CN109930028A - One kind being based on stamping forming metal plate plate and its processing technology - Google Patents
One kind being based on stamping forming metal plate plate and its processing technology Download PDFInfo
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Abstract
The invention discloses one kind to be based on stamping forming metal plate plate and its processing technology, it should be made after heat stamping and shaping based on stamping forming metal plate plate by raw material titanium ingot casting, and be somebody's turn to do the processing technology based on stamping forming metal plate plate are as follows: Homogenization Treatments are carried out to raw material titanium ingot casting;The preparation of extrusion plate;The preparation of rolled plate;Ultrasound detection is carried out to rolled plate;Rolled plate is pre-processed;Rolled plate is subjected to heat stamping and shaping, is obtained based on stamping forming metal plate plate;The experimental results showed that, higher tensile strength and plasticity are had based on stamping forming metal plate plate obtained by the present invention, its tensile strength is up to 2100MPa or more, elongation percentage is up to 15% or more, it can adapt in the production of complicated shape structural member, lumber recovery is improved, punch forming process of the invention can avoid the problem that drop stamping titanium alloy plate crackle easy to form, cracking breakout are low very well.
Description
Technical field
It is specifically a kind of to be based on stamping forming metal plate plate and its add the present invention relates to metal plate plate stamping technology field
Work technique.
Background technique
Punch forming refers to that depended on pressure machine and mold apply external force to plate, band, tubing and profile etc., is allowed to generate modeling
Property deformation or separation, thus obtain needed for shape and size workpiece (stamping parts) processing molding method.Heat stamping and shaping work
Skill is also hardened at punching press, is one occurred in recent years and is produced the new technology of high-intensitive punch forming part, using heat stamping and shaping
Stamping parts made from technology, intensity may be up to 1500MPa, and be formed at high temperature almost without rebound, common compared at present
Cold-stamped part there are formed precision high, good moldability and the outstanding advantages such as light-weight.
Titanium alloy due to low-density, very high anti-corrosion capability and be widely used in the fields such as aviation, ship, chemical industry,
Its plate can be applied to the conventional parts of 350 DEG C or less work, such as aircraft skin, thermal insulation board, heat exchanger, with work
The continuous development of industry technology and special components constantly being applied in high-end devices, the application field of titanium alloy is also continuous
It expands.Relationship between its punching formation property and material property value, deformation currently are concentrated mainly on to the research hotspot of titanium alloy
The correlation research of mode and sheet fabrication hardening.But because titanium alloy is close-packed hexagonal lattice, plasticity is poor, it is difficult to shape, make
At developing slowly for titanium alloy plate plastic forming technology, its application range is limited.In addition the surface and inherence of Stamping Sheet material
Performance is very big on the influence of the quality of presswork, in existing production method, only to the stamping parts finished product after the completion of production link
It is checked, is partially produced without stamping forming substandard product without detecting same progress punch forming process
Stamping parts finished product is unable to satisfy customer demand, cannot use, and the stamping material after punch forming, can not reuse,
While causing the waste of stamping material, a large amount of production time is occupied, very influence working efficiency.
Summary of the invention
The purpose of the present invention is to provide one kind to be based on stamping forming metal plate plate and its processing technology, existing to solve
The problems in technology.
To achieve the above object, the invention provides the following technical scheme:
One kind being based on stamping forming metal plate plate, should be based on stamping forming metal plate plate by raw material titanium ingot casting through overheating
It is made after punch forming.
As optimization, raw material titanium ingot casting contains following components in percentage by weight: iron 0.001-0.05%, oxygen 0.005-
0.07%, carbon 0.001-0.005%, molybdenum 0.001-0.003%, boron 0.001-0.005%, remaining is titanium.
A kind of processing technology based on stamping forming metal plate plate, should the processing work based on stamping forming metal plate plate
Skill the following steps are included:
(1) Homogenization Treatments are carried out to raw material titanium ingot casting;
(2) preparation of extrusion plate;
(3) preparation of rolled plate;
(4) ultrasound detection is carried out to the resulting rolled plate of step (3);
(5) step (4) resulting rolled plate is pre-processed;
(6) the resulting rolled plate of step (5) is subjected to heat stamping and shaping, obtained based on stamping forming metal plate plate.
As optimization, a kind of processing technology based on stamping forming metal plate plate should be based on stamping forming panel beating plate
The processing technology of material the following steps are included:
(1) Homogenization Treatments are carried out to raw material titanium ingot casting, is heated raw material titanium ingot casting using resistance furnace, kept the temperature, so
After quench;
(2) the obtained titanium ingot casting of step (1) is heated, keeps the temperature, then squeezes, obtain extrusion plate;
(3) the obtained extrusion plate surface of step (2) is polished, then descale rolls, milled sheet is made
Material;
(4) to the resulting rolled plate of step (3) carry out ultrasound detection, according to testing result to the quality of rolled plate into
Row judgement, until subject to rolled plate qualification;
(5) rolled plate of the obtained qualification of step (4) is heated, keeps the temperature, then cools down, kept the temperature, rolling
Plate surface coats the ethanol solution of one layer of alumina silicate, dries;
(6) step (5) resulting rolled plate is put into heating furnace and is heated, then taken out and put hot forming tool into
In, stamping, pressure maintaining is cooling, pickling, trimming, and drilling is obtained based on stamping forming metal plate plate.
