CN110029489A - A kind of preparation process of cotton yarn - Google Patents
A kind of preparation process of cotton yarn Download PDFInfo
- Publication number
- CN110029489A CN110029489A CN201910393832.7A CN201910393832A CN110029489A CN 110029489 A CN110029489 A CN 110029489A CN 201910393832 A CN201910393832 A CN 201910393832A CN 110029489 A CN110029489 A CN 110029489A
- Authority
- CN
- China
- Prior art keywords
- cotton yarn
- dipping
- cotton
- liquid
- nano particle
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 229920000742 Cotton Polymers 0.000 title claims abstract description 85
- 238000002360 preparation method Methods 0.000 title claims abstract description 21
- 241000219146 Gossypium Species 0.000 claims abstract description 72
- 239000007788 liquid Substances 0.000 claims abstract description 63
- 239000002105 nanoparticle Substances 0.000 claims abstract description 44
- 238000007598 dipping method Methods 0.000 claims abstract description 39
- 239000001301 oxygen Substances 0.000 claims abstract description 18
- 229910052760 oxygen Inorganic materials 0.000 claims abstract description 18
- 229910052754 neon Inorganic materials 0.000 claims abstract description 17
- GKAOGPIIYCISHV-UHFFFAOYSA-N neon atom Chemical compound [Ne] GKAOGPIIYCISHV-UHFFFAOYSA-N 0.000 claims abstract description 17
- 238000004519 manufacturing process Methods 0.000 claims abstract description 15
- 240000000047 Gossypium barbadense Species 0.000 claims abstract description 6
- 235000009429 Gossypium barbadense Nutrition 0.000 claims abstract description 6
- 238000001035 drying Methods 0.000 claims abstract 2
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 17
- 239000002131 composite material Substances 0.000 claims description 16
- 238000012986 modification Methods 0.000 claims description 16
- 230000004048 modification Effects 0.000 claims description 16
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 15
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 12
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 10
- SOQBVABWOPYFQZ-UHFFFAOYSA-N oxygen(2-);titanium(4+) Chemical compound [O-2].[O-2].[Ti+4] SOQBVABWOPYFQZ-UHFFFAOYSA-N 0.000 claims description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 10
- 238000005470 impregnation Methods 0.000 claims description 6
- 239000000377 silicon dioxide Substances 0.000 claims description 6
- UIIMBOGNXHQVGW-DEQYMQKBSA-M Sodium bicarbonate-14C Chemical compound [Na+].O[14C]([O-])=O UIIMBOGNXHQVGW-DEQYMQKBSA-M 0.000 claims description 5
- 238000009835 boiling Methods 0.000 claims description 5
- 235000019441 ethanol Nutrition 0.000 claims description 5
- 239000007789 gas Substances 0.000 claims description 5
- 238000002156 mixing Methods 0.000 claims description 5
- 238000003756 stirring Methods 0.000 claims description 5
- 238000004321 preservation Methods 0.000 claims description 2
- 240000005109 Cryptomeria japonica Species 0.000 claims 2
- 238000003851 corona treatment Methods 0.000 claims 1
- 239000008187 granular material Substances 0.000 claims 1
- 238000001802 infusion Methods 0.000 claims 1
- 238000000034 method Methods 0.000 abstract description 4
- MYMOFIZGZYHOMD-UHFFFAOYSA-N Dioxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 abstract 1
- 239000002585 base Substances 0.000 description 13
- 241000218692 Cryptomeria Species 0.000 description 8
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 8
- 239000000835 fiber Substances 0.000 description 4
- 229910052710 silicon Inorganic materials 0.000 description 4
- 239000010703 silicon Substances 0.000 description 4
- 239000004408 titanium dioxide Substances 0.000 description 4
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 102000004190 Enzymes Human genes 0.000 description 2
- 108090000790 Enzymes Proteins 0.000 description 2
- 238000005265 energy consumption Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000003513 alkali Substances 0.000 description 1
- 238000002306 biochemical method Methods 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 230000008595 infiltration Effects 0.000 description 1
- 238000001764 infiltration Methods 0.000 description 1
- 230000001788 irregular Effects 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 239000001814 pectin Substances 0.000 description 1
- 235000010987 pectin Nutrition 0.000 description 1
- 229920001277 pectin Polymers 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 238000009987 spinning Methods 0.000 description 1
- 238000009955 starching Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000008961 swelling Effects 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
- 239000001993 wax Substances 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M10/00—Physical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. ultrasonic, corona discharge, irradiation, electric currents, or magnetic fields; Physical treatment combined with treatment with chemical compounds or elements
- D06M10/02—Physical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. ultrasonic, corona discharge, irradiation, electric currents, or magnetic fields; Physical treatment combined with treatment with chemical compounds or elements ultrasonic or sonic; Corona discharge
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
- D06M11/46—Oxides or hydroxides of elements of Groups 4 or 14 of the Periodic Table; Titanates; Zirconates; Stannates; Plumbates
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/73—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with carbon or compounds thereof
