CN110026296B - Crystal centrifuge is used in potassium aurous cyanide production - Google Patents

Crystal centrifuge is used in potassium aurous cyanide production Download PDF

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Publication number
CN110026296B
CN110026296B CN201910359079.XA CN201910359079A CN110026296B CN 110026296 B CN110026296 B CN 110026296B CN 201910359079 A CN201910359079 A CN 201910359079A CN 110026296 B CN110026296 B CN 110026296B
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Prior art keywords
drum wall
shell
wall
inner drum
cavity
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CN110026296A (en
Inventor
郭盈怀
刁建元
赵培
马涛
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Sanmenxia Zhaoyang Tech Co ltd
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Sanmenxia Zhaoyang Tech Co ltd
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B04CENTRIFUGAL APPARATUS OR MACHINES FOR CARRYING-OUT PHYSICAL OR CHEMICAL PROCESSES
    • B04BCENTRIFUGES
    • B04B1/00Centrifuges with rotary bowls provided with solid jackets for separating predominantly liquid mixtures with or without solid particles
    • B04B1/04Centrifuges with rotary bowls provided with solid jackets for separating predominantly liquid mixtures with or without solid particles with inserted separating walls
    • B04B1/08Centrifuges with rotary bowls provided with solid jackets for separating predominantly liquid mixtures with or without solid particles with inserted separating walls of conical shape
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B04CENTRIFUGAL APPARATUS OR MACHINES FOR CARRYING-OUT PHYSICAL OR CHEMICAL PROCESSES
    • B04BCENTRIFUGES
    • B04B11/00Feeding, charging, or discharging bowls
    • B04B11/02Continuous feeding or discharging; Control arrangements therefor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B04CENTRIFUGAL APPARATUS OR MACHINES FOR CARRYING-OUT PHYSICAL OR CHEMICAL PROCESSES
    • B04BCENTRIFUGES
    • B04B11/00Feeding, charging, or discharging bowls
    • B04B11/06Arrangement of distributors or collectors in centrifuges
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B04CENTRIFUGAL APPARATUS OR MACHINES FOR CARRYING-OUT PHYSICAL OR CHEMICAL PROCESSES
    • B04BCENTRIFUGES
    • B04B15/00Other accessories for centrifuges
    • B04B15/06Other accessories for centrifuges for cleaning bowls, filters, sieves, inserts, or the like
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B04CENTRIFUGAL APPARATUS OR MACHINES FOR CARRYING-OUT PHYSICAL OR CHEMICAL PROCESSES
    • B04BCENTRIFUGES
    • B04B15/00Other accessories for centrifuges
    • B04B15/08Other accessories for centrifuges for ventilating or producing a vacuum in the centrifuge

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  • Centrifugal Separators (AREA)

Abstract

The invention discloses a crystal centrifuge for producing potassium aurous cyanide, which aims to solve the technical problem that the traditional classifying centrifuge cannot continuously produce. According to the invention, crystals are separated in a grading way through the inner drum wall and the outer drum wall, and then the crystals are discharged out of the centrifugal machine through the cooperation of the rotating upper annular plate, the rotating lower annular plate and the rotating material guide plate.

