CN109928644A - Surface treatment method is used in a kind of production of safety glass - Google Patents
Surface treatment method is used in a kind of production of safety glass Download PDFInfo
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- CN109928644A CN109928644A CN201910279846.6A CN201910279846A CN109928644A CN 109928644 A CN109928644 A CN 109928644A CN 201910279846 A CN201910279846 A CN 201910279846A CN 109928644 A CN109928644 A CN 109928644A
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Abstract
The invention discloses a kind of safety glass production surface treatment methods, it is related to safety glass production technical field, surface treatment method is following steps: S1, first pretreatment: S2, secondary pretreatment: S3, heat treatment: S4, coating film treatment: S5, baking processing: S6, applies plating.The present invention pre-processes safety glass surface using Duplex treatment mode, keep its surface cleanness height, glossiness good, and grease proofing pollution layer is coated in glass surface, make safety glass surface that there is high-intensitive oil-stain-preventing, make its oil-stain-preventing up to 99%, while having transparent Tio in safety glass Coating2Photocatalyst protection film layer; it can make safety glass after encountering sunlight or ultraviolet light irradiation; light reaction occurs; and then bacterium or the virus of glass surface can be eliminated; also the organic pollutant of glass surface can be oxidized away, and the present invention is not only easy to operate, it is at low cost; and high treating effect, cleannes are high.
Description
Technical field
The present invention relates to safety glass production technical field, surface treatment method is used in specifically a kind of safety glass production.
Background technique
Safety glass is that one kind is not crushed through high vibration or shock, is not easy the glass hurted sb.'s feelings broken.For vapour
Vehicle, aircraft and door and window of special constructure etc..Building uses safety glass, can resist bullet or per hour 100 kms
The attack of folded chopped cooked entrails of sheep stone in hurricane, this has especially important meaning to the modern architecture of host glass structure.Common peace
Full glass types have pad pasting glass, tempered glass etc..
It in safety glass production, needs to handle its surface, its spatter property on the one hand can be improved, on the other hand
Its protective performance can be improved, but existing safety glass surface treatment mode is excessively complicated, and to safety glass surface
It can not implement safeguard measure, safety glass surface is be easy to cause not bear dirty, intolerant to greasy dirt, organic dirt easy to breed, Er Qieshi
Between its long surface glossiness it is poor, cause aesthetics to reduce, therefore, those skilled in the art provide a kind of safety glass
Production surface treatment method, to solve the problems mentioned in the above background technology.
Summary of the invention
The purpose of the present invention is to provide a kind of safety glass production surface treatment methods, to solve above-mentioned background technique
The problem of middle proposition.
To achieve the above object, the invention provides the following technical scheme: a kind of safety glass, which produces, uses surface treatment method,
Its surface treatment method is following steps:
S1, first pretreatment: the surface of safety glass to be processed is pre-processed, first with organic solvent to glass table
Face is atomized, and is uniformly sprayed on glass surface using the pressure of 5~15MPa, safety glass is then placed on black
Background before, the clearing glass cleanliness after observation is spraying;
S2, secondary pretreatment: after S1, the glass surface after first cleaning is carried out using filtered pure water
Secondary spraying, pressure when spraying is uniform, until the surface cleanness of safety glass reaches requirement;
S3, heat treatment: heating the safety glass after cleaning, and heating condition is 100~400 DEG C, the time
For 5min;
S4, coating film treatment: carrying out plated film to S3 treated safety glass, using electron gun by the raw material of oil-stain-preventing film
After conjunction object is evaporated, raw material compound is deposited on the surface of glass, shape in the form of nanoscale molecular under the action of ion source
At oil-stain-preventing film layer;
S5, baking processing: after the completion of S4 plated film, the safety glass after plated film is put into baking oven baking 15min, temperature control
System after cooling, can be covered with oil-stain-preventing film layer in glass surface at 60~100 DEG C;
S6, plating is applied: after S5, in the Coating layer protecting film layer of oil-stain-preventing film layer, thicknesses of layers control
System after the completion of plated film, is put into heater box and is heated at 5~8 μm, and temperature is controlled at 50~90 DEG C, after cooling, Ji Ke
Safety glass surface is covered with protective film layer.
As a further solution of the present invention: the cleannes observation condition in the S1 are as follows: when glass surface is cleaned
When cleaning, the surface of glass can show black and breathe out trace, and when the surface cleanness of glass is inadequate, glass surface will appear grey
Breathe out trace.
As further scheme of the invention: organic solvent is ethyl alcohol, acetone, carbon tetrachloride, three chloroethenes in the S1
One of alkene and isopropyl acetone.
As further scheme of the invention: the secondary pretreatment condition in the S2 are as follows: cleaned according to glass surface
Degree judges whether to comply with standard, and does not meet, repeats above-mentioned cleaning step, until cleannes comply with standard.
As further scheme of the invention: the raw material compound of the oil-stain-preventing film layer in the S4 includes following weight
Than the mixture of component: magnesium fluoride 40~70%, zirconium oxide 20~40%, nano hybridization fluorine silicon resin 10~20%, and oil resistant
The thicknesses of layers of dirty film is 2~5 μm.
As further scheme of the invention: the protective film layer in the S6 is a kind of transparent Tio2Photochemical catalyst applies
Layer.
Compared with prior art, the beneficial effects of the present invention are: a kind of safety glass production surface that the present invention designs
Processing method pre-processes safety glass surface using Duplex treatment mode, makes its surface cleanness in actual use
Height, glossiness are good, and are coated with grease proofing pollution layer in glass surface, and safety glass surface can be made to have high-intensitive oil-stain-preventing
Property, make its oil-stain-preventing up to 99%, while having transparent Tio in safety glass Coating2Photocatalyst protection film layer, can
So that safety glass occurs light reaction, reacts the active material of generation after encountering sunlight or ultraviolet light irradiation
With stronger oxidability, and then bacterium or the virus of glass surface can be eliminated, while can also oxidize away glass surface
Organic pollutant, makes that it is oxidized to carbon dioxide and water vapors away automatically, thereby further ensures that the cleaning on safety glass surface
Property and glossiness, and the present invention design safety glass surface treatment method it is not only easy to operate, it is at low cost, and handle
Effect is good, and cleannes are high.
Detailed description of the invention
Fig. 1 is the flow diagram that surface treatment method is used in a kind of production of safety glass;
Fig. 2 is comparative test result schematic diagram in a kind of safety glass production surface treatment method.
Specific embodiment
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete
Site preparation description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on
Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts every other
Embodiment shall fall within the protection scope of the present invention.
Please refer to Fig. 1~2, in the embodiment of the present invention,
Embodiment 1
A kind of safety glass production surface treatment method, surface treatment method is following steps:
S1, first pretreatment: the surface of safety glass to be processed is pre-processed, first with organic solvent to glass table
Face is atomized, and is uniformly sprayed on glass surface using the pressure of 5~15MPa, safety glass is then placed on black
Background before, the clearing glass cleanliness after observation is spraying;
S2, secondary pretreatment: after S1, the glass surface after first cleaning is carried out using filtered pure water
Secondary spraying, pressure when spraying is uniform, until the surface cleanness of safety glass reaches requirement;
S3, heat treatment: heating the safety glass after cleaning, and heating condition is 100~400 DEG C, the time
For 5min;
S4, coating film treatment: carrying out plated film to S3 treated safety glass, using electron gun by the raw material of oil-stain-preventing film
After conjunction object is evaporated, raw material compound is deposited on the surface of glass, shape in the form of nanoscale molecular under the action of ion source
At oil-stain-preventing film layer;
S5, baking processing: after the completion of S4 plated film, the safety glass after plated film is put into baking oven baking 15min, temperature control
System after cooling, can be covered with oil-stain-preventing film layer in glass surface at 60~100 DEG C;
S6, plating is applied: after S5, in the Coating layer protecting film layer of oil-stain-preventing film layer, thicknesses of layers control
System after the completion of plated film, is put into heater box and is heated at 5~8 μm, and temperature is controlled at 50~90 DEG C, after cooling, Ji Ke
Safety glass surface is covered with protective film layer.
Further, the cleannes observation condition in S1 are as follows: when glass surface cleaned cleaning, the surface meeting of glass
It shows black and breathes out trace, when the surface cleanness of glass is inadequate, glass surface will appear grey and breathe out trace.
Further, organic solvent is one of ethyl alcohol, acetone, carbon tetrachloride, trichloro ethylene and isopropyl acetone in S1.
Further, the secondary pretreatment condition in S2 are as follows: judge whether to comply with standard according to glass surface cleannes, no
Meet, repeat above-mentioned cleaning step, until cleannes comply with standard.
Further, the raw material compound of the oil-stain-preventing film layer in S4 includes the mixture of following weight ratio ingredient: fluorine
Change magnesium 40%, zirconium oxide 40%, nano hybridization fluorine silicon resin 20%, and the thicknesses of layers for the film of resistance to greasy dirt is 2~5 μm.
Further, the protective film layer in S6 is a kind of transparent Tio2Photocatalytic coating.
Embodiment 2
The present embodiment is unlike the first embodiment: the raw material compound of the oil-stain-preventing film layer in S4 includes following weight ratio
The mixture of component: magnesium fluoride 70%, zirconium oxide 20%, nano hybridization fluorine silicon resin 10%, and the thicknesses of layers for the film of resistance to greasy dirt
It is 2~5 μm.
Embodiment 3
The present embodiment is unlike the first embodiment: the raw material compound of the oil-stain-preventing film layer in S4 includes following weight ratio
The mixture of component: magnesium fluoride 55%, zirconium oxide 30%, nano hybridization fluorine silicon resin 15%, and the thicknesses of layers for the film of resistance to greasy dirt
It is 2~5 μm.
Comparative example 1
Select the safety glass after being surface-treated in common safety glass production technology.
Embodiment 1, embodiment 2 and embodiment 3 are compared with comparative example 1 respectively, and to embodiment 1, implementation
Safety glass compares after example 2, embodiment 3 and comparative example 1 are surface-treated, and detects the cleannes and oil-stain-preventing on its surface
Property, comparing result is as shown in Figure 2.
In conclusion a kind of safety glass production surface treatment method that the present invention designs, using Duplex treatment mode
Safety glass surface is pre-processed, it is high to make its surface cleanness, and be coated with grease proofing pollution layer to make safety glass surface
With high-intensitive oil-stain-preventing, while there is layer protecting film layer in safety glass Coating, which is a kind of saturating
Bright Tio2After encountering sunlight or ultraviolet light irradiation light reaction can occur for photocatalytic coating, and reaction produces
Raw active material has stronger oxidability, and then can eliminate bacterium or the virus of glass surface, while can also aoxidize
The organic pollutant for falling glass surface, makes that it is oxidized to carbon dioxide and water vapors away automatically, thereby further ensures that safe glass
The spatter property and glossiness on glass surface.
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie
In the case where without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power
Benefit requires rather than above description limits, it is intended that all by what is fallen within the meaning and scope of the equivalent elements of the claims
Variation is included within the present invention.Any reference signs in the claims should not be construed as limiting the involved claims.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped
Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should
It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
The other embodiments being understood that.
Claims (6)
1. a kind of safety glass production surface treatment method, which is characterized in that its surface treatment method is following steps:
S1, first pretreatment: the surface of safety glass to be processed is pre-processed, first with organic solvent to glass surface into
Row atomization, is uniformly sprayed on glass surface using the pressure of 5~15MPa, then safety glass is placed on to the back of black
Jing Qian, the clearing glass cleanliness after observation is spraying;
S2, secondary pretreatment: after S1, the glass surface after first cleaning is carried out using filtered pure water secondary
Spraying, pressure when spraying is uniform, until the surface cleanness of safety glass reaches requirement;
S3, heat treatment: heating the safety glass after cleaning, and heating condition is 100~400 DEG C, and the time is
5min;
S4, coating film treatment: carrying out plated film to S3 treated safety glass, using electron gun by the raw material compound of oil-stain-preventing film
After being evaporated, raw material compound is deposited on the surface of glass in the form of nanoscale molecular under the action of ion source, is formed anti-
Greasy dirt film layer;
S5, baking processing: after the completion of S4 plated film, the safety glass after plated film is put into baking oven baking 15min, temperature control exists
60~100 DEG C, after cooling, oil-stain-preventing film layer can be covered in glass surface;
S6, apply plating: after S5, in the Coating layer protecting film layer of oil-stain-preventing film layer, thicknesses of layers is controlled 5
It~8 μm, after the completion of plated film, is put into heater box and is heated, temperature is controlled at 50~90 DEG C, can be in safety after cooling
Glass surface is covered with protective film layer.
2. a kind of safety glass production surface treatment method according to claim 1, which is characterized in that in the S1
Cleannes observation condition are as follows: when glass surface cleaned cleaning, the surface of glass can show black and breathe out trace, when glass
When surface cleanness is inadequate, glass surface will appear grey and breathe out trace.
3. a kind of safety glass production surface treatment method according to claim 1, which is characterized in that have in the S1
Solvent is one of ethyl alcohol, acetone, carbon tetrachloride, trichloro ethylene and isopropyl acetone.
4. a kind of safety glass production surface treatment method according to claim 1, which is characterized in that in the S2
Secondary pretreatment condition are as follows: judge whether to comply with standard according to glass surface cleannes, not meet, repeats above-mentioned cleaning step,
Until cleannes comply with standard.
5. a kind of safety glass production surface treatment method according to claim 1, which is characterized in that in the S4
The raw material compound of oil-stain-preventing film layer includes the mixture of following weight ratio ingredient: magnesium fluoride 40~70%, zirconium oxide 20~
40%, nano hybridization fluorine silicon resin 10~20%, and the thicknesses of layers for the film of resistance to greasy dirt is 2~5 μm.
6. a kind of safety glass production surface treatment method according to claim 1, which is characterized in that in the S6
Protective film layer is a kind of transparent Tio2Photocatalytic coating.
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Cited By (3)
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CN111487256A (en) * | 2020-03-24 | 2020-08-04 | 信义节能玻璃(四川)有限公司 | Method for inspecting sucker seal of coated glass and coated glass |
CN111929922A (en) * | 2020-07-02 | 2020-11-13 | 滁州优立光学眼镜有限公司 | Manufacturing method of spectacle lens capable of preventing blue light |
CN112285811A (en) * | 2020-11-30 | 2021-01-29 | 江苏中新瑞光学材料有限公司 | Antistatic AF (aluminum fluoride) coating material and preparation method thereof |
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CN112285811A (en) * | 2020-11-30 | 2021-01-29 | 江苏中新瑞光学材料有限公司 | Antistatic AF (aluminum fluoride) coating material and preparation method thereof |
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Application publication date: 20190625 |