CN110038484A - A kind of high-temperature high-pressure reaction kettle with on-line period device - Google Patents
A kind of high-temperature high-pressure reaction kettle with on-line period device Download PDFInfo
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- CN110038484A CN110038484A CN201910478541.8A CN201910478541A CN110038484A CN 110038484 A CN110038484 A CN 110038484A CN 201910478541 A CN201910478541 A CN 201910478541A CN 110038484 A CN110038484 A CN 110038484A
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J3/00—Processes of utilising sub-atmospheric or super-atmospheric pressure to effect chemical or physical change of matter; Apparatus therefor
- B01J3/002—Component parts of these vessels not mentioned in B01J3/004, B01J3/006, B01J3/02 - B01J3/08; Measures taken in conjunction with the process to be carried out, e.g. safety measures
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J3/00—Processes of utilising sub-atmospheric or super-atmospheric pressure to effect chemical or physical change of matter; Apparatus therefor
- B01J3/03—Pressure vessels, or vacuum vessels, having closure members or seals specially adapted therefor
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/02—Devices for withdrawing samples
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Abstract
The invention discloses a kind of high-temperature high-pressure reaction kettles with on-line period device, including main casing and reaction chamber is set in the main casing, end wall fixed placement has a station on the downside of the reaction chamber, a dodge gate is provided in end wall on front side of the reaction chamber, a driving mechanism based on power motor is provided in the main casing, the pressurizing device in the reaction chamber is driven to move down by the driving mechanism, push the opening opened simultaneously between cooling device and the reaction chamber, to be cooled down while compressing the reaction chamber inner space, when the temperature in the reaction chamber reaches preset value, the pressure in the reaction chamber is further finely adjusted by cam gear, this apparatus structure is simple, and pressure process cooling to reaction chamber is completed by compact drive connection, preferable sealing is protected Having demonstrate,proved reaction chamber temperature in a longer period of time and pressure will not change.
Description
Technical field
The present invention relates to chemical process technology field, specially a kind of high-temperature high-voltage reaction with on-line period device
Kettle.
Background technique
In the present society of rapid technological growth, chemical industry plays indispensable role, chemical reaction wherein
Refer to the technology for changing synthesis novel substance after the composition of substance, structure with the method for chemistry, in the historical process of human development
Middle chemical industry plays important function, and the reaction unit of traditional high temperature and pressure is directly by coolant liquid directly to reaction ring
Border is cooled down, simultaneously because sealing at this stage realizes that leakproofness is poor by spiral mostly, so as to cause cannot be guaranteed
Initial temperature and pressure are remained during the reaction, are being affected the smooth of reaction down to a certain degree, are being reduced chemical industry
The quality of finished product.
Summary of the invention
It is existing for overcoming the purpose of the present invention is to provide a kind of high-temperature high-pressure reaction kettle with on-line period device
Drawbacks described above in technology.
A kind of high-temperature high-pressure reaction kettle with on-line period device according to the present invention, including main casing and setting exist
Reaction chamber in the main casing, reaction chamber downside end wall fixed placement has a station, on front side of the reaction chamber in end wall
It is provided with a dodge gate, is provided with a driving mechanism based on power motor in the main casing, under the driving mechanism
End has been connected by power an output shaft, and the driving mechanism upper end drives driven shaft and the output shaft synchronous to turn by belt wheel transmission
It is dynamic, so that the pressurizing device in the reaction chamber be driven to move down, pushing open simultaneously cooling device and the reaction chamber it
Between opening, to be cooled down while compressing the reaction chamber inner space, when the temperature in the reaction chamber reaches
When preset value, the pressure in the reaction chamber is further finely adjusted by cam gear, to reach required pressure
By force.
Further technical solution, the driving device include being arranged in the upper left power motor of the main casing, institute
The drive cavity for being provided in main casing above the power motor and extending to the right is stated, power motor upper end power connects
It is connected to a first rotating shaft upwardly extended, and the first rotating shaft upper end is rotationally protruded into the drive cavity, the transmission
It is provided with the driving pulley for being fixedly mounted on the first rotating shaft upper end in chamber, one or so extension is provided in the main casing
Chamber is pushed, and the pushing chamber lower end wall is connected with the reaction chamber, can be rotated between the pushing chamber and the drive cavity
Ground is provided with the second shaft of about one extension, and the driven shaft lower end and pushings chamber downside end wall are rotatably assorted company
Connect, be provided with a driven pulley being fixedly mounted on the upside of the driven shaft in the drive cavity, the driving pulley with it is described
A transmission belt is connected by power between driven pulley, the power motor lower end is connected by power the third that one extends downwardly and turns
Axis, and the output shaft lower end is rotationally protruded into the pushing chamber and is rotatably assorted company with end wall on the downside of the pushing chamber
It connects.
