CN110029302A - The coating spraying tooling of matrix of samples for the observation of coating material original position stretching - Google Patents
The coating spraying tooling of matrix of samples for the observation of coating material original position stretching Download PDFInfo
- Publication number
- CN110029302A CN110029302A CN201910368708.5A CN201910368708A CN110029302A CN 110029302 A CN110029302 A CN 110029302A CN 201910368708 A CN201910368708 A CN 201910368708A CN 110029302 A CN110029302 A CN 110029302A
- Authority
- CN
- China
- Prior art keywords
- fixed
- coating
- matrix
- barrier bed
- fixed section
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000000576 coating method Methods 0.000 title claims abstract description 137
- 239000011248 coating agent Substances 0.000 title claims abstract description 135
- 239000011159 matrix material Substances 0.000 title claims abstract description 84
- 239000000463 material Substances 0.000 title claims abstract description 72
- 238000005507 spraying Methods 0.000 title claims abstract description 65
- 230000004888 barrier function Effects 0.000 claims abstract description 93
- 125000006850 spacer group Chemical group 0.000 claims description 24
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 6
- 229910052742 iron Inorganic materials 0.000 claims description 3
- 208000037656 Respiratory Sounds Diseases 0.000 abstract description 12
- 230000007246 mechanism Effects 0.000 abstract description 7
- 238000004458 analytical method Methods 0.000 abstract description 6
- 238000003780 insertion Methods 0.000 abstract description 5
- 230000037431 insertion Effects 0.000 abstract description 5
- 238000000034 method Methods 0.000 description 42
- 230000008569 process Effects 0.000 description 22
- 238000012360 testing method Methods 0.000 description 11
- 230000008859 change Effects 0.000 description 7
- 239000007921 spray Substances 0.000 description 6
- 238000005336 cracking Methods 0.000 description 5
- 230000033001 locomotion Effects 0.000 description 5
- 238000005422 blasting Methods 0.000 description 4
- 238000010586 diagram Methods 0.000 description 4
- 238000012545 processing Methods 0.000 description 4
- 238000011282 treatment Methods 0.000 description 4
- 230000023753 dehiscence Effects 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 238000002474 experimental method Methods 0.000 description 3
- 238000011065 in-situ storage Methods 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- 230000003321 amplification Effects 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 238000005524 ceramic coating Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 238000003199 nucleic acid amplification method Methods 0.000 description 2
- 238000005240 physical vapour deposition Methods 0.000 description 2
- 238000005452 bending Methods 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 230000001276 controlling effect Effects 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000002596 correlated effect Effects 0.000 description 1
- 230000008878 coupling Effects 0.000 description 1
- 238000010168 coupling process Methods 0.000 description 1
- 238000005859 coupling reaction Methods 0.000 description 1
- 238000006073 displacement reaction Methods 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 230000005489 elastic deformation Effects 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 238000004049 embossing Methods 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 230000000977 initiatory effect Effects 0.000 description 1
- 230000001788 irregular Effects 0.000 description 1
- 238000010422 painting Methods 0.000 description 1
- 238000007750 plasma spraying Methods 0.000 description 1
- 238000005498 polishing Methods 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 230000001360 synchronised effect Effects 0.000 description 1
- 238000009864 tensile test Methods 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C4/00—Coating by spraying the coating material in the molten state, e.g. by flame, plasma or electric discharge
- C23C4/12—Coating by spraying the coating material in the molten state, e.g. by flame, plasma or electric discharge characterised by the method of spraying
- C23C4/134—Plasma spraying
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N23/00—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00
- G01N23/22—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by measuring secondary emission from the material
- G01N23/2202—Preparing specimens therefor
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N23/00—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00
- G01N23/22—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by measuring secondary emission from the material
- G01N23/225—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by measuring secondary emission from the material using electron or ion
- G01N23/2251—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by measuring secondary emission from the material using electron or ion using incident electron beams, e.g. scanning electron microscopy [SEM]
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N3/00—Investigating strength properties of solid materials by application of mechanical stress
- G01N3/02—Details
- G01N3/06—Special adaptations of indicating or recording means
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N3/00—Investigating strength properties of solid materials by application of mechanical stress
- G01N3/08—Investigating strength properties of solid materials by application of mechanical stress by applying steady tensile or compressive forces
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2203/00—Investigating strength properties of solid materials by application of mechanical stress
- G01N2203/0014—Type of force applied
- G01N2203/0016—Tensile or compressive
- G01N2203/0017—Tensile
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2203/00—Investigating strength properties of solid materials by application of mechanical stress
- G01N2203/02—Details not specific for a particular testing method
- G01N2203/026—Specifications of the specimen
- G01N2203/0262—Shape of the specimen
- G01N2203/0278—Thin specimens
- G01N2203/0282—Two dimensional, e.g. tapes, webs, sheets, strips, disks or membranes
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2203/00—Investigating strength properties of solid materials by application of mechanical stress
- G01N2203/02—Details not specific for a particular testing method
- G01N2203/06—Indicating or recording means; Sensing means
- G01N2203/0641—Indicating or recording means; Sensing means using optical, X-ray, ultraviolet, infrared or similar detectors
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2203/00—Investigating strength properties of solid materials by application of mechanical stress
- G01N2203/02—Details not specific for a particular testing method
- G01N2203/06—Indicating or recording means; Sensing means
- G01N2203/067—Parameter measured for estimating the property
- G01N2203/0682—Spatial dimension, e.g. length, area, angle
Abstract
The invention discloses a kind of coating spraying toolings of matrix of samples for the observation of coating material original position stretching, and the coating spraying tooling includes: the first barrier bed, and first barrier bed wraps up the first fixed section；Second barrier bed, second barrier bed wrap up the second fixed section；First fixed pin, the first fixed pin insertion first positioning hole is interior and passes through first barrier bed；Second fixed pin, the second fixed pin insertion second location hole is interior and passes through second barrier bed；Fixture, the fixture is for clamping multiple matrix of samples and making the spray-coating surface of multiple matrix of samples towards same direction.Coating spraying tooling according to an embodiment of the present invention can in the matrix of samples of small size spray-on coating, so as to be placed in scanning electronic microscope observation, and then it is conducive to the micromechanism of damage of analysis the coating material germinating of crackle and extension mechanism and material during stretching.