As optimization, a kind of processing technology based on stamping forming metal plate plate should be based on stamping forming panel beating plate
The processing technology of material the following steps are included:
(1) Homogenization Treatments are carried out to raw material titanium ingot casting, raw material titanium ingot casting are heated to 300-500 DEG C using resistance furnace,
8-12h is kept the temperature, is then quenched, hardening heat is 10-30 DEG C;The purpose of Homogenization Treatments is by the precipitated phase of raw material titanium ingot casting
Ti17Fe12 is sufficiently dissolved into matrix, is improved the tissue and performance of raw material titanium ingot casting, is improved its plasticity and formability;
(2) the obtained titanium ingot casting of step (1) is heated to 450-550 DEG C, keeps the temperature 1-3h, is then carried out on extruder
It squeezes, extrusion ratio 5-7 obtains extrusion plate;
(3) the obtained extrusion plate surface of step (2) is polished, and scale removal, extrusion plate is carried out
Rolling, rolling carry out 25-40 passage altogether, 300-500 DEG C are heated between passage, keep the temperature 0.5-1.5h, per pass rolling reduction
For 12-18%, extrusion plate is made annealing treatment between passage, rolled plate is made;Extrusion plate surface is removed and is aoxidized
The purpose of skin is to prevent extrusion plate oxide skin bring face checking problem during the rolling process;The purpose of annealing is anti-
The stress collection that only extrusion plate generates during the rolling process neutralizes the problem of residual stress causes extrusion plate to crack, and improves and squeezes
Plate plasticity and improvement interior tissue;
(4) ultrasound detection is carried out to the resulting rolled plate of step (3), starts ultrasonic inspection probe, by ultrasound emission end
Ultrasonic signal is issued, short pulse sound energy is emitted into rolled plate, monitors and analyze the sound by reflection by ultrasound detection instrument
Wave signal obtains testing result, judges according to testing result the quality of rolled plate, will be underproof through ultrasound detection
Rolled plate is removed, and after the rolled plate more renewed, is reused ultrasonic detection equipment and is carried out quality testing to rolled plate, directly
To rolled plate qualification;Rolled plate is detected before stamping, convenient for finding underproof rolled plate in advance, is subtracted
Few production time wasted by substandard product, improve the working efficiency of punch forming process;
(5) rolled plate of the obtained qualification of step (4) is heated to 700-800 with the speed of 10-20 DEG C/s
DEG C, 8-15min is kept the temperature, is then cooled to 300-350 DEG C with the speed of 20-30 DEG C/s, 1-3min is kept the temperature, on rolled plate surface
The ethanol solution of one layer of alumina silicate is coated, coating thickness 0.5-1mm dries coating surface;It is coated on rolled plate surface
The ethanol solution of alumina silicate can preferably guarantee the intensity and plasticity of rolled plate;
(6) step (5) resulting rolled plate being put into heating in heating furnace, the temperature of heating furnace is 900-1000 DEG C,
It then takes out and is put into mold rapidly, stamping, pressure maintaining 10-20s is carried out to rolled plate, in a mold with 30-40 DEG C/s
Speed be cooled to room temperature, take out stamping parts, carry out pickling with sulfuric acid solution, to stamping parts progress trimming and drilling, obtain base
In stamping forming metal plate plate.Rolled plate after heating stove heating is quickly put into mold, it is ensured that rolled plate
Still there is good plasticity in forming;It is rapidly cooled in a mold after stamping parts forming, returning after shaping stamping parts
Bullet amount very little greatly improves the forming accuracy of stamping parts, preferably ensure that the dimensional accuracy of stamping parts.
Occur as optimization, in step (3) longer or when compared with deep torn grain on rolled plate, fragmented parts are cut off, then
Continue to roll.
As optimization, when fine cracks occurs in rolled plate edge surface in step (3), it is polishing to abrasive machine bright and clean flat
It is whole, it is further continued for being rolled.It prevents fine cracks in the subsequent operation of rolling, is gradually expanded, it is final to crack, lead to milled sheet
Material preparation failure.
As optimization, annealing time is 10-20min in step (3).The too long extrusion plate that will lead to of annealing time is rolling
Internal grain is grown up in the process, so as to cause extrusion plate cracking, is more suitable for when annealing time is 10-20min.
As optimization, the mass fraction of the ethanol solution of alumina silicate is 0.5-2% in step (5).
As optimization, the mass fraction of sulfuric acid solution is 5-10% in step (6).
Compared with prior art, the beneficial effects of the present invention are:
The present invention first carries out Homogenization Treatments to raw material titanium ingot casting, and the precipitated phase Ti17Fe12 of raw material titanium ingot casting is sufficiently molten
Solution improves the tissue and performance of raw material titanium ingot casting, improves its plasticity and formability into matrix;Next is squeezed, is rolled,
Before rolling to plate surface scale removal, plate oxide skin bring face checking problem during the rolling process is prevented,
It is made annealing treatment between passage, the stress collection for preventing plate from generating during the rolling process, which neutralizes residual stress, leads to extrusion plate
The problem of cracking, improves plate plasticity and improves interior tissue;Ultrasound detection is carried out to plate before stamping again, convenient in advance
It was found that underproof plate, reduces the production time wasted by substandard product, the working efficiency of punch forming process is improved;Again
Plate is pre-processed, in the ethanol solution of plate surface coating alumina silicate, can preferably guarantee the intensity of rolled plate
And plasticity;It is finally stamping to plate progress, in stamping process, the plate after heating stove heating is quickly put
Into mold, it is ensured that plate still has good plasticity in forming;It is rapidly cooled, makes in a mold after stamping parts forming
Springback capacity very little after stamping parts forming, greatly improves the forming accuracy of stamping parts, preferably ensure that stamping parts
Dimensional accuracy;Higher tensile strength and modeling are had based on stamping forming metal plate plate as made from above-mentioned processing technology
Property, up to 2100MPa or more, elongation percentage can adapt to up to 15% or more in the life of complicated shape structural member tensile strength
It produces, improves lumber recovery, punch forming process of the invention can avoid drop stamping titanium alloy plate crackle easy to form very well
The problem of, cracking breakout is low.
