PPm, 800 μ s/cm of conductivity <.
Preferably, 400 ~ 500 revs/min of brush roll revolving speed in the hot finishing, play frequency is 20 ~ 30 beats/min, and throw-on pressure is 300~400N。
Preferably, the first passage uncoiling tension≤6N/mm2 in once cold rolling described in step e, per pass reduction ratio be 25 ~ 40%, gloss level of roll Ra are 0.3 ~ 0.4 μm.
Preferably, the first passage uncoiling tension≤8N/mm2 in secondary cold-rolling described in step g, per pass reduction ratio be 25 ~ 45%, gloss level of roll Ra are 0.18 ~ 0.22 μm.
Preferably, the first passage uncoiling tension≤16N/mm2 in cold rolling three times described in step i, per pass reduction ratio It is 20 ~ 25%, gloss level of roll Ra is 0.18 ~ 0.22 μm.
Preferably, uncoiling tension≤800N of straightening described in step j.
Compared with prior art, the beneficial effects of the present invention are:
The present invention passes through the content and Fe/Si ratio of tri- kinds of elements of strict control Fe, Si, Cu, and optimization homogenization heat treatment adds Hot temperature and soaking time, by improving hot rolling blank finishing temperature, to mitigate the anisotropy of hot rolling blank;Cold rolling part is logical It crosses and carries out intermediate annealing twice in certain thickness, balance heat treating regime and the deformed rolling texture of final cold rolling and annealing Texture makes mill product thickness in 1mm hereinafter, reducing the earing rate after material punching simultaneously, practical earing rate is up to 2.5% Below;The present invention ensure that high table of the material after anodic oxidation and coloring by optimizing to hot rolling and cold-rolling process Uniform color is consistent after face characteristic, oxidation and coloring, and appearance metal-like is strong, is satisfied with the use of high-end cosmetic cap material substrate It is required that.
The present invention further pass through control roll for hot-rolling glue aluminium situation so that roll for hot-rolling surface glue aluminum layer thickness and its Even property is effectively controlled;By improving hot rolling emulsion cleanliness, enhances emulsion lubrication ability, improve hot rolling blank surface matter Amount mitigates hot rolled coil putty remained on surface;It adjusts gloss level of roll in cold rolling, controls blank uncoiling tension and each passage tension Matching hurts point, wipes scuffing, presses through scratch to reduce cold rolled surface mass defect such as viscous;By the uncoiling for controlling straightening Power, reduces dust and foreign matter is attached on band, to greatly improve the surface matter of 1100-H14 state aluminium alloy band Amount, high surface requirements and earing rate requirement after ensure that high-end bottle lid of cosmetics material oxidation.
Specific embodiment
The following examples are intended to illustrate the invention, but is not used to limit the scope of protection of the present invention.Unless otherwise specified, real Apply the conventional means that technological means used in example is well known to those skilled in the art.Test method in following embodiments, such as It is conventional method without special instruction.
1+1 formula Hot Rolling Mill model 3300mm1+1 hot rolling line in the present invention is big by middle color science and technology and Beijing science and technology Learn common develop.
Embodiment one
It is a kind of for processing the 1100-H14 state aluminium alloy band production method of high-end bottle lid of cosmetics, comprising the following steps:
Step a: melting, smelting temperature are 700 DEG C, smelting time 5h;Each composition quality percentage in the aluminium alloy of the melting Number are as follows: Si:0.127%, Fe:0.393%, Cu:0.188%, Mn:0.0034%, Mg:0.00085%, Ti:0.027%, other impurities Total≤0.05%, remaining is Al.
Step b: using semi-continuous process ingot casting, and the casting temperature of semi-continuous process ingot casting is 715 DEG C, casting speed 55mm/ min。
Step c: ingot casting carries out homogenization heat treatment in 600 ± 15 DEG C of heat preservation 12h, and cutting head, back-end crop mill face.