Description
Technical field
The present invention relates to coating testing experiment fields, more particularly, to a kind of examination for the observation of coating material original position stretching
The coating spraying tooling of sample matrix.
Background technique
Probing into for coating material mechanics properties testing and micromechanism of damage in the related technology is usually tried using universal tensile
Machine is tested to carry out under macro-scale, for example, by using the tension crack process of the method observation coating of high resolution camera shooting, and
In conjunction with the strain variation situation of Digital Image Correlation Method measurement coating front surface.
Since coating material mostly passes through what the methods of plasma spraying or physical vapour deposition (PVD) were prepared, due to spray
The particularity of coating method, the coating thickness of coating material may be subjected to limitation, such as the spraying system of certain ceramic coating materials
Standby thickness is generally within the scope of tens microns to several millimeters, since thickness is smaller, even if so utilizing under macro-scale
High resolution camera also it is more difficult in detail observe coating material dehiscence process, coating material can not be effectively observed and stretched
The micromechanism of damage of the germinating of crackle and extension mechanism and material in journey.
Summary of the invention
The present invention is directed at least solve one of the technical problems existing in the prior art.For this purpose, one object of the present invention
It is to propose a kind of coating spraying tooling of matrix of samples for the observation of coating material original position stretching, the coating spraying tooling energy
Enough spray-on coatings in the matrix of samples of small size so as to be placed in scanning electronic microscope observation, and then are conducive to analysis coating
The micromechanism of damage of the material germinating of crackle and extension mechanism and material during stretching.
Embodiment according to the present invention proposes a kind of coating spray of matrix of samples for the observation of coating material original position stretching
Tooling is applied, the matrix of samples is including the first fixed section, the second fixed section and is connected to first fixed section and described second
Linkage section between fixed section, the width of first fixed section is equal with the width of second fixed section and is greater than the company
The width of section is connect, first fixed section is equipped with first positioning hole, and second fixed section is equipped with second location hole, the connection
Section is equipped with spray-coating surface, and the coating spraying tooling includes: the first barrier bed, and the first barrier bed package described first is fixed
Section；Second barrier bed, second barrier bed wrap up second fixed section；First fixed pin, the first fixed pin insertion
In the first positioning hole and pass through first barrier bed；Second fixed pin, the second fixed pin insertion described second are fixed
In the hole of position and pass through second barrier bed；Fixture, the fixture is for clamping multiple matrix of samples and making multiple described
The spray-coating surface of matrix of samples is towards same direction.
Coating spraying tooling according to an embodiment of the present invention can in the matrix of samples of small size spray-on coating, so as to
Be placed in scanning electronic microscope observation, so be conducive to analysis coating material during stretching the germinating of crackle and extension mechanism with
And the micromechanism of damage of material.
Some specific embodiments according to the present invention, the thickness of the thickness of first fixed section, second fixed section
It is equal to each other with the thickness of the linkage section, the spray-coating surface is formed in the upper surface of the linkage section；Each described first is solid
Determine section and is enclosed with the first barrier bed respectively, respectively inserted with the first fixed pin in each first positioning hole, each described
Two fixed sections are enclosed with the second barrier bed respectively, respectively inserted with the second fixed pin in each second location hole.
Further, the both ends of first barrier bed bypass two lateral edges and the interval setting of first fixed section respectively
To avoid first fixed pin；The both ends of second barrier bed bypass two lateral edges of second fixed section and interval respectively
It is arranged to avoid second fixed pin.
Further, the fixture includes: bottom plate；First side clamping plate and second side clamping plate, first side clamping plate and institute
State the opposite sides edge that second side clamping plate is respectively arranged on the bottom plate, first side clamping plate, second side clamping plate and described
Bottom plate limits clip slot jointly, and the second fixed section of multiple matrix of samples is set in the clip slot.
Further, the height of second side clamping plate is higher than the height of first side clamping plate.
Some specific embodiments according to the present invention, the thickness of the thickness of first fixed section and second fixed section
Thickness that is equal and being less than the linkage section, the spray-coating surface are formed in the side surface of the linkage section；First barrier bed
The first fixed section of multiple matrix of samples is integrally wrapped up, second barrier bed integrally wraps up the second fixation of multiple matrix of samples
Section.
Further, the both ends of first barrier bed are rotating around outermost two in excessively multiple first fixed sections, and
The both ends interval of first barrier bed is arranged to allow at least one first fixed section to pass through；The both ends of second barrier bed
Rotating around outermost two in excessively multiple second fixed sections, and the both ends interval of second barrier bed is arranged to allow at least
One the second fixed section passes through.
Further, the coating spraying tooling further include: multiple first spacer blocks, each first spacer block are set to
Between adjacent first fixed section；Multiple second spacer blocks, each second spacer block are set between adjacent second fixed section.
Further, multiple first fixed sections share first fixed pin and first fixed pin passes through multiple institutes
State the first spacer block；Multiple second fixed sections share second fixed pin and second fixed pin passes through between multiple described second
Spacer block.
Some specific examples according to the present invention, first barrier bed and second barrier bed are iron sheet.
Additional aspect and advantage of the invention will be set forth in part in the description, and will partially become from the following description
Obviously, or practice through the invention is recognized.
Detailed description of the invention
Above-mentioned and/or additional aspect of the invention and advantage will become from the description of the embodiment in conjunction with the following figures
Obviously and it is readily appreciated that, in which:
Fig. 1 is the structural schematic diagram of coating material original position stretching observation system according to an embodiment of the present invention.
Fig. 2 is the structural representation of the matrix of samples of coating material original position stretching observation system according to an embodiment of the present invention
Figure.
Fig. 3 is the structure of the matrix of samples of coating material original position stretching observation system in accordance with another embodiment of the present invention
Schematic diagram.
Fig. 4 is the structural schematic diagram of matrix of samples according to an embodiment of the present invention and its coating spraying tooling.
Fig. 5 is the structural schematic diagram of matrix of samples in accordance with another embodiment of the present invention and its coating spraying tooling.
Fig. 6 is the flow chart of the coating spraying method of matrix of samples according to an embodiment of the present invention.