Specific embodiment
Below in conjunction with the embodiment of the present invention, technical scheme in the embodiment of the invention is clearly and completely described,
Obviously, described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Based in the present invention
Embodiment, every other embodiment obtained by those of ordinary skill in the art without making creative efforts, all
Belong to the scope of protection of the invention.
Embodiment 1:
One kind being based on stamping forming metal plate plate, should be based on stamping forming metal plate plate by raw material titanium ingot casting through overheating
It is made after punch forming;Raw material titanium ingot casting contains following components in percentage by weight: iron 0.001%, oxygen 0.005%, carbon
0.001%, molybdenum 0.001%, boron 0.001%, remaining is titanium.
One kind is processed based on stamping forming metal plate plate using above-mentioned raw materials, is somebody's turn to do based on stamping forming metal plate plate
Processing technology the following steps are included:
(1) Homogenization Treatments are carried out to raw material titanium ingot casting, raw material titanium ingot casting is heated to 300 DEG C using resistance furnace, heat preservation
Then 8h is quenched, hardening heat is 10 DEG C;
(2) the obtained titanium ingot casting of step (1) is heated to 450 DEG C, keeps the temperature 1h, is then squeezed on extruder,
Extrusion ratio is 5, obtains extrusion plate;
(3) the obtained extrusion plate surface of step (2) is polished, and scale removal, extrusion plate is carried out
Rolling, rolling carry out 25 passages altogether, and 300 DEG C are heated between passage, keep the temperature 0.5h, and rolling reduction is 12% per pass, in road
Extrusion plate is made annealing treatment between secondary, annealing time 10min, rolled plate is made, it is longer when occurring on rolled plate
Or when compared with deep torn grain, fragmented parts are cut off, it is further continued for being rolled;
(4) ultrasound detection is carried out to the resulting rolled plate of step (3), starts ultrasonic inspection probe, by ultrasound emission end
Ultrasonic signal is issued, short pulse sound energy is emitted into rolled plate, monitors and analyze the sound by reflection by ultrasound detection instrument
Wave signal obtains testing result, judges according to testing result the quality of rolled plate, will be underproof through ultrasound detection
Rolled plate is removed, and after the rolled plate more renewed, is reused ultrasonic detection equipment and is carried out quality testing to rolled plate, directly
To rolled plate qualification;
(5) rolled plate of the obtained qualification of step (4) is heated to 700 DEG C with the speed of 10 DEG C/s, heat preservation
Then 8min is cooled to 300 DEG C with the speed of 20 DEG C/s, keep the temperature 1min, coats the second of one layer of alumina silicate on rolled plate surface
Alcoholic solution, coating thickness 0.5mm, the mass fraction of the ethanol solution of alumina silicate are 0.5%, and coating surface is dried;
(6) step (5) resulting rolled plate is put into heating in heating furnace, the temperature of heating furnace is 900 DEG C, is then taken
It is put into mold rapidly out, stamping to rolled plate progress, pressure maintaining 10s is cooled in a mold with the speed of 30 DEG C/s
Room temperature takes out stamping parts, carries out pickling with sulfuric acid solution, and the mass fraction of sulfuric acid solution is 5%, to stamping parts carry out trimming with
Drilling is obtained based on stamping forming metal plate plate.
Embodiment 2:
One kind being based on stamping forming metal plate plate, should be based on stamping forming metal plate plate by raw material titanium ingot casting through overheating
It is made after punch forming;Raw material titanium ingot casting contains following components in percentage by weight: iron 0.003%, oxygen 0.008%, carbon
0.002%, molybdenum 0.001%, boron 0.002%, remaining is titanium.
One kind is processed based on stamping forming metal plate plate using above-mentioned raw materials, is somebody's turn to do based on stamping forming metal plate plate
Processing technology the following steps are included:
(1) Homogenization Treatments are carried out to raw material titanium ingot casting, raw material titanium ingot casting is heated to 350 DEG C using resistance furnace, heat preservation
Then 9h is quenched, hardening heat is 15 DEG C;
(2) the obtained titanium ingot casting of step (1) is heated to 460 DEG C, keeps the temperature 1.5h, is then squeezed on extruder
Pressure, extrusion ratio 5.5 obtain extrusion plate;
(3) the obtained extrusion plate surface of step (2) is polished, and scale removal, extrusion plate is carried out
Rolling, rolling carry out 26 passages altogether, and 350 DEG C are heated between passage, keep the temperature 0.6h, and rolling reduction is 13% per pass, in road
Extrusion plate is made annealing treatment between secondary, annealing time 11min, rolled plate is made, when rolled plate edge surface goes out
Existing fine cracks, are polishing to bright and clean smooth with abrasive machine, are further continued for being rolled;
(4) ultrasound detection is carried out to the resulting rolled plate of step (3), starts ultrasonic inspection probe, by ultrasound emission end
Ultrasonic signal is issued, short pulse sound energy is emitted into rolled plate, monitors and analyze the sound by reflection by ultrasound detection instrument
Wave signal obtains testing result, judges according to testing result the quality of rolled plate, will be underproof through ultrasound detection
Rolled plate is removed, and after the rolled plate more renewed, is reused ultrasonic detection equipment and is carried out quality testing to rolled plate, directly
To rolled plate qualification;
(5) rolled plate of the obtained qualification of step (4) is heated to 750 DEG C with the speed of 11 DEG C/s, heat preservation
Then 9min is cooled to 310 DEG C with the speed of 22 DEG C/s, keep the temperature 1.5min, coats one layer of alumina silicate on rolled plate surface
Ethanol solution, coating thickness 0.6mm, the mass fraction of the ethanol solution of alumina silicate are 0.6%, and coating surface is dried;
(6) step (5) resulting rolled plate is put into heating in heating furnace, the temperature of heating furnace is 920 DEG C, is then taken
It is put into mold rapidly out, stamping to rolled plate progress, pressure maintaining 12s is cooled in a mold with the speed of 32 DEG C/s
Room temperature takes out stamping parts, carries out pickling with sulfuric acid solution, and the mass fraction of sulfuric acid solution is 6%, to stamping parts carry out trimming with
Drilling is obtained based on stamping forming metal plate plate.
Embodiment 3:
One kind being based on stamping forming metal plate plate, should be based on stamping forming metal plate plate by raw material titanium ingot casting through overheating
It is made after punch forming;Raw material titanium ingot casting contains following components in percentage by weight: iron 0.01%, oxygen 0.03%, carbon
0.003%, molybdenum 0.002%, boron 0.003%, remaining is titanium.
One kind is processed based on stamping forming metal plate plate using above-mentioned raw materials, is somebody's turn to do based on stamping forming metal plate plate
Processing technology the following steps are included:
(1) Homogenization Treatments are carried out to raw material titanium ingot casting, raw material titanium ingot casting is heated to 400 DEG C using resistance furnace, heat preservation
Then 10h is quenched, hardening heat is 20 DEG C;
(2) the obtained titanium ingot casting of step (1) is heated to 500 DEG C, keeps the temperature 2h, is then squeezed on extruder,
Extrusion ratio is 6, obtains extrusion plate;
(3) the obtained extrusion plate surface of step (2) is polished, and scale removal, extrusion plate is carried out
Rolling, rolling carry out 22 passages altogether, and 400 DEG C are heated between passage, keep the temperature 1h, and rolling reduction is 15% per pass, in passage
Between extrusion plate is made annealing treatment, annealing time 15min, be made rolled plate, when occur on rolled plate it is longer or
When person is compared with deep torn grain, fragmented parts are cut off, are further continued for being rolled;
(4) ultrasound detection is carried out to the resulting rolled plate of step (3), starts ultrasonic inspection probe, by ultrasound emission end
Ultrasonic signal is issued, short pulse sound energy is emitted into rolled plate, monitors and analyze the sound by reflection by ultrasound detection instrument
Wave signal obtains testing result, judges according to testing result the quality of rolled plate, will be underproof through ultrasound detection
Rolled plate is removed, and after the rolled plate more renewed, is reused ultrasonic detection equipment and is carried out quality testing to rolled plate, directly
To rolled plate qualification;
(5) rolled plate of the obtained qualification of step (4) is heated to 750 DEG C with the speed of 15 DEG C/s, heat preservation
Then 11min is cooled to 325 DEG C with the speed of 25 DEG C/s, keep the temperature 2min, coats the second of one layer of alumina silicate on rolled plate surface
Alcoholic solution, coating thickness 0.8mm, the mass fraction of the ethanol solution of alumina silicate are 1.2%, and coating surface is dried;
(6) step (5) resulting rolled plate is put into heating in heating furnace, the temperature of heating furnace is 950 DEG C, is then taken
It is put into mold rapidly out, stamping to rolled plate progress, pressure maintaining 15s is cooled in a mold with the speed of 35 DEG C/s
Room temperature takes out stamping parts, carries out pickling with sulfuric acid solution, and the mass fraction of sulfuric acid solution is 8%, to stamping parts carry out trimming with
Drilling is obtained based on stamping forming metal plate plate.
Embodiment 4:
One kind being based on stamping forming metal plate plate, should be based on stamping forming metal plate plate by raw material titanium ingot casting through overheating
It is made after punch forming;Raw material titanium ingot casting contains following components in percentage by weight: iron 0.04%, oxygen 0.06%, carbon
0.004%, molybdenum 0.003%, boron 0.004%, remaining is titanium.
