CN110041709A - Elasticity squeezes out the effective glue preparation method of fiber glass coating - Google Patents
Elasticity squeezes out the effective glue preparation method of fiber glass coating Download PDFInfo
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- CN110041709A CN110041709A CN201910332013.1A CN201910332013A CN110041709A CN 110041709 A CN110041709 A CN 110041709A CN 201910332013 A CN201910332013 A CN 201910332013A CN 110041709 A CN110041709 A CN 110041709A
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- silicone oil
- glass coating
- fiber glass
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L83/00—Compositions of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon only; Compositions of derivatives of such polymers
- C08L83/04—Polysiloxanes
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/014—Additives containing two or more different additives of the same subgroup in C08K
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2203/00—Applications
- C08L2203/18—Applications used for pipes
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
- C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
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- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Adhesives Or Adhesive Processes (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
Elasticity provided by the present invention squeezes out the effective glue preparation method of fiber glass coating and belongs to industrial glue technical field, and it is an object of the present invention to provide a kind of method that can be prepared the biggish elasticity of tensile strength and elongation and squeeze out the effective glue of fiber glass coating.The present invention includes following preparation step: preparation component A；Prepare B component；The component A and the B component are uniformly mixed.
Description
Technical field
The present invention relates to a kind of industrial glue, and in particular to a kind of elasticity extrusion effective glue of fiber glass coating.
Background technique
Glass fibre sleeve be with glass fiber yarn weave packaged tube, then pass through high-temperature process, be coated with organic siliconresin,
Silicon rubber and be made, glass fibre sleeve itself has higher electrical apparatus insulation, heat resistance, corrosion resistance, ageing resistance and dissipate
It is hot to have splendid characteristic, and it is also able to maintain because it is with excellent flexibility and elasticity, therefore in subzero 50 DEG C of low temperature
The resistance to complications of flexibility, will not detract its electric insulating quality.But existing insulating sleeve glue is in tensile strength and elongation side
Face is limited without breaking through sexual tension, therefore using the tensile strength of its insulating sleeve made and elongation always, cannot
Meet application demand in special circumstances.
Summary of the invention
For the defects in the prior art, the present invention provides prepared glue tensile strength and elongation in the solid state
Biggish elasticity squeezes out fiber glass coating tube preparation method, to produce the biggish glass fibre of tensile strength and elongation
Casing provides solution.
The present invention provides a kind of method for preparing elasticity and squeezing out the effective glue of fiber glass coating, includes the following steps:
Prepare component A；By 41-49 parts of 600# white carbon black, 23-30 parts of QS-40 white carbon black, 11-13 parts of vinyl silicone oil,
1-3 parts of 3-7 parts of MBT silicone oil and inhibitor are put into mixer respectively；Control mixer is warming up to 130-160 DEG C, then takes out
It is vacuum-treated 2-3 hours；Control mixer is warming up to 160-190 DEG C again, until viscosity is -280 kilograms of 200 kilograms, then
It is secondary to vacuumize 3.5-4 hours, so far obtain component A；
Prepare B component；By 12-20 parts of vinyl silicone oil, 2-4 parts of MBT silicone oil, 2-10 parts of containing hydrogen silicone oil, adhesive accelerant
0.5-2 parts of 1-3 parts, 1-4 parts of fire retardant and catalyst are put into mixer respectively, and control mixer is warming up to 160-200
DEG C, until the viscosity is -290 kilograms of 220 kilograms, then vacuumize process 2-3 hours, so far obtain component A；
The component A and the B component are uniformly mixed and squeeze out the effective glue of fiber glass coating to get to elasticity.
Further, the method that preparation elasticity provided by the present invention squeezes out the effective glue of fiber glass coating, the bonding promote
Into agent be γ-glycidyl-oxygen propyl group-trimethoxy silane, vinyl glycidyl ether, butanediol glycidol, and/or,
Tetramethyldihydrogendisiloxane.
Further, the method that preparation elasticity provided by the present invention squeezes out the effective glue of fiber glass coating, the catalyst
For alkane platinum complex, four triphenyl phosphorus platinum, platinum chitosan, and/or, tetramethyldihydrogendisiloxane.
Further, the method that preparation elasticity provided by the present invention squeezes out the effective glue of fiber glass coating, the inhibitor
For acetenyl ring body, and/or, acetylene alcohol.
Experiment proves that the effective glue of fiber glass coating prepared by process through the invention, compared to existing bullet
Property squeeze out the effective glue of fiber glass coating for, tensile strength and elongation improve 2 times, to produce tensile strength and elongation
The biggish glass fibre sleeve of rate provides solution.
