CN109988982A - Copper post anaerobic annealing process - Google Patents

Copper post anaerobic annealing process Download PDF

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Publication number
CN109988982A
CN109988982A CN201711491966.XA CN201711491966A CN109988982A CN 109988982 A CN109988982 A CN 109988982A CN 201711491966 A CN201711491966 A CN 201711491966A CN 109988982 A CN109988982 A CN 109988982A
Authority
CN
China
Prior art keywords
copper
copper post
annealing
cylinder
post
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201711491966.XA
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Chinese (zh)
Inventor
崔锡恩
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Qingdao Jin Yue Long Machinery Co Ltd
Original Assignee
Qingdao Jin Yue Long Machinery Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Qingdao Jin Yue Long Machinery Co Ltd filed Critical Qingdao Jin Yue Long Machinery Co Ltd
Priority to CN201711491966.XA priority Critical patent/CN109988982A/en
Publication of CN109988982A publication Critical patent/CN109988982A/en
Pending legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D1/00General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering
    • C21D1/26Methods of annealing
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D1/00General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering
    • C21D1/68Temporary coatings or embedding materials applied before or during heat treatment
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22FCHANGING THE PHYSICAL STRUCTURE OF NON-FERROUS METALS AND NON-FERROUS ALLOYS
    • C22F1/00Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working
    • C22F1/08Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working of copper or alloys based thereon

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Processing Of Solid Wastes (AREA)

Abstract

The invention discloses a kind of copper post anaerobic annealing process, including following work step: cleaning copper post gasoline before annealing and dries;Copper post is packed into copper cylinder;Copper cylinder is put into electric furnace, fire door is shut;It is made annealing treatment;Copper cylinder is come out of the stove, and copper cylinder is put into sink, after flowing cool water cooling, takes out copper post;It is characterized by: filling up pig scrap in copper cylinder after copper post is packed into copper cylinder.When annealing, for heating temperature between 450 DEG C~650 DEG C, soaking time is 100 minutes~200 minutes.Present invention process is oxidized when copper post annealing can be effectively prevented, and reduces the scrappage of copper post, reduces production cost, and simple process, safe and reliable.

Description

Copper post anaerobic annealing process
Technical field
The present invention relates to a kind of copper post anaerobic annealing process.
Background technique
Copper post is the element for measuring various weapon gun pressures, it is the core element of Cu atomic weight.It is passed through by copper ingot It draws to dial repeatedly and copper wire is made, then made of vehicle system, copper post should have good surface quality, and deform uniform.Copper cylinder has Taper copper post and two kinds of cylindricality copper post.Copper post annealing is one of very important process, the purpose of annealing in copper post process It is to eliminate copper wire in order to refine grain structure and draw the internal stress dialled and generated in copper post mechanical processing process repeatedly.Copper post annealing With copper cylinder or the box-packed Sheng copper post of copper, auxiliary material has asbestos board, asbestos cord, waterglass, gasoline, alcohol, copper sheet, red copper bits etc..For Copper post is prevented to be oxidized in annealing, when copper post is packed into copper cylinder (copper box), red copper bits are filled up in the space for being underfilled with copper post, And separated copper post and red copper bits with copper sheet, asbestos board, finally it is sealed with asbestos cord and waterglass.When poorly sealed or Person puts when having large quantity of air in cylinder after copper post, and in annealing, with copper scale, copper post oxidation reaction will occur for the oxygen in air, It generates copper oxide and causes scrapping for copper post so that there is oxidized streak on copper post surface.
Summary of the invention
It is an object of the invention to: it is oxidized when one kind being provided, copper post annealing can be effectively prevented, reduces copper post scrappage Copper post anaerobic annealing process.
Present invention process includes following work step: cleaning copper post gasoline before annealing and dries;Copper post is packed into copper cylinder;It will Copper cylinder is put into electric furnace, shuts fire door;It is made annealing treatment;Copper cylinder is come out of the stove, and copper cylinder is put into sink, cooling with flowing cool water Afterwards, copper post is taken out;It is characterized by: filling up pig scrap in copper cylinder after copper post is packed into copper cylinder.
When the present invention makes annealing treatment, for heating temperature between 450 DEG C~650 DEG C, soaking time is 100 minutes~200
Minute.
When the present invention makes annealing treatment, for heating temperature between 500 DEG C~600 DEG C, soaking time is 120 minutes~160 points Clock.
Present invention process is oxidized when copper post annealing can be effectively prevented, and reduces the scrappage of copper post, reduces production cost, And it is simple process, safe and reliable.
Specific embodiment
The present invention is described in detail with reference to embodiments.
The annealing operation of copper post is divided into five work steps and carries out:
It is dried 1. cleaning copper post gasoline before annealing.
2. copper post is packed into copper cylinder (copper box).
3. copper cylinder (copper box) is put into electric furnace, fire door is shut.
4. being made annealing treatment, for heating temperature between 450 DEG C~650 DEG C, soaking time is 100 minutes~200 minutes, And it makes a record.
5. bronze medal cylinder (copper box) is come out of the stove, copper cylinder (copper box) is put into sink, after flowing cool water cooling, takes out copper post.
The invention is in work step 2 different from original process.After installing copper post, copper post is underfilled in copper cylinder (copper box) Space fill up pig scrap, with pig scrap instead of red copper consider to be worth doing;Because iron is the active metal of comparison, its movable metallic ratio Copper is strong, and when having large quantity of air in poorly sealed or cylinder, at high temperature, oxidation reaction will occur with the oxygen in air for iron, raw At iron oxide, the oxygen in air is consumed, and the activity of copper is weaker, and oxidation reaction will not occur with oxygen, to protect copper post.
Embodiment 1:
First copper post gasoline is cleaned and is dried, then copper post is packed into copper cylinder (copper box), is underfilled with copper post in copper cylinder (copper box) Pig scrap is filled up in space, and copper cylinder (copper box) is put into electric furnace, fire door is shut.Made annealing treatment, heating temperature 450 DEG C~ Between 650 DEG C, soaking time is 100 minutes~200 minutes, and is made a record.Copper cylinder (copper box) is come out of the stove, and copper cylinder (copper box) is put Enter in sink, after flowing cool water cooling, takes out copper post.
Embodiment 2:
It is made annealing treatment, heating temperature is between 500 DEG C~600 DEG C, and soaking time is 120 minutes~180 minutes, Qi Tagong It walks same as Example 1.
Embodiment 3:
It is made annealing treatment, heating temperature is between 550 DEG C~600 DEG C, and soaking time is 130 minutes~160 minutes, Qi Tagong It walks same as Example 1.
Embodiment 4:
When annealing, for heating temperature between 500 DEG C~600 DEG C, soaking time is 120 minutes~160 minutes.Other work steps It is same as Example 1.
Through practical proof: after replacing pig scrap red copper to consider to be worth doing, having carried out copper post annealing test 50 times, do not found 1 Example copper post is oxidized phenomenon.
What has been described above is only a preferred embodiment of the present invention, it is noted that for those skilled in the art, Without departing from the structure of the invention, several modifications and improvements can also be made, these also should be considered as guarantor of the invention Range is protected, these all will not influence the effect and patent practicability that the present invention is implemented.

Claims (3)

1. a kind of copper post anaerobic annealing process, including following work step: cleaning copper post gasoline before annealing and dry;Copper post is packed into In copper cylinder;Copper cylinder is put into electric furnace, fire door is shut;It is made annealing treatment;Copper cylinder is come out of the stove, and copper cylinder is put into sink, with stream After dynamic cold water is cooling, copper post is taken out;It is characterized by: filling up pig scrap in copper cylinder after copper post is packed into copper cylinder.
2. copper post anaerobic annealing process according to claim 1, it is characterised in that: when annealing, heating temperature is 450 DEG C~650 DEG C between, soaking time be 100 minutes~200 minutes.
3. copper post anaerobic annealing process according to claim 1, it is characterised in that: when annealing, heating temperature is 500 DEG C~600 DEG C between, soaking time be 120 minutes~160 minutes.
CN201711491966.XA 2017-12-30 2017-12-30 Copper post anaerobic annealing process Pending CN109988982A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201711491966.XA CN109988982A (en) 2017-12-30 2017-12-30 Copper post anaerobic annealing process

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201711491966.XA CN109988982A (en) 2017-12-30 2017-12-30 Copper post anaerobic annealing process

Publications (1)

Publication Number Publication Date
CN109988982A true CN109988982A (en) 2019-07-09

Family

ID=67110730

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201711491966.XA Pending CN109988982A (en) 2017-12-30 2017-12-30 Copper post anaerobic annealing process

Country Status (1)

Country Link
CN (1) CN109988982A (en)

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WD01 Invention patent application deemed withdrawn after publication

Application publication date: 20190709

WD01 Invention patent application deemed withdrawn after publication