CN110031347A - A method of measurement spring steel wire rod segregation - Google Patents

A method of measurement spring steel wire rod segregation Download PDF

Info

Publication number
CN110031347A
CN110031347A CN201910261872.6A CN201910261872A CN110031347A CN 110031347 A CN110031347 A CN 110031347A CN 201910261872 A CN201910261872 A CN 201910261872A CN 110031347 A CN110031347 A CN 110031347A
Authority
CN
China
Prior art keywords
wire rod
segregation
spring steel
hardness
sample
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201910261872.6A
Other languages
Chinese (zh)
Inventor
张博
郭大勇
高航
马立国
王秉喜
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Angang Steel Co Ltd
Original Assignee
Angang Steel Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Angang Steel Co Ltd filed Critical Angang Steel Co Ltd
Priority to CN201910261872.6A priority Critical patent/CN110031347A/en
Publication of CN110031347A publication Critical patent/CN110031347A/en
Pending legal-status Critical Current

Links

Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N3/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N3/40Investigating hardness or rebound hardness
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/20Metals
    • G01N33/202Constituents thereof
    • G01N33/2028Metallic constituents

Abstract

A kind of method that the present invention discloses quantitative determination spring steel wire rod segregation, includes the following steps: that a carries out wire cutting along vertical wire rod rolling direction, then corrodes sample;Then the blackening point that b looks for wire rod transverse direction metallographic phase sample center color most deep measures the HV1 hardness at this using micro-vickers hardness instrument, be then both horizontally and vertically successively spaced 0.5mm~1mm measurement HV1 hardness until measurement to sample edge along by the point;It is very poor that c calculates HV1.

Description

A method of measurement spring steel wire rod segregation
Technical field
The invention belongs to field of steel metallurgy, are related to a kind of with the very poor side to measure spring steel wire rod segregation of HV1 hardness Method.
Background technique
Segregation is to measure one of the important technology index of spring steel wire rod metallurgical quality quality, is segregated the height of controlled level Directly affect the fatigue life length for being finally made spring.The center of wire rod is generally all provided in spring steel wire rod technical protocol Segregation.The evaluation method of center segregation is mainly according to GB/T19530 appendix A or YB/T5365 appendix A, both evaluation method roots It grades according to normal segregation rank map, subjective factor is larger, and does not quantify.
Summary of the invention
It is an object of the invention to propose a kind of method of measurement spring steel wire rod segregation that can quantify.
In order to achieve the above object, the present invention is implemented with the following technical solutions:
A method of measurement spring steel wire rod segregation, it is characterised in that include the following steps:
A carries out wire cutting along vertical wire rod rolling direction, then corrodes sample;
Then the blackening point that b looks for wire rod transverse direction metallographic phase sample center color most deep is measured at this using micro-vickers hardness instrument HV1 hardness, then along by the point both horizontally and vertically successively interval 0.5mm~1mm measurement HV1 hardness until measurement To sample edge;
It is very poor that c calculates HV1.
The erosion sample uses nital.
With the height of HV1 very poor size characterization segregation controlled level, very poor big segregation is big, otherwise segregation is small.
The method of measurement spring steel wire rod segregation of the invention, realizes the segregation of quantitative determination spring steel wire rod.
Specific embodiment
It is illustrated combined with specific embodiments below:
By taking 55SiCr as an example, table 1 is that A steel mill, B steel mill, C steel mill and D steel mill 55SiCr wire rod HV1 hardness are very poor.By table 1 As can be seen that A steel mill, B steel mill, C steel mill and D steel mill 55SiCr wire rod segregation controlled level successively reduce.
1 each producer 55SiCr wire rod cross section HV1 hardness of table is very poor
Steel mill Minimum value Maximum value HV1 is very poor
A 241.4 273.6 32.2
B 229.8 270.7 40.9
C 229.9 291.0 61.1
D 172.3 251.8 79.5

Claims (2)

1. a kind of method of measurement spring steel wire rod segregation, it is characterised in that include the following steps:
A carries out wire cutting along vertical wire rod rolling direction, then corrodes sample;
Then the blackening point that b looks for wire rod transverse direction metallographic phase sample center color most deep measures the HV1 at this using micro-vickers hardness instrument Then hardness measures HV1 hardness until measurement to examination along the 0.5mm~1mm that is both horizontally and vertically successively spaced for passing through the point Sample edge;
It is very poor that c calculates HV1.
2. the method for measurement spring steel wire rod segregation according to claim 1, it is characterised in that: the erosion sample uses Nital.
CN201910261872.6A 2019-04-02 2019-04-02 A method of measurement spring steel wire rod segregation Pending CN110031347A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201910261872.6A CN110031347A (en) 2019-04-02 2019-04-02 A method of measurement spring steel wire rod segregation

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201910261872.6A CN110031347A (en) 2019-04-02 2019-04-02 A method of measurement spring steel wire rod segregation

Publications (1)

Publication Number Publication Date
CN110031347A true CN110031347A (en) 2019-07-19