Appended drawing reference:
Coating material original position stretching observation system 1,
Original position stretching machine 100, workbench 110, slide rail 111, anticreep groove 112, the first objective table 120, first folder
Plate 121, the first threaded hole 122, the first dowel hole 123, the second objective table 130, second clamping plate 131, the second threaded hole 132,
Second dowel hole 133, driver 140, sliding guide 141, drive screw 142,
Matrix of samples 200, the first fixed section 210, first positioning hole 211, the second fixed section 220, second location hole 221,
Linkage section 230, spray-coating surface 231,
Sample bin 400,
First barrier bed 510, the second barrier bed 520, the first fixed pin 530, the second fixed pin 540,
Fixture 600, bottom plate 610, the first side clamping plate 620, second side clamping plate 630,
First spacer block 710, the second spacer block 720.
Specific embodiment
The embodiment of the present invention is described below in detail, examples of the embodiments are shown in the accompanying drawings, wherein from beginning to end
Same or similar label indicates same or similar element or element with the same or similar functions.Below with reference to attached
The embodiment of figure description is exemplary, and for explaining only the invention, and is not considered as limiting the invention.
In the description of the present invention, it is to be understood that, term " center ", " longitudinal direction ", " transverse direction ", " length ", " width ",
" thickness ", "upper", "lower", "front", "rear", "left", "right", "vertical", "horizontal", "top", "bottom", "inner", "outside", " up time
The orientation or positional relationship of the instructions such as needle ", " counterclockwise ", " axial direction ", " radial direction ", " circumferential direction " be orientation based on the figure or
Positional relationship is merely for convenience of description of the present invention and simplification of the description, rather than the device or element of indication or suggestion meaning must
There must be specific orientation, be constructed and operated in a specific orientation, therefore be not considered as limiting the invention.In the present invention
Description in, " fisrt feature ", " second feature " may include one or more of the features.In the description of the present invention,
The meaning of " plurality " is two or more.
Coating material mechanics properties testing and micromechanism of damage are probed into the related technology and tested mostly using universal tensile
Machine carries out under macro-scale, generallys use the tension crack process of the method observation coating of high resolution camera shooting, and ties
Close the strain variation situation of Digital Image Correlation Method measurement coating front surface.
It needs to make tensile sample matrix under normal conditions, coating material to be tested is then sprayed on basis material, it
Typical spray speckle is carried out to coating material surface afterwards, it is therefore an objective to calculate strain for subsequent digital image correlation method and mark is provided
Point.Tension test is carried out to tensile sample using universal tensile testing machine after being ready to complete, needs to utilize height in experimentation
Resolution camera records drawing process to observe the detailed process of coating cracking, and serialograph, so as to utilize number
The strain variation situation of word DIC Method calculating coating front surface.
The changing rule of speckle during stretching is calculated using digital picture related algorithm, obtains strain stress relation.It will apply
Layer material is broadly divided into 4 stages to face crack cracking in receiving tensile load:
(1) when coating just starts to bear tensile load, irregular variation is presented in strain；
(2) with the increase of tensile load, coating surface strain is orderly fluctuation status, is similar to sine curve, maximum
Strain is respectively wave crest and trough with minimum strain, and wave crest and trough are constantly mobile to same direction；
(3) when tensile load reaches certain phase, the fraction areal strain of coating is sharply increased；
(4) it when the strain of the coating area sharply increased reaches capacity, i.e., the stress in region reaches ultimate tensile, applies
Layer is broken.
But since coating is too thin, this method can only detect coating surface strain variation and crack propagation, can not observe
The changing rule extended to the lateral position Interface Crack and face crack of coating to Interface Crack.
The observing interface crackle and face crack generallyd use to the method that Interface Crack extends be by controlling omnipotent examination
Test the load gradual change realization of machine.Such as prepare the identical multiple matrix of samples for being coated with coating material of parameter, respectively with gradually
Increased constantly acting load tensile sample matrix stops stretching, sample is removed tensile sample when stretching reaches determined load
Section metallographic specimen is made, observed under a scanning electron microscope to determine crackle form in drawing process and crackle transformation
Process.But this method can not real time reaction crackle expansion process, and the selection of load range have it is certain random
Property, cause resulting crackle discontinuous with tensile load changing rule, the accuracy of crack propagation process may be will affect.In addition
It is lack of standardization due to grinding and polishing in the preparation process of observation sample, it is likely to result in cracked inside brittle coating, influences to tie
The accuracy of fruit observation.
In view of the status of the relevant technologies coating material tension test observed pattern, embodiment according to the present invention is proposed
Below with reference to the accompanying drawings it is in situ to describe coating material according to an embodiment of the present invention for a kind of coating material original position stretching observation system 1
Stretch observation system 1.
As shown in Figure 1-Figure 3, coating material original position stretching observation system 1 according to an embodiment of the present invention includes original position stretching
Machine 100, matrix of samples 200, scanning electron microscope and computer system (not shown).
Matrix of samples 200 is equipped with the spray-coating surface of coating to be measured, and matrix of samples 200 is fixed on original position stretching machine 100, in situ to draw
Stretch tensile sample matrix 200 and coating to be measured thereon when machine 100 works.The scanning electron microscope has sample bin 400,
Original position stretching machine 100 is set in sample bin 400, and the scanning electron microscope is continuously shot when the coating to be measured is stretched
Image carries out overall process video recording.The computer system respectively with 100 phase of the scanning electron microscope and original position stretching machine
Even, picture is handled using loading by means of digital image correlation method to obtain the strain size and its change procedure on coating material surface.
Coating material original position stretching observation system 1 according to an embodiment of the present invention can be placed in scanning electricity by setting
Original position stretching machine 100 in the microscopical sample bin 400 of son, so as to utilize the scanning electron microscope to drawing process
It is observed, realizes the dehiscence process from micro-nano rank observation coating, can clearly capture the specific of coating cracking
Process, the position including crack initiation, the path of crack propagation and speed etc..Furthermore with scanning electron microscope in Gao Fang great
In-situ observation is carried out under multiple, can observe the variation of coating material microscopic appearance, facilitates the mechanism for analyzing coating cracking.