Further technical solution, the pressurizing device include the rectangle being slidably arranged between the pushing cavity wall
Lower platen, and the output shaft and the driven shaft lower end both pass through the rectangle lower platen and with the rectangle lower platen screw thread
It is cooperatively connected, rectangle lower platen lower end is fixedly installed with a link block, and the link block is slided with the cavity wall that reacts
Dynamic to be connected with, the link block lower end is fixedly installed with one and pushes with the annular for reacting cavity wall sliding connection
Block is provided with and communicated with symmetrical mating cavity in end wall on the downside of the reaction chamber, on the downside of the mating cavity there are two settings
Hydraulic cavities control and are provided with and communicated with hydraulic pipeline between two hydraulic cavities, and the annular lower lock block lower end surface is fixedly connected with a left side
Right symmetrical first connecting rod, and the two first connecting rod lower ends in left and right are slideably protruded into two hydraulic cavities being located remotely from each other, institute
It states and is provided with first sliding block that can slide up and down between hydraulic cavity wall, and first upper end of slide block face and the first connecting rod
It is fixedly connected, is fixedly connected with the first spring, the cooperation between end wall on the downside of first sliding block lower end and the hydraulic cavities
One is provided in chamber can slide up and down supporting block, and the supporting block upper surface is fixedly connected with a sealing block, under the annular
Briquetting lower end surface is provided with the seal groove that an opening is matched with the sealing block, and the supporting block lower end surface is fixedly connected oriented
The second connecting rod of lower extension, and the two second connecting rod lower ends in left and right are slideably protruded into two hydraulic cavities close to each other, institute
The second sliding block for being slidably provided with and being fixedly mounted on the downside of the second connecting rod between hydraulic cavity wall is stated, described second is sliding
Symmetrical second spring is fixedly connected between block upper surface and the hydraulic cavities upper end wall.
Further technical solution, the cooling device include the cold air storage chamber being arranged on the left of the reaction chamber, institute
It states and is provided with a refrigerator pipe being connected with extraneous cold air on the downside of the wall of cold air storage chamber left end, be provided with one on the refrigerator pipe and enter
Mouth control valve, is slidably connected with third connecting rod, and the third connecting rod between the pushing chamber and the cold air storage chamber
Upper end is fixedly connected with rectangle lower platen lower end surface, and being provided with one between the cold air storage cavity wall can slide up and down
Third sliding block, and be fixedly connected on the downside of the third upper end of slide block and the third connecting rod, in the cold air storage chamber lower end wall
It is provided with and communicated with a L shape delivery pipe, and the L shape delivery pipe right end is connected with the external world and is fixedly installed a control of export
Valve is provided with the snorkel of one or so perforation in the station, and one is provided with and communicated in the middle part of the snorkel lower end wall downwards
The connecting tube of extension, and the connecting tube lower end is connected with the L shape delivery pipe, is symmetrically arranged in the station
There is the electromagnetic cavity being located on the upside of the snorkel, one is provided between the electromagnetism cavity wall can slide up and down Four-slider,
It is fixedly installed with symmetrical third spring on the downside of Four-slider lower end surface and the electromagnetic cavity between end wall, described the
Four-slider lower end surface is fixedly connected with an armature block, and the armature block lower end is slidably disposed through the electromagnetic cavity lower side
Wall, the electromagnet that bilateral symmetry is provided in the snorkel lower end wall and is matched with the armature block, in the station
Be provided with symmetrical sliding slot, and the sliding slot passes through the snorkel, be provided in the sliding slot can slide up and down it is close
Bar is sealed, the through-hole of one or so perforation is provided in the sealing bar, and the through-hole is staggered with the snorkel when original state
It opens, is fixedly connected with one the 4th spring between the sealing bar upper surface and the sliding slot upper end wall, in the sliding slot lower end wall
It is provided with and communicated with an open slot being connected with the mating cavity, and the open slot is slideably protruded into the sealing bar lower end
In, the 5th sliding block that can slide up and down is provided in the open slot, and the 5th upper end of slide block is fixed with the sealing bar
Connection, the supporting block upper surface is fixedly installed with a pushing block being located on the downside of the open slot, and the pushing block is slideably
It protrudes into the open slot.