Specific embodiment
Technical solution of the present invention is described in detail below in conjunction with specific embodiment.Following embodiment is only used for
Clearly illustrate technical solution of the present invention, therefore be intended only as example, and cannot be used as a limitation and limit protection of the invention
Range.
Experimental method in following embodiments is unless otherwise specified conventional method.Examination as used in the following examples
Material is tested, is to be commercially available from routine biochemistry reagent shop unless otherwise specified.
Embodiment one
The present invention provides a kind of elasticity extrusion effective glue of fiber glass coating, in mass, component are as follows: 600# white carbon black
41kg；QS-40 white carbon black 23kg；Vinyl silicone oil 33kg；MBT silicone oil 11kg；Containing hydrogen silicone oil 3kg；Adhesive accelerant 1kg；Resistance
Fire agent 4kg；Inhibitor 3kg；Catalyst 0.5kg.
Elasticity provided by the present embodiment squeezes out the effective glue preparation process of fiber glass coating and includes the following steps:
S01: preparation component A；By 600# white carbon black 41kg, QS-40 white carbon black 23kg, vinyl silicone oil 13kg, MBT silicone oil
7kg and inhibitor 3kg are put into mixer respectively；Control mixer is warming up to 130-160 DEG C, then vacuumize process 2-3
Hour；Control mixer is warming up to 160-190 DEG C again, vacuumizes 3.5-4 hours again, so far obtains component A；
SO2: preparation B component；By vinyl silicone oil 20kg, MBT silicone oil 4kg, containing hydrogen silicone oil 3kg, adhesive accelerant 1kg,
Fire retardant 4kg and catalyst 0.5kg are put into mixer respectively, and control mixer is warming up to 160-200 DEG C, are then taken out true
Vacancy is managed 2-3 hours, and component A is so far obtained；
S03: all B components made from all component As made from S01 and S02 are uniformly mixed and squeeze out glass to get to elasticity
Glass fiber sleeve glue.
Embodiment two
The present invention provides a kind of elasticity extrusion effective glue of fiber glass coating, in mass, component are as follows: 600# white carbon black
49kg；QS-40 white carbon black 30kg；Vinyl silicone oil 27kg；MBT silicone oil 5kg；Containing hydrogen silicone oil 10kg；Adhesive accelerant 3kg；Resistance
Fire agent 1kg；Inhibitor 1kg；Catalyst 2kg.
Elasticity provided by the present embodiment squeezes out the effective glue preparation process of fiber glass coating and includes the following steps:
S01: preparation component A；By 600# white carbon black 49kg, QS-40 white carbon black 30kg, vinyl silicone oil 10kg, MBT silicone oil
3kg and inhibitor 1kg are put into mixer respectively；Control mixer is warming up to 130-160 DEG C, then vacuumize process 2-3
Hour；Control mixer is warming up to 160-190 DEG C again, until viscosity is 2,680,000 kg, vacuumizes 3.5-4 hours, so far obtains again
To component A；
SO2: preparation B component；By vinyl silicone oil 17kg, MBT silicone oil 2kg, containing hydrogen silicone oil 10kg, adhesive accelerant 3kg,
Fire retardant 1kg and catalyst 2kg are put into mixer respectively, and control mixer is warming up to 160-200 DEG C, until viscosity is 260
Ten thousand kg then vacuumize process 2-3 hours, so far obtain component A；
S03: all B components made from all component As made from S01 and S02 are uniformly mixed and squeeze out glass to get to elasticity
Glass fiber sleeve glue.
Embodiment three
The present invention provides a kind of elasticity extrusion effective glue of fiber glass coating, in mass, component are as follows: 600# white carbon black
45kg；QS-40 white carbon black 25kg；Vinyl silicone oil 29kg；MBT silicone oil 9kg；Containing hydrogen silicone oil 8kg；Adhesive accelerant 1.5kg；Resistance
Fire agent 2kg；Inhibitor 2.5kg；Catalyst 1kg.
Elasticity provided by the present embodiment squeezes out the effective glue preparation process of fiber glass coating and includes the following steps:
S01: preparation component A；By 600# white carbon black 45kg, QS-40 white carbon black 25kg, vinyl silicone oil 11kg, MBT silicone oil
6kg and inhibitor 2.5kg are put into mixer respectively；Control mixer is warming up to 130-160 DEG C, then vacuumize process
2-3 hours；Control mixer is warming up to 160-190 DEG C again, until viscosity is 2,800,000 kg, vacuumizes again 3.5-4 hours, until
This obtains component A；
SO2: preparation B component；By vinyl silicone oil 18kg, MBT silicone oil 3kg, containing hydrogen silicone oil 8kg, adhesive accelerant
1.5kg, fire retardant 2kg and catalyst 1kg are put into mixer respectively, and control mixer is warming up to 160-200 DEG C, until viscous
Degree is 2,700,000 kg, then vacuumize process 2-3 hours, so far obtains component A；
S03: all B components made from all component As made from S01 and S02 are uniformly mixed and squeeze out glass to get to elasticity
Glass fiber sleeve glue.