Description

Crystal centrifuge is used in potassium aurous cyanide production
Technical Field
The invention relates to the technical field of potassium aurous cyanide production equipment, in particular to a crystal centrifuge for potassium aurous cyanide production.
Background
The potassium aurous cyanide is white crystal and is a double salt formed by aurous ions and cyanide ions. Dissolving in water, slightly dissolving in ethanol, insoluble in diethyl ether, being easy to wet and extremely toxic, gold potassium cyanide is a highly toxic chemical, the toxicity is basically the same as potassium cyanide, and the lethal dose is about 0.1 g. Preparation: the pure gold reacts with aqua regia, filtered, concentrated hydrochloric acid is added to remove nitrogen oxides, then the pure gold reacts with potassium cyanide, and then the pure gold is crystallized to obtain the finished product.
The centrifuge is an indispensable device for separating gold potassium cyanide crystals. Centrifugal machines are various, but the centrifugal machines are basically the same in distance, and the rotary drum is used for driving crystals to rotate so that the crystals are separated from a solution under the action of centrifugal force. The Chinese patent with the bulletin number of CN201866240U discloses a classifying centrifuge, the classifying centrifuge comprises a centrifuge shell, an air inlet is arranged at the left part of the upper end of the centrifuge shell, an air outlet is arranged at the right part of the upper side of the centrifuge shell, an exhaust fan is arranged on the air outlet, the exhaust fan is connected with a waste gas treatment device through a pipeline, a supporting leg is arranged at the lower end of the centrifuge shell, a supporting plate is arranged at the middle part of the supporting leg, a damping motor is arranged at the upper part of the supporting plate, an output shaft of the motor is connected with a rotary disc arranged inside the centrifuge shell through a rotary shaft, and a first centrifugal layer, a second centrifugal layer and a third centrifugal layer are arranged at the upper end of the rotary disc.
The centrifugal machine realizes the grading separation of crystals with different particle diameters by using the first centrifugal layer, the second centrifugal layer and the third centrifugal layer which are coaxially arranged, but due to the action of centrifugal force, part of crystals with large particle diameters in the first centrifugal layer can easily cross the first centrifugal layer to be mixed with crystals with medium particle diameters in the second centrifugal layer, and part of crystals with medium particle diameters in the second centrifugal layer can easily cross the second centrifugal layer to be mixed with crystals with small particle diameters in the third centrifugal layer, so that the grading effect of the crystals is poor. Meanwhile, as the centrifugal machine is an intermittent centrifugal machine, namely after the separation of liquid and crystals is completed, the separation operation is stopped, and the top cover is opened to take out the crystals with various particle sizes; the centrifuge is extremely dangerous to toxic substances such as potassium aurous cyanide, so that only a continuous centrifuge can be used, in other words, the existing centrifuge with the classification function is not suitable for producing the potassium aurous cyanide.
Secondly, because of continuous production, the filter holes on the rotary drum of the existing continuous centrifugal machine are easy to be blocked, and the filter performance of the rotary drum is slowly reduced after the filter holes are blocked, so that the production efficiency is seriously affected.
Disclosure of Invention
In view of the above, the invention aims to provide a crystal centrifuge for producing potassium aurous cyanide, which solves the technical problem that the existing classifying centrifuge can not continuously produce.
The technical scheme adopted by the invention is as follows:
A crystal centrifuge for producing potassium aurous cyanide is designed, which comprises
The bottom of the shell is provided with a liquid outlet;
the top cover is connected to the top of the shell in a sealing way;
the rotary drum is arranged in the shell;
The rotary drum comprises an inverted truncated cone-shaped inner drum wall and an inverted truncated cone-shaped outer drum wall, filter holes are formed in the inner drum wall and the outer drum wall, the diameter of the filter holes in the inner drum wall is larger than that of the filter holes in the outer drum wall, the top end of the inner drum wall is higher than that of the outer drum wall, an upper annular plate and a lower annular plate are correspondingly connected to the top ends of the inner drum wall and the outer drum wall respectively, and the inner space of the shell is divided into an upper cavity, a middle cavity and a lower cavity by the upper annular plate and the lower annular plate;
a rotating shaft coaxial with the inner drum wall is arranged in the upper cavity, an elastic telescopic rod is arranged on the rotating shaft, the other end of the elastic telescopic rod is connected with a scraping plate, the inclined direction of the scraping plate is consistent with that of the inner drum wall, the interior of the rotating shaft is hollow to form a liquid inlet channel, the inner cavity at the top end of the rotating shaft is connected with a feeding pipe, and the outer wall of the rotating shaft is in transmission connection with a motor;
the inner side of the shell, the upper annular plate and the upper annular plate are respectively provided with a material guide plate, the outer side of the shell is provided with a charging barrel, and the shell is provided with a material outlet matched with the material guide plates and the charging barrels;
The top cover is provided with an air inlet, the air inlet is connected with an air source through an air supply pipe, the bottom of the shell is provided with an air outlet, one side of the outer wall of the shell is provided with an upper drainage pipe used for communicating an upper cavity with a middle cavity, and the other side of the outer wall of the shell is provided with a lower drainage pipe used for communicating the middle cavity with a lower cavity.