Step d: being heated to 530 DEG C for ingot casting, keep the temperature 3h, and using 1+1 formula Hot Rolling Mill, first hot roughing, rolls through 17 passages System, by ingot casting roughing to a thickness of 35mm, the hot rolling blank of rear hot finishing to 9.0mm, finishing temperature is 313 DEG C;In hot roughing Lotion parameter are as follows: concentration 4.0%, temperature 45 C, pH value 7.5, ash content 800PPm, 500 μ s/cm of conductivity;Lotion is joined in hot finishing Number are as follows: concentration 7.0%, temperature 45 C, pH value 7.5, ash content 1000PPm, 800 μ s/cm of conductivity, are altered by 400 revs/min of brush roll revolving speed Dynamic frequency is 20 beats/min, throw-on pressure 300N.
Step e: through 2 passes, the first passage uncoiling tension 6N/mm2, gloss level of roll Ra is 0.3 μm, 40 DEG C of movements 2.2 ~ 2.4mm2/s of viscosity number, between 35 DEG C ~ 45 DEG C, cold rolling oil controls index of refraction and is greater than 90% ROLLING OIL Oil-temperature control, Once cold rolling is to a thickness of 4.0mm.
Step f: by blank heating to 200 ~ 220 DEG C and keep the temperature 4h carry out an oil removing, an intermediate annealing;It is primary intermediate Annealing temperature is 380 DEG C, keeps the temperature 20h.Natural cooling in feeding rack is put after coming out of the stove.
Step g: through 4 passes, the first passage uncoiling tension 16N/mm2, gloss level of roll Ra is 0.18 μm, 40 DEG C of fortune Kinetic viscosity 2.2 ~ 2.4mm2/s of value, between 35 DEG C ~ 45 DEG C, cold rolling oil control index of refraction is greater than ROLLING OIL Oil-temperature control 90%, secondary cold-rolling is to a thickness of 0.67mm.
Step h: blank heating to 200 ~ 220 DEG C and is kept the temperature 4h and carries out secondary oil removing, secondary intermediate annealing;Secondary centre Annealing temperature is 320 DEG C, keeps the temperature 20h.Natural cooling in feeding rack is put after coming out of the stove.
Step i: through 2 passes, the first passage uncoiling tension 16N/mm2, gloss level of roll Ra is 0.18 μm, 40 DEG C of fortune Kinetic viscosity 2.2 ~ 2.4mm2/s of value, between 35 DEG C ~ 50 DEG C, cold rolling oil control index of refraction is greater than ROLLING OIL Oil-temperature control 90%, it is cold-rolled to finished product thickness 0.4mm three times.
Step j: cleaning, straightening, uncoiling tension≤800N of straightening, elongation control is 0.3%.
Embodiment two
It is a kind of for processing the 1100-H14 state aluminium alloy band production method of high-end bottle lid of cosmetics, comprising the following steps:
Step a: melting, smelting temperature are 720 DEG C, smelting time 5h;Each composition quality percentage in the aluminium alloy of the melting Number are as follows: Si:0.125%, Fe:0.381%, Cu:0.161%, Mn:0.0038%, Mg:0.00095%, Ti:0.031%, other impurities Total≤0.05%, remaining is Al.
Step b: using semi-continuous process ingot casting, and the casting temperature of semi-continuous process ingot casting is 715 DEG C, casting speed 55mm/ min。
Step c: ingot casting carries out homogenization heat treatment in 600 ± 15 DEG C of heat preservation 12h, and cutting head, back-end crop mill face.
Step d: being heated to 525 DEG C for ingot casting, keep the temperature 4h, and using 1+1 formula Hot Rolling Mill, first hot roughing, rolls through 17 passages System, by ingot casting roughing to a thickness of 35mm, the hot rolling blank of rear hot finishing to 9.0mm, finishing temperature is 320 DEG C;In hot roughing Lotion parameter are as follows: concentration 4.0%, temperature 45 C, pH value 7.5, ash content 800PPm, 500 μ s/cm of conductivity;Lotion is joined in hot finishing Number are as follows: concentration 7.0%, temperature 45 C, pH value 7.5, ash content 1000PPm, 800 μ s/cm of conductivity, are altered by 400 revs/min of brush roll revolving speed Dynamic frequency is 20 beats/min, throw-on pressure 300N.