Example IV
The present invention provides a kind of elasticity extrusion effective glue of fiber glass coating, in mass, component are as follows: 600# white carbon black
42kg；QS-40 white carbon black 27kg；Vinyl silicone oil 31kg；MBT silicone oil 7kg；Containing hydrogen silicone oil 5kg；Adhesive accelerant 2kg；It is fire-retardant
Agent 3kg；Inhibitor 1.5kg；Catalyst 1.5kg.
Elasticity provided by the present embodiment squeezes out the effective glue preparation process of fiber glass coating and includes the following steps:
S01: preparation component A；By 600# white carbon black 42kg, QS-40 white carbon black 27kg, vinyl silicone oil 13kg, MBT silicone oil
5kg and inhibitor 1.5kg are put into mixer respectively；Control mixer is warming up to 130-160 DEG C, then vacuumize process
2-3 hours；Control mixer is warming up to 160-190 DEG C again, until viscosity is 2,000,000 kg, vacuumizes again 3.5-4 hours, until
This obtains component A；
SO2: preparation B component；By vinyl silicone oil 18kg, MBT silicone oil 2kg, containing hydrogen silicone oil 5kg, adhesive accelerant 2kg,
Fire retardant 3kg and catalyst 1.5kg are put into mixer respectively, and control mixer is warming up to 160-200 DEG C, until viscosity is
2900000 kg then vacuumize process 2-3 hours, so far obtain component A；
S03: all B components made from all component As made from S01 and S02 are uniformly mixed and squeeze out glass to get to elasticity
Glass fiber sleeve glue.
Embodiment five
The present invention provides a kind of elasticity extrusion effective glue of fiber glass coating, in terms of quality g, component are as follows: 600# white carbon black
46kg；QS-40 white carbon black 28kg；Vinyl silicone oil 32kg；MBT silicone oil 8kg；Containing hydrogen silicone oil 7kg；Adhesive accelerant 2.2kg；Resistance
Fire agent 2kg；Inhibitor 1.5kg；Catalyst 0.9kg.
Elasticity provided by the present embodiment squeezes out the effective glue preparation process of fiber glass coating and includes the following steps:
S01: preparation component A；By 600# white carbon black 46kg, QS-40 white carbon black 28kg, vinyl silicone oil 13kg, MBT silicone oil
5kg and inhibitor 1.5kg are put into mixer respectively；Control mixer is warming up to 130-160 DEG C, then vacuumize process
2-3 hours；Control mixer is warming up to 160-190 DEG C again, until viscosity is 2,300,000 kg, vacuumizes again 3.5-4 hours, until
This obtains component A；
SO2: preparation B component；By vinyl silicone oil 19kg, MBT silicone oil 3kg, containing hydrogen silicone oil 7kg, adhesive accelerant
2.2kg, fire retardant 2kg and catalyst 0,9kg is put into mixer respectively, and control mixer is warming up to 160-200 DEG C, until
Viscosity is 2,400,000 kg, then vacuumize process 2-3 hours, so far obtains component A；
S03: all B components made from all component As made from S01 and S02 are uniformly mixed and squeeze out glass to get to elasticity
Glass fiber sleeve glue.
Elasticity provided by the embodiment of the present invention squeezes out in the effective glue of fiber glass coating, and the adhesive accelerant is γ-ring
Oxygen propyl group-oxygen propyl group-trimethoxy silane, vinyl glycidyl ether, butanediol glycidol, and/or, tetramethyl dihydro two
Siloxanes；The catalyst be alkane platinum complex, four triphenyl phosphorus platinum, platinum chitosan, and/or, tetramethyldihydrogendisiloxane；
The inhibitor is acetenyl ring body, and/or, acetylene alcohol.
Following table is the extrusion effective glue of fiber glass coating of elasticity corresponding to above-mentioned five embodiments, and in the market existing two
The parameter comparison of the similar glue of money.
As seen from the above table, elasticity provided by the present invention squeezes out the effective glue of fiber glass coating and squeezes out compared to existing elasticity
For the effective glue of fiber glass coating, tensile strength and elongation improve 2 times, for produce tensile strength and elongation compared with
Big glass fibre sleeve provides solution.In addition, the elasticity extrusion effective glue of fiber glass coating provided by the present invention is complete
Unused dimethylbenzene entirely, has avoided damage of the dimethylbenzene to environment and human body.