Preferably, the elastic telescopic rod comprises a first connecting rod, a spring and a second connecting rod, wherein the first connecting rod is in sliding connection with the second connecting rod, one end of the spring is fixedly connected with the first connecting rod, and the other end of the spring is fixedly connected with the second connecting rod.
Preferably, the bottom of the rotating shaft is rotationally connected with a disc-shaped distributor, and a plurality of arc-shaped distributing channels communicated with the liquid inlet channels are arranged on the distributor.
Preferably, the inner drum wall and the outer drum wall are coaxial.
Preferably, the guide plate is a curved plate.
Preferably, a brush is arranged on the scraping plate.
Preferably, the bottom of the shell is provided with a shock-absorbing strut.
Preferably, the included angle between the generatrix of the inner drum wall and the horizontal plane is larger than the included angle between the generatrix of the outer drum wall and the horizontal plane.
Compared with the prior art, the invention has the beneficial technical effects that:
1. The top ends of the inner drum wall and the outer drum wall are correspondingly connected with an upper annular plate and a lower annular plate respectively, and the upper annular plate and the lower annular plate divide the inner space of the shell into an upper cavity, a middle cavity and a lower cavity, so that crystals with different particle size grades which are thrown outwards under the action of centrifugal force are positioned in the different cavities, and the crystals with different particle size grades are completely separated.
2. According to the invention, the material guide plate is arranged on the inner side of the shell, the material cylinder is arranged on the outer side of the shell, so that crystals rotating along with the upper annular plate or the lower annular plate enter the material cylinder through the material outlet on the shell to be collected under the action of centrifugal force and the guiding action of the material guide plate.
3. According to the invention, the air inlet is arranged at the top of the shell, the air outlet is arranged at the bottom of the shell, and the upper drainage tube and the lower drainage tube are further arranged on the outer wall of the shell, so that the gas in the three cavities in the centrifuge is completely discharged through nitrogen, and poisoning accidents caused by gas leakage in the centrifuge are prevented.
4. According to the centrifugal machine, the rotating shaft is arranged in the inner drum wall, the scraping plate and the hairbrush are connected with the rotating shaft through the elastic telescopic rod, and when the rotating shaft rotates, the elastic telescopic rod stretches under the action of centrifugal force, so that the scraping plate and the hairbrush are contacted with the inner drum wall, crystals are scraped from the inner drum wall, the blocking probability of filter holes in the inner drum wall can be effectively reduced, and the cleaning period of the centrifugal machine is prolonged.
5. The invention is characterized in that the bottom end of the rotating shaft is rotationally connected with the distributor, and the distributor is provided with the arc-shaped distributing channel communicated with the liquid inlet channel, so that under the impact of a solution, the distributor performs distributing while moving in a circular motion, and the materials can be uniformly dispersed to all positions at the bottom of the inner drum wall.
Drawings
FIG. 1 is a schematic diagram of the structure of the present invention;
FIG. 2 is a view A-A of FIG. 1;
FIG. 3 is a view B-B of FIG. 1;
FIG. 4 is a schematic view of the structure of an elastic telescopic rod;
FIG. 5 is a schematic diagram of the connection of the rotating shaft to the dispenser;
FIG. 6 is a view C-C of FIG. 5;
1 is a shell, 2 is a top cover, 3 is a rotary drum, 4 is a driving motor, 5 is a liquid outlet, 6 is an air outlet, 7 is an air inlet, 8 is an air source, 9 is an inner drum wall, 10 is an outer drum wall, 11 is an upper annular plate, 12 is a lower annular plate, 13 is an upper cavity, 14 is a middle cavity, 15 is a lower cavity, 16 is a guide plate, 17 is a charging barrel, 18 is a discharge outlet, 19 is a rotating shaft, 20 is an elastic telescopic rod, 21 is a scraper blade, 22 is a brush, 23 is a liquid inlet channel, 24 is a feed pipe, 25 is a motor, 26 is a transmission shaft, 27 is a first connecting rod, 28 is a spring, 29 is a second connecting rod, 30 is an upper drainage tube, 31 is a lower drainage tube, 32 is a distributor, 33 is a distribution channel, and 34 is a shock absorption support.
Detailed Description
The following examples are given to illustrate the invention in detail, but are not intended to limit the scope of the invention in any way. The components, structures, mechanisms, sensors, and the like of the unit modules according to the following embodiments are commercially available products unless otherwise specified.
Examples: as shown in FIGS. 1-6, a crystal centrifuge for potassium aurous cyanide production comprises
The device comprises a shell 1, wherein a liquid outlet 5 is formed in the bottom of the left side of the shell 1, and an exhaust port 6 is formed in the right lower part of the shell 1;
the top cover 2 is connected to the top of the shell 1 in a sealing way, the left side of the top cover 2 is provided with an air inlet 7, the air inlet 7 is connected with an air source 8 through an air supply pipe, and the air source 8 is used for providing sufficient nitrogen for the centrifugal machine;
The rotary drum 3, the rotary drum 3 includes the inner drum wall 9 and outer drum wall 10 coaxially set up in chassis 1, take the form of inverted round table, there are filter pores on inner drum wall 9 and outer drum wall 10, and the pore size of the filter pore on the inner drum wall 9 is greater than the filter pore on the outer drum wall 10, thus the crystal of the smaller particle size can pass the filter pore on the inner drum wall 9, and filter by the filter pore on the outer drum wall 10; the top end of the inner drum wall 9 is higher than the top end of the outer drum wall 10, and the top ends of the inner drum wall 9 and the outer drum wall 10 are correspondingly connected with an upper annular plate 11 and a lower annular plate 12 respectively, and the upper annular plate 11 and the lower annular plate 12 divide the inner space of the shell 1 into an upper cavity 13, a middle cavity 14 and a lower cavity 15.