Step e: through 2 passes, the first passage uncoiling tension 6N/mm2, gloss level of roll Ra is 0.35 μm, 40 DEG C of fortune Kinetic viscosity 2.2 ~ 2.4mm2/s of value, between 35 DEG C ~ 45 DEG C, cold rolling oil control index of refraction is greater than ROLLING OIL Oil-temperature control 90%, once cold rolling is to a thickness of 4.0mm.
Step f: by blank heating to 200 ~ 220 DEG C and keep the temperature 4h carry out an oil removing, an intermediate annealing;It is primary intermediate Annealing temperature is 400 DEG C, keeps the temperature 20h.Natural cooling in feeding rack is put after coming out of the stove.
Step g: through 3 passes, the first passage uncoiling tension 8N/mm2, gloss level of roll Ra is 0.20 μm, 40 DEG C of fortune Kinetic viscosity 2.2 ~ 2.4mm2/s of value, between 35 DEG C ~ 45 DEG C, cold rolling oil control index of refraction is greater than ROLLING OIL Oil-temperature control 90%, secondary cold-rolling is to a thickness of 0.83mm.
Step h: blank heating to 200 ~ 220 DEG C and is kept the temperature 4h and carries out secondary oil removing, secondary intermediate annealing;Secondary centre Annealing temperature is 320 DEG C, keeps the temperature 20h.Natural cooling in feeding rack is put after coming out of the stove.
Step i: through 2 passes, the first passage uncoiling tension 16N/mm2, gloss level of roll Ra is 0.20 μm, 40 DEG C of fortune Kinetic viscosity 2.2 ~ 2.4mm2/s of value, between 35 DEG C ~ 50 DEG C, cold rolling oil control index of refraction is greater than ROLLING OIL Oil-temperature control 90%, it is cold-rolled to finished product thickness 0.5mm three times.
Step j: cleaning, straightening, uncoiling tension≤800N of straightening, elongation control is 0.4%.
Embodiment three
It is a kind of for processing the 1100-H14 state aluminium alloy band production method of high-end bottle lid of cosmetics, comprising the following steps:
Step a: melting, smelting temperature are 750 DEG C, smelting time 5h;Each composition quality percentage in the aluminium alloy of the melting Number is Si:0.136%, Fe:0.417%, Cu:0.173%, Mn:0.0042%, Mg:0.00086%, Ti:0.026%, other impurities are closed Meter≤0.05%, remaining is Al.
Step b: using semi-continuous process ingot casting, and the casting temperature of semi-continuous process ingot casting is 710 DEG C, casting speed 55mm/ min。
Step c: ingot casting carries out homogenization heat treatment in 600 ± 15 DEG C of heat preservation 12h, and cutting head, back-end crop mill face.
Step d: being heated to 530 DEG C for ingot casting, keep the temperature 4h, and using 1+1 formula Hot Rolling Mill, first hot roughing, rolls through 17 passages System, by ingot casting roughing to a thickness of 35mm, the hot rolling blank of rear hot finishing to 9.0mm, finishing temperature is 320 DEG C;In hot roughing Lotion parameter are as follows: concentration 4.0%, temperature 45 C, pH value 7.5, ash content 800PPm, 500 μ s/cm of conductivity;Lotion is joined in hot finishing Number are as follows: concentration 7.0%, temperature 45 C, pH value 7.5, ash content 1000PPm, 800 μ s/cm of conductivity, are altered by 400 revs/min of brush roll revolving speed Dynamic frequency is 20 beats/min, throw-on pressure 300N.