Further technical solution, the cam gear include connection be arranged in it is convex in the middle part of end wall on the upside of the pushing chamber
Take turns chamber, be fixedly connected with a rotary electric machine on the left of the cam chamber in end wall, the rotary electric machine right end be connected by power one to
4th shaft of right extension, and the 4th shaft right end is rotatably assorted with end wall on the right side of the cam chamber and connect, the cam
A cam for being fixedly connected on the 4th shaft outer surface is provided in chamber, being additionally provided with one between the cam cavity wall can
The 6th sliding block slided up and down, and the 6th sliding block lower end is fixedly connected with a fourth link extended downwardly, and described convex
Wheel chamber lower end is protruded into the reaction chamber after slideably sequentially passing through the rectangle lower platen, the link block, the reaction
Be provided in chamber one can slide up and down and with the 7th sliding block that is abutted against with the annular lower lock block, and the 7th upper end of slide block
It is fixedly connected, is fixedly connected between the 7th upper end of slide block face and the link block symmetrical with the fourth link
5th spring, the 6th sliding block are mutually abutted with the cam always under the action of five spring force.
It pressurizeed the beneficial effects of the present invention are: the present invention is completed by compact drive mechanism to the cooling of reaction chamber
Journey is pressed into cold air during pressurizeing to reaction chamber, reduces the temperature of reaction chamber, while passing through sealing block and the seal groove
Between cooperation guarantee the leakproofness of reaction chamber during cooling pressurization, and by cam structure to the pressure in reaction chamber
Play the role of further controlling, to ensure that the reaction temperature and pressure that can reach required in reaction chamber, while longer
Time in reaction chamber temperature and pressure will not change, ensure that going on smoothly for reaction, make sufficiently anti-between chemical reagent
It answers.
Detailed description of the invention
Fig. 1 is overall structure diagram inside a kind of high-temperature high-pressure reaction kettle with on-line period device of the invention；
Fig. 2 is the structural schematic diagram in the present invention in Fig. 1 at A.
Specific embodiment
Below with reference to Fig. 1-2, the present invention is described in detail, for sake of convenience, now such as to hereafter described orientation regulation
Under: hereafter described front-rear direction up and down is consistent with the front-rear direction up and down of Fig. 1 projection relation itself.
Referring to Fig.1-2, a kind of high-temperature high-pressure reaction kettle with on-line period device of embodiment according to the present invention, packet
Including main casing 100 and reaction chamber 132, the 132 downside end wall fixed placement of reaction chamber is arranged in the main casing 100 has
One station 168 is provided with a dodge gate 131 in the 132 front side end wall of reaction chamber, is provided with one in the main casing 100
Driving mechanism based on power motor 101, the driving mechanism lower end have been connected by power an output shaft 104, the driving
Mechanism upper end drives driven shaft 140 and the output shaft 104 to rotate synchronously by belt wheel transmission, to drive the reaction chamber
Pressurizing device in 132 moves down, and pushes the opening opened simultaneously between cooling device and the reaction chamber 132, thus
It is cooled down while compressing 132 inner space of reaction chamber, when the temperature in the reaction chamber 132 reaches preset value,
The pressure in the reaction chamber 132 is further finely adjusted by cam gear, to reach required pressure.
Valuably or illustratively, the driving device includes being arranged in the upper left power motor of the main casing 100
101, the drive cavity 151 for being provided with above the power motor 101 and extending to the right in the main casing 100 is described dynamic
101 upper end of force motor is connected by power a first rotating shaft 153 upwardly extended, and 153 upper end of the first rotating shaft is rotationally
It protrudes into the drive cavity 151, the active for being fixedly mounted on 153 upper end of first rotating shaft is provided in the drive cavity 151
Belt wheel 152 is provided with the pushing chamber 105 of one or so extension, and 105 lower end wall of pushing chamber and institute in the main casing 100
It states reaction chamber 132 to be connected, described push can be rotatably set about one extension between chamber 105 and the drive cavity 151
Second shaft 140, and 140 lower end of the driven shaft is rotatably assorted with the 105 downside end wall of pushing chamber and connect, the drive cavity
Be provided with a driven pulley 141 for being fixedly mounted on 140 upside of the driven shaft in 151, the driving pulley 152 with it is described from
A transmission belt 147 it has been connected by power between movable belt pulley 141,101 lower end of power motor is connected by power one and extends downwardly
Third shaft 104, and 104 lower end of the output shaft rotationally protrude into the pushing chamber 105 and under the pushing chamber 105
Side wall is rotatably assorted connection, and effect is: directly driving the output shaft 104 to rotate by the power motor 101, simultaneously
Drive the driving pulley 152 to rotate by the first rotating shaft 153, the driving pulley 152 by with the driven pulley
Drive connection between 141 drives the driven shaft 140 to rotate, to drive the third to turn by the power motor 101
Axis 104 and second shaft 140 rotate synchronously, and transmit as the power of pressurizing device and cooling device.