Family

ID=67237275

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201910261872.6A Pending CN110031347A (en) 2019-04-02 2019-04-02 A method of measurement spring steel wire rod segregation

Country Status (1)

Country Link
CN (1) CN110031347A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110646306A (en) * 2019-11-06 2020-01-03 湖南华菱湘潭钢铁有限公司 Method for evaluating segregation of continuous casting billet through hardness
CN113567281A (en) * 2021-06-22 2021-10-29 武汉钢铁有限公司 Method for quantitatively characterizing center segregation of medium-high carbon wire rod

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102665963A (en) * 2009-12-21 2012-09-12 Posco公司 Martensitic stainless steel and a production method therefor
CN102954976A (en) * 2011-08-19 2013-03-06 鞍钢股份有限公司 Method for quantitatively examining center segregations of wire rod
CN102978355A (en) * 2012-11-30 2013-03-20 张家港浦项不锈钢有限公司 Thermal annealing method for martensite stainless steel, and stainless steel manufactured therefrom
CN103781928A (en) * 2011-10-20 2014-05-07 浦项工科大学校产学协力团 Non-heat treated magnesium alloy sheet with excellent formability at room temperature in which segregation is minimized
CN104535737A (en) * 2014-12-19 2015-04-22 钢铁研究总院 Statistical distribution analysis mapping characterization method for original material position
CN107290199A (en) * 2017-08-10 2017-10-24 南京钢铁股份有限公司 A kind of method that utilization electron probe quickly characterizes bearing steel segregation

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102665963A (en) * 2009-12-21 2012-09-12 Posco公司 Martensitic stainless steel and a production method therefor
CN102954976A (en) * 2011-08-19 2013-03-06 鞍钢股份有限公司 Method for quantitatively examining center segregations of wire rod
CN103781928A (en) * 2011-10-20 2014-05-07 浦项工科大学校产学协力团 Non-heat treated magnesium alloy sheet with excellent formability at room temperature in which segregation is minimized
CN102978355A (en) * 2012-11-30 2013-03-20 张家港浦项不锈钢有限公司 Thermal annealing method for martensite stainless steel, and stainless steel manufactured therefrom
CN104535737A (en) * 2014-12-19 2015-04-22 钢铁研究总院 Statistical distribution analysis mapping characterization method for original material position
CN107290199A (en) * 2017-08-10 2017-10-24 南京钢铁股份有限公司 A kind of method that utilization electron probe quickly characterizes bearing steel segregation

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
任润清 等: "钢丝质量与盘条标准", 《金属制品》 *
王荣: "2CrMoA钢制内齿圈开裂失效分析", 《机械工程材料》 *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110646306A (en) * 2019-11-06 2020-01-03 湖南华菱湘潭钢铁有限公司 Method for evaluating segregation of continuous casting billet through hardness
CN113567281A (en) * 2021-06-22 2021-10-29 武汉钢铁有限公司 Method for quantitatively characterizing center segregation of medium-high carbon wire rod

Similar Documents

Publication Publication Date Title
Bei-fan Body Mass Index in Chinese Adults'
RU2509827C2 (en) Hot formed element and method of its production
Li et al. Determination of the fatigue PSN curves–A critical review and improved backward statistical inference method
CN110031347A (en) A method of measurement spring steel wire rod segregation
CN105445306A (en) Method for evaluating element segregation degree in steel
CN110462085A (en) Martensitic stain less steel material
CN107179749B (en) Hot dip zinc product whole process method of quality control
US20090126492A1 (en) Method for evaluating reliability of steel and high-relaibility steel obtained by the same
CN105203732A (en) Spring steel slab component segregation quantitative analysis method
CN102954976A (en) Method for quantitatively examining center segregations of wire rod
CN107132244A (en) A kind of steel inclusion quantitative evaluation method
JP2013124398A (en) Steel sheet for high strength sour resistant line pipe, and material therefor
EP3249069A1 (en) Rail
CN106908436B (en) The analysis ranking method of manganese sulfide type impurity in steel based on calibration curve
CN112816280B (en) Preparation method of 7XXX series aluminum alloy as-cast single-point spectrum standard sample
JP2014077642A (en) Estimation method of hic sensitivity of steel material and manufacturing method of high strength thick steel plate for line pipe superior in anti hic performance using the same
CN103791862A (en) Method for measuring interval of continuous casting blank dendritic crystal with manganese steel
CN106841208A (en) A kind of method for detecting bulky grain oxide inclusion content in steel
CN105606414A (en) A set of wire spectrum standard samples and preparation method
JP2009041993A (en) Predicting method of residual life of rolling bearing
CN101349635A (en) Method for testing reinforcing steel bar center martensite structure
CN109406524A (en) Aluminium alloy impurity phase quantitative detecting method
JP6044247B2 (en) Method for evaluating the resistance to hydrogen cracking of steel materials and steel sheets for high strength sour line pipes with good resistance to hydrogen cracking
CN107486587B (en) Thinning compensation method for improving control precision of shearing setting model
AU2016202249A1 (en) Grinding Media Fabrication

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication
RJ01 Rejection of invention patent application after publication

Application publication date: 20190719