CN110004709A - A kind of preparation and application of energy-efficient bath agent - Google Patents

A kind of preparation and application of energy-efficient bath agent Download PDF

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Publication number
CN110004709A
CN110004709A CN201810006898.1A CN201810006898A CN110004709A CN 110004709 A CN110004709 A CN 110004709A CN 201810006898 A CN201810006898 A CN 201810006898A CN 110004709 A CN110004709 A CN 110004709A
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minutes
energy
agent
bath agent
efficient
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林丽
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Quanzhou Bluebird Trading Co Ltd
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Quanzhou Bluebird Trading Co Ltd
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Priority to CN201810006898.1A priority Critical patent/CN110004709A/en
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    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06L—DRY-CLEANING, WASHING OR BLEACHING FIBRES, FILAMENTS, THREADS, YARNS, FABRICS, FEATHERS OR MADE-UP FIBROUS GOODS; BLEACHING LEATHER OR FURS
    • D06L4/00—Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs
    • D06L4/10—Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs using agents which develop oxygen
    • D06L4/12—Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs using agents which develop oxygen combined with specific additives
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06L—DRY-CLEANING, WASHING OR BLEACHING FIBRES, FILAMENTS, THREADS, YARNS, FABRICS, FEATHERS OR MADE-UP FIBROUS GOODS; BLEACHING LEATHER OR FURS
    • D06L4/00—Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs
    • D06L4/10—Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs using agents which develop oxygen
    • D06L4/13—Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs using agents which develop oxygen using inorganic agents
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06L—DRY-CLEANING, WASHING OR BLEACHING FIBRES, FILAMENTS, THREADS, YARNS, FABRICS, FEATHERS OR MADE-UP FIBROUS GOODS; BLEACHING LEATHER OR FURS
    • D06L4/00—Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs
    • D06L4/40—Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs using enzymes
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/73—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with carbon or compounds thereof
    • D06M11/74—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with carbon or compounds thereof with carbon or graphite; with carbides; with graphitic acids or their salts
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/77—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof
    • D06M11/79—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof with silicon dioxide, silicic acids or their salts
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/16—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using dispersed, e.g. acetate, dyestuffs
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/38—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using reactive dyes
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/445—Use of auxiliary substances before, during or after dyeing or printing
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/673—Inorganic compounds
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/673—Inorganic compounds
    • D06P1/67383—Inorganic compounds containing silicon
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
    • D06P3/58—Material containing hydroxyl groups
    • D06P3/60—Natural or regenerated cellulose
    • D06P3/66—Natural or regenerated cellulose using reactive dyes
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/02—Natural fibres, other than mineral fibres
    • D06M2101/04—Vegetal fibres
    • D06M2101/06—Vegetal fibres cellulosic

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Cosmetics (AREA)
  • Coloring (AREA)

Abstract

The present invention provides the preparation and its application of a kind of energy-efficient bath agent, integrate that refining, alkali, oxygen bleaching be stable, oxidation bleaching, have the advantages that easy to operate, efficient and convenient, refining floats bottom and do not need to add other auxiliary agents.Suitable for the boiling-off of the fabrics such as cotton, polyester-cotton blend, yarn and staple in bulk etc., degreasing, the disposable pre-treatment deoiled and bleached.Fabric damage caused by scouringing and bleaching can be effectively reduced, weight-loss ratio improves white goods feel, improves textile added value.Pre-treatment process time is greatly reduced, shortens washing step after pre-treatment, improves production efficiency.