Valuably or illustratively, the pressurizing device includes slidably being arranged between 105 inner wall of pushing chamber
Rectangle lower platen 102, and the output shaft 104 and 140 lower end of driven shaft both pass through the rectangle lower platen 102 and with institute
It states rectangle lower platen 102 and is threadedly engaged connection, 102 lower end of rectangle lower platen is fixedly installed with a link block 136, and described
Link block 136 is slidably connected with 132 inner wall of reaction chamber, and 136 lower end of link block is fixedly installed with one and institute
The annular lower lock block 133 of 132 inner wall of reaction chamber sliding connection is stated, is provided with and communicated in the 132 downside end wall of reaction chamber
Symmetrical mating cavity 113, the hydraulic cavities 116 on the downside of the mating cavity 113 there are two settings, two hydraulic cavities 116 in left and right
Between be provided with and communicated with hydraulic pipeline 126,133 lower end surface of the annular lower lock block is fixedly connected with symmetrical first connecting rod
114, and two 114 lower ends of first connecting rod in left and right are slideably protruded into two hydraulic cavities 116 being located remotely from each other, the hydraulic cavities
First sliding block 115 that can slide up and down is provided between 116 inner walls, and 115 upper surface of the first sliding block and described first connects
Bar 114 is fixedly connected, and is fixedly connected with the first bullet between 116 downside end wall of 115 lower end of the first sliding block and the hydraulic cavities
Spring 128, one is provided in the mating cavity 113 can slide up and down supporting block 118, and 118 upper surface of supporting block is fixed to be connected
Be connected to a sealing block 117,133 lower end surface of the annular lower lock block be provided with an opening matched with the sealing block 117 it is close
Sealing groove 120,118 lower end surface of supporting block are fixedly connected with the second connecting rod 124 extended downwardly, and two second connecting rods in left and right
124 lower ends are slideably protruded into two hydraulic cavities 116 close to each other, are slideably set between 116 inner wall of hydraulic cavities
It is equipped with the second sliding block 122 for being fixedly mounted on 124 downside of second connecting rod, 122 upper surface of the second sliding block and the liquid
Be fixedly connected with symmetrical second spring 125 between pressure 116 upper end wall of chamber, effect is: by the output shaft 104,
Being threadedly engaged between the driven shaft 140 and the rectangle lower platen 102 drives the rectangle lower platen 102 to move down,
The rectangle lower platen 102 drives the first connecting rod 114 downwards by the link block 136 and the annular lower lock block 133
It is mobile, the hydraulic oil in be located remotely from each other two hydraulic cavities 116 is pressed by the other side by first sliding block 115 at this time, from
And drive the supporting block 118 to move up by second sliding block 122, at this time by the sealing block 117 with it is described close
Cooperation between sealing groove 120 completely encloses the reaction chamber 132, to pass through the connection while guaranteeing sealing performance
The pushing of block 136 plays the role of pressurization to reaction compartment.