Step e: through 2 passes, the first passage uncoiling tension 6N/mm2, gloss level of roll Ra is 0.4 μm, 40 DEG C of movements 2.2 ~ 2.4mm2/s of viscosity number, between 35 DEG C ~ 45 DEG C, cold rolling oil controls index of refraction and is greater than 90% ROLLING OIL Oil-temperature control, Once cold rolling is to a thickness of 4.0mm.
Step f: by blank heating to 200 ~ 220 DEG C and keep the temperature 4h carry out an oil removing, an intermediate annealing;It is primary intermediate Annealing temperature is 420 DEG C, keeps the temperature 20h.Natural cooling in feeding rack is put after coming out of the stove.
Step g: through 2 passes, the first passage uncoiling tension 8N/mm2, gloss level of roll Ra is 0.20 μm, 40 DEG C of fortune Kinetic viscosity 2.2 ~ 2.4mm2/s of value, between 35 DEG C ~ 45 DEG C, cold rolling oil control index of refraction is greater than ROLLING OIL Oil-temperature control 90%, secondary cold-rolling is to a thickness of 1.17mm.
Step h: blank heating to 200 ~ 220 DEG C and is kept the temperature 4h and carries out secondary oil removing, secondary intermediate annealing;Secondary centre Annealing temperature is 320 DEG C, keeps the temperature 20h.Natural cooling in feeding rack is put after coming out of the stove.
Step i: through 1 passes, uncoiling tension 8N/mm2, gloss level of roll Ra are 0.18 μm, 40 DEG C of kinematic viscosity values 2.2 ~ 2.4mm2/s, for ROLLING OIL Oil-temperature control between 35 DEG C ~ 50 DEG C, cold rolling oil control index of refraction is cold three times greater than 90% It is rolled to finished product thickness 0.7mm.
Step j: cleaning, straightening, uncoiling tension≤800N of straightening, elongation control is 0.5%.
The 1100-H14 state aluminium alloy band inspection result that embodiment 1 ~ 3 produces is as shown in table 1.
The 1100-H14 state aluminium alloy band inspection result of 1 embodiment 1 ~ 3 of table production
Embodiment Finished product thickness Tensile strength Elongation percentage A50% Earing rate % Anodic oxidation effect
Embodiment 1 0.4mm 133MPa 4.5% 2.4% Level-one (excellent)
Embodiment 2 0.5mm 131MPa 5% 2.5% Level-one (excellent)
Embodiment 3 0.7mm 138MPA 6% 2.4% Level-one (excellent)
The embodiment of the above, only presently preferred embodiments of the present invention, is only used to explain the present invention, not limits this Invention practical range to those of ordinary skill in the art certainly can be according in technology disclosed in this specification Hold, makes other embodiments easily by way of replacing or changing, therefore all variations made in the principle of the present invention With improve etc., should be included in scope of the present invention patent.

Claims (10)

1. a kind of for processing the 1100-H14 state aluminium alloy band production method of high-end bottle lid of cosmetics, which is characterized in that The following steps are included:
Step a: melting, smelting temperature are 700 DEG C ~ 750 DEG C;Each composition quality percentage in the aluminium alloy of the melting are as follows: 0.05%≤Si≤0.15%、0.35%≤Fe≤0.55%、0.10%≤Cu≤0.20%、Mn≤0.02%、Mg≤0.05%、Ti≤ 0.04%, other impurities total≤0.05%, remaining is Al;
Step b: semi-continuous process ingot casting is used;
Step c: ingot casting carries out homogenization heat treatment in 600 ± 15 DEG C of 12 ~ 16h of heat preservation, and cutting head, back-end crop mill face;
Step d: being hot-rolled down to the hot rolling blank of 8.0mm or more, and finishing temperature is greater than 300 DEG C;
Step e: through 2 passes, once cold rolling is to a thickness of 3.5 ~ 4.5mm;
Step f: by blank heating to 200 ~ 220 DEG C and keep the temperature 4 ~ 5h carry out an oil removing, an intermediate annealing;It is described it is primary in Between annealing temperature be 360 ~ 450 DEG C, heat preservation 20 ~ for 24 hours;
Step g: through 2 ~ 4 passes, 38 ~ 42% processing capacity, secondary cold-rolling are reserved according to finished product thickness;
Step h: blank heating to 200 ~ 220 DEG C and is kept the temperature 4 ~ 5h and carries out secondary oil removing, secondary intermediate annealing;It is described it is secondary in Between annealing temperature be 320 ~ 360 DEG C, heat preservation 20 ~ for 24 hours;
Step i: through 1 ~ 2 passes, it is cold-rolled to 0.7mm finished product thickness below three times;
Step j: cleaning, straightening.
2. a kind of 1100-H14 state aluminium alloy band for processing high-end bottle lid of cosmetics according to claim 1 is raw Production method, which is characterized in that the casting temperature of semi-continuous process ingot casting described in step b be 690 ~ 730 DEG C, casting speed be 50 ~ 65mm/min。
3. a kind of 1100-H14 state aluminium alloy band for processing high-end bottle lid of cosmetics according to claim 1 is raw Production method, which is characterized in that hot rolling described in step d is that ingot casting is heated to 450 ~ 530 DEG C, keeps the temperature 3h or more, first hot roughing, Afterwards hot finishing to 8.0mm or more hot rolling blank.
4. a kind of 1100-H14 state aluminium alloy band for processing high-end bottle lid of cosmetics according to claim 3 is raw Production method, which is characterized in that lotion parameter in the hot roughing are as follows: concentration 4.0 ~ 6.0%, 45 ~ 60 DEG C of temperature, pH value 7.5 ~ 8.5, ash content is less than 800PPm, 500 μ s/cm of conductivity <.
5. a kind of 1100-H14 state aluminium alloy band for processing high-end bottle lid of cosmetics according to claim 3 is raw Production method, which is characterized in that lotion parameter in the hot finishing are as follows: concentration 7.0 ~ 8.0%, 45 ~ 65 DEG C of temperature, pH value 7.5 ~ 8.5, ash content is less than 1000PPm, 800 μ s/cm of conductivity <.
6. a kind of 1100-H14 state aluminium alloy band for processing high-end bottle lid of cosmetics according to claim 3 is raw Production method, which is characterized in that 400 ~ 500 revs/min of brush roll revolving speed in the hot finishing, play frequency are 20 ~ 30 beats/min, are pressed against Power is 300 ~ 400N.
7. a kind of 1100-H14 state aluminium alloy band for processing high-end bottle lid of cosmetics according to claim 1 is raw Production method, which is characterized in that the first passage uncoiling tension≤6N/mm2 in once cold rolling described in step e is depressed per pass Rate is 25 ~ 40%, and gloss level of roll Ra is 0.3 ~ 0.4 μm.
8. a kind of 1100-H14 state aluminium alloy band for processing high-end bottle lid of cosmetics according to claim 1 is raw Production method, which is characterized in that the first passage uncoiling tension≤8N/mm2 in secondary cold-rolling described in step g is depressed per pass Rate is 25 ~ 45%, and gloss level of roll Ra is 0.18 ~ 0.22 μm.
9. a kind of 1100-H14 state aluminium alloy band for processing high-end bottle lid of cosmetics according to claim 1 is raw Production method, which is characterized in that the first passage uncoiling tension≤16N/mm2 in cold rolling three times described in step i is depressed per pass Rate is 20 ~ 25%, and gloss level of roll Ra is 0.18 ~ 0.22 μm.
10. according to claim 1 a kind of for processing the 1100-H14 state aluminium alloy band of high-end bottle lid of cosmetics Production method, which is characterized in that uncoiling tension≤800N of straightening described in step j.
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Cited By (3)

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