- D06M11/76—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with carbon or compounds thereof with carbon oxides or carbonates
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/77—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof
- D06M11/79—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof with silicon dioxide, silicic acids or their salts
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/144—Alcohols; Metal alcoholates
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/144—Alcohols; Metal alcoholates
- D06M13/148—Polyalcohols, e.g. glycerol or glucose
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
- D06M2101/06—Vegetal fibres cellulosic
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/10—Repellency against liquids
- D06M2200/11—Oleophobic properties
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Physics & Mathematics (AREA)
- Plasma & Fusion (AREA)
- Health & Medical Sciences (AREA)
- Emergency Medicine (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
Abstract
The present invention provides a kind of preparation process of cotton yarn, the diameter of cotton fiber is 14.0~17.0 μm in cotton yarn, and the mass percent of mature cotton fiber is 55~75%, and the mass percent of long-staple cotton is 80~86%, single thread force >=350CN/tex;Cotton yarn is used at normal temperature weak base complex liquid be mixed with dipping, cotton yarn is subjected to dipping 4-8min processing for the first time using modified Nano particle liquid again, it then takes out, after drying, Quality Pure Cotton Yarn Production is surface-treated using neon/oxygen low temperature plasma under 80-90Pa pressure, cotton yarn is then subjected to second of dipping 10-15min processing using modified Nano particle liquid again, is then taken out, naturally dry.The technique can be improved the wettability of cotton yarn.
Description
Technical field
The invention belongs to textile technology fields, and in particular to a kind of preparation process of cotton yarn.
Background technique
Cotton fiber natural commensal containing there are many, such as the oil in cotton wax, pectin, nitrogen substance, ash content and spinning process
Agent or greasy dirt etc., these impurity cause starching irregular if do not removed the infiltration that will affect slurries in the yarn and wettability.It passes
The cotton yarn treatment process of system has one step single bath process of alkali oxygen and biochemical method.The former be in the state of high temperature highly basic to yarn at
Reason, energy consumption is high and will increase the swelling of fiber, influences yarn property.The latter is using enzyme as pretreating reagent, although before reducing
Treatment temperature and production energy consumption, but due to the use scope and specificity of enzyme itself, also allow the application of this pre-treating technology
Certain limitation is received, therefore, how to obtain a kind of can be improved cotton yarn wettability again and will not reducing the place of mechanical property
Science and engineering skill is current technical problem to be solved.
Summary of the invention
The purpose of the present invention is being directed to existing problem, a kind of preparation process of cotton yarn is provided, which can be improved cotton
The wettability of yarn.
In order to achieve the object of the present invention, the present invention is implemented by following scheme:
A kind of preparation process of cotton yarn, the diameter of cotton fiber is 14.0~17.0 μm in cotton yarn, the quality of mature cotton fiber
Percentage is 55~75%, and the mass percent of long-staple cotton is 80~86%, single thread force >=350CN/tex;Including following step
It is rapid:
(1) weak base complex liquid cotton yarn is used at normal temperature to be mixed with dipping, impregnation pressure 2.5-2.9MPa, dip time
For 50-60min;The weak base complex liquid is made of the following components by weight: 3.0-4.0 parts of sodium bicarbonate, ethyl alcohol 3-7
Part, 1-5 parts of glycerol, 30-38 parts of water;The weak base complex liquid and cotton yarn mixed proportion is 100mL:(20~40) g;
(2) nano-titanium dioxide is uniformly mixed with nano silica, the nano-titanium dioxide and nanometer titanium dioxide
The mixing mass ratio of silicon is 1:(2~4), composite nanoparticle is obtained, composite nanoparticle is uniformly mixed with modification liquid, then
Impregnated ground is handled 4 hours under vacuum, obtains modified Nano particle liquid;The modification liquid is the preparation method comprises the following steps: take a certain amount of
Then cryptomeria leaf adds 8 times of clear water of cryptomeria leaf quality, is heated to 90 DEG C, under 20MPa pressure, with the stirring of 3800r/min revolving speed
1h, is then again heated to boiling, after heat preservation 10min, then cooled to room temperature, be filtered to get;The composite Nano
Particle and modification liquid mixed proportion are 100g:(180-220) mL;
(3) cotton yarn is first subjected to dipping 4-8min processing for the first time using modified Nano particle liquid, then takes out, dries
Afterwards, Quality Pure Cotton Yarn Production is surface-treated using neon/oxygen low temperature plasma under 80-90Pa pressure, then again by cotton yarn
Second of dipping 10-15min processing is carried out using modified Nano particle liquid, is then taken out, naturally dry.