Valuably or illustratively, the cooling device includes the cold air storage chamber that 132 left side of reaction chamber is arranged in
107, the 107 left end wall downside of cold air storage chamber is provided with a refrigerator pipe 110 being connected with extraneous cold air, the refrigerator pipe
It is provided with an inlet control valve 111 on 110, is slidably connected between the pushing chamber 105 and the cold air storage chamber 107
Third connecting rod 103, and 103 upper end of the third connecting rod is fixedly connected with 102 lower end surface of rectangle lower platen, the cold air is deposited
One is provided between 107 inner wall of storage chamber can slide up and down third sliding block 106, and 106 upper end of third sliding block and described the
It is fixedly connected on the downside of three-link 103, a L shape delivery pipe 112, and institute is provided with and communicated in 107 lower end wall of cold air storage chamber
It states 112 right end of L shape delivery pipe to be connected with the external world and be fixedly installed a discharge control valve 127, be arranged in the station 168
There is the snorkel 156 of one or so perforation, is provided with and communicated with a connecting tube extended downwardly in the middle part of 156 lower end wall of snorkel
162, and 162 lower end of the connecting tube is connected with the L shape delivery pipe 112, is symmetrically arranged in the station 168
There is the electromagnetic cavity 165 for being located at 156 upside of snorkel, being provided with one between 165 inner wall of electromagnetic cavity can slide up and down
Four-slider 166 is fixedly installed with left and right pair between 165 downside end wall of 166 lower end surface of Four-slider and the electromagnetic cavity
The third spring 164 of title, 166 lower end surface of Four-slider are fixedly connected with an armature block 167, and under the armature block 167
End be slidably disposed through the 165 downside end wall of electromagnetic cavity, be provided in 156 lower end wall of snorkel bilateral symmetry and with institute
The electromagnet 163 that armature block 167 matches is stated, symmetrical sliding slot 171, and the cunning are provided in the station 168
Slot 171 passes through the snorkel 156, is provided with the sealing bar 155 that can slide up and down, the sealing bar 155 in the sliding slot 171
In be provided with the through-hole 157 of one or so perforation, and the through-hole 157 is staggered with the snorkel 156 when original state, described
One the 4th spring 170,171 lower end of sliding slot are fixedly connected between 171 upper end wall of 155 upper surface of sealing bar and the sliding slot
An open slot 160 being connected with the mating cavity 113 is provided with and communicated in wall, and 155 lower end of the sealing bar is slideably
It protrudes into the open slot 160, the 5th sliding block 161 that can slide up and down is provided in the open slot 160, and the described 5th is sliding
161 upper end of block is fixedly connected with the sealing bar 155, and 118 upper surface of supporting block is fixedly installed with one and is located at the opening
The pushing block 121 of 160 downside of slot, and the pushing block 121 slideably protrudes into the open slot 160, effect is: by described
Pushing block 121 drives the 5th sliding block 161 to move up while moving up, thus drive the through-hole 157 with it is described
Snorkel 156 is interconnected, while the rectangle lower platen 102 pushes the cold air storage chamber by the third sliding block 106
Cold air in 107 pass sequentially through enter after the L shape delivery pipe 112, the connecting tube 162 and the snorkel 156 it is described
In reaction chamber 132, the reaction chamber 132 is added simultaneously to be reduced the temperature in the reaction chamber 132 by cold air
Pressure closes the power motor 101 when temperature reaches required reaction temperature in the reaction chamber 132, while starting institute
State electromagnet 163, by attracting each other between the electromagnet 163 and the armature block 167 drive the armature block 167 to
Lower movement, the connecting tube 162 is isolated with the reaction chamber 132 by the armature block 167 at this time, so that cold air stops entering institute
It states in reaction chamber 132, by drive mechanism by the synchronous indentation reaction of cold air while being pressurizeed by the link block 136
It is intracavitary, play the role of dropping to the reaction temperature in reaction chamber into predetermined value, while by calutron to the temperature in reaction chamber
Degree closes opening when reaching predetermined value, guarantees to make the temperature in reaction chamber keep steady in a long time while leakproofness
It is fixed.
Valuably or illustratively, the cam gear includes that connection is arranged in the middle part of the 105 upside end wall of pushing chamber
Cam chamber 145, a rotary electric machine 150 is fixedly connected in the 145 left side end wall of cam chamber, the rotary electric machine 150 is right
End is connected by power the 4th shaft 146 extended to the right, and 145 right side of 146 right end of the 4th shaft and the cam chamber
End wall is rotatably assorted connection, and a cam for being fixedly connected on 146 outer surface of the 4th shaft is provided in the cam chamber 145
144, one is additionally provided between 145 inner wall of cam chamber can slide up and down the 6th sliding block 143, and the 6th sliding block 143
Lower end is fixedly connected with a fourth link 142 extended downwardly, and 145 lower end of the cam chamber slideably sequentially pass through it is described
Protruded into after rectangle lower platen 102, the link block 136 in the reaction chamber 132, be provided in the reaction chamber 132 one can on
Lower slider and with the 7th sliding block 134 that is abutted against with the annular lower lock block 133, and 134 upper end of the 7th sliding block with it is described
Fourth link 142 is fixedly connected, and left and right pair is fixedly connected between 134 upper surface of the 7th sliding block and the link block 136
Claim the 5th spring 135, the 6th sliding block 143 under the action of the 5th 135 elastic force of spring always with the cam 144
It mutually abuts, effect is: driving the cam 144 to rotate by the 4th shaft 146 by the rotary electric machine 150,
The 6th sliding block 143 is driven to rise or fall by the cam structure of the cam 144, to drive the 7th sliding block
134 move up and down and are adjusted to the pressure in the reaction chamber 132 until reaching the required pressure of reaction, thus logical
It crosses cam structure and controls moving up and down for the 7th sliding block 134, play the role of accurately controlling to the pressure inside reaction chamber.
In use, laboratory technician places needs at high temperature under high pressure on the station 168 after opening the dodge gate 131
The chemical reagent of reaction starts the power motor 101 after closing the dodge gate 131, passes through the output shaft 104 and institute
Stating being threadedly engaged between driven shaft 140 and 102 drives the rectangle lower platen 102 to move down, and is pushed by the rectangle
Hydraulic oil in be located remotely from each other two hydraulic cavities 116 is pressed into the other side by plate 102, drives institute by second sliding block 122
It states supporting block 118 to move up, to react by the cooperation between the sealing block 117 and the seal groove 120 by described
Chamber 132 is completely enclosed, while driving the 5th sliding block 161 to move up by the pushing block 121, to drive the through-hole
157 are interconnected with the snorkel 156, while the rectangle lower platen 102 drives the third sliding block 106 by the cold air
Cold air in storage chamber 107 is pressed into the reaction chamber 132, to be reduced the temperature in the reaction chamber 132 by cold air
It pressurizes to the reaction chamber 132, will be opened when temperature reaches required in the reaction chamber 132 by calutron simultaneously
Mouth closing so that cold air stops entering in the reaction chamber 132, while starting the rotary electric machine 150, passes through the cam
144, which drive the 7th sliding block 134 to move up and down, is adjusted the pressure in the reaction chamber 132 until reaching reaction
Required pressure.
The beneficial effects of the present invention are:
The present invention completes the cooling pressure process to reaction chamber by compact drive mechanism, in the process pressurizeed to reaction chamber
Middle indentation cold air reduces the temperature of reaction chamber, while by the cooperation between sealing block and the seal groove in cooling pressurization
Guarantee the leakproofness of reaction chamber in the process, and play the role of further controlling to the pressure in reaction chamber by cam structure,
To ensure that the reaction temperature and pressure that can reach required in reaction chamber, at the same in a longer period of time reaction chamber temperature and
Pressure will not change, and ensure that going on smoothly for reaction, make sufficiently to react between chemical reagent.
Those skilled in the art can define, can in the case of not departing from overall spirit of the invention and design
To make the various modifications for above embodiments, fall within the scope of protection of the present invention, protection scheme of the invention
It is subject to claims appended hereto.
Claims (5)
1. a kind of high-temperature high-pressure reaction kettle with on-line period device, including main casing and it is arranged in the main casing anti-
Answer chamber, it is characterised in that: end wall fixed placement has a station on the downside of the reaction chamber, is arranged in end wall on front side of the reaction chamber
There is a dodge gate, a driving mechanism based on power motor is provided in the main casing, driving mechanism lower end is dynamic
Power is connected with an output shaft, and the driving mechanism upper end drives driven shaft and the output shaft synchronous to rotate by belt wheel transmission,
To drive the pressurizing device in the reaction chamber to move down, pushing is opened simultaneously between cooling device and the reaction chamber
Opening, to be cooled down while compressing the reaction chamber inner space, when the temperature in the reaction chamber reaches default
When value, the pressure in the reaction chamber is further finely adjusted by cam gear, to reach required pressure.
2. a kind of high-temperature high-pressure reaction kettle with on-line period device according to claim 1, it is characterised in that: described
Driving device includes that setting is provided in the upper left power motor of the main casing, the main casing positioned at the power electric
The drive cavity extended above machine and to the right, the power motor upper end is connected by power a first rotating shaft upwardly extended, and institute
It states first rotating shaft upper end rotationally to protrude into the drive cavity, is provided in the drive cavity and is fixedly mounted on described first turn
The driving pulley of axis upper end is provided with the pushing chamber of one or so extension, and the pushing chamber lower end wall and institute in the main casing
Reaction chamber is stated to be connected, it is described to push the second shaft that can be rotatably set about one extension between chamber and the drive cavity,
And the driven shaft lower end is rotatably assorted with end wall on the downside of the pushing chamber and connect, and a fixed installation is provided in the drive cavity
Driven pulley on the upside of the driven shaft has been connected by power a transmission belt between the driving pulley and the driven pulley,
The power motor lower end is connected by power a third shaft extended downwardly, and institute is rotationally protruded into the output shaft lower end
It states to push in chamber and be rotatably assorted with end wall on the downside of the pushing chamber and connect.
3. a kind of high-temperature high-pressure reaction kettle with on-line period device according to claim 1, it is characterised in that: described
Pressurizing device include slidably be arranged in it is described pushing cavity wall between rectangle lower platen, and the output shaft with it is described driven
Axis lower end both passes through the rectangle lower platen and is threadedly engaged with the rectangle lower platen and connect, and rectangle lower platen lower end is solid
Dingan County is equipped with a link block, and the link block is slidably connected with the cavity wall that reacts, and the link block lower end is solid
Dingan County is equipped with one and the annular lower lock block for reacting cavity wall sliding connection, is connected to and sets in end wall on the downside of the reaction chamber
It is equipped with symmetrical mating cavity, the hydraulic cavities on the downside of the mating cavity there are two settings are controlled and are connected between two hydraulic cavities
It is provided with hydraulic pipeline, the annular lower lock block lower end surface is fixedly connected with symmetrical first connecting rod, and left and right two the
One connecting rod lower end is slideably protruded into two hydraulic cavities being located remotely from each other, and downslide can be gone up by being provided between the hydraulic cavity wall
The first dynamic sliding block, and first upper end of slide block face is fixedly connected with the first connecting rod, first sliding block lower end and institute
It states and is fixedly connected with the first spring between end wall on the downside of hydraulic cavities, one is provided in the mating cavity can slide up and down support
Block, the supporting block upper surface are fixedly connected with a sealing block, the annular lower lock block lower end surface be provided with an opening with it is described
The seal groove that sealing block matches, the supporting block lower end surface are fixedly connected with the second connecting rod extended downwardly, and left and right two
Second connecting rod lower end is slideably protruded into two hydraulic cavities close to each other, is mounted slidably between the hydraulic cavity wall
Have the second sliding block being fixedly mounted on the downside of the second connecting rod, second upper end of slide block face and the hydraulic cavities upper end wall it
Between be fixedly connected with symmetrical second spring.
4. a kind of high-temperature high-pressure reaction kettle with on-line period device according to claim 1, it is characterised in that: described
Cooling device includes the cold air storage chamber being arranged on the left of the reaction chamber, is provided with one on the downside of the wall of cold air storage chamber left end
The refrigerator pipe being connected with extraneous cold air is provided with an inlet control valve, the pushing chamber and the cold air on the refrigerator pipe
Third connecting rod is slidably connected between storage chamber, and the third connecting rod upper end is fixed with rectangle lower platen lower end surface
Connection, one is provided between cold air storage cavity wall can slide up and down third sliding block, and the third upper end of slide block with
It is fixedly connected on the downside of the third connecting rod, a L shape delivery pipe, and the L is provided with and communicated in the cold air storage chamber lower end wall
Shape delivery pipe right end is connected with the external world and is fixedly installed a discharge control valve, and one or so perforation is provided in the station
Snorkel, be provided with and communicated with a connecting tube extended downwardly in the middle part of the snorkel lower end wall, and the connecting tube lower end with
The L shape delivery pipe is connected, the electromagnetic cavity being symmetrically provided on the upside of the snorkel in the station, institute
It states and is provided with one between electromagnetism cavity wall and can slide up and down Four-slider, under Four-slider lower end surface and the electromagnetic cavity
Symmetrical third spring is fixedly installed between the wall of side, Four-slider lower end surface is fixedly connected with an armature block,
And the armature block lower end is slidably disposed through end wall on the downside of the electromagnetic cavity, and left and right pair is provided in the snorkel lower end wall
Claim and the electromagnet that is matched with the armature block, is provided with symmetrical sliding slot in the station, and the sliding slot is worn
The snorkel is crossed, the sealing bar that can slide up and down is provided in the sliding slot, one or so perforation is provided in the sealing bar
Through-hole, and the through-hole is staggered with the snorkel when original state, the sealing bar upper surface and the sliding slot upper end
It is fixedly connected with one the 4th spring between wall, one is provided with and communicated in the sliding slot lower end wall and is opened with what the mating cavity was connected
Mouth slot, and the sealing bar lower end is slideably protruded into the open slot, being provided in the open slot can slide up and down
5th sliding block, and the 5th upper end of slide block is fixedly connected with the sealing bar, the supporting block upper surface is fixedly installed with one
Pushing block on the downside of the open slot, and the pushing block slideably protrudes into the open slot.
5. a kind of high-temperature high-pressure reaction kettle with on-line period device according to claim 1, it is characterised in that: described
Cam gear includes that the cam chamber pushed on the upside of chamber in the middle part of end wall is arranged in connection, fixed in end wall on the left of the cam chamber
It is connected with a rotary electric machine, the rotary electric machine right end is connected by power the 4th shaft extended to the right, and described 4th turn
Axis right end is rotatably assorted with end wall on the right side of the cam chamber and connect, and one is provided in the cam chamber and is fixedly connected on the described 4th
The cam of shaft outer surface, one is additionally provided between the cam cavity wall can slide up and down the 6th sliding block, and the described 6th
Sliding block lower end is fixedly connected with a fourth link extended downwardly, and the cam chamber lower end slideably sequentially passes through the square
Protruded into the reaction chamber after shape lower platen, the link block, be provided in the reaction chamber one can slide up and down and with institute
The 7th sliding block that annular lower lock block abuts against is stated, and the 7th upper end of slide block is fixedly connected with the fourth link, described
Symmetrical 5th spring is fixedly connected between seven upper end of slide block faces and the link block, the 6th sliding block is described
It is mutually abutted with the cam always under the action of five spring forces.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910478541.8A CN110038484A (en) | 2019-06-03 | 2019-06-03 | A kind of high-temperature high-pressure reaction kettle with on-line period device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910478541.8A CN110038484A (en) | 2019-06-03 | 2019-06-03 | A kind of high-temperature high-pressure reaction kettle with on-line period device |
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| CN110038484A true CN110038484A (en) | 2019-07-23 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201910478541.8A Withdrawn CN110038484A (en) | 2019-06-03 | 2019-06-03 | A kind of high-temperature high-pressure reaction kettle with on-line period device |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111359559A (en) * | 2020-04-13 | 2020-07-03 | 余文姣 | A biological catalyst ware for high temperature steam |
| CN111361064A (en) * | 2020-04-15 | 2020-07-03 | 王辉 | Be used for novel rubber synthesis device |
| CN111425924A (en) * | 2020-04-27 | 2020-07-17 | 张翠川 | Comprehensive office equipment for enterprise |
| CN113791178A (en) * | 2021-09-16 | 2021-12-14 | 中国恩菲工程技术有限公司 | Sampling detection device and reaction kettle with same |
| CN114625190A (en) * | 2022-03-19 | 2022-06-14 | 江苏新瑞药业有限公司 | Temperature measurement and adjustment method for preparing polypeptide complex and application |
-
2019
- 2019-06-03 CN CN201910478541.8A patent/CN110038484A/en not_active Withdrawn
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111359559A (en) * | 2020-04-13 | 2020-07-03 | 余文姣 | A biological catalyst ware for high temperature steam |
| CN111361064A (en) * | 2020-04-15 | 2020-07-03 | 王辉 | Be used for novel rubber synthesis device |
| CN111425924A (en) * | 2020-04-27 | 2020-07-17 | 张翠川 | Comprehensive office equipment for enterprise |
| CN113791178A (en) * | 2021-09-16 | 2021-12-14 | 中国恩菲工程技术有限公司 | Sampling detection device and reaction kettle with same |
| CN113791178B (en) * | 2021-09-16 | 2024-01-26 | 中国恩菲工程技术有限公司 | Sampling detection device and reaction kettle with same |
| CN114625190A (en) * | 2022-03-19 | 2022-06-14 | 江苏新瑞药业有限公司 | Temperature measurement and adjustment method for preparing polypeptide complex and application |
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Application publication date: 20190723 |
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