Finally, it should be noted that the above embodiments are only used to illustrate the technical solution of the present invention., rather than its limitations；To the greatest extent
Pipe present invention has been described in detail with reference to the aforementioned embodiments, those skilled in the art should understand that: its according to
So be possible to modify the technical solutions described in the foregoing embodiments, or to some or all of the technical features into
Row equivalent replacement；And these are modified or replaceed, various embodiments of the present invention technology that it does not separate the essence of the corresponding technical solution
The range of scheme should all cover within the scope of the claims and the description of the invention.
Claims (4)
1. the method that preparation elasticity squeezes out the effective glue of fiber glass coating, includes the following steps:
Prepare component A；By 41-49 parts of 600# white carbon black, 23-30 parts of QS-40 white carbon black, 11-13 parts of vinyl silicone oil, MBT silicon
Oily 3-7 parts and 1-3 parts of inhibitor are put into mixer respectively；Control mixer is warming up to 130-160 DEG C, then vacuumizes
Processing 2-3 hours；Control mixer is warming up to 160-190 DEG C again, until viscosity is -280 kilograms of 200 kilograms, takes out again
Vacuum 3.5-4 hours, so far obtain component A；
Prepare B component；By 12-20 parts of vinyl silicone oil, 2-4 parts of MBT silicone oil, 2-10 parts of containing hydrogen silicone oil, adhesive accelerant 1-3
0.5-2 parts of part, 1-4 parts of fire retardant and catalyst are put into mixer respectively, and control mixer is warming up to 160-200 DEG C, until
The viscosity is -290 kilograms of 220 kilograms, then vacuumize process 2-3 hours, so far obtains component A；
The component A and the B component are uniformly mixed and squeeze out the effective glue of fiber glass coating to get to elasticity.
2. elasticity according to claim 1 squeezes out the effective glue of fiber glass coating, which is characterized in that the adhesive accelerant is
γ-glycidyl-oxygen propyl group-trimethoxy silane, vinyl glycidyl ether, butanediol glycidol, and/or, tetramethyl
Dihydro disiloxane.
3. elasticity according to claim 1 squeezes out the effective glue of fiber glass coating, which is characterized in that the catalyst is alkane platinum
Complex compound, four triphenyl phosphorus platinum, platinum chitosan, and/or, tetramethyldihydrogendisiloxane.
4. elasticity according to claim 1 squeezes out the effective glue of fiber glass coating, which is characterized in that the inhibitor is acetylene
Basic ring body, and/or, acetylene alcohol.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910332013.1A CN110041709A (en) | 2019-04-24 | 2019-04-24 | Elasticity squeezes out the effective glue preparation method of fiber glass coating |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910332013.1A CN110041709A (en) | 2019-04-24 | 2019-04-24 | Elasticity squeezes out the effective glue preparation method of fiber glass coating |
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| Publication Number | Publication Date |
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| CN110041709A true CN110041709A (en) | 2019-07-23 |
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|---|---|---|---|
| CN201910332013.1A Pending CN110041709A (en) | 2019-04-24 | 2019-04-24 | Elasticity squeezes out the effective glue preparation method of fiber glass coating |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101386706A (en) * | 2008-05-16 | 2009-03-18 | 卢儒 | Solvent-free flame-retardant glass fiber silicone resin |
| CN105754543A (en) * | 2016-04-06 | 2016-07-13 | 深圳市欧普特工业材料有限公司 | Organic silicon pouring sealant containing functional group MQ resin for LED and preparation method of organic silicon pouring sealant |
| US20170354032A1 (en) * | 2014-12-26 | 2017-12-07 | Shengyi Technology Co., Ltd. | Halogen-free and phosphorus-free silicone resin composition, prepreg, laminate board, copper-clad plate using the same, and printed circuit board |
-
2019
- 2019-04-24 CN CN201910332013.1A patent/CN110041709A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101386706A (en) * | 2008-05-16 | 2009-03-18 | 卢儒 | Solvent-free flame-retardant glass fiber silicone resin |
| US20170354032A1 (en) * | 2014-12-26 | 2017-12-07 | Shengyi Technology Co., Ltd. | Halogen-free and phosphorus-free silicone resin composition, prepreg, laminate board, copper-clad plate using the same, and printed circuit board |
| CN105754543A (en) * | 2016-04-06 | 2016-07-13 | 深圳市欧普特工业材料有限公司 | Organic silicon pouring sealant containing functional group MQ resin for LED and preparation method of organic silicon pouring sealant |
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Application publication date: 20190723 |
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