It for example, during stretching can be with synchronous recording displacement/load signal, so as to realize to coating material
The analysis of mechanical property；And the change procedure of coating material can be recorded, under micro-nano-scale so as to infer coating
Micromechanism of damage of material during stretching/compressing；A label is identified on coating surface to be observed with nano-imprinting method
Later, the image shot during stretching experiment using loading by means of digital image correlation method processing scanning electron microscope, can obtain
Obtain the strain size and local train change procedure of coating surface.
Therefore, coating material original position stretching observation system 1 according to an embodiment of the present invention, can observe coating material in detail
The dehiscence process of material, conducive to the damage machine of the analysis coating material germinating of crackle and extension mechanism and material during stretching
Reason.
In some embodiments of the invention, as shown in Figure 1, original position stretching machine 100 includes workbench 110, first
Objective table 120, the second objective table 130 and driver 140.
First objective table 120 and the second objective table 130 are set to workbench 110, the first objective table 120 and the second objective table
At least one of 130 can be mobile to the direction far from another, and the first objective table 120 is fixed in one end of matrix of samples 200
And the other end is fixed on the second objective table 130.Driver 140 with it is described in the first objective table 120 and the second objective table 130
At least one transmission connection, when the first objective table 120 and the second objective table 130 are relatively distant from movement, tensile sample matrix 200,
To the coating material on tensile sample matrix 200.
Further, workbench 110 is equipped with slide rail 111, the institute in the first objective table 120 and the second objective table 130
It states at least one to slidably engage in slide rail 111, to guarantee that the first objective table 120 and/or the second objective table 130 move
When dynamic with the alignment of workbench 110.Driver 140 is connected with sliding guide 141, the first objective table 120 and the second objective table
In 130 it is described at least one slidably engage in sliding guide 141, to guarantee that the first objective table 120 and/or second carries
The alignment when movement of object platform 130 with driver 140.
Wherein, the both side surface of slide rail 111 is equipped with anticreep groove 112, the first objective table 120 and the second objective table
In 130 it is described at least one be equipped with and be matched with the anticreep rib of anticreep groove 112, to prevent the first objective table 120 and second
At least one described disengaging slide rail 111 in objective table 130.
In some specific examples of the invention, driver 140 is servo motor, and the motor shaft of the servo motor passes through
Shaft coupling is connected with drive screw 142, in drive screw 142 and the first objective table 120 and the second objective table 130 it is described at least
One is threadedly engaged, convert the rotary motion of motor shaft in the first objective table 120 and the second objective table 130 described in
The linear movement of at least one.For example, there is contrary screw thread at the both ends of drive screw 142 respectively, drive screw 142
Rotation the first objective table 120 of drive and the second objective table 130 reach the function of stretching to reverse movement respectively.
In some embodiments of the invention, as shown in Figure 1, the first objective table 120 is equipped with dismountable first folder
Plate 121, the second objective table 130 are equipped with dismountable second clamping plate 131, and one end of matrix of samples 200 is clamped in the first loading
Between platform 120 and first clamping plate 121, the other end of matrix of samples 200 is clamped in the second objective table 130 and second clamping plate 131
Between.
Specifically, as shown in Figure 1, first clamping plate 121 is equipped with the first threaded hole 122 and the first dowel hole 123, example
Such as, the first threaded hole 122 is two and the first dowel hole 123 is located between two the first threaded holes 122, first clamping plate 121
The first threaded fastener (such as bolt) by being matched with the first threaded hole 122 is removably installed in the first objective table 120,
First clamping plate 121 carries out described one end of matrix of samples 200 by being matched with the first positioning pin of the first dowel hole 123
Fixed, which can be further inserted into the first objective table 120.
Second clamping plate 131 is equipped with the second threaded hole 132 and the second dowel hole 133, for example, the second threaded hole 132 is two
A and the second dowel hole 133 is located between two the second threaded holes 132, and second clamping plate 131 is by being matched with the second threaded hole
132 the second threaded fastener (such as bolt) is removably installed in the second objective table 130, and second clamping plate 131 passes through cooperation
The other end of matrix of samples 200 is fixed in the second positioning pin of the second dowel hole 133, which can
To be further inserted into the second objective table 130.
In some specific examples of the invention, the rate of extension, maximum load of original position stretching machine 100, scanning electron are aobvious
The amplification factor and observation scope of micro mirror can real-time quantitative adjust, rate of extension may be implemented in 0.036mm/min~1mm/min
In the range of linear regulation, maximum load amount can reach 1kN, stretches maximum range up to 10mm, can meet different performance
The testing requirement of coating material.
In view of the coating of such as ceramic fragile material, elastic deformation stage is very short during stretching, fracture behaviour
Generation is very rapid, when being tested using large-scale cupping machine, since testing machine tensile load is higher, stretches speed
Rate is very fast, therefore is difficult to capture the detailed fracture process of coating material.
Original position stretching machine 100 according to an embodiment of the present invention, rate of extension adjustable extent is in 0.036mm/min-
Within the scope of 1mm/min, by slowing down rate of extension, it can be achieved that " delay " Tensile Fracture Process to brittle ceramic coating, thus
Observation coating material may be implemented slowly to crack to the detailed process for disconnecting peeling.
In some embodiments of the invention, as shown in Figures 2 and 3, it is two kinds that matrix of samples 200, which is divided to,.Wherein, one
Kind of matrix of samples 200 for (as shown in Figure 2) from being carried out from the front of coating material, another matrix of samples 200 for from
(as shown in Figure 3) is observed in the side of coating, the germinating and expansion of crackle when thus, it is possible to obtain coating cracking in further detail
The relevant informations such as the situation of change of exhibition and surface strain.
Specifically, as shown in Fig. 2, a kind of matrix of samples 200 includes the first fixed section 210, the second fixed section
220 and linkage section 230.
First fixed section 210 and the second fixed section 220 are respectively equipped with first positioning hole 211 and second location hole 221, thus
The first objective table 120 and the second objective table 130 are fixed on by the first positioning pin and the second positioning pin respectively.Linkage section 230 connects
It connects between the first fixed section 210 and the second fixed section 220.