One kind is processed based on stamping forming metal plate plate using above-mentioned raw materials, is somebody's turn to do based on stamping forming metal plate plate
Processing technology the following steps are included:
(1) Homogenization Treatments are carried out to raw material titanium ingot casting, raw material titanium ingot casting is heated to 450 DEG C using resistance furnace, heat preservation
Then 11h is quenched, hardening heat is 25 DEG C;
(2) the obtained titanium ingot casting of step (1) is heated to 540 DEG C, keeps the temperature 2.5h, is then squeezed on extruder
Pressure, extrusion ratio 6.5 obtain extrusion plate;
(3) the obtained extrusion plate surface of step (2) is polished, and scale removal, extrusion plate is carried out
Rolling, rolling carry out 38 passages altogether, and 450 DEG C are heated between passage, keep the temperature 1.3h, and rolling reduction is 17% per pass, in road
Extrusion plate is made annealing treatment between secondary, annealing time 19min, rolled plate is made, when rolled plate edge surface goes out
Existing fine cracks, are polishing to bright and clean smooth with abrasive machine, are further continued for being rolled;
(4) ultrasound detection is carried out to the resulting rolled plate of step (3), starts ultrasonic inspection probe, by ultrasound emission end
Ultrasonic signal is issued, short pulse sound energy is emitted into rolled plate, monitors and analyze the sound by reflection by ultrasound detection instrument
Wave signal obtains testing result, judges according to testing result the quality of rolled plate, will be underproof through ultrasound detection
Rolled plate is removed, and after the rolled plate more renewed, is reused ultrasonic detection equipment and is carried out quality testing to rolled plate, directly
To rolled plate qualification;
(5) rolled plate of the obtained qualification of step (4) is heated to 780 DEG C with the speed of 19 DEG C/s, heat preservation
Then 14min is cooled to 340 DEG C with the speed of 28 DEG C/s, keep the temperature 2.5min, coats one layer of alumina silicate on rolled plate surface
Ethanol solution, coating thickness 0.9mm, the mass fraction of the ethanol solution of alumina silicate are 1.8%, and coating surface is dried;
(6) step (5) resulting rolled plate is put into heating in heating furnace, the temperature of heating furnace is 980 DEG C, is then taken
It is put into mold rapidly out, stamping to rolled plate progress, pressure maintaining 18s is cooled in a mold with the speed of 38 DEG C/s
Room temperature takes out stamping parts, carries out pickling with sulfuric acid solution, and the mass fraction of sulfuric acid solution is 9%, to stamping parts carry out trimming with
Drilling is obtained based on stamping forming metal plate plate.
Embodiment 5:
One kind being based on stamping forming metal plate plate, should be based on stamping forming metal plate plate by raw material titanium ingot casting through overheating
It is made after punch forming;Raw material titanium ingot casting contains following components in percentage by weight: iron 0.05%, oxygen 0.07%, carbon
0.005%, molybdenum 0.003%, boron 0.005%, remaining is titanium.
One kind is processed based on stamping forming metal plate plate using above-mentioned raw materials, is somebody's turn to do based on stamping forming metal plate plate
Processing technology the following steps are included:
(1) Homogenization Treatments are carried out to raw material titanium ingot casting, raw material titanium ingot casting is heated to 500 DEG C using resistance furnace, heat preservation
Then 12h is quenched, hardening heat is 30 DEG C;
(2) the obtained titanium ingot casting of step (1) is heated to 550 DEG C, keeps the temperature 3h, is then squeezed on extruder,
Extrusion ratio is 7, obtains extrusion plate;
(3) the obtained extrusion plate surface of step (2) is polished, and scale removal, extrusion plate is carried out
Rolling, rolling carry out 40 passages altogether, and 500 DEG C are heated between passage, keep the temperature 1.5h, and rolling reduction is 18% per pass, in road
Extrusion plate is made annealing treatment between secondary, annealing time 20min, rolled plate is made, it is longer when occurring on rolled plate
Or when compared with deep torn grain, fragmented parts are cut off, it is further continued for being rolled;
(4) ultrasound detection is carried out to the resulting rolled plate of step (3), starts ultrasonic inspection probe, by ultrasound emission end
Ultrasonic signal is issued, short pulse sound energy is emitted into rolled plate, monitors and analyze the sound by reflection by ultrasound detection instrument
Wave signal obtains testing result, judges according to testing result the quality of rolled plate, will be underproof through ultrasound detection
Rolled plate is removed, and after the rolled plate more renewed, is reused ultrasonic detection equipment and is carried out quality testing to rolled plate, directly
To rolled plate qualification;
(5) rolled plate of the obtained qualification of step (4) is heated to 800 DEG C with the speed of 20 DEG C/s, heat preservation
Then 15min is cooled to 350 DEG C with the speed of 30 DEG C/s, keep the temperature 3min, coats the second of one layer of alumina silicate on rolled plate surface
Alcoholic solution, coating thickness 1mm, the mass fraction of the ethanol solution of alumina silicate are 2%, and coating surface is dried;
(6) step (5) resulting rolled plate is put into heating in heating furnace, the temperature of heating furnace is 1000 DEG C, then
Taking-up is put into mold rapidly, carries out stamping, pressure maintaining 20s to rolled plate, cooling with the speed of 40 DEG C/s in a mold
To room temperature, stamping parts is taken out, carries out pickling with sulfuric acid solution, the mass fraction of sulfuric acid solution is 10%, is cut to stamping parts
Side and drilling are obtained based on stamping forming metal plate plate.
Comparative example 1:
One kind being based on stamping forming metal plate plate, should be based on stamping forming metal plate plate by raw material titanium ingot casting through overheating
It is made after punch forming;Raw material titanium ingot casting contains following components in percentage by weight: iron 0.01%, oxygen 0.03%, carbon
0.003%, molybdenum 0.002%, boron 0.003%, remaining is titanium.
One kind is processed based on stamping forming metal plate plate using above-mentioned raw materials, is somebody's turn to do based on stamping forming metal plate plate
Processing technology the following steps are included:
(1) Homogenization Treatments are carried out to raw material titanium ingot casting, raw material titanium ingot casting is heated to 400 DEG C using resistance furnace, heat preservation
Then 10h is quenched, hardening heat is 20 DEG C;
(2) the obtained titanium ingot casting of step (1) is heated to 500 DEG C, keeps the temperature 2h, is then squeezed on extruder,
Extrusion ratio is 6, obtains extrusion plate;
(3) the obtained extrusion plate surface of step (2) is polished, extrusion plate is rolled, rolling altogether into
22 passage of row is heated to 400 DEG C between passage, keeps the temperature 1h, and rolling reduction is 15% per pass, between passage to extrusion plate into
Rolled plate is made in row annealing, annealing time 15min, longer or when compared with deep torn grain when occurring on rolled plate, will
Fragmented parts excision, is further continued for being rolled;
(4) ultrasound detection is carried out to the resulting rolled plate of step (3), starts ultrasonic inspection probe, by ultrasound emission end
Ultrasonic signal is issued, short pulse sound energy is emitted into rolled plate, monitors and analyze the sound by reflection by ultrasound detection instrument
Wave signal obtains testing result, judges according to testing result the quality of rolled plate, will be underproof through ultrasound detection
Rolled plate is removed, and after the rolled plate more renewed, is reused ultrasonic detection equipment and is carried out quality testing to rolled plate, directly
To rolled plate qualification;
(5) rolled plate of the obtained qualification of step (4) is heated to 750 DEG C with the speed of 15 DEG C/s, heat preservation
Then 11min is cooled to 325 DEG C with the speed of 25 DEG C/s, keep the temperature 2min, coats the second of one layer of alumina silicate on rolled plate surface
Alcoholic solution, coating thickness 0.8mm, the mass fraction of the ethanol solution of alumina silicate are 1.2%, and coating surface is dried;
(6) step (5) resulting rolled plate is put into heating in heating furnace, the temperature of heating furnace is 950 DEG C, is then taken
It is put into mold rapidly out, stamping to rolled plate progress, pressure maintaining 15s is cooled in a mold with the speed of 35 DEG C/s
Room temperature takes out stamping parts, carries out pickling with sulfuric acid solution, and the mass fraction of sulfuric acid solution is 8%, to stamping parts carry out trimming with
Drilling is obtained based on stamping forming metal plate plate.
Comparative example 1 compared with Example 3, not to extrusion plate surface scale removal in step (3).
Comparative example 2:
One kind being based on stamping forming metal plate plate, should be based on stamping forming metal plate plate by raw material titanium ingot casting through overheating
It is made after punch forming;Raw material titanium ingot casting contains following components in percentage by weight: iron 0.01%, oxygen 0.03%, carbon
0.003%, molybdenum 0.002%, boron 0.003%, remaining is titanium.
One kind is processed based on stamping forming metal plate plate using above-mentioned raw materials, is somebody's turn to do based on stamping forming metal plate plate
Processing technology the following steps are included:
(1) Homogenization Treatments are carried out to raw material titanium ingot casting, raw material titanium ingot casting is heated to 400 DEG C using resistance furnace, heat preservation
Then 10h is quenched, hardening heat is 20 DEG C;
(2) the obtained titanium ingot casting of step (1) is heated to 500 DEG C, keeps the temperature 2h, is then squeezed on extruder,
Extrusion ratio is 6, obtains extrusion plate;
(3) the obtained extrusion plate surface of step (2) is polished, and scale removal, extrusion plate is carried out
Rolling, rolling carry out 22 passages altogether, and 400 DEG C are heated between passage, keep the temperature 1h, and rolling reduction is 15% per pass, in passage
Between extrusion plate is made annealing treatment, annealing time 25min, be made rolled plate, when occur on rolled plate it is longer or
When person is compared with deep torn grain, fragmented parts are cut off, are further continued for being rolled;
(4) ultrasound detection is carried out to the resulting rolled plate of step (3), starts ultrasonic inspection probe, by ultrasound emission end
Ultrasonic signal is issued, short pulse sound energy is emitted into rolled plate, monitors and analyze the sound by reflection by ultrasound detection instrument
Wave signal obtains testing result, judges according to testing result the quality of rolled plate, will be underproof through ultrasound detection
Rolled plate is removed, and after the rolled plate more renewed, is reused ultrasonic detection equipment and is carried out quality testing to rolled plate, directly
To rolled plate qualification;
(5) rolled plate of the obtained qualification of step (4) is heated to 750 DEG C with the speed of 15 DEG C/s, heat preservation
Then 11min is cooled to 325 DEG C with the speed of 25 DEG C/s, keep the temperature 2min, coats the second of one layer of alumina silicate on rolled plate surface
Alcoholic solution, coating thickness 0.8mm, the mass fraction of the ethanol solution of alumina silicate are 1.2%, and coating surface is dried;
(6) step (5) resulting rolled plate is put into heating in heating furnace, the temperature of heating furnace is 950 DEG C, is then taken
It is put into mold rapidly out, stamping to rolled plate progress, pressure maintaining 15s is cooled in a mold with the speed of 35 DEG C/s
Room temperature takes out stamping parts, carries out pickling with sulfuric acid solution, and the mass fraction of sulfuric acid solution is 8%, to stamping parts carry out trimming with
Drilling is obtained based on stamping forming metal plate plate.
Compared with Example 3, annealing time is 25min to comparative example 2 in step (3).
Comparative example 3:
One kind being based on stamping forming metal plate plate, should be based on stamping forming metal plate plate by raw material titanium ingot casting through overheating
It is made after punch forming;Raw material titanium ingot casting contains following components in percentage by weight: iron 0.01%, oxygen 0.03%, carbon
0.003%, molybdenum 0.002%, boron 0.003%, remaining is titanium.
One kind is processed based on stamping forming metal plate plate using above-mentioned raw materials, is somebody's turn to do based on stamping forming metal plate plate
Processing technology the following steps are included:
(1) Homogenization Treatments are carried out to raw material titanium ingot casting, raw material titanium ingot casting is heated to 400 DEG C using resistance furnace, heat preservation
Then 10h is quenched, hardening heat is 20 DEG C;
(2) the obtained titanium ingot casting of step (1) is heated to 500 DEG C, keeps the temperature 2h, is then squeezed on extruder,
Extrusion ratio is 6, obtains extrusion plate;
(3) the obtained extrusion plate surface of step (2) is polished, and scale removal, extrusion plate is carried out
Rolling, rolling carry out 22 passages altogether, and 400 DEG C are heated between passage, keep the temperature 1h, and rolling reduction is 15% per pass, in passage
Between extrusion plate is made annealing treatment, annealing time 15min, be made rolled plate, when occur on rolled plate it is longer or
When person is compared with deep torn grain, fragmented parts are cut off, are further continued for being rolled;
(4) ultrasound detection is carried out to the resulting rolled plate of step (3), starts ultrasonic inspection probe, by ultrasound emission end
Ultrasonic signal is issued, short pulse sound energy is emitted into rolled plate, monitors and analyze the sound by reflection by ultrasound detection instrument
Wave signal obtains testing result, judges according to testing result the quality of rolled plate, will be underproof through ultrasound detection
Rolled plate is removed, and after the rolled plate more renewed, is reused ultrasonic detection equipment and is carried out quality testing to rolled plate, directly
To rolled plate qualification;
(5) rolled plate of the obtained qualification of step (4) is heated to 750 DEG C with the speed of 15 DEG C/s, heat preservation
Then 11min is cooled to 325 DEG C with the speed of 25 DEG C/s, keep the temperature 2min, coats the second of one layer of alumina silicate on rolled plate surface
Alcoholic solution, coating thickness 0.8mm, the mass fraction of the ethanol solution of alumina silicate are 1.2%, and coating surface is dried;
(6) step (5) resulting rolled plate is put into heating in heating furnace, the temperature of heating furnace is 950 DEG C, is then taken
It is put into mold rapidly out, stamping to rolled plate progress, pressure maintaining 15s is cooled in a mold with the speed of 25 DEG C/s
Room temperature takes out stamping parts, carries out pickling with sulfuric acid solution, and the mass fraction of sulfuric acid solution is 8%, to stamping parts carry out trimming with
Drilling is obtained based on stamping forming metal plate plate.
Compared with Example 3, step (6) rolled plate is cooled to room temperature in a mold with the speed of 25 DEG C/s comparative example 3.
Effect example:
(1) laboratory sample: obtained by the embodiment of the present invention 1 to 5 based on stamping forming metal plate plate and comparative example 1 to
Based on stamping forming metal plate plate obtained by 3.
(2) experimental method: using universal testing machine to the tensile strength, yield strength and elongation percentage of laboratory sample into
Row test, test result are shown in Table 1, produce 1000 respectively according to the processing technology of the embodiment of the present invention 1 to 5 and comparative example 1 to 3
Based on stamping forming metal plate plate, its yield rate is tested, to generate the cracking breakout of the crackle test product of 1mm, test result
It is shown in Table 1.
Table 1
(3) experimental result: from table 1 it follows that based on stamping forming metal plate obtained by the embodiment of the present invention 1 to 5
The tensile strength of golden plate material be 2136MPa or more, yield strength be 2011MPa or more, elongation percentage A50 be 15.3% and with
On, yield rate is 98% or more, cracking breakout 0.03% and hereinafter, and based on stamping forming metal plate obtained by comparative example 1 to 3
The compression strength of golden plate material is respectively 1637MPa, 1648MPa and 1631MPa, and yield strength is respectively 1534MPa, 1542MPa
And 1536MPa, elongation percentage are respectively 7.3%, 7.8% and 7.1%, yield rate is respectively 83%, 86% and 81%, cracking breakout point
Not Wei 0.2%, 0.3% and 0.4%, the experimental results showed that, based on stamping forming metal plate obtained by the embodiment of the present invention 1 to 5
Golden plate material has higher tensile strength and plasticity, can adapt to improve lumber recovery, energy in the production of complicated shape structural member
It is enough to avoid the problem that drop stamping titanium alloy plate crackle easy to form, cracking breakout are low very well.
Comparative example 1 obtained by the embodiment of the present invention 1 to 5 based on stamping forming metal plate plate compared with, processed
Due to extrusion plate surface scale removal, not be easy to causeing extrusion plate oxide skin bring table during the rolling process in journey
Face problem of Cracking, make tensile strength, yield strength and plasticity based on stamping forming metal plate plate made from comparative example 1 compared with
Low, yield rate is low, and cracking breakout is high.
Comparative example 2 obtained by the embodiment 1 to 5 based on stamping forming metal plate plate compared with, in process due to
Annealing time is too long, and extrusion plate during the rolling process grow up by internal grain, so as to cause extrusion plate cracking, makes comparative example 2
Tensile strength obtained based on stamping forming metal plate plate, yield strength and plasticity are lower, and yield rate is low, and cracking breakout is high.
Comparative example 3 obtained by the embodiment 1 to 5 based on stamping forming metal plate plate compared with, in process, due to
The speed that rolled plate cools down in a mold is slower, and the springback capacity after shaping stamping parts is larger, significantly reduces stamping parts
Forming accuracy, make tensile strength, yield strength and plasticity based on stamping forming metal plate plate made from comparative example 3 compared with
Low, yield rate is low, and cracking breakout is high.
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie
In the case where without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power
Benefit requires rather than above description limits, it is intended that all by what is fallen within the meaning and scope of the equivalent elements of the claims
Variation is included within the present invention.Any label in claim should not be construed as limiting the claims involved.
Claims (10)
1. one kind is based on stamping forming metal plate plate, it is characterised in that: should be based on stamping forming metal plate plate by raw material titanium
Ingot casting is made after heat stamping and shaping.
2. according to claim 1 a kind of based on stamping forming metal plate plate, which is characterized in that the raw material titanium ingot casting
Contain following components in percentage by weight: iron 0.001-0.05%, oxygen 0.005-0.07%, carbon 0.001-0.005%, molybdenum
0.001-0.003%, boron 0.001-0.005%, remaining is titanium.
3. a kind of processing technology based on stamping forming metal plate plate, which is characterized in that stamping forming panel beating plate should be based on
The processing technology of material the following steps are included:
(1) Homogenization Treatments are carried out to raw material titanium ingot casting;
(2) preparation of extrusion plate;
(3) preparation of rolled plate;
(4) ultrasound detection is carried out to the resulting rolled plate of step (3);
(5) step (4) resulting rolled plate is pre-processed;
(6) the resulting rolled plate of step (5) is subjected to heat stamping and shaping, obtained based on stamping forming metal plate plate.
4. a kind of processing technology based on stamping forming metal plate plate according to claim 3, which is characterized in that the base
In stamping forming metal plate plate processing technology the following steps are included:
(1) Homogenization Treatments are carried out to raw material titanium ingot casting, is heated raw material titanium ingot casting using resistance furnace, kept the temperature, then quench
Fire;
(2) the obtained titanium ingot casting of step (1) is heated, keeps the temperature, then squeezes, obtain extrusion plate;
(3) the obtained extrusion plate surface of step (2) is polished, then descale rolls, rolled plate is made;
(4) ultrasound detection is carried out to the resulting rolled plate of step (3), the quality of rolled plate is sentenced according to testing result
It is disconnected, until subject to rolled plate qualification;
(5) rolled plate of the obtained qualification of step (4) is heated, keeps the temperature, then cools down, kept the temperature, in rolled plate
Surface coats the ethanol solution of one layer of alumina silicate, dries;
(6) step (5) resulting rolled plate is put into heating furnace and is heated, then taken out and put into hot forming tool,
Stamping, pressure maintaining is cooling, pickling, trimming, and drilling is obtained based on stamping forming metal plate plate.
5. a kind of processing technology based on stamping forming metal plate plate according to claim 4, which is characterized in that the base
In stamping forming metal plate plate processing technology the following steps are included:
(1) Homogenization Treatments are carried out to raw material titanium ingot casting, raw material titanium ingot casting is heated to 300-500 DEG C using resistance furnace, heat preservation
Then 8-12h is quenched, hardening heat is 10-30 DEG C;
(2) the obtained titanium ingot casting of step (1) is heated to 450-550 DEG C, keeps the temperature 13h, is then squeezed on extruder,
Extrusion ratio is 5-7, obtains extrusion plate;
(3) the obtained extrusion plate surface of step (2) is polished, and scale removal, extrusion plate is rolled,
Rolling carries out 25-40 passage altogether, and 300-500 DEG C is heated between passage, keeps the temperature 0.51.5h, and rolling reduction is 12- per pass
18%, extrusion plate is made annealing treatment between passage, rolled plate is made;
(4) ultrasound detection is carried out to the resulting rolled plate of step (3), starts ultrasonic inspection probe, is issued by ultrasound emission end
Ultrasonic signal emits short pulse sound energy into rolled plate, monitors and analyze the sound wave letter by reflection by ultrasound detection instrument
Number, testing result is obtained, the quality of rolled plate is judged according to testing result, it will be through the underproof rolling of ultrasound detection
Plate is removed, and after the rolled plate more renewed, is reused ultrasonic detection equipment and is carried out quality testing to rolled plate, until rolling
Subject to panel qualification;
(5) rolled plate of the obtained qualification of step (4) is heated to 700-800 DEG C with the speed of 10-20 DEG C/s, protected
Then warm 8-15min is cooled to 300-350 DEG C with the speed of 20-30 DEG C/s, keep the temperature 1-3min, coats on rolled plate surface
The ethanol solution of one layer of alumina silicate, coating thickness 0.5-1mm, coating surface is dried;
(6) step (5) resulting rolled plate is put into heating in heating furnace, the temperature of heating furnace is 900-1000 DEG C, then
Taking-up is put into mold rapidly, stamping, pressure maintaining 10-20s is carried out to rolled plate, in a mold with the speed of 30-40 DEG C/s
Degree is cooled to room temperature, and is taken out stamping parts, is carried out pickling with sulfuric acid solution, is carried out trimming and drilling to stamping parts, is obtained based on punching
Molded metal plate plate.
6. a kind of processing technology based on stamping forming metal plate plate according to claim 5, it is characterised in that: described
Occur longer or when compared with deep torn grain in step (3) on rolled plate, fragmented parts are cut off, are further continued for being rolled.
7. a kind of processing technology based on stamping forming metal plate plate according to claim 5, it is characterised in that: described
It when fine cracks occurs in rolled plate edge surface in step (3), is polishing to abrasive machine bright and clean smooth, is further continued for being rolled
System.
8. a kind of processing technology based on stamping forming metal plate plate according to any one of claims 5 to 7, special
Sign is: annealing time is 10-20min in the step (3).
9. a kind of processing technology based on stamping forming metal plate plate according to claim 8, it is characterised in that: described
The mass fraction of the ethanol solution of alumina silicate is 0.5-2% in step (5).
10. a kind of processing technology based on stamping forming metal plate plate according to claim 9, it is characterised in that: institute
The mass fraction for stating sulfuric acid solution in step (6) is 5-10%.
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