Description

A kind of preparation and application of energy-efficient bath agent
Technical field
The present invention relates to filed of daily-use chemical industry, and in particular to a kind of energy-efficient one bathes agent and application.
Background technique
Textile industry is China's conventional column industry, wherein textile dyeing and finishing be dyeing and weaving basis and textile industry one A important link.It is well known that during textile fabric embryo cloth is made based on cottonseed, ash impurity, oil content in fiber itself etc. with spinning The compositions such as the greasy dirt of generation must first remove the compositions such as this oil content, impurity before subsequent dyeing process, and here it is pre-treatment works Sequence improves bright and clean fabrics cloth cover, dye-uptake, the uniform level dyeing of enhancing after the processing of the physico-chemical process such as degradation, emulsification or dissolution Property, reduce dyeing defect rate；Dyeing and finishing process dyeing postprocessing working procedures be then the cloth hair that will be attached on dyed fabric, it is loose colour, miscellaneous Matter etc., by being cleaned multiple times, soaping etc., techniques obtain clean and tidy cloth cover, it is ensured that product items fastness and its physics, appearance index Reach requirement, by this common process method, contaminating the straight-through production of a cylinder dark color cloth is generally about needed 10 hours or more.
The generally first oxygen bleaching pre-treatment of traditional processing method, then carry out dispersing/two one-bath two-step process dyeings of activity, i.e., in weak acid It contaminates and washs under the conditions of property；Add alkali reduction cleaning with sodium hydrosulfite again, remove PET fiber surface and stains the dispersion on cotton component Dyestuff；Then it is neutralized with acetic acid, then with Dyeing of Cotton Fabric with Reactive Dyes component；It finally carries out after washing and being soaped with soaping agent into high temperature Reason, the complex process, time-consuming, water consumption, energy consumption, production cost is also higher, also gives off a large amount of waste water, and handles before tradition It is the major part of the energy and cost, especially water consume and a large amount of row with the water in dyeing postprocessing working procedures, vapour, electric energy consumption Put the problem of always enterprise.
Therefore, how the dyeing and finishing technology that a kind of high-efficient effect is good and low energy consumption is provided, be those skilled in the art urgently It solves the problems, such as.
Summary of the invention
In view of the above-mentioned problems, the purpose of the present invention is to provide a kind of high efficiency and good energy-efficient one that low energy consumption of effect It bathes agent and its uses technique.
To achieve the goals above, the present invention adopts the following technical scheme:
A kind of energy-efficient bath agent, which is characterized in that including following components:
Calculate by mass percentage, cross carbon:, sodium metasilicate: 8-15%, surface activity carbon: 1.5%-5.5%, blue grain Son: 0.02-0.05%, green particles: 0.02-0.05%.
It is another object of the present invention to provide a kind of preparation methods of energy-efficient bath agent, comprising the following steps:
(1) the inclined silicon for crossing carbon, 8-15% of mass ratio 79.4%-90.46% is sequentially added in 0.5 ton of horizontal mixer Sour sodium, the surface activity carbon of 1.5%-5.5%, the blue particles of 0.02-0.05%, the green particles of 0.02-0.05% are opened Stirring；
(2) by blender revolving speed be 25-30 revs/min in the case of rotates forward and inverts 6-10 minutes after 6-10 minute, stir Up to energy-efficient bath agent, discharging packaging after uniformly.
The beneficial effect of above scheme is: providing a kind of energy-efficient bath agent, no added alkyl phenol polyoxyethylene ether The addition of the toxic chemical substance such as class compound, it is more environmentally-friendly, and have higher efficiency, it is dyed using the product Pre-treatment has higher production efficiency.
It is a further object to provide a kind of application methods of energy-efficient bath agent, specifically take following technology Scheme:
A kind of use technique of energy-efficient bath agent, which is characterized in that for the bleaching of pure cotton, process are as follows: enter water → energy-efficient bath agent, degreaser and bleeding agent is added → is warming up to 70 DEG C → addition hydrogen peroxide → 10 minute after ten minutes After be warming up to 98 DEG C react adjust within 60 minutes → be cooled to 60 DEG C → pH to 4.5-5 be added acidic bio enzyme → addition brightening agent → It is warming up to 98 DEG C to react 30 minutes → being cooled to 60 DEG C → washing → softness → cylinder out；
The ratio of an energy-efficient bath agent and the degreaser and bleeding agent and hydrogen peroxide is 6: 1: 1: 10.
In some schemes, it may also be used for the dyeing pre-treatment of shallow, the gorgeous color of pure cotton, process are as follows: it is efficient to enter water → addition Agent is bathed in energy conservation one, degreaser and bleeding agent → be warming up to 70 DEG C → hydrogen peroxide are added → after ten minutes are warming up to 98 after ten minutes DEG C reaction 60 minutes → being cooled to 60 DEG C to plate → be warming up to 60-70 DEG C wash 15 minutes → adjust pH to 6-7 be added it is neutral raw Reactive dye → dyeing is added in object enzyme after ten minutes；
The ratio of an energy-efficient bath agent and the degreaser and bleeding agent and hydrogen peroxide is 6: 1: 1: 6-10.
In other schemes, it may also be used in pure cotton, the pre-treatment of deep colour dyeing, process are as follows: it is high to enter water → addition Effect energy conservation one bathe agent, degreaser and bleeding agent → being warming up to 98 DEG C after ten minutes to react 60 minutes → be cooled to 60 DEG C → be warming up to 60-70 DEG C is washed 15 minutes → adjusting pH to 6-7 addition neutrophilous organism enzyme and reactive dye → dyeing is added after ten minutes；
The ratio of an energy-efficient bath agent and the degreaser and bleeding agent is 4: 1: 1.
In other schemes, it may also be used for T/C bleaching, process are as follows: enter water → addition energy-efficient a bath agent, degreaser With bleeding agent → hydrogen peroxide is added after ten minutes and is warming up to 70 reaction 10 minutes → and is warming up to 98 DEG C and reacts 30 minutes → cooling To 80 DEG C to be cooled to after sample 60 DEG C → adjust pH to 4.5-510 minutes after be warming up to 55 DEG C of addition acidic bios enzyme 50 minutes after It is added brightening agent → be warming up to 130 DEG C after ten minutes to react 30 minutes → → being cooled to 60 DEG C → washing that is cooled to 80 DEG C to sample → Soft treatment → go out cylinder.
The ratio of an energy-efficient bath agent and the degreaser and bleeding agent and hydrogen peroxide is 5: 1: 1: 8.
In some other concrete schemes, it may also be used for T/C dispersion/vital staining, process are as follows: it is efficient to enter water → addition Energy conservation one bathe agent, degreaser and bleeding agent → being warming up to 98 DEG C after ten minutes to react 40 minutes → be cooled to 60 DEG C → change cylinder adjusting Score material → 10 minute are added after pH to 4.5-5.5 → be warming up to 55 DEG C after ten minutes and be added acidic bio enzyme reaction 50 minutes After be warming up to 130 DEG C of reactions 30-60 minutes → being cooled to 80 DEG C to sample → be cooled to 60 degrees Celsius → plus water and reactive dye → Dyeing；
The ratio of an energy-efficient bath agent and the degreaser and bleeding agent is 4: 1: 1.
The beneficial effects of the present invention are: a kind of technique that dyeing pre-treatment is carried out using energy-efficient bath agent is provided, It can be obtained excellent whiteness and scouring result without using caustic soda, scouring agent, stabilizer etc., and then can be effectively reduced to scouring and bleaching and make At fabric damage, weight-loss ratio, improve white goods feel, improve textile added value.It is poor that cylinder can also dramatically be improved, Dyeing uniformity is more preferably.It is important that pre-treatment process time can also be greatly reduced, shortens washing step after pre-treatment, mention High efficiency, and handle after without neutralize, draining water inlet can carry out dyeing process, not only save dyeing and finishing water, electricity consumption, With vapour, discharge of wastewater is reduced.And without any harmful chemicals such as APEO, meet outlet environmental requirement.
Specific embodiment
Technical solution provided by the invention will be described further below.
Embodiment 1
The preparation of energy-efficient bath agent:
(1) the inclined silicon for crossing carbon, 8-15% of mass ratio 79.4%-90.46% is sequentially added in 0.5 ton of horizontal mixer Sour sodium, the surface activity carbon of 1.5%-5.5%, the blue particles of 0.02-0.05%, the green particles of 0.02-0.05% are opened Stirring；
(2) by blender revolving speed be 25-30 revs/min in the case of rotates forward and inverts 6-10 minutes after 6-10 minute, stir Up to energy-efficient bath agent, discharging packaging after uniformly.
Fabric will be handled using energy-efficient bath agent made from this method below:
Embodiment 2
The bleaching (being handled containing defeathering) of pure cotton:
Embodiment 3
Pure cotton is shallow, gorgeous color (handling containing defeathering)
Note: defeathering is not handled, and 60 DEG C of hot wash of pre-treatment are cancelled；Degreaser containing spandex thread 1%；8 cylinder water are handled containing defeathering； 7 cylinder water are handled without defeathering.
Embodiment 4
In pure cotton, dark (being handled containing defeathering)
Note: defeathering is not handled, and 60 DEG C of hot wash of pre-treatment are cancelled.Defeathering handles 8 cylinder water, and defeathering does not handle 7 cylinder water.
Embodiment 5
T/C bleaching (is handled) containing defeathering
Note: the direct water inlet of defeathering processing is not brightened；Totally 4 cylinder water.
Embodiment 6
T/C dispersion/vital staining (is handled) containing defeathering
Note: fixed normal reduction cleaning in bright red system and need.Others not wash without exception and reduction cleaning；Specific demand According to circumstances whether reduction cleaning is used with color.
By being measured to embodiment 1, the energy-efficient bath agent pH is between 6-8；
By measuring embodiment 2-6 effluent quality, COD is discharged between 60-70%；
It is measured by the fabric handled embodiment 2-6, weight-loss ratio is respectively less than 3%, and bursting ability exists 90-100%.
Above-described embodiment shows using technical solution provided by the invention compared with traditional soda boiling technique, saves individually Pretreatment procedure will boil drift and be combined into one with dyeing, compared with prior art, saves reaction process, substantially reduce entire Time needed for process, and reduce steam consumption, and then improve dyeing efficiency, and dyeing effect can still meet existing dye Colour standard.And without adding auxiliary agent etc., a part of cost is eliminated, damage of the auxiliary agent to cloth, strength loss are also reduced It is small, it is soft after processing, it is important that water consumption is in 4-10 cylinder, and for traditional soda boiling technique, cloth per ton at least subtracts Water consumption is greatly saved in few water consumption 3-4 cylinder, and due to APEO of the additive without poisonous and harmful substances, dye in a bath agent Effluent quality COD content after color is between 60-70%, and tradition soda boiling Process for Effluent COD is 100% or so, therefore with Traditional handicraft is compared, and technical solution provided by the invention also reduces the pollution to environment.
The above shows and describes the basic principles and main features of the present invention and the advantages of the present invention.The technology of the industry Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the above embodiments and description only describe this The principle of invention, without departing from the spirit and scope of the present invention, various changes and improvements may be made to the invention, these changes Change and improvement all fall within the protetion scope of the claimed invention.

Claims (8)

1. a kind of energy-efficient bath agent, which is characterized in that the energy-efficient bath agent includes following components:
Calculate by mass percentage, cross carbon:, sodium metasilicate: 8-15%, surface activity carbon: 1.5%-5.5%, blue particles: 0.02-0.05%, green particles: 0.02-0.05%.
2. a kind of preparation method of energy-efficient bath agent, which comprises the following steps:
(1) mass ratio 79.4%-90.46% is sequentially added in blender crosses carbon, the sodium metasilicate of 8-15%, 1.5%- Blue particles, the green particles of 0.02-0.05% of 5.5% surface activity carbon, 0.02-0.05% open stirring；
(2) it is inverted after rotating forward blender, after mixing evenly up to energy-efficient bath agent, discharging packaging.
3. a kind of application of energy-efficient bath agent, which is characterized in that for the bleaching of pure cotton, process are as follows: enter water → addition Energy-efficient one bathes agent, degreaser and is warming up to 70-75 DEG C → addition hydrogen peroxide → 10-15 after bleeding agent → 10-15 minutes 96-100 DEG C of reaction 50-70 minutes → being cooled to 55-60 DEG C → is warming up to after minute to adjust pH to 4.5-5, acidic bio is added Enzyme → addition brightening agent → is warming up to 96-100 DEG C of reaction 25-35 minutes → being cooled to 55-65 DEG C → washing → softness → and goes out cylinder；
Wherein, an energy-efficient bath agent and the mass ratio of the degreaser, bleeding agent, hydrogen peroxide are 6: 1: 1: 10.
4. the application of the energy-efficient bath agent of one kind according to claim 1, which is characterized in that can also be used in pure cotton it is shallow, The dyeing pre-treatment of gorgeous color, process are as follows: enter water → the energy-efficient bath agent of addition, degreaser and bleeding agent → and rise after ten minutes Temperature is to 70 DEG C → to be added hydrogen peroxide → to be warming up to 98 DEG C of reactions 60 minutes → being cooled to 60 DEG C to plate → after ten minutes to be warming up to 60-70 DEG C is washed 15 minutes → adjusting pH to 6-7 addition neutrophilous organism enzyme and reactive dye → dyeing is added after ten minutes；
Wherein, an energy-efficient bath agent and the mass ratio of the degreaser, bleeding agent, hydrogen peroxide are 6: 1: 1: 6-10.
5. the application of the energy-efficient bath agent of one kind according to claim 1, which is characterized in that can also be used in pure cotton, The pre-treatment of deep colour dyeing, process are as follows: enter water → the energy-efficient bath agent of addition, degreaser and bleeding agent → and rise after ten minutes Temperature is reacted to 98 DEG C is warming up to 60-70 DEG C of washing 15 minutes → adjusting pH to 6-7 addition neutrality for 60 minutes → being cooled to 60 DEG C → Reactive dye → dyeing is added in biological enzyme after ten minutes；
Wherein, the mass ratio of an energy-efficient bath agent and the degreaser, bleeding agent is 4: 1: 1.
6. the application of the energy-efficient bath agent of one kind according to claim 1, which is characterized in that it can also be used in T/C bleaching, Its process are as follows: enter the energy-efficient bath agent of water → addition, degreaser and bleeding agent → hydrogen peroxide is added after ten minutes are warming up to 70 reactions 10 minutes → be warming up to 98 DEG C react 30 minutes → be cooled to 80 DEG C to be cooled to after sample 60 DEG C → adjust pH to 4.5- 5, it is warming up to 55 DEG C of addition acidic bios after ten minutes, brightening agent → be warming up to 130 DEG C of reactions after ten minutes is added after enzyme 50 minutes Be cooled within 30 minutes → being cooled to 80 DEG C to sample → 60 DEG C → washing → soft treatment → go out cylinder；
Wherein, an energy-efficient bath agent and the mass ratio of the degreaser, bleeding agent, hydrogen peroxide are 5: 1: 1: 8.
7. the application of the energy-efficient bath agent of one kind according to claim 1, which is characterized in that can also be used in T/C dispersion/ Vital staining, process are as follows: enter the energy-efficient bath agent of water → addition, degreaser and bleeding agent → be warming up to 98 DEG C after ten minutes Reaction 40 minutes → be cooled to 60 DEG C → adjusting pH to 4.5-5.5 → is warming up to 55 DEG C after ten minutes and that acidic bio enzyme is added is anti- Score material → being warming up to 130 DEG C of reactions 30-60 minutes after ten minutes → is added after answering 50 minutes and is cooled to 80 DEG C to sample → cooling To 60 degrees Celsius → plus water and reactive dye → dyeing；
Wherein, the mass ratio of an energy-efficient bath agent and the degreaser and bleeding agent is 4: 1: 1.
8. according to the application of the energy-efficient bath agent of the described in any item one kind of claim 3-7, which is characterized in that addition activity It, can be according to the difference of coloured silk to be dyed and the different addition anhydrous sodium sulphate of material to be dyed cloth and and alkali before dyestuff.
CN201810006898.1A 2018-01-04 2018-01-04 A kind of preparation and application of energy-efficient bath agent Pending CN110004709A (en)

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CN201810006898.1A CN110004709A (en) 2018-01-04 2018-01-04 A kind of preparation and application of energy-efficient bath agent

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Application Number Priority Date Filing Date Title
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