The inner side of the shell 1, the upper annular plate 11 and the upper annular plate 12 are respectively provided with a material guide plate 16, the outer side of the shell 1 is provided with a plurality of material cylinders 17, the shell 1 is provided with material discharge openings 18 matched with the material guide plates 16 and the material cylinders 17, and part of the material cylinders 17 are communicated with the upper cavity 13 through the material discharge openings 18, and part of the material cylinders 17 are communicated with the middle cavity 13 through the material discharge openings 18.
The upper cavity 13 is internally provided with a rotating shaft 19 coaxial with the inner drum wall 9, the rotating shaft 19 is provided with an elastic telescopic rod 20, the other end of the elastic telescopic rod 20 is connected with a scraping plate 21, the scraping plate 21 is provided with a brush 22, the inclined direction of the scraping plate 22 is consistent with that of the inner drum wall 9, the rotating shaft 19 is hollow to form a liquid inlet channel 23, the top end of the rotating shaft 19 upwards penetrates through the top cover 2, the inner cavity of the rotating shaft 19 is rotationally connected with a feeding pipe 24 through a bearing, and the outer wall of the rotating shaft is in transmission connection with a motor 25 (gear transmission or chain transmission).
The driving motor 4 is fixedly arranged at the bottom of the casing 1, a power output shaft of the driving motor 4 is in transmission connection with the bottom end of the transmission shaft 26, and the top end of the transmission shaft 26 penetrates through the bottom plate of the casing 1 and is fixedly connected with the rotary drum 3 so as to drive the rotary drum 3 to rotate, namely, drive the inner drum wall 9 and the outer drum wall 10 to rotate.
In this embodiment, the elastic telescopic rod 20 includes a first connecting rod 27, a spring 28 and a second connecting rod 29, where the first connecting rod 27 is composed of a first round rod and a second round rod coaxially arranged, the radial dimension of the first round rod is greater than that of the second round rod, the second connecting rod 29 is hollow and is slidably connected with the second round rod, the spring 28 is sleeved on the second round rod, one end of the spring 28 is fixedly connected with the first round rod, and the other end is fixedly connected with the second connecting rod 29.
In this embodiment, in order to smoothly discharge the gas in the casing 1, an upper drainage tube 30 for communicating the upper cavity 13 with the middle cavity 14 is provided on one side of the outer wall of the casing 1, and a lower drainage tube 31 for communicating the middle cavity 14 with the lower cavity 15 is provided on the other side of the outer wall of the casing 1.
In this embodiment, in order to uniformly disperse the material to the bottom of the inner drum wall 9, a disc-shaped distributor 32 is rotatably connected to the bottom of the rotating shaft 19, and a plurality of arc-shaped distributing channels 33 communicating with the liquid inlet channel 23 are provided on the distributor 32.
In this embodiment, the guide plate 16 is a curved plate.
In this embodiment, the bottom of the housing 1 is provided with shock struts 34.
In this embodiment, the included angle between the generatrix of the inner drum wall 9 and the horizontal plane is larger than the included angle between the generatrix of the outer drum wall 10 and the horizontal plane.
The operation and use method of the centrifugal machine is as follows:
The solution containing the crystals enters the feeding channel 23 through the feeding pipe 24, and at the bottom of the rotary drum 3, the solution is uniformly dispersed at all positions at the bottom of the rotary drum 3 through the distributing channel 33; under the drive of the driving motor 4, the inner drum wall 9 and the outer drum wall 10 rotate around the axis of the inner drum wall 9, and under the action of centrifugal force, crystals with large particle size level are filtered by the inner drum wall 9 and are thrown onto the upper annular plate 11, and as the upper annular plate 11 is fixedly connected with the inner drum wall 9, the crystals with large particle size level continue to perform centrifugal motion on the upper annular plate 11 and enter the charging barrel 17 through the discharging hole 18 to be collected under the action of the material guide plate 16. The crystals with small particle size level pass through the filtering holes on the inner drum wall 9 and are filtered by the outer drum wall 10, and then are thrown on the lower annular plate 12 under the action of centrifugal force, and the crystals with small particle size level continue to do centrifugal motion on the lower annular plate 12 due to the fixed connection of the lower annular plate 12 and the outer drum wall 10, and enter the charging barrel 17 through the discharging hole 18 under the action of the material guiding plate 16 for collection.
When the centrifugal machine runs for a period of time, part of filter holes on the inner drum wall 9 are blocked by crystals, the filtering effect of the inner drum wall 9 on the crystals is reduced, at this time, the motor 25 drives the rotating shaft 26 to rotate, under the action of centrifugal force, the elastic telescopic rod 20 stretches to enable the scraping plate 21 and the hairbrush 22 to be in contact with the inner drum wall 9, and then the crystals on the inner drum wall 9 are scraped off, and after the rotating shaft 26 stops rotating, under the action of the elastic force of the spring 28, the elastic telescopic rod 20 shortens to enable the scraping plate 21 and the hairbrush 22 to be out of contact with the inner drum wall 9.
Nitrogen enters the upper cavity 13 from the left upper part of the shell 1 through the air inlet 7, enters the middle cavity 14 through the upper drainage tube 30, enters the lower cavity 15 through the lower drainage tube 31, and is discharged through the air outlet 6 at the right lower part of the shell 1, so that toxic gas in the shell 1 is completely discharged.
Finally, it is noted that the above-mentioned embodiments are merely for illustrating the technical solution of the present invention, and that other modifications and equivalents thereof by those skilled in the art should be included in the scope of the claims of the present invention without departing from the spirit and scope of the technical solution of the present invention.

Claims (8)

1. A crystal centrifuge for producing potassium aurous cyanide comprises
The bottom of the shell is provided with a liquid outlet;
the top cover is connected to the top of the shell in a sealing way;
the rotary drum is arranged in the shell;
The method is characterized in that: the rotary drum comprises an inverted truncated cone-shaped inner drum wall and an inverted truncated cone-shaped outer drum wall, filter holes are formed in the inner drum wall and the outer drum wall, the diameter of the filter holes in the inner drum wall is larger than that of the filter holes in the outer drum wall, the top end of the inner drum wall is higher than that of the outer drum wall, an upper annular plate and a lower annular plate are correspondingly connected to the top ends of the inner drum wall and the outer drum wall respectively, and the inner space of the shell is divided into an upper cavity, a middle cavity and a lower cavity by the upper annular plate and the lower annular plate;
a rotating shaft coaxial with the inner drum wall is arranged in the upper cavity, an elastic telescopic rod is arranged on the rotating shaft, the other end of the elastic telescopic rod is connected with a scraping plate, the inclined direction of the scraping plate is consistent with that of the inner drum wall, the interior of the rotating shaft is hollow to form a liquid inlet channel, the inner cavity at the top end of the rotating shaft is connected with a feeding pipe, and the outer wall of the rotating shaft is in transmission connection with a motor;
the inner side of the shell, the upper annular plate and the upper annular plate are respectively provided with a material guide plate, the outer side of the shell is provided with a charging barrel, and the shell is provided with a material outlet matched with the material guide plates and the charging barrels;
The top cover is provided with an air inlet, the air inlet is connected with an air source through an air supply pipe, the bottom of the shell is provided with an air outlet, one side of the outer wall of the shell is provided with an upper drainage pipe used for communicating an upper cavity with a middle cavity, and the other side of the outer wall of the shell is provided with a lower drainage pipe used for communicating the middle cavity with a lower cavity.
2. The crystal centrifuge for producing potassium aurous cyanide according to claim 1, wherein: the elastic telescopic rod comprises a first connecting rod, a spring and a second connecting rod, wherein the first connecting rod is in sliding connection with the second connecting rod, one end of the spring is fixedly connected with the first connecting rod, and the other end of the spring is fixedly connected with the second connecting rod.
3. The crystal centrifuge for producing potassium aurous cyanide according to claim 1, wherein: the rotary shaft bottom is rotationally connected with a discoid distributor, and a plurality of arc-shaped distributing channels communicated with the liquid inlet channels are arranged on the distributor.
4. The crystal centrifuge for producing potassium aurous cyanide according to claim 1, wherein: the inner drum wall and the outer drum wall are coaxial.
5. The crystal centrifuge for producing potassium aurous cyanide according to claim 1, wherein: the material guide plate is a curved plate.
6. The crystal centrifuge for producing potassium aurous cyanide according to claim 1, wherein: and the scraping plate is provided with a hairbrush.
7. The crystal centrifuge for producing potassium aurous cyanide according to claim 1, wherein: and a shock absorption support column is arranged at the bottom of the shell.
8. The crystal centrifuge for producing potassium aurous cyanide according to claim 1, wherein: and the included angle between the generatrix of the inner drum wall and the horizontal plane is larger than the included angle between the generatrix of the outer drum wall and the horizontal plane.
CN201910359079.XA 2019-04-30 2019-04-30 Crystal centrifuge is used in potassium aurous cyanide production Active CN110026296B (en)

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Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110918273A (en) * 2019-11-19 2020-03-27 刘晓慧 High-efficient type centrifuge of stability
CN110813558A (en) * 2019-11-19 2020-02-21 蚌埠精工制药机械有限公司 Drum device of sedimentation centrifuge
CN111774190B (en) * 2020-06-19 2021-10-01 甘肃普罗生物科技有限公司 Casein production is with continuous mechanism of getting rid of impurity on centrifugal slag removal device surface

Citations (4)

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CN204448303U (en) * 2015-03-02 2015-07-08 江西北辰德天然生物科技有限公司 A kind of automation centrifuge extracting natural borneol
WO2015181177A1 (en) * 2014-05-28 2015-12-03 Gea Mechanical Equipment Gmbh Separator
CN206104135U (en) * 2016-08-13 2017-04-19 安徽东至广信农化有限公司 A centrifuge for $drafting sweet phosphine production
CN209968659U (en) * 2019-04-30 2020-01-21 三门峡朝阳科技有限公司 Crystal centrifuge is used in potassium aurous cyanide production

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2015181177A1 (en) * 2014-05-28 2015-12-03 Gea Mechanical Equipment Gmbh Separator
CN204448303U (en) * 2015-03-02 2015-07-08 江西北辰德天然生物科技有限公司 A kind of automation centrifuge extracting natural borneol
CN206104135U (en) * 2016-08-13 2017-04-19 安徽东至广信农化有限公司 A centrifuge for $drafting sweet phosphine production
CN209968659U (en) * 2019-04-30 2020-01-21 三门峡朝阳科技有限公司 Crystal centrifuge is used in potassium aurous cyanide production

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