Preferably, vacuum degree is 0.010MPa in dipping under step (2) described vacuum.
Preferably, gas flow neon is 0.40mL/ in step (3) neon/oxygen Low Temperature Plasma Treating
Min, oxygen 0.08mL/min, processing time are 45s, power 70w.
Preferably, cotton yarn and modified Nano particle liquid mixed proportion are 100g in step (3) the first time dipping:
(250-400) mL, dipping temperature are 78 DEG C.
Preferably, Quality Pure Cotton Yarn Production and modified Nano particle liquid mixed proportion are 100g in step (3) second of dipping:
(200-300) mL, dipping temperature are 82 DEG C.
The contact angle of the present invention treated cotton is substantially reduced, and cotton wettability is significantly improved;This
Invention carries out room temperature processing to Quality Pure Cotton Yarn Production by using the weak base complex liquid of preparation under a certain pressure, can effectively make yarn
Many channels are formed in line between fiber and fiber, these channels make yarn have wicking, and liquid exists along these channels
Do not have to flow under the action of external force field, so as to effectively improve the wettability of Quality Pure Cotton Yarn Production, by using the modification of preparation
Then liquid and the compound obtained modified Nano particle liquid of composite nanoparticle are assisted again after modified Nano particle liquid impregnation
It uses neon/oxygen low temperature plasma to be surface-treated Quality Pure Cotton Yarn Production under 80-90Pa pressure, can significantly enhance
While purified cotton yarns fiber strength, the also limited contact angle for reducing purified cotton yarns surface further improves pure cotton
The wettability of yarn.
Specific embodiment
The present invention will be further described with reference to the examples below.
Embodiment 1
A kind of preparation process of cotton yarn, the diameter of cotton fiber is 14.0 μm in cotton yarn, the mass percent of mature cotton fiber
It is 55%, the mass percent of long-staple cotton is 80%, single thread force >=350CN/tex;The following steps are included:
(1) weak base complex liquid cotton yarn is used at normal temperature to be mixed with dipping, impregnation pressure 2.5-2.9MPa, dip time
For 50-60min;The weak base complex liquid is made of the following components by weight: 3.0-4.0 parts of sodium bicarbonate, ethyl alcohol 3-7
Part, 1-5 parts of glycerol, 30-38 parts of water;The weak base complex liquid and cotton yarn mixed proportion is 100mL:(20~40) g;
(2) nano-titanium dioxide is uniformly mixed with nano silica, the nano-titanium dioxide and nanometer titanium dioxide
The mixing mass ratio of silicon is 1:(2~4), composite nanoparticle is obtained, composite nanoparticle is uniformly mixed with modification liquid, then
In the case where vacuum degree is the vacuum of 0.010MPa, impregnated ground is handled 4 hours, obtains modified Nano particle liquid;The modification liquid preparation
Method are as follows: a certain amount of cryptomeria leaf is taken, 8 times of clear water of cryptomeria leaf quality is then added, is heated to 90 DEG C, under 20MPa pressure, with
3800r/min revolving speed stirs 1h, is then again heated to boiling, after keeping the temperature 10min, then cooled to room temperature, is filtered, i.e.,
?;The composite nanoparticle and modification liquid mixed proportion is 100g:(180-220) mL;
(3) cotton yarn is first subjected to dipping 4-8min processing for the first time using modified Nano particle liquid, then takes out, dries
Afterwards, Quality Pure Cotton Yarn Production is surface-treated using neon/oxygen low temperature plasma under 80-90Pa pressure, then again by cotton yarn
Second of dipping 10-15min processing is carried out using modified Nano particle liquid, is then taken out, naturally dry;The neon/
In oxygen Low Temperature Plasma Treating gas flow neon be 0.40mL/min, oxygen 0.08mL/min, processing the time be
45s, power 70w;Cotton yarn and modified Nano particle liquid mixed proportion are 100g:(250-400 in dipping for the first time) mL, dipping
Temperature is 78 DEG C;Quality Pure Cotton Yarn Production and modified Nano particle liquid mixed proportion are 100g:(200-300 in second of dipping) mL, dipping
Temperature is 82 DEG C.
Embodiment 2
A kind of preparation process of cotton yarn, the diameter of cotton fiber is 15.0 μm in cotton yarn, the mass percent of mature cotton fiber
It is 65%, the mass percent of long-staple cotton is 83%, single thread force >=350CN/tex;The following steps are included:
(1) weak base complex liquid cotton yarn is used at normal temperature to be mixed with dipping, impregnation pressure 2.5-2.9MPa, dip time
For 50-60min;The weak base complex liquid is made of the following components by weight: 3.0-4.0 parts of sodium bicarbonate, ethyl alcohol 3-7
Part, 1-5 parts of glycerol, 30-38 parts of water;The weak base complex liquid and cotton yarn mixed proportion is 100mL:(20~40) g;
(2) nano-titanium dioxide is uniformly mixed with nano silica, the nano-titanium dioxide and nanometer titanium dioxide
The mixing mass ratio of silicon is 1:(2~4), composite nanoparticle is obtained, composite nanoparticle is uniformly mixed with modification liquid, then
In the case where vacuum degree is the vacuum of 0.010MPa, impregnated ground is handled 4 hours, obtains modified Nano particle liquid;The modification liquid preparation
Method are as follows: a certain amount of cryptomeria leaf is taken, 8 times of clear water of cryptomeria leaf quality is then added, is heated to 90 DEG C, under 20MPa pressure, with
3800r/min revolving speed stirs 1h, is then again heated to boiling, after keeping the temperature 10min, then cooled to room temperature, is filtered, i.e.,
?;The composite nanoparticle and modification liquid mixed proportion is 100g:(180-220) mL;
(3) cotton yarn is first subjected to dipping 4-8min processing for the first time using modified Nano particle liquid, then takes out, dries
Afterwards, Quality Pure Cotton Yarn Production is surface-treated using neon/oxygen low temperature plasma under 80-90Pa pressure, then again by cotton yarn
Second of dipping 10-15min processing is carried out using modified Nano particle liquid, is then taken out, naturally dry;The neon/
In oxygen Low Temperature Plasma Treating gas flow neon be 0.40mL/min, oxygen 0.08mL/min, processing the time be
45s, power 70w;Cotton yarn and modified Nano particle liquid mixed proportion are 100g:(250-400 in dipping for the first time) mL, dipping
Temperature is 78 DEG C;Quality Pure Cotton Yarn Production and modified Nano particle liquid mixed proportion are 100g:(200-300 in second of dipping) mL, dipping
Temperature is 82 DEG C.
Embodiment 3
A kind of preparation process of cotton yarn, the diameter of cotton fiber is 17.0 μm in cotton yarn, the mass percent of mature cotton fiber
It is 75%, the mass percent of long-staple cotton is 86%, single thread force >=350CN/tex;The following steps are included:
(1) weak base complex liquid cotton yarn is used at normal temperature to be mixed with dipping, impregnation pressure 2.5-2.9MPa, dip time
For 50-60min;The weak base complex liquid is made of the following components by weight: 3.0-4.0 parts of sodium bicarbonate, ethyl alcohol 3-7
Part, 1-5 parts of glycerol, 30-38 parts of water;The weak base complex liquid and cotton yarn mixed proportion is 100mL:(20~40) g;
(2) nano-titanium dioxide is uniformly mixed with nano silica, the nano-titanium dioxide and nanometer titanium dioxide
The mixing mass ratio of silicon is 1:(2~4), composite nanoparticle is obtained, composite nanoparticle is uniformly mixed with modification liquid, then
In the case where vacuum degree is the vacuum of 0.010MPa, impregnated ground is handled 4 hours, obtains modified Nano particle liquid;The modification liquid preparation
Method are as follows: a certain amount of cryptomeria leaf is taken, 8 times of clear water of cryptomeria leaf quality is then added, is heated to 90 DEG C, under 20MPa pressure, with
3800r/min revolving speed stirs 1h, is then again heated to boiling, after keeping the temperature 10min, then cooled to room temperature, is filtered, i.e.,
?;The composite nanoparticle and modification liquid mixed proportion is 100g:(180-220) mL;
(3) cotton yarn is first subjected to dipping 4-8min processing for the first time using modified Nano particle liquid, then takes out, dries
Afterwards, Quality Pure Cotton Yarn Production is surface-treated using neon/oxygen low temperature plasma under 80-90Pa pressure, then again by cotton yarn
Second of dipping 10-15min processing is carried out using modified Nano particle liquid, is then taken out, naturally dry;The neon/
In oxygen Low Temperature Plasma Treating gas flow neon be 0.40mL/min, oxygen 0.08mL/min, processing the time be
45s, power 70w;Cotton yarn and modified Nano particle liquid mixed proportion are 100g:(250-400 in dipping for the first time) mL, dipping
Temperature is 78 DEG C;Quality Pure Cotton Yarn Production and modified Nano particle liquid mixed proportion are 100g:(200-300 in second of dipping) mL, dipping
Temperature is 82 DEG C.
Claims (5)
1. a kind of preparation process of cotton yarn, which is characterized in that the diameter of cotton fiber is 14.0~17.0 μm in cotton yarn, and ripe cotton is fine
The mass percent of dimension is 55~75%, and the mass percent of long-staple cotton is 80~86%, single thread force >=350CN/tex;Packet
Include following steps:
(1) cotton yarn is used to the hybrid infusion of weak base complex liquid, impregnation pressure 2.5-2.9MPa at normal temperature, dip time is
50-60min;The weak base complex liquid is made of the following components by weight: 3.0-4.0 parts of sodium bicarbonate, 3-7 parts of ethyl alcohol,
1-5 parts of glycerol, 30-38 parts of water;The weak base complex liquid and cotton yarn mixed proportion is 100mL:(20~40) g;
(2) nano-titanium dioxide is uniformly mixed with nano silica, the nano-titanium dioxide and nano silica
Mixing mass ratio is 1:(2~4), composite nanoparticle is obtained, composite nanoparticle is uniformly mixed with modification liquid, then true
The lower impregnated ground of sky is handled 4 hours, obtains modified Nano particle liquid;The modification liquid is the preparation method comprises the following steps: take a certain amount of cryptomeria
Then leaf adds 8 times of clear water of cryptomeria leaf quality, is heated to 90 DEG C, under 20MPa pressure, stir 1h with 3800r/min revolving speed,
Then be again heated to boiling, after heat preservation 10min, then cooled to room temperature, be filtered to get;The composite nano-granule
Son is 100g:(180-220 with modification liquid mixed proportion) mL;
(3) cotton yarn is first subjected to dipping 4-8min processing for the first time using modified Nano particle liquid, then taken out, after drying,
Quality Pure Cotton Yarn Production is surface-treated using neon/oxygen low temperature plasma under 80-90Pa pressure, then cotton yarn is used again and is changed
Property nanoparticle liquid carry out second dipping 10-15min processing, then take out, naturally dry.
2. a kind of preparation process of cotton yarn as described in claim 1, which is characterized in that under step (2) described vacuum in dipping
Vacuum degree is 0.010MPa.
3. a kind of preparation process of cotton yarn as described in claim 1, which is characterized in that step (3) neon/oxygen low temperature
In corona treatment gas flow neon be 0.40mL/min, oxygen 0.08mL/min, the processing time is 45s, and power is
70w。
4. a kind of preparation process of cotton yarn as described in claim 1, which is characterized in that in step (3) the first time dipping
Cotton yarn and modified Nano particle liquid mixed proportion are 100g:(250-400) mL, dipping temperature is 78 DEG C.
5. a kind of preparation process of cotton yarn as described in claim 1, which is characterized in that in step (3) second of dipping
Quality Pure Cotton Yarn Production and modified Nano particle liquid mixed proportion are 100g:(200-300) mL, dipping temperature is 82 DEG C.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201910393832.7A CN110029489A (en) | 2019-05-13 | 2019-05-13 | A kind of preparation process of cotton yarn |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201910393832.7A CN110029489A (en) | 2019-05-13 | 2019-05-13 | A kind of preparation process of cotton yarn |
Publications (1)
Publication Number | Publication Date |
---|---|
CN110029489A true CN110029489A (en) | 2019-07-19 |
Family
ID=67242009
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201910393832.7A Pending CN110029489A (en) | 2019-05-13 | 2019-05-13 | A kind of preparation process of cotton yarn |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN110029489A (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108914285A (en) * | 2018-09-06 | 2018-11-30 | 海安联发棉纺有限公司 | The conformal Quality Pure Cotton Yarn Production of height and its production method of highly dense crease resistant fabric |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104911909A (en) * | 2015-05-29 | 2015-09-16 | 安徽省含山县顺天纺织有限公司 | Strength-improvable blended regenerated cotton yarn and preparation method thereof |
CN108796728A (en) * | 2018-08-17 | 2018-11-13 | 安徽天源纺织有限公司 | A kind of degerming hydrophobic type cotton and preparation method thereof |
CN109162090A (en) * | 2018-09-13 | 2019-01-08 | 合肥巧织纺织科技有限公司 | A kind for the treatment of process improving Quality Pure Cotton Yarn Production wettability |
-
2019
- 2019-05-13 CN CN201910393832.7A patent/CN110029489A/en active Pending
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104911909A (en) * | 2015-05-29 | 2015-09-16 | 安徽省含山县顺天纺织有限公司 | Strength-improvable blended regenerated cotton yarn and preparation method thereof |
CN108796728A (en) * | 2018-08-17 | 2018-11-13 | 安徽天源纺织有限公司 | A kind of degerming hydrophobic type cotton and preparation method thereof |
CN109162090A (en) * | 2018-09-13 | 2019-01-08 | 合肥巧织纺织科技有限公司 | A kind for the treatment of process improving Quality Pure Cotton Yarn Production wettability |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108914285A (en) * | 2018-09-06 | 2018-11-30 | 海安联发棉纺有限公司 | The conformal Quality Pure Cotton Yarn Production of height and its production method of highly dense crease resistant fabric |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN101591854B (en) | Nano durable super hydrophobicity finishing method for cellulose fabric | |
CN103225203B (en) | Preparation method of carbon fiber-graphene oxide-carbon nanotube multi-scale reinforcement | |
CN102296464B (en) | Wook lubricating oil, preparation method for wook lubricating oil, and application of wook lubricating oil in improvement of fiber spinning performance | |
CN103361768A (en) | Surface modification method of polyacrylonitrile-based carbon fiber | |
CN103835002B (en) | A kind of bluish dogbane low-temperature plasma and Bio-enzyme Combined Pre-treatment Degumming method | |
CN103132311A (en) | Ecological and environment-friendly high-count cotton yarn sizing method | |
CN102311505B (en) | Method for preparing cellulose nanospheres based on waste dissolvable fibers | |
CN107988713A (en) | A kind of method for preparing carbon nano-fiber non-woven fabrics using coal hydroliquefaction residue base pitch alkenes material | |
CN107419553A (en) | A kind of colouring method of silicon substrate non-aqueous media suitable for reactive dye | |
AU2020100083A4 (en) | Preparation method of basalt fiber paper | |
CN107190513A (en) | The method of the twice-modified chopped carbon fiber of polyethyleneimine | |
CN101270547A (en) | Method for processing nano-function textile | |
CN108330564A (en) | A kind of high-performance heatproof textile fabric and its preparation process | |
CN110029489A (en) | A kind of preparation process of cotton yarn | |
CN104004104B (en) | A kind of method of ramie nano-cellulose hydrophobic modification | |
CN106751799B (en) | A kind of basalt fibre reinforced polyamide composite material and preparation method | |
CN101962912A (en) | Method for manufacturing super absorbent acrylon | |
CN108395202A (en) | A kind of preparation method of fibre modification aerogel material | |
CN102953159A (en) | Production method of carbon fibers | |
CN111172624B (en) | Preparation method of carbon/silicon hybrid fiber and carbon-silicon hybrid fiber | |
CN109162090B (en) | A kind for the treatment of process improving Quality Pure Cotton Yarn Production wettability | |
CN110804885A (en) | Method for improving dye-uptake of flax blended fiber fabric | |
CN108977930A (en) | A kind of high strength acid resistant alkali tencel | |
CN110130100B (en) | Continuous sintering method of boron-containing SiC fibers | |
CN102899881A (en) | Method for preparing super-hydrophilic polyester fabric with sulfuric acid |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
PB01 | Publication | ||
PB01 | Publication | ||
SE01 | Entry into force of request for substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
RJ01 | Rejection of invention patent application after publication |
Application publication date: 20190719 |
|
RJ01 | Rejection of invention patent application after publication |