Wherein, the width of the first fixed section 210 is equal with the width of the second fixed section 220 and is greater than the width of linkage section 230
Degree, the thickness of the first fixed section 210, the second fixed section 220 the thickness of thickness and linkage section 230 be equal to each other, linkage section 230
Upper surface be formed with spray-coating surface 231, coating spraying is in spray-coating surface 231, convenient for the front of scanning electron microscope observation coating.
As shown in figure 3, the another kind matrix of samples 200 includes the first fixed section 210, the second fixed section 220 and connection
Section 230.
First fixed section 210 and the second fixed section 220 are respectively equipped with first positioning hole 211 and second location hole 221, thus
The first objective table 120 and the second objective table 130 are fixed on by the first positioning pin and the second positioning pin respectively.Linkage section 230 connects
It connects between the first fixed section 210 and the second fixed section 220.
Wherein, the width of the first fixed section 210 is equal with the width of the second fixed section 220 and is greater than the width of linkage section 230
Degree, the thickness of the first fixed section 210 is equal with the thickness of the second fixed section 220 and is less than the thickness of linkage section 230, linkage section
230 side surface is formed with spray-coating surface 231, and coating spraying is in spray-coating surface 231, convenient for the side of scanning electron microscope observation coating
Face.
By designing the matrix of samples 200 of two kinds of different structures, coating material can be effectively observed after spraying
The situation of change of front surface and side during stretching, in addition by the high-amplification-factor of scanning electron microscope, Ke Yi
Processing is marked using nano-imprinting method to the front of coating and side before tension test, then utilizes digital picture phase
The photo that pass method processing scanning electron microscope is shot can obtain the strained situation of coating front and side simultaneously.
Below with reference to the accompanying drawings the coating spraying tooling and coating spraying of matrix of samples 200 according to an embodiment of the present invention are described
Method.
As Figure 2-Figure 5, matrix of samples 200 includes the first fixed section 210, the second fixed section 220 and is connected to first
Linkage section 230 between fixed section 210 and the second fixed section 220, the width of the first fixed section 210 and the second fixed section 220
Width is equal and is greater than the width of linkage section 230, and the first fixed section 210 is equipped with first positioning hole 211, and the second fixed section 220 is set
There is second location hole 221, linkage section 230 is equipped with spray-coating surface 231.
The coating spraying tooling is solid including the first barrier bed 510, the second barrier bed 520, the first fixed pin 530, second
Rationed marketing 540 and fixture 600.
First barrier bed 510 wraps up the first fixed section 210, and the second barrier bed 520 wraps up the second fixed section 220, and first is solid
The first barrier bed 510 is inserted into first positioning hole 211 and passes through in rationed marketing 530, and it is fixed that the first barrier bed 510 is fixed on first
Section 210, the second fixed pin 540 are inserted into second location hole 221 and pass through the second barrier bed 520, the second barrier bed 520 is consolidated
Due to the second fixed section 220.Fixture 600 is used to clamp multiple matrix of samples 200 and makes the spray-coating surface of multiple matrix of samples 200
231 towards same direction, to spray simultaneously to the spray-coating surface 231 of multiple matrix of samples 200.
As shown in fig. 6, the coating spraying method of matrix of samples 200 according to an embodiment of the present invention the following steps are included:
First fixed section 210 is wrapped up using the first barrier bed 510 and is inserted into the first fixed pin in first positioning hole 211
530 to fix the first barrier bed 510, wraps up the second fixed section 220 using the second barrier bed 520 and in second location hole 221
The second fixed pin 540 of interior insertion is to fix the second barrier bed 520；
Blasting treatment is carried out to the spray-coating surface 231 of linkage section 230；
Matrix of samples 200 after multiple blasting treatments is placed in fixture 600；
Spray-coating surface 231 is sprayed using supersonic speed plasma apparatus.
Coating spraying tooling and coating spraying method according to an embodiment of the present invention, can be in the matrix of samples of small size
Spray-on coating on 200, and coating is blocked by the first barrier bed 510 and the second barrier bed 520, exists only in linkage section 230
Spray-coating surface 231, without being sprayed into the first fixed section 210 and the second fixed section 220, to avoid coating to linkage section 230
There is interference in drawing effect, further, it is possible to prevent coating from entering first positioning hole 211 and second location hole 221, to prevent first
Location hole 211 goes wrong with the first positioning pin and second location hole 221 and the cooperation of the second positioning pin, after thus spraying
Matrix of samples 200, can be placed in scanning electronic microscope observation, and then is conducive to analysis coating material crackle is sprouted during stretching
The micromechanism of damage of raw and extension mechanism and material.
Wherein, the first barrier bed 510 and the second barrier bed 520 are iron sheet, with fusing point with higher, are avoided in high temperature
Flame flows down fusing and loses the protection to the first fixed section 210 and the second fixed section 220.
In some specific examples of the invention, the coating spraying method of matrix of samples 200 will be filled before blasting treatment
There is the matrix of samples 200 of the first barrier bed 510, the second barrier bed 520, the first fixed pin 530 and the second fixed pin 540 advanced
Row cleaning.
Further, the pressure of the blasting treatment is no more than 60MPa, to prevent that pressure is excessive and makes matrix of samples
200 bendings.
In some specific examples of the invention, it after every spraying for carrying out pre-determined number, is spaced after predetermined cooling time again
It is sprayed, which is 2, in other words, avoids 200 continuous several times of matrix of samples from spraying, to prevent sample base
The temperature of body 200 is excessively high.
In some embodiments of the invention, as shown in Figure 2 and Figure 4, the thickness of the first fixed section 210, second are consolidated
The thickness for determining the thickness and linkage section 230 of section 220 is equal to each other, and spray-coating surface 231 is formed in the upper surface of linkage section 230.
Each first fixed section 210 is enclosed with the first barrier bed 510 respectively, is inserted into respectively in each first positioning hole 211
There is the first fixed pin 530, each second fixed section 220 is enclosed with the second barrier bed 520 respectively, and each second location hole 221 is divided
Not inserted with the second fixed pin 540.I.e. first barrier bed 510 wraps up first fixed section 210 and passes through one first
Fixed pin 530 is fixed, and second barrier bed 520 wraps up second fixed section 220 and consolidated by second fixed pin 540
It is fixed.
Wherein, the both ends of the first barrier bed 510 bypass two lateral edges of the first fixed section 210, the first barrier bed 510 respectively
Both ends interval be arranged to avoid the first fixed pin 530, the both ends of the second barrier bed 520 bypass the second fixed section 220 respectively
Two lateral edges, and the both ends interval of the second barrier bed 520 is arranged to avoid the second fixed pin 540, is thus convenient for the first barrier bed 510
With the package and fixed operation of the second barrier bed 520.
Further, as shown in figure 4, multiple matrix of samples 200 are carried out while being sprayed in order to realize, to improve spraying effect
Rate, fixture 600 include bottom plate 610, the first side clamping plate 620 and second side clamping plate 630.
First side clamping plate 620 and second side clamping plate 630 are respectively arranged on the opposite sides edge of bottom plate 610, second side clamping plate
630 height can be higher than the height of the first side clamping plate 620, and the first side clamping plate 620, second side clamping plate 630 and bottom plate 610 are total
With clip slot is limited, the second fixed section 220 of multiple matrix of samples 200 (has wrapped up the second barrier bed 520 at this time and has been combined with
Second fixed pin 540) it is set in the clip slot, it is fixed to be realized to multiple matrix of samples 200, convenient for spraying simultaneously, citing
For, specific spray parameters can refer to shown in following table:
In some embodiments of the invention, as shown in Figure 3 and Figure 5, the thickness of the first fixed section 210 and second is consolidated
The thickness for determining section 220 is equal and be less than the thickness of linkage section 230, and spray-coating surface 231 is formed in the side surface of linkage section 230.
Whole the first fixed section 210 for wrapping up multiple matrix of samples 200 of first barrier bed 510, the second barrier bed 520 are whole
Wrap up the second fixed section 220 of multiple matrix of samples 200.That is, the first fixed section 210 of multiple matrix of samples 200 by
Same first barrier bed 510 wraps up, and the second fixed section 220 of multiple matrix of samples 200 is wrapped up by same second barrier bed 520.
Specifically, the both ends of the first barrier bed 510 are rotating around outermost two in excessively multiple first fixed sections 210, and
The both ends interval of first barrier bed 510 is arranged.The both ends of second barrier bed 520 rotating around in excessively multiple second fixed sections 220 most
Two of outside, and the both ends interval setting of the second barrier bed 520.
Wherein, the spacing distance at the both ends of the first barrier bed 510 at least allows first fixed section 210 to pass through, i.e., and
The spacing distance at the both ends of one barrier bed 510 is greater than the thickness of first fixed section 210.The both ends of second barrier bed 520
Spacing distance at least allows second fixed section 220 to pass through, i.e., the spacing distance at the both ends of the second barrier bed 520 is greater than one
The thickness of second fixed section 220.
Preferably, the both ends of the first barrier bed 510 are only rotating around outermost two in excessively multiple first fixed sections 210
Can, the both ends of the second barrier bed 520 are only rotating around outermost two in excessively multiple second fixed sections 220.
Further, the coating spraying tooling of matrix of samples 200 further includes between multiple first spacer blocks 710 and multiple second
Spacer block 720.
Each first spacer block 710 be set to adjacent first fixed section 210 between, with multiple first fixed sections 210 of fixation it
Between distance, each second spacer block 720 be set to adjacent second fixed section 220 between, with multiple second fixed sections 220 of fixation
The distance between, such as the distance between adjacent linkage section 230 is made to be greater than 2mm, to avoid the painting on adjacent linkage section 230
Layer sticks together.
In order to by multiple matrix of samples 200 and the first barrier bed 510, the second barrier bed 520, multiple first spacer blocks 710,
The relative position of multiple second spacer blocks 720 is fixed, multiple first fixed sections 210 share first fixed pin 530 and this
One fixed pin 530 passes through multiple first spacer blocks 710, and multiple second fixed sections 220 share second fixed pin 540 and should
Second fixed pin 540 passes through multiple second spacer blocks 720.I.e. for multiple matrix of samples 200, using first fixed pin
530 and second fixed pin 540 be fixed, the first fixed pin 530 pass through multiple first fixed sections 210 first positioning
Hole 211 and multiple first spacer blocks 710 and the first barrier bed 510, the second fixed pin 540 pass through multiple second fixed sections 220
Second location hole 221 and multiple second spacer blocks 720 and the second barrier bed 520.
Multiple matrix of samples 200 are wrapped using first barrier bed 510 and second barrier bed 520 as a result,
It wraps up in, and is fixed using first fixed pin 530 and second fixed pin 540, save the time of assembly tooling, improve
Spray efficiency.
Citing describes the course of work of coating material original position stretching observation system 1 according to an embodiment of the present invention below.
For coating material to be observed, it is necessary first to matrix of samples is chosen according to coating material attribute, then in sample base
Coating material to be observed is sprayed on body, is carried out later using nanometer embossing on the surface to be observed (front or side) of coating
Location hole in matrix of samples is aligned by the label of speckle with the location hole on the first objective table 120 and the second objective table 130,
Cover first clamping plate 121 and second clamping plate 131, be inserted into the first positioning pin and the second positioning pin, tighten the first threaded fastener and
Second threaded fastener after being then dusted processing to original position stretching machine 100, is sent into scanning electron microscope, sample bin
400 sides have chip and scanning electron microscope to connect, it can be achieved that control of the computer system to original position stretching machine 100.
The parameters such as rate of extension, tensile load are set on the computer systems, then adjust scanning electron microscope to suitable amplification
Multiple finds region to be observed to defocused.It is then turned on scanning electron microscope kinescope recording function, stretching experiment can be started
It is observed, original position stretching machine 100 can be suspended at any time during stretching, then carry out high magnification numbe using scanning electron microscope
Photographing operation can get the correlated process picture of coating germinating and extension.
Coating material original position stretching observation system 1 according to an embodiment of the present invention, using scanning electron microscope from microcosmic
The tension crack process that thin coating materials are observed on scale can show damage of material under the conditions of extension test completely and open
Split process.And it is possible to which the rate of extension and load by adjusting original position stretching machine 100 realize that brittle coating material slowly cracks
Process.Furthermore, it is possible to the strained situation of coating front surface and side be measured simultaneously, using scanning electron microscope to extension test
Process is recorded at any time or whole record.
In the description of this specification, the description of reference term " specific embodiment ", " specific example " etc. means to combine and be somebody's turn to do
Embodiment or example particular features, structures, materials, or characteristics described are contained at least one embodiment of the present invention or show
In example.In the present specification, schematic expression of the above terms may not refer to the same embodiment or example.
Although an embodiment of the present invention has been shown and described, it will be understood by those skilled in the art that: not
A variety of change, modification, replacement and modification can be carried out to these embodiments in the case where being detached from the principle of the present invention and objective, this
The range of invention is defined by the claims and their equivalents.
Claims (10)
1. a kind of coating spraying tooling of the matrix of samples for the observation of coating material original position stretching, which is characterized in that the examination
Sample matrix includes the first fixed section, the second fixed section and the company being connected between first fixed section and second fixed section
Section is connect, the width of first fixed section is equal with the width of second fixed section and is greater than the width of the linkage section, institute
The first fixed section is stated equipped with first positioning hole, second fixed section is equipped with second location hole, and the linkage section is equipped with spray-coating surface,
The coating spraying tooling includes:
First barrier bed, first barrier bed wrap up first fixed section；
Second barrier bed, second barrier bed wrap up second fixed section；
First fixed pin, first fixed pin are inserted into the first positioning hole and pass through first barrier bed；
Second fixed pin, second fixed pin are inserted into the second location hole and pass through second barrier bed；
Fixture, the fixture is for clamping multiple matrix of samples and making the spray-coating surface of multiple matrix of samples towards same
Direction.
2. the coating spraying tooling of the matrix of samples according to claim 1 for the observation of coating material original position stretching,
Be characterized in that, the thickness of first fixed section, second fixed section the thickness of thickness and the linkage section be equal to each other,
The spray-coating surface is formed in the upper surface of the linkage section；
Each first fixed section is enclosed with the first barrier bed respectively, respectively inserted with first in each first positioning hole
Fixed pin, each second fixed section are enclosed with the second barrier bed respectively, in each second location hole respectively inserted with
Second fixed pin.
3. the coating spraying tooling of the matrix of samples according to claim 2 for the observation of coating material original position stretching,
It is characterized in that, the both ends of first barrier bed bypass two lateral edges of first fixed section respectively and interval is arranged to avoid
State the first fixed pin；
The both ends of second barrier bed bypass two lateral edges of second fixed section and interval setting respectively to avoid described the
Two fixed pins.
4. the coating spraying tooling of the matrix of samples according to claim 2 for the observation of coating material original position stretching,
It is characterized in that, the fixture includes:
Bottom plate；
First side clamping plate and second side clamping plate, first side clamping plate and second side clamping plate are respectively arranged on the phase of the bottom plate
To two lateral edges, first side clamping plate, second side clamping plate and the bottom plate limit clip slot, multiple sample bases jointly
Second fixed section of body is set in the clip slot.
5. the coating spraying tooling of the matrix of samples according to claim 4 for the observation of coating material original position stretching,
It is characterized in that, the height of second side clamping plate is higher than the height of first side clamping plate.
6. the coating spraying tooling of the matrix of samples according to claim 1 for the observation of coating material original position stretching,
It is characterized in that, the thickness of first fixed section is equal with the thickness of second fixed section and is less than the thickness of the linkage section
Degree, the spray-coating surface are formed in the side surface of the linkage section；
First barrier bed integrally wraps up the first fixed section of multiple matrix of samples, and second barrier bed integrally wraps up multiple
Second fixed section of matrix of samples.
7. the coating spraying tooling of the matrix of samples according to claim 6 for the observation of coating material original position stretching,
It being characterized in that, the both ends of first barrier bed are rotating around outermost two in excessively multiple first fixed sections, and described first
The both ends interval of barrier bed is arranged to allow at least one first fixed section to pass through；
The both ends of second barrier bed are rotating around outermost two in excessively multiple second fixed sections, and second barrier bed
Both ends interval be arranged to allow at least one second fixed section to pass through.
8. the coating spraying tooling of the matrix of samples according to claim 6 for the observation of coating material original position stretching,
It is characterized in that, further includes:
Multiple first spacer blocks, each first spacer block are set between adjacent first fixed section；
Multiple second spacer blocks, each second spacer block are set between adjacent second fixed section.
9. the coating spraying tooling of the matrix of samples according to claim 8 for the observation of coating material original position stretching,
It is characterized in that, multiple first fixed sections share first fixed pin and first fixed pin passes through between multiple described first
Spacer block；
Multiple second fixed sections share second fixed pin and second fixed pin passes through multiple second spacer blocks.
10. the coating of the matrix of samples according to claim 1 to 9 for the observation of coating material original position stretching
Spraying frock, which is characterized in that first barrier bed and second barrier bed are iron sheet.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910368708.5A CN110029302B (en) | 2019-05-05 | 2019-05-05 | Coating spraying tool for sample matrix for in-situ tensile observation of coating material |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910368708.5A CN110029302B (en) | 2019-05-05 | 2019-05-05 | Coating spraying tool for sample matrix for in-situ tensile observation of coating material |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN110029302A true CN110029302A (en) | 2019-07-19 |
| CN110029302B CN110029302B (en) | 2021-03-23 |
Family
ID=67241296
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201910368708.5A Active CN110029302B (en) | 2019-05-05 | 2019-05-05 | Coating spraying tool for sample matrix for in-situ tensile observation of coating material |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN110029302B (en) |
Citations (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3192766A (en) * | 1962-08-14 | 1965-07-06 | Martin Marietta Corp | Multi-specimen testing apparatus |
| DE1807682C3 (en) * | 1968-11-08 | 1974-10-17 | Phoenix Gummiwerke Ag, 2100 Hamburg | Device for simultaneous and similar testing of several rubber-metal spring elements |
| FR2797052A1 (en) * | 1999-07-30 | 2001-02-02 | Metravib Sa | METHOD AND INSTALLATION FOR ENSURING THE AUTOMATIC CLAMPING OF A TEST FOR MECHANICAL TESTS |
| CN101697501A (en) * | 2009-10-19 | 2010-04-21 | 北京交通大学 | Platform for testing radio-frequency wireless energy and signal transmission |
| CN102225512A (en) * | 2011-06-08 | 2011-10-26 | 上海电气核电设备有限公司 | Tensile test piece processing tool jig |
| CN104198272A (en) * | 2014-08-29 | 2014-12-10 | 上海交通大学 | 3D-TSV (Through Silicon Via) in-situ tension test sample and preparation method thereof |
| CN105004610A (en) * | 2015-09-09 | 2015-10-28 | 海安县石油科研仪器有限公司 | Device for tensile test of metal material under function of current |
| CN105223055A (en) * | 2015-10-16 | 2016-01-06 | 内蒙古工业大学 | For the original position stretching sample and preparation method thereof of transmission electron microscope |
| CN206154710U (en) * | 2016-10-12 | 2017-05-10 | 福融辉实业（福建）有限公司 | BOPP membrane lateral stretching mechanism entry presss from both sides edge domination device |
| CN206248469U (en) * | 2016-12-15 | 2017-06-13 | 通标标准技术服务（青岛）有限公司 | T-shaped sample stretching tool |
| CN107894364A (en) * | 2018-01-17 | 2018-04-10 | 兰州理工大学 | A kind of scanning electron microscope home position stretches servicing unit |
| CN109307629A (en) * | 2018-09-30 | 2019-02-05 | 合肥高益机电科技有限公司 | A kind of electric wire bending survey number machine |
-
2019
- 2019-05-05 CN CN201910368708.5A patent/CN110029302B/en active Active
Patent Citations (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3192766A (en) * | 1962-08-14 | 1965-07-06 | Martin Marietta Corp | Multi-specimen testing apparatus |
| DE1807682C3 (en) * | 1968-11-08 | 1974-10-17 | Phoenix Gummiwerke Ag, 2100 Hamburg | Device for simultaneous and similar testing of several rubber-metal spring elements |
| FR2797052A1 (en) * | 1999-07-30 | 2001-02-02 | Metravib Sa | METHOD AND INSTALLATION FOR ENSURING THE AUTOMATIC CLAMPING OF A TEST FOR MECHANICAL TESTS |
| CN101697501A (en) * | 2009-10-19 | 2010-04-21 | 北京交通大学 | Platform for testing radio-frequency wireless energy and signal transmission |
| CN102225512A (en) * | 2011-06-08 | 2011-10-26 | 上海电气核电设备有限公司 | Tensile test piece processing tool jig |
| CN104198272A (en) * | 2014-08-29 | 2014-12-10 | 上海交通大学 | 3D-TSV (Through Silicon Via) in-situ tension test sample and preparation method thereof |
| CN105004610A (en) * | 2015-09-09 | 2015-10-28 | 海安县石油科研仪器有限公司 | Device for tensile test of metal material under function of current |
| CN105223055A (en) * | 2015-10-16 | 2016-01-06 | 内蒙古工业大学 | For the original position stretching sample and preparation method thereof of transmission electron microscope |
| CN206154710U (en) * | 2016-10-12 | 2017-05-10 | 福融辉实业（福建）有限公司 | BOPP membrane lateral stretching mechanism entry presss from both sides edge domination device |
| CN206248469U (en) * | 2016-12-15 | 2017-06-13 | 通标标准技术服务（青岛）有限公司 | T-shaped sample stretching tool |
| CN107894364A (en) * | 2018-01-17 | 2018-04-10 | 兰州理工大学 | A kind of scanning electron microscope home position stretches servicing unit |
| CN109307629A (en) * | 2018-09-30 | 2019-02-05 | 合肥高益机电科技有限公司 | A kind of electric wire bending survey number machine |
Non-Patent Citations (1)
| Title |
|---|
| GREGORY M. SMITH等: "In-situ observation of strain and cracking in coated laminates by digital image correlation", 《SURFACE & COATINGS TECHNOLOGY》 * |
Also Published As
| Publication number | Publication date |
|---|---|
| CN110029302B (en) | 2021-03-23 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN109946161A (en) | Original position stretching machine for coating material original position stretching observation system | |
| CN109975122A (en) | Coating material method for testing fatigue | |
| CN109060575A (en) | Driving type piezoelectric actuator low-temperature in-site high-frequency reciprocating micro-moving frictional wear test platform | |
| CN109946160A (en) | Coating material original position stretching observation system | |
| CN105203391B (en) | Micro-hardness testing fixture | |
| CN103575593A (en) | In-situ uniaxial tension observation device for mesoscale metal material | |
| CN109781516A (en) | A kind of material strain original position EBSD observation test fixture and the test method | |
| CN109991065A (en) | The coating spraying method of matrix of samples for the observation of coating material original position stretching | |
| CN205787586U (en) | A kind of Automatic continuous focusing test equipment for big wide-angle camera | |
| CN100561210C (en) | Method for measuring several critical strain values of metal membrane in flexible substrate | |
| CN110029302A (en) | The coating spraying tooling of matrix of samples for the observation of coating material original position stretching | |
| CN110044702A (en) | Vacuum sound emission nondestructive detection system | |
| CN101718541B (en) | Automatic measuring device and method of coating layer ND direction film thickness | |
| CN1621802A (en) | Coating mechanical testing equipment | |
| CN109959558A (en) | Matrix of samples for coating material original position stretching observation system | |
| CN209894601U (en) | In-situ stretching equipment for coating material in-situ stretching observation system | |
| CN110082194A (en) | Coating material original position stretching observation method | |
| CN210037436U (en) | In-situ stretching equipment for coating material in-situ stretching observation system | |
| He et al. | Elastic property characterization of soft substrate-supported thin films using multiscale digital image correlation | |
| CN110006755A (en) | Original position stretching machine for coating material original position stretching observation system | |
| CN109142041A (en) | A method of detection sample sliding and bending deformation | |
| CN106525584A (en) | Preparation method for in-situ mechanic loading tool under transmission electron microscope | |
| Bezák et al. | Surface roughness determination using laser scanning confocal microscope Zeiss LSM 700 | |
| CN109540742A (en) | A kind of multifunctional access feeler in-situ test pond and its application for measuring surface wettability matter | |
| CN113176163A (en) | Static contact component high-low temperature surface micro-abrasion dynamic testing machine |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |