CN109966769A - A kind of butanediol low-temperature water removal equipment and its application method - Google Patents
A kind of butanediol low-temperature water removal equipment and its application method Download PDFInfo
- Publication number
- CN109966769A CN109966769A CN201910281967.4A CN201910281967A CN109966769A CN 109966769 A CN109966769 A CN 109966769A CN 201910281967 A CN201910281967 A CN 201910281967A CN 109966769 A CN109966769 A CN 109966769A
- Authority
- CN
- China
- Prior art keywords
- butanediol
- heating tube
- distillation still
- temperature water
- water removal
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/10—Vacuum distillation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/14—Fractional distillation or use of a fractionation or rectification column
- B01D3/30—Fractionating columns with movable parts or in which centrifugal movement is caused
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/14—Fractional distillation or use of a fractionation or rectification column
- B01D3/32—Other features of fractionating columns ; Constructional details of fractionating columns not provided for in groups B01D3/16 - B01D3/30
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C31/00—Saturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
- C07C31/18—Polyhydroxylic acyclic alcohols
- C07C31/20—Dihydroxylic alcohols
- C07C31/207—1,4-Butanediol; 1,3-Butanediol; 1,2-Butanediol; 2,3-Butanediol
Abstract
The present invention relates to a kind of butanediol low-temperature water removal equipment and its application methods, belong to butanediol processing technique field, equipment includes distillation still and the capping for sealing distillation still, heating tube is connected in distillation still, the side wall of distillation still is the double-layer structure that inner and outer wall is constituted, double-layer structure is divided into mutually independent lower space and upper space, and lower space and upper space are vacuum；The outer wall of upper space is equipped with vacuum pump insert port, and the inner wall of upper space is equipped with the first check valve for passing to the accommodating chamber of distillation still；Heating tube is embedded in distillation still, and the interlude of heating tube is located in the accommodating chamber of distillation still.The present invention removes water inflammable butanediol, is reduced butanediol by the possibility of thermal oxide and burning, improve production security by the way of vacuum distillation.
Description
Technical field
The present invention relates to butanediol processing technique fields, specifically, be related to a kind of butanediol low-temperature water removal equipment and its
Application method.
Background technique
Butanediol is also referred to as 1.3- butanediol, has the characteristics that the reactive, odorless, less toxic of dihydric alcohol, good water solubility, main
It is used for organic synthesis, is the raw material of polyester resin, alkyd resin, the raw material of plasticizer, the raw material of polyurethane coating, wetting agent
And softening agent, the intermediate of medicine, dyestuff, surfactant, plasticiser, hygroscopic agent (humectant), coupling agent, solvent, food
Product addition and flavouring agent.
Butanediol is in water, acetone, methyl/ethyl (first) ketone, ethyl alcohol, dibutyl phthalate, castor oil, hardly
It is dissolved in aliphatic hydrocarbon, benzene, toluene, carbon tetrachloride, ethanolamines, mineral oil, Linseed oil.Because its boiling point is higher, steamed under normal pressure
Vulnerable to air oxidation when evaporating, in order to overcome the problem, it is usually performed under reduced pressure distillation, existing distillation equipment generallys use
Large tank cooperates related control device to carry out, but can face following problems: 1. large tank surface areas are big, and integrality is kept
Difficulty is big, and pressure keeps difficulty big, especially during carrying out relevant operation progress, and after long-time service；2. operation subtracts
It presses program and operation sealing schedule to mismatch, causes working efficiency low；3. existing vacuum distillation program control system is complicated, cooperation
Equipment is more, and use cost is high, and maintenance difficulties are big；4. distillation process is not easy the problems such as observation in time and control.
In order to better solve problem above, people are there is an urgent need to a kind of easy to use, and manipulation is simple, and distilling effect is good,
The low equipment of process control difficulties and related distillation technique.
Summary of the invention
1, it to solve the problems, such as
The big problem of control difficulty is distilled for large tank in the prior art, and the present invention provides a kind of butanediol low temperature and removes
Wetting system and its application method carry out temperature control using heating tube, and cooperation butanediol mixed flowing mode improves butanediol temperature, and
Finally realize that butanediol is evaporated under reduced pressure water removal purpose under vacuum conditions by decompression control system.
2, technical solution
To solve the above problems, the present invention adopts the following technical scheme that.
A kind of butanediol low-temperature water removal equipment, the capping including distillation still and for sealing distillation still, in the distillation still
It is connected with heating tube, the side wall of the distillation still is the double-layer structure that inner and outer wall is constituted, and the double-layer structure is divided into mutually solely
Vertical lower space and upper space, the lower space and upper space are vacuum；It is set on the outer wall of the upper space
There is vacuum pump insert port, the inner wall of upper space is equipped with the first check valve for passing to the accommodating chamber of distillation still；The heating tube
It is embedded in distillation still, two ports of heating tube extend to outside distillation still, and the interlude of heating tube is located at the appearance of distillation still
It receives in chamber；The capping includes cricoid frame, and the frame inner sidewall is equipped with stop collar, and the lower inside of frame is equipped with net
Structure, the web frame top are equipped with ventilative dottle pin, and the ventilative dottle pin is equipped with anhydrous cupric sulfate, sets above the capping
There is transparent sealant, the sealant is supported by stop collar.
Preferably, the heating tube is segmental structure, is provided with an air deflector between every two sections of heating tubes；The water conservancy diversion
Device includes the rotary clip that sealing is stuck between two heating tubes, is respectively equipped on the medial surface and lateral surface of the rotary clip
Intra vane and outer leafs, the intra vane are located inside heating tube and the sealing space of rotary clip formation, the outer leafs position
Outside above-mentioned sealing space.
Preferably, the air deflector uses in pairs, and two air deflectors being oppositely arranged constitute a convection device.
Preferably, the heating tube is equipped with card cover, and the card cover is equipped with the through-hole passed through for butanediol；Position respectively
The air deflector between two heating tubes is surrounded in the card cover in adjacent two heating tubes；On the lateral wall of the card cover
Stretching forms several strip structures, and two matched are blocked cover and mutually plugged together using strip structure thereon, the strip structure
On locking clip is cased with by way of being threadedly engaged.
Preferably, card cover is using activity rotation set by the way of being threadedly coupled in correspondence heating tube.
Preferably, it there are two the locking clip is total to, and is bonded to each other and to form anti-skid structure, being bonded to each other on face for locking clip is all provided with
There is anti-slip rubber, face of the anti-slip rubber for fitting is rough surface.
Preferably, the snap ring be equipped with annular groove on the side that is in contact of heating tube end, in the groove
Equipped with U-shaped sealing ring, in the annular groove of the end insertion respective side of the heating tube, and sealed by U-shaped sealing ring.
Preferably, steam is connected with inside the heating tube, heating tube is located at the part in the accommodating chamber of distillation still using spiral shell
Circular mode is revolved to be arranged；Second one-way valve is equipped between the upper space and lower space.
Preferably, the opening of the distillation still is equipped with annular seal groove, and the section configuration of the annular seal groove is V
Type, the capping are equipped with ring type seal compatible with annular seal groove；The upper surface of the distillation still is equipped with several
Negative pressure trough, the bottom of the negative pressure trough are equipped with interlayer made of rubber material, the interlayer be located at negative pressure trough and upper space it
Between.
A kind of application method of butanediol low-temperature water removal equipment, the steps include:
S1, charging: the butanediol containing moisture is poured into the accommodating chamber of distillation still, and the liquid level line of butanediol is maintained at
Below one check valve, capping is covered；
S2, sealing: being closed accommodating chamber using the sealing structure formed between ring type seal and annular seal groove, and benefit
Interlayer is pulled down with the negative pressure state of upper space, makes to form negative pressure state in negative pressure trough, capping is further attracted；
S3, it vacuumizes: further being vacuumized the accommodating chamber of upper space and distillation still using external vacuum pump, reduce
Moisture boiling point in butanediol；
S4, heating: it is passed through steam into heating tube using steam-out (SO) pipeline, butanediol is heated, in butanediol
Moisture evaporated by thermal acceleration；
S5, stirring: steam flows and intra vane is pushed to rotate, and the intra vane drives outer leafs to turn using rotary clip
Dynamic, outer leafs push butanediol flowing, improve being heated evenly property of butanediol, further, the siphonal lobe relatively rotated using a pair
Piece can push butanediol therebetween is opposite to spring up, and improve mixed flow efficiency and effect；
S6, supervision: moisture is mixed through ventilative dottle pin with anhydrous cupric sulfate, and anhydrous cupric sulfate, which meets water, becomes blue five water sulphur
Sour copper, observing the blue degree of anhydrous cupric sulfate change by transparent sealant can be appreciated that distilling effect and progress；
S7, adjustment: anhydrous slufuric acid copper powders are embedded in the mode in ventilative dottle pin, the openable sealant in midway more renews
Ventilative dottle pin containing anhydrous cupric sulfate guarantees ventilative dottle pin to the assimilation effect of moisture, accurate understanding distillation situation.
3, beneficial effect
Compared with the prior art, the invention has the benefit that
(1) present invention removes water inflammable butanediol by the way of vacuum distillation, reduces the heated oxygen of butanediol
The possibility changed and burnt, improves production security.
(2) present invention depressurizes distillation still by the way of vacuumizing, while having extracted oxygen out, reduces butanediol quilt
The possibility of oxidation reduces the temperature requirement in heating process, has saved the energy.
(3) present invention is provided with the anhydrous cupric sulfate for observing and detecting distillation progress at sealing cover, helps to operate
Personnel understand water content situation in distillation situation and butanediol in time, and can replace nothing by opening transparent sealant
Brochanite and ventilative dottle pin, to guarantee that ventilative dottle pin and anhydrous cupric sulfate have good water absorbing properties, detection performance.
(4) present invention adsorbs capping using the negative pressure trough that spatial volume can be changed, and improves the leakproofness of capping, keeps away
Exempt from vacuum environment in the accommodating chamber of distillation still to be destroyed, and the subnormal ambient results from and vacuumizes journey after distillation starts
Sequence, there is no need to manually individually be sealed operation, sealing movement and the distillation of capping produce progress of keeping strokes, and production is automatic
Change degree is higher, is conducive to improve production efficiency, reduces manual operation burden.
(5) present invention is stirred the butanediol in accommodating chamber using the air deflector being mounted between heating tube, makes fourth
Glycol uniformly contacts heating tube, and wherein the movement of air deflector is not by the driving device and transmission being arranged separately in accommodating chamber
System saves labyrinth and stringent seal request that driving device and transmission system are separately provided in accommodating chamber, this
Invention is dexterously rotated using the steam passed through in heating tube as power drive intra vane, and utilizes the rotation being stuck in heating tube
Turn snap ring the movement of intra vane is transmitted in outer leafs, so that outer leafs is received the internal motivation for being heated pipe barrier, in turn
Push butanediol flowing.
(6) present invention use segmented vacuum structure, by the vacuum environment of distillation still sidewall portion be divided into upper space and
Lower space, upper space assist simultaneously as the channel that accommodating chamber and vacuum pump is connected, and as negative pressure trough pressure regulator
As the space of isolation temperature transmitting, plays the role of adjusting top motion flow and function is realized；Lower space is as true
Empty barrier isolation temperature transmitting, guarantees butanediol heat efficiency.
Detailed description of the invention
Fig. 1 is side view stereo figure of the invention；
Fig. 2 is other side view stereo figure of the invention；
Fig. 3 is top view of the invention；
Fig. 4 be Fig. 3 along the sectional view of A-A；
Fig. 5 is cross-sectional view of the Fig. 3 along B-B；
Fig. 6 is the enlarged drawing of C in Fig. 5；
Fig. 7 is the schematic perspective view of air deflector of the invention；
Fig. 8 be rotary clip of the invention, intra vane, outer leafs positional diagram.
In figure:
1, distillation still；101, lower space；102, upper space；103, vacuum pump insert port；104, the first check valve；
105, second one-way valve；106, annular seal groove；107, negative pressure trough；108, interlayer；
2, it covers；201, frame；202, web frame；203, ventilative dottle pin；204, anhydrous cupric sulfate；205, sealant；
206, ring type seal；
3, heating tube；301, card cover；302, through-hole；303, strip structure；304, locking clip；305, annular groove；
4, air deflector；401, rotary clip；402, intra vane；403, outer leafs.
Specific embodiment
In order to be easy to understand the technical means, the creative features, the aims and the efficiencies achieved by the present invention, tie below
Specific embodiment is closed the present invention is further described.
Embodiment 1
As shown in Figures 1 to 8, a kind of butanediol low-temperature water removal equipment, including distillation still 1 and for sealing distillation still 1
2 are covered, the heating tube 3 heated for butanediol is connected in the distillation still 1, the side wall of the distillation still 1 is for inner wall and outside
The double-layer structure that wall is constituted, the double-layer structure are divided into mutually independent lower space 101 and upper space 102, the lower part
Space 101 and upper space 102 are vacuum, to realize the heat preservation purpose of accommodating chamber；It is set on the outer wall of the upper space 102
There is vacuum pump insert port 103, the inner wall of upper space 102 is equipped with the first check valve 104 for passing to the accommodating chamber of distillation still 1,
External vacuum pump extracts the air in upper space 102 out, and utilizes the first check valve 104 by the air pressure drop in accommodating chamber
It is low, channel of the upper space 102 as vacuum pump at this time；The heating tube 3 is embedded in distillation still 1, two ends of heating tube 3
Mouth extends to outside distillation still 1, and to receive and discharge steam, the interlude of heating tube 3 is located in the accommodating chamber of distillation still 1,
Butanediol is heated when steam is by inside accommodating chamber；The capping 2 includes cricoid frame 201, in the frame 201
Side wall is equipped with stop collar, and the lower inside of frame 201 is equipped with web frame 202, be equipped with above the web frame 202 it is ventilative every
Pad 203, the ventilative dottle pin 203 are equipped with anhydrous cupric sulfate 204, and 2 top of capping is equipped with transparent sealant 205, institute
It states sealant 205 to be supported by stop collar, in use, steam is contacted by ventilative dottle pin 203 with anhydrous cupric sulfate 204, make anhydrous
Copper sulphate 204 becomes blue, becomes Lan Chengdu by the transparent observation of sealant 205 it can be seen that distillation process and water content size, more
Further, anhydrous cupric sulfate 204 being embedded can prevent anhydrous cupric sulfate 204 from spreading out in ventilative dottle pin 203, therefore ventilative
Cavity structure is provided in dottle pin 203, ventilative dottle pin 203 is divided into surface layer and bottom, the surface layer and bottom by cavity structure
Between also tightened by elastic connection silk thread, guarantee space tightness.
The heating tube 3 is segmental structure, is provided with an air deflector 4 between every two sections of heating tubes 3；The air deflector 4
Including sealing the rotary clip 401 being stuck between two heating tubes 3, divide on the medial surface and lateral surface of the rotary clip 401
Not She You intra vane 402 and outer leafs 403, it is empty that the intra vane 402 is located at the sealing that heating tube 3 and rotary clip 401 are formed
Between it is internal, the outer leafs 403 are located at outside above-mentioned sealing space, in use, high steam drives quickly through heating tube 3
Intra vane 402 rotates, and intra vane 402 is linked together by rotary clip 401 and outer leafs 403, utilizes the rotation of outer leafs 403
Butanediol Uniform Flow is pushed, realization is evenly heated butanediol.
The heating tube 3 is equipped with card cover 301, and the card cover 301 is equipped with the through-hole 302 passed through for butanediol；Point
Not Wei Yu the card cover 301 in adjacent two heating tubes 3 air deflector 4 between two heating tubes 3 is surrounded；The card cover
It is stretched out on 301 lateral wall and forms several strip structures 303 axially extending along air deflector 4, two cards cover, 301 benefit matched
It is mutually plugged together with strip structure 303 thereon, is cased with locking clip 304, institute on the strip structure 303 by way of being threadedly engaged
It states locking clip 304 to be linked together the card cover 301 of two sides, two sides are had free end by two card covers 301 for forming rigid structure
Heating tube 3 connects, and guarantees the accurate positioning of heating tube 3, and then guarantees the accurate sealing installation and smooth work of air deflector 4
Make.
It is equipped with annular groove 305 on the side of the snap ring being in contact with 3 end of heating tube, is equipped in the groove
The end of U-shaped sealing ring, the heating tube 3 is inserted into the annular groove 305 of respective side, and is sealed by U-shaped sealing ring.
Steam is connected with inside the heating tube 3, heating tube 3 is located at the part in the accommodating chamber of distillation still 1 using helical ring
Around mode be arranged, further, in order to guarantee the accurate installation of air deflector 4, the heating tube 3 with air deflector 4 for contacting
Free end be set as linear structure, reduce heating tube 3 and air deflector 4 cooperate difficulty.
The opening of the distillation still 1 is equipped with annular seal groove 106, and the section configuration of the annular seal groove 106 is V
Type, the capping 2 are equipped with ring type seal 206 compatible with annular seal groove 106；On the upper surface of the distillation still 1
Equipped with several negative pressure troughs 107, the bottom of the negative pressure trough 107 is equipped with interlayer 108 made of rubber material, the interlayer 108
Between negative pressure trough 107 and upper space 102, when upper space forms negative pressure or vacuum state, deformation occurs for interlayer 108,
Make to generate negative pressure in negative pressure trough 107, capping 2 is closely attracted.
A kind of application method of butanediol low-temperature water removal equipment, the steps include:
S1, charging: the butanediol containing moisture being poured into the accommodating chamber of distillation still 1, and the liquid level line of butanediol is maintained at
Below first check valve, capping 2 is covered；
S2, sealing: accommodating chamber is sealed using the sealing structure formed between ring type seal 206 and annular seal groove 106
It closes, and is pulled down interlayer 108 using the negative pressure state of upper space 102, make to form negative pressure state in negative pressure trough 107,2 will be covered
Further it is attracted；
S3, it vacuumizes: further being vacuumized the accommodating chamber of upper space 102 and distillation still 1 using external vacuum pump,
Reduce the moisture boiling point in butanediol；
S4, heating: it is passed through steam into heating tube 3 using steam-out (SO) pipeline, butanediol is heated, in butanediol
Moisture evaporated by thermal acceleration；
S5, stirring: steam flows and intra vane 402 is pushed to rotate, and the intra vane 402 is driven using rotary clip 401
Outer leafs 403 rotate, and outer leafs 403 push butanediol flowing, being heated evenly property of butanediol are improved, further, using a pair
The outer leafs 403 of relative rotation can push butanediol therebetween is opposite to spring up, and improve mixed flow efficiency and effect；
S6, supervision: moisture is mixed through ventilative dottle pin 203 with anhydrous cupric sulfate 204, and anhydrous cupric sulfate 204, which meets water, to be become
Blue cupric sulfate pentahydrate, by transparent sealant 205 observe anhydrous cupric sulfate 204 turn blue degree can be appreciated that distilling effect and into
Degree；
S7, adjustment: 204 powder of anhydrous cupric sulfate is embedded in the mode in ventilative dottle pin 203, the openable sealant in midway
The 205 ventilative dottle pins 203 containing anhydrous cupric sulfate 204 more renewed guarantee ventilative dottle pin 203 to the assimilation effect of moisture, standard
Really understand distillation situation.
Embodiment 2
On the basis of above-mentioned other technologies scheme remains unchanged, 301 activity by the way of being threadedly coupled of card cover
Rotation set is in corresponding heating tube 3, to carry out a more step section to card cover 301.
Embodiment 3
On the basis of above-mentioned other technologies scheme remains unchanged, the air deflector 4 uses in pairs, and two are oppositely arranged
Air deflector 4 constitutes a convection device, and then the butanediol of each region is mutually impacted and merged, and more uniformly flows to
Peripheral region.
Embodiment 4
On the basis of above-mentioned other technologies scheme remains unchanged, the locking clip 304 altogether there are two, and mutually screw fitting
Anti-skid structure is formed, being bonded to each other on face for locking clip 304 is equipped with anti-slip rubber, and face of the anti-slip rubber for fitting is
Rough surface.
Embodiment 5
On the basis of above-mentioned other technologies scheme remains unchanged, set between the upper space 102 and lower space 101
There is second one-way valve 105, for adjusting air pressure and the vacuum state of lower space.
Embodiment 6
On the basis of above-mentioned other technologies scheme remains unchanged, the heat medium that the heating tube 3 is passed through is hot oil, with
The propulsion effect to intra vane is improved, thermal capacitance and heating efficiency are improved.
Embodiment 7
On the basis of above-mentioned other technologies scheme remains unchanged, hot oil or vapor enter cavity in order to prevent,
The metal cap extended to the side far from end face is enclosed in setting one on rotary clip 401, and the metal cap is preferable by heating conduction
Copper sheet is made, and the annular outer edge of metal cap is against respectively on 3 outer surface of heating tube of respective side, forms seal chamber, works as hot oil
Metal cap is heated, metal cap expansion and deformation are more closely against in heating tube 3, automatically improve leakproofness, guarantees hot oil
With the isolation effect of butanediol.
In the description of this patent, it is to be understood that term " on ", "lower", "left", "right", "vertical", "horizontal",
The orientation or positional relationship of the instructions such as "top", "bottom", "inner", "outside", "front", "rear" is orientation based on the figure or position
Relationship is merely for convenience of description of the present invention and simplification of the description, rather than the device or element of indication or suggestion meaning must have
There is specific orientation, be constructed and operated in a specific orientation, therefore should not be understood as the limitation to this patent.
In this patent unless specifically defined or limited otherwise, term " installation ", " connected ", " connection ", " fixation " etc.
Term shall be understood in a broad sense, for example, it may be being fixedly connected, may be a detachable connection, or be integrally connected；It can be straight
Connect it is connected, can also be indirectly connected through an intermediary.It for the ordinary skill in the art, can be according to specific feelings
Condition understands the concrete meaning of above-mentioned term in this patent.
The basic principles, main features and advantages of the present invention have been shown and described above.This field it is common
Technical staff is it is to be appreciated that the present invention is not limited to the above embodiments, and what is described in the above embodiment and the description is only this
The principle of invention, without departing from the spirit and scope of the present invention, various changes and improvements may be made to the invention, these changes
Changing and improving should all fall into claimed invention.The claimed scope of the invention is by appended claims and its waits
Effect object defines.
Claims (10)
1. a kind of butanediol low-temperature water removal equipment, the capping (2) including distillation still (1) and for sealing distillation still (1), the steaming
It evaporates in kettle (1) and is connected with heating tube (3), it is characterised in that:
The side wall of the distillation still (1) is the double-layer structure that inner and outer wall is constituted, and the double-layer structure is divided into mutually independent
Lower space (101) and upper space (102), the lower space (101) and upper space (102) are vacuum；On described
The outer wall in portion space (102) is equipped with vacuum pump insert port (103), and the inner wall of upper space (102), which is equipped with, passes to distillation still
(1) the first check valve (104) of accommodating chamber；
The heating tube (3) is embedded in distillation still (1), and two ports of heating tube (3) extend to distillation still (1) outside, adds
The interlude of heat pipe (3) is located in the accommodating chamber of distillation still (1)；
The capping (2) includes cricoid frame (201), and frame (201) inner sidewall is equipped with stop collar, frame (201)
Lower inside be equipped with web frame (202), be equipped with ventilative dottle pin (203) above the web frame (202), the ventilative dottle pin
(203) anhydrous cupric sulfate (204) are equipped with, transparent sealant (205), the sealant is equipped with above the capping (2)
(205) it is supported by stop collar.
2. a kind of butanediol low-temperature water removal equipment according to claim 1, it is characterised in that: the heating tube (3) is point
Segment structure is provided with an air deflector (4) between every two sections of heating tubes (3)；The air deflector (4) is stuck in two including sealing and adds
Rotary clip (401) between heat pipe (3) is respectively equipped with intra vane on the medial surface and lateral surface of the rotary clip (401)
(402) and outer leafs (403), the intra vane (402) are located at the sealing space that heating tube (3) and rotary clip (401) are formed
Inside, the outer leafs (403) are located at outside above-mentioned sealing space.
3. a kind of butanediol low-temperature water removal equipment according to claim 2, it is characterised in that: the air deflector (4) is pairs of
It uses, two air deflectors (4) being oppositely arranged constitute a convection device；Setting one is enclosed to separate on rotary clip (401)
The metal cap that the side of end face extends, the annular outer edge of the metal cap are against respectively on the heating tube outer surface of respective side,
Form seal chamber.
4. a kind of butanediol low-temperature water removal equipment according to claim 2, it is characterised in that: set on the heating tube (3)
There is card to cover (301), the card cover (301) is equipped with the through-hole (302) passed through for butanediol；It is located at adjacent two heating
The card cover (301) managed on (3) surrounds the air deflector (4) between two heating tubes (3)；Outside the card cover (301)
It is stretched out on side wall and forms several strip structures (303) axially extending along air deflector (4), two cards cover (301) benefit matched
It is mutually plugged together with strip structure (303) thereon, is cased with locking clip by way of being threadedly engaged on the strip structure (303)
(304)。
5. a kind of butanediol low-temperature water removal equipment according to claim 4, it is characterised in that: the card cover (301) uses
The mode activity rotation set of threaded connection is on corresponding heating tube (3).
6. a kind of butanediol low-temperature water removal equipment according to claim 4, it is characterised in that: the locking clip (304) is shared
Two, and mutually screw fitting and form anti-skid structure, being bonded to each other on face for locking clip (304) is equipped with anti-slip rubber, described anti-
Face of the sliding rubber for fitting is rough surface.
7. a kind of butanediol low-temperature water removal equipment according to claim 2, it is characterised in that: the snap ring and heating tube
(3) it is equipped on the side that end is in contact annular groove (305), U-shaped sealing ring, the heating tube is equipped in the groove
(3) it in the annular groove (305) of end insertion respective side, and is sealed by U-shaped sealing ring.
8. a kind of butanediol low-temperature water removal equipment according to claim 1, it is characterised in that: the heating tube (3) is internal
It is connected with steam, the part that heating tube (3) is located in the accommodating chamber of distillation still (1) is arranged by the way of spiral surrounding；On described
Second one-way valve (105) are equipped between portion space (102) and lower space (101).
9. a kind of butanediol low-temperature water removal equipment according to claim 1, it is characterised in that: distillation still (1) is opened
Annular seal groove (106) are equipped at mouthful, the section configuration of the annular seal groove (106) is V-type, and the capping (2) is equipped with
The compatible ring type seal (206) with annular seal groove (106)；The upper surface of the distillation still (1) is equipped with several negative pressure
Slot (107), the bottom of the negative pressure trough (107) are equipped with interlayer (108) made of rubber material, and the interlayer (108) is located at negative
Between indent (107) and upper space (102).
10. a kind of application method of butanediol low-temperature water removal equipment, the steps include:
S1, charging: the butanediol containing moisture being poured into the accommodating chamber of distillation still (1), and the liquid level line of butanediol is maintained at
Below one check valve, capping (2) are covered；
S2, sealing: accommodating chamber is sealed using the sealing structure formed between ring type seal (206) and annular seal groove (106)
It closes, and is pulled down interlayer (108) using the negative pressure state of upper space (102), make to form negative pressure state in negative pressure trough (107),
Capping (2) is further attracted；
S3, it vacuumizes: further being vacuumized the accommodating chamber of upper space (102) and distillation still (1) using external vacuum pump,
Reduce the moisture boiling point in butanediol；
S4, heating: it is passed through steam into heating tube (3) using steam-out (SO) pipeline, butanediol is heated, in butanediol
Moisture is evaporated by thermal acceleration；
S5, stirring: steam flows and intra vane (402) is pushed to rotate, and the intra vane (402) utilizes rotary clip (401) band
Dynamic outer leafs (403) rotation, outer leafs (403) push butanediol flowing, improve being heated evenly property of butanediol and further adopt
It can push butanediol therebetween is opposite to spring up with the outer leafs (403) that a pair relatively rotates, improve mixed flow efficiency and effect；
S6, supervision: moisture is mixed through ventilative dottle pin (203) with anhydrous cupric sulfate (204), and anhydrous cupric sulfate (204) is met water and become
For blue cupric sulfate pentahydrate, becoming blue degree by transparent sealant (205) observation anhydrous cupric sulfate (204) can be appreciated that distillation effect
Fruit and progress；
S7, adjustment: anhydrous cupric sulfate (204) powder is embedded in the mode in ventilative dottle pin (203), the openable sealant in midway
(205) the ventilative dottle pin (203) containing anhydrous cupric sulfate (204) more renewed guarantees the ventilative absorption of dottle pin (203) to moisture
Effect, it is accurate to understand distillation situation.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910281967.4A CN109966769B (en) | 2019-04-09 | 2019-04-09 | Butanediol low-temperature water removal equipment and use method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910281967.4A CN109966769B (en) | 2019-04-09 | 2019-04-09 | Butanediol low-temperature water removal equipment and use method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN109966769A true CN109966769A (en) | 2019-07-05 |
| CN109966769B CN109966769B (en) | 2021-06-04 |
Family
ID=67083751
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201910281967.4A Active CN109966769B (en) | 2019-04-09 | 2019-04-09 | Butanediol low-temperature water removal equipment and use method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109966769B (en) |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE202009015336U1 (en) * | 2009-11-09 | 2010-01-14 | Asia Vital Components Co., Ltd., Hsin Chuan City | heat pipe |
| CN204197378U (en) * | 2014-11-03 | 2015-03-11 | 佛山市三水合成电器实业有限公司 | Without the vacuum extractor that lock is self-styled |
| CN206526526U (en) * | 2017-02-23 | 2017-09-29 | 江西赫信化学有限公司 | A kind of refined terpinol low energy cost vacuum drying device |
| CN109187109A (en) * | 2018-10-12 | 2019-01-11 | 安徽兴锂新能源有限公司 | A kind of solvent dehydration/purificasystem system and its application method with novel sampling device |
| CN109260951A (en) * | 2018-10-14 | 2019-01-25 | 苏州五颗星特种超滤膜科技有限公司 | Ultrafiltration apparatus |
-
2019
- 2019-04-09 CN CN201910281967.4A patent/CN109966769B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE202009015336U1 (en) * | 2009-11-09 | 2010-01-14 | Asia Vital Components Co., Ltd., Hsin Chuan City | heat pipe |
| CN204197378U (en) * | 2014-11-03 | 2015-03-11 | 佛山市三水合成电器实业有限公司 | Without the vacuum extractor that lock is self-styled |
| CN206526526U (en) * | 2017-02-23 | 2017-09-29 | 江西赫信化学有限公司 | A kind of refined terpinol low energy cost vacuum drying device |
| CN109187109A (en) * | 2018-10-12 | 2019-01-11 | 安徽兴锂新能源有限公司 | A kind of solvent dehydration/purificasystem system and its application method with novel sampling device |
| CN109260951A (en) * | 2018-10-14 | 2019-01-25 | 苏州五颗星特种超滤膜科技有限公司 | Ultrafiltration apparatus |
Also Published As
| Publication number | Publication date |
|---|---|
| CN109966769B (en) | 2021-06-04 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN207591325U (en) | A kind of industrial hemp extraction cannabidiol isolates and purifies device | |
| CN205287666U (en) | Concentrated cauldron of extrinsic cycle fractionation by distillation | |
| CN205603472U (en) | Novel fertilizer fermentation device | |
| CN109966769A (en) | A kind of butanediol low-temperature water removal equipment and its application method | |
| CN203816239U (en) | Rotary evaporator | |
| CN206168416U (en) | Purification device of o dichlorobenzene mother liquor during solid purple RL produces forever | |
| CN206529481U (en) | It is a kind of can enzyme digestion reaction vacuum scraper concentrator | |
| CN212491602U (en) | Chloroform evaporation frequency conversion evacuating device | |
| CN211734303U (en) | Distilling still and hydrolat distilling and extracting device | |
| CN208678412U (en) | A kind of low-temperature reduced-pressure distilling apparatus | |
| CN204224532U (en) | The sharp separation equipment of wood vinegar | |
| CN207980633U (en) | A kind of adjustable toluene filter device | |
| CN206736204U (en) | A kind of tea oil low temperature dewatering device | |
| CN206256051U (en) | Distill the cooling device of brewer | |
| CN113952759A (en) | Lutein purification crystallization system | |
| CN208448684U (en) | One kind prevents material from polymerizeing novel reboiler | |
| CN209081871U (en) | A kind of Ferment of Gibberellin Acid filtrated air condenser | |
| CN209500831U (en) | Automatic pressure-reducing distilling apparatus | |
| CN110960879A (en) | Purification device for volatile chemical organic compounds | |
| CN207012606U (en) | A kind of Multifunctional pot for extracting Chinese medicine | |
| CN219815319U (en) | Molecular distillation glass equipment | |
| CN219558766U (en) | Extraction tank with high extraction efficiency | |
| CN206318234U (en) | Vacuum keeping fresh device | |
| CN206111458U (en) | MVR is double -cylinder piston steam pump for evaporimeter | |
| CN109163128A (en) | A kind of high sealing performance shut-off valve |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |