CN110068434B - Pulse type cyclohexane gas cold generator for detecting leakage rate of iodine adsorber - Google Patents

Pulse type cyclohexane gas cold generator for detecting leakage rate of iodine adsorber Download PDF

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Publication number
CN110068434B
CN110068434B CN201910248298.0A CN201910248298A CN110068434B CN 110068434 B CN110068434 B CN 110068434B CN 201910248298 A CN201910248298 A CN 201910248298A CN 110068434 B CN110068434 B CN 110068434B
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cyclohexane
leading
gasified
pipe
compressed air
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CN110068434A (en
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俞杰
李永国
侯建荣
邱继林
吴波
高琳锋
陈建利
韩丽红
张崇文
韩明
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China Institute for Radiation Protection
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China Institute for Radiation Protection
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01MTESTING STATIC OR DYNAMIC BALANCE OF MACHINES OR STRUCTURES; TESTING OF STRUCTURES OR APPARATUS, NOT OTHERWISE PROVIDED FOR
    • G01M3/00Investigating fluid-tightness of structures
    • G01M3/02Investigating fluid-tightness of structures by using fluid or vacuum
    • G01M3/26Investigating fluid-tightness of structures by using fluid or vacuum by measuring rate of loss or gain of fluid, e.g. by pressure-responsive devices, by flow detectors
    • G01M3/32Investigating fluid-tightness of structures by using fluid or vacuum by measuring rate of loss or gain of fluid, e.g. by pressure-responsive devices, by flow detectors for containers, e.g. radiators
    • G01M3/3236Investigating fluid-tightness of structures by using fluid or vacuum by measuring rate of loss or gain of fluid, e.g. by pressure-responsive devices, by flow detectors for containers, e.g. radiators by monitoring the interior space of the containers
    • G01M3/3272Investigating fluid-tightness of structures by using fluid or vacuum by measuring rate of loss or gain of fluid, e.g. by pressure-responsive devices, by flow detectors for containers, e.g. radiators by monitoring the interior space of the containers for verifying the internal pressure of closed containers
    • GPHYSICS
    • G21NUCLEAR PHYSICS; NUCLEAR ENGINEERING
    • G21CNUCLEAR REACTORS
    • G21C17/00Monitoring; Testing ; Maintaining
    • G21C17/002Detection of leaks
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E30/00Energy generation of nuclear origin
    • Y02E30/30Nuclear fission reactors

Abstract

The invention relates to a pulse type cyclohexane gas cold generator for detecting the leakage rate of an iodine adsorber, which comprises a gasification cavity, wherein a hexane liquid adding component, an air tightness checking component, a compressed air introducing component and a gasified cyclohexane gas leading-out component are connected with the gasification cavity; the gasified cyclohexane gas leading-out component comprises a gasified cyclohexane gas leading-out pipe connected with the gasification chamber, a quick connector and a switch valve are mounted on the gasified cyclohexane gas leading-out pipe, and the quick connector is connected with a test system of the iodine adsorber. The generator has the advantages of easy control of gas generation conditions, convenient operation and good field adaptability, and all performance indexes can meet the requirements of leakage rate tests.

Description

Pulse type cyclohexane gas cold generator for detecting leakage rate of iodine adsorber
Technical Field
The invention relates to leak detection test equipment in the nuclear field, in particular to a pulse type cyclohexane gas cold generator for detecting the leakage rate of an iodine adsorber.
Background
The iodine adsorber of the nuclear air purification system is key equipment for controlling the radioactive iodine of the effluent to achieve safe discharge, and ensuring that the iodine adsorber is in a good state is an important link for reducing radioactive substance release source items and ensuring the safe operation of a reactor. In order to ensure the safe and reliable operation of the nuclear air purification system and ensure that the exhaust of the ventilation system of the nuclear facility meets the effluent discharge limit value required by the national relevant standard, a field test of leakage rate detection must be carried out before the operation of the newly installed iodine adsorber, and a field test of periodic leakage rate detection must be carried out during the operation of the installed iodine adsorber to evaluate the functional effectiveness of the iodine adsorber.
The methods for confirming the effectiveness of the iodine filter include, for example, the freon method, the radioactive methyl iodine method, and the cyclohexane method. The cyclohexane method has good superiority when validity confirmation is carried out on the iodine adsorber ventilation system, the nuclear island ventilation system and the like in the habitable space (a central control room and an emergency command center) of the nuclear power station personnel, so that the radiation safety problem caused by possible radioactive leakage when the iodine adsorber performance test is carried out on the habitable space and the nuclear island ventilation system of the nuclear power station personnel is avoided, and meanwhile, the cyclohexane method can replace a Freon method to carry out iodine adsorber leakage rate test on ventilation systems of third-generation nuclear power, CNP300, CANDU reactors and the like, so that the use of Freon can be effectively reduced, and the damage to the ozone layer can be relieved.
When a cyclohexane method is used for carrying out a leakage rate detection test of an iodine adsorber, cyclohexane gas with a certain concentration is injected into a preset position at the upstream of a ventilation system of the iodine adsorber by using a cyclohexane gas generator, the upstream sampling port and the downstream sampling port are used for sampling and measuring the concentrations of upstream and downstream gas samples respectively, and whether the mechanical leakage rate of the iodine adsorber meets the standard requirement or not is judged according to the ratio of the upstream and downstream concentrations, wherein the safe and stable injection of the cyclohexane gas is one of key factors for smooth performance of the whole test. Therefore, a pulse type cyclohexane gas cold generator is developed for the field leakage rate detection test of the iodine adsorber of the ventilation system of the nuclear facility, and the product performance completely meets the design requirement.
Disclosure of Invention
The invention aims to solve the defects in the prior art and provides a pulse type cyclohexane gas cold generator for detecting the leakage rate of an iodine adsorber.
In order to achieve the purpose, the technical scheme adopted by the invention is as follows:
the pulse type cyclohexane gas cold generator for detecting the leakage rate of the iodine adsorber comprises a gasification cavity, wherein a hexane liquid adding component, an air tightness checking component, a compressed air introducing component and a gasified cyclohexane gas leading-out component are connected with the gasification cavity;
the gasified cyclohexane gas leading-out component comprises a gasified cyclohexane gas leading-out pipe connected with the gasification chamber, a quick connector and a switch valve are mounted on the gasified cyclohexane gas leading-out pipe, and the quick connector is connected with a test system of the iodine adsorber.
Furthermore, the compressed air leading-in assembly comprises a compressed air leading-in pipe connected with the gasification chamber, the end part of the compressed air leading-in pipe is connected with a compressed air source, and a pressure reducing valve, a switch valve and a one-way valve are arranged on the compressed air leading-in pipe.
Further, the gas tightness inspection assembly comprises a vacuum generator, a first vacuum tube and a second vacuum tube which are connected with the inlet end of the vacuum generator, the free end of the first vacuum tube is connected with a compressed air inlet tube, the free end of the second vacuum tube is connected with a gasification chamber, the output end of the vacuum generator is connected with a third vacuum tube, and the free end of the third vacuum tube is connected with a gasified cyclohexane gas outlet tube.
Furthermore, a pressure reducing valve is arranged on the first vacuum tube, and a switch valve is arranged on the second vacuum tube.
Further, a pressure indicator is installed on the gasification chamber, the liquid cyclohexane inlet pipe and the gasified cyclohexane gas outlet pipe are both connected to the top of the gasification chamber, and the compressed air inlet pipe is connected to the bottom of the gasification chamber.
Further, the outside of liquid cyclohexane holding vessel is equipped with the safety cover, is equipped with the window on the safety cover, and liquid cyclohexane holding vessel adopts transparent material.
Further, the compressed air source is an air pump.
Furthermore, the quick connector comprises a male connector and a female connector, the female connector is fixedly connected with the gasified cyclohexane gas delivery pipe, the female connector is quickly connected with the male connector, and the male connector is connected with a test system of the iodine adsorber.
The invention has the beneficial effects that: the generator has the advantages of easy control of gas generation conditions, convenient operation and good field adaptability, and all performance indexes can meet the requirements of leakage rate tests.
Drawings
FIG. 1 is a schematic structural diagram of the present invention.
Detailed Description
As shown in fig. 1, the pulse type cyclohexane gas cold generator for detecting the leakage rate of the iodine adsorber comprises a gasification chamber 1, wherein the gasification chamber 1 is connected with a cyclohexane liquid feeding assembly, an air tightness checking assembly, a compressed air feeding assembly and a gasified cyclohexane gas leading-out assembly, the cyclohexane liquid feeding assembly comprises a liquid cyclohexane leading-in pipe 2 connected with the gasification chamber 1, the end part of the liquid cyclohexane leading-in pipe 2 is connected with a hollow needle 3, the hollow needle 3 is inserted into a sealed liquid cyclohexane storage tank 4, and the liquid cyclohexane leading-in pipe 2 is provided with a switch valve V6;
the gasified cyclohexane gas leading-out component comprises a gasified cyclohexane gas leading-out pipe 5 connected with the gasification chamber 1, a quick connector and a switch valve V7 are installed on the gasified cyclohexane gas leading-out pipe 5, and the quick connector is connected with a test system of the iodine adsorber.
Further, the compressed air introducing module includes a compressed air introducing pipe 6 connected to the gasification chamber 1, a compressed air source is connected to an end of the compressed air introducing pipe 6, and a pressure reducing valve V3, a switching valve V4 and a check valve V5 are provided on the compressed air introducing pipe 6.
The gas tightness inspection assembly comprises a vacuum generator 7, a first vacuum tube 8 and a second vacuum tube 9 which are connected with the inlet end of the vacuum generator 7, the free end of the first vacuum tube 8 is connected with a compressed air inlet tube 6, the free end of the second vacuum tube 9 is connected with a gasification chamber 1, the output end of the vacuum generator 7 is connected with a third vacuum tube 10, and the free end of the third vacuum tube 10 is connected with a gasified cyclohexane gas outlet tube 5. The first vacuum tube 8 is provided with a pressure reducing valve V1, and the second vacuum tube 9 is provided with a switch valve V2.
Further, a pressure indicator 11 is installed on the gasification chamber 1, the liquid cyclohexane inlet pipe 2 and the gasified cyclohexane gas outlet pipe 5 are both connected to the top of the gasification chamber 1, and the compressed air inlet pipe 6 is connected to the bottom of the gasification chamber 1.
The outside of the liquid cyclohexane storage tank 4 is provided with a protective cover 12, the protective cover 12 is provided with a window 13, and the liquid cyclohexane storage tank 4 is made of transparent materials. The compressed air source is preferably an air pump. The quick connector comprises a male connector 14 and a female connector 15, the female connector 15 is fixedly connected with the gasified cyclohexane gas delivery pipe 5, the female connector 15 is quickly connected with the male connector 14, and the male connector 14 is connected with a test system of the iodine adsorber.
The specific operation procedure of the system is as follows:
1. air tightness inspection
And (3) connecting a compressed air source, closing valves V3, V4, V5, V6 and V7, opening a valve V2, adjusting a pressure reducing valve V1, starting the vacuum generator 7 to work, observing the reading of a pressure indicator 11, reducing the pressure in the gasification chamber 1 to-0.8 bar, then closing the valve V2 and the pressure reducing valve V1, observing the pressure value, and judging that the change is not more than 0.05bar within 5min, wherein the air tightness is qualified.
2. Liquid feeding device
5-10 mL of cyclohexane is packaged into a liquid cyclohexane storage tank 4 made of 10Ml glass, the liquid cyclohexane storage tank is inversely inserted into a protective cover 12, a hollow needle 3 in the protective cover 12 is inserted into a rubber plug of the liquid cyclohexane storage tank 4, a valve V6 is opened, cyclohexane liquid in the liquid cyclohexane storage tank 4 is sucked into a gasification chamber 1 under the action of negative pressure in the gasification chamber 1, and the valve V6 is closed after the liquid in the liquid cyclohexane storage tank 4 completely flows into the gasification chamber 1.
3. Gasification of
The boiling point of the cyclohexane in the gasification chamber 1 is reduced under the condition of negative pressure, and the gasification rate is accelerated. When the gasification chamber 1 is kept still for 10-15min or the reading of the pressure indicator is increased by 1-2bar, the cyclohexane liquid is completely gasified.
4. Injection of
The pressure indicator reading was raised to 3-6bar by opening switch valve V4 and slowly adjusting pressure relief valve V3, switch valve V7 was opened and the vaporized hexane gas was injected into the test system via the generator outlet under a compressed air load.
5. Close off
After the test is completed, the gasification chamber 1 is purged for at least 5min, the valve V3 and the valve V4 are closed, and finally the valve V7 is closed.
Because the amount of the cyclohexane liquid added at a time can be accurately controlled, and the single use amount is only a few milliliters, the generator is safe in generation and operation, good in injection concentration repeatability, easy to control the gas generation condition, convenient and fast to operate, good in field adaptability, and capable of meeting the leakage rate test requirements in all performance indexes.
Finally, it should be noted that the above embodiments are only used for illustrating the technical solutions of the present invention, and not for limiting the same; while the invention has been described in detail and with reference to the foregoing embodiments, it will be understood by those skilled in the art that: the technical solutions described in the foregoing embodiments may be modified, or some or all of the technical features may be equally replaced; however, these modifications and substitutions do not substantially depart from the scope of the embodiments of the present invention.

Claims (6)

1. The pulse type cyclohexane gas cold generator for detecting the leakage rate of the iodine adsorber comprises a gasification cavity, a hexane liquid adding assembly, an air tightness checking assembly, a compressed air introducing assembly and a gasified cyclohexane gas leading-out assembly, and is characterized in that the cyclohexane liquid adding assembly comprises a liquid cyclohexane leading-in pipe connected with the gasification cavity, the end part of the liquid cyclohexane leading-in pipe is connected with a hollow needle, the hollow needle is inserted into a sealed liquid cyclohexane storage tank, and a switch valve is arranged on the liquid cyclohexane leading-in pipe;
the gasified cyclohexane gas leading-out component comprises a gasified cyclohexane gas leading-out pipe connected with the gasification chamber, a quick connector and a switch valve are mounted on the gasified cyclohexane gas leading-out pipe, and the quick connector is connected with a test system of the iodine adsorber;
the compressed air leading-in assembly comprises a compressed air leading-in pipe connected with the gasification chamber, the end part of the compressed air leading-in pipe is connected with a compressed air source, and a pressure reducing valve, a switch valve and a one-way valve are arranged on the compressed air leading-in pipe;
the air tightness inspection assembly comprises a vacuum generator, a first vacuum tube and a second vacuum tube, wherein the first vacuum tube and the second vacuum tube are connected with the inlet end of the vacuum generator, the free end of the first vacuum tube is connected with a compressed air inlet tube, the free end of the second vacuum tube is connected with a gasification chamber, the output end of the vacuum generator is connected with a third vacuum tube, and the free end of the third vacuum tube is connected with a gasified cyclohexane gas outlet tube.
2. The pulse type cyclohexane gas cold generator for detecting the leakage rate of the iodine adsorber as claimed in claim 1, wherein the first vacuum tube is provided with a pressure reducing valve, and the second vacuum tube is provided with a switch valve.
3. The pulse type cyclohexane gas cold generator for detecting the leakage rate of the iodine adsorber as claimed in claim 2, wherein a pressure indicator is installed on the gasification chamber, the liquid cyclohexane inlet pipe and the gasified cyclohexane gas outlet pipe are connected to the top of the gasification chamber, and the compressed air inlet pipe is connected to the bottom of the gasification chamber.
4. The pulse type cyclohexane gas cold generator for detecting the leakage rate of the iodine adsorber as claimed in claim 1, wherein a protective cover is provided outside the liquid cyclohexane storage tank, a window is provided on the protective cover, and the liquid cyclohexane storage tank is made of transparent material.
5. The pulse type cyclohexane gas cold generator for iodine adsorber leakage rate detection according to claim 1, wherein the compressed air source is an air pump.
6. The pulse type cyclohexane gas cold generator for detecting the leakage rate of the iodine adsorber as claimed in claim 1, wherein the quick connector comprises a male connector and a female connector, the female connector is fixedly connected with the gasified cyclohexane gas outlet pipe, the female connector is quickly connected with the male connector, and the male connector is connected with a test system of the iodine adsorber.
CN201910248298.0A 2019-03-29 2019-03-29 Pulse type cyclohexane gas cold generator for detecting leakage rate of iodine adsorber Active CN110068434B (en)

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