CN109836722A - A kind of preparation method of the sprayed film with bactericidal effect - Google Patents
A kind of preparation method of the sprayed film with bactericidal effect Download PDFInfo
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- CN109836722A CN109836722A CN201711221624.6A CN201711221624A CN109836722A CN 109836722 A CN109836722 A CN 109836722A CN 201711221624 A CN201711221624 A CN 201711221624A CN 109836722 A CN109836722 A CN 109836722A
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Abstract
The invention discloses a kind of preparation methods of sprayed film with bactericidal effect, comprising the following steps: PVC, phenolic resin, lecithin and medical stone are added in blender and are uniformly mixed by step a, obtain material a；Material a is transferred in reaction kettle by step b, and melamine and hydroxypropyl methyl cellulose is added, and 65-70 DEG C is heated under condition of negative pressure, is stirred 10-15 minutes, is obtained material b；Antioxidant, barium stearate and sodium benzoate are added in material b, is uniformly mixed, obtains material c by step c；Step d, by material c in double screw extruder extruding pelletization, obtain master batch, by master batch using plastic film blowing machine squeeze out blown film, obtain the preventing atomization medical films with sterilization functions.The beneficial effects of the present invention are: the medical atomized film is with good performance, heat distortion temperature has reached 160 DEG C or more, and preventing atomization performance has reached level-one, has good thermal stability and preventing atomization performance.
Description
Technical field
The present invention relates to a kind of preparation method of sprayed film more particularly to a kind of preparations of the sprayed film with bactericidal effect
Method.
Background technique
With the development and improvement of living standard of social economy, the mankind are just unprecedentedly paying close attention to the medical treatment & health cause of itself.
The increasing of survival pressure, the accelerating rhythm of life, the aggravation of environmental pollution, the safety accidents such as food, traffic and production and office
The frequent generation of portion's war, natural calamity etc. causes disease and wound to become the haze that the mankind can't get rid of forever.As the modern times
The important foundation and component part of the important means of medicine --- medical instrument, biomaterial for disease diagnosing and treating,
Reparation, replacement or the function of histoorgan are promoted, and making largely to struggle rehabilitates in the sufferer at residual, dead painful edge.In recent years,
Global medical instrument industry high speed development, average annual growth rate are same period increasing speed of national economy more than 2 times, are known as " rising industry ",
Have become the 21st century very active new source of economic growth.By taking China as an example, China's Medical Device Market speedup height in 2010
Up to 23%, market scale breaks through 1,00,000,000,000 yuan of high pointes for the first time, becomes the second-biggest-in-the-world Medical Device Market for being only second to the U.S.,
Expecting market scale in 2015 will be close to 3,40000000000 yuan.Just because of the so huge society of biomaterial and economic value,
Its R&D work is increasingly subject to the highest attention of countries in the world government, industrial circle and scientific and technological circle, successively by beauty, moral, day, Australia and
The Chinese government is included in high-tech key new material development plan.In presently used biological medicine material, suppression itself can be played
The material of bacterium effect has had many researchs and application, but the material that can play sterilizing is actually rare, while
The material that medical industry is used has special requirement under conditions of special, if membrane material needs good permeability, no
Atomizing effect can be generated because of the change of temperature, affect normal use.
Therefore, to solve the above problems, providing a kind of new technical solution.
Summary of the invention
The present invention provides a kind of preparation method of sprayed film with bactericidal effect.
The technical solution adopted by the present invention is that:
A kind of preparation method of the sprayed film with bactericidal effect, comprising the following steps:
PVC, phenolic resin, lecithin and medical stone are added in blender and are uniformly mixed by step a, obtain material a；
Material a is transferred in reaction kettle by step b, and melamine and hydroxypropyl methyl cellulose is added, and is added under condition of negative pressure
Heat stirs 10-15 minutes to 65-70 DEG C, obtains material b；
Antioxidant, barium stearate and sodium benzoate are added in material b, is uniformly mixed, obtains material c by step c；
Step d, by material c in double screw extruder extruding pelletization, obtain master batch, by master batch using plastic film blowing machine extrusion blow
Film obtains the preventing atomization medical films with sterilization functions.
Further, the parts by weight of the PVC, phenolic resin, lecithin and medical stone are respectively as follows:
30-40 parts of PVC；
10-15 parts of phenolic resin；
5-10 parts of lecithin；
1-4 parts of medical stone.
Further, the parts by weight of the melamine are 3-5 parts, the parts by weight of the hydroxypropyl methyl cellulose
It is 4-8 parts.
Further, the parts by weight of the antioxidant are 1-3 parts, and the parts by weight of the barium stearate are 3-7 parts, institute
The parts by weight for stating sodium benzoate are 4-8 parts.
The beneficial effects of the present invention are: the medical atomized film is with good performance, heat distortion temperature reached 160 DEG C with
On, preventing atomization performance has reached level-one, has good thermal stability and preventing atomization performance, while having the effect of antibacterial, full
Sufficient demand.
Specific embodiment
In order to deepen the understanding of the present invention, the present invention will be described in further detail with reference to the examples below, the embodiment
For explaining only the invention, it does not restrict the protection scope of the present invention.
Embodiment 1
A kind of preparation method of the sprayed film with bactericidal effect, comprising the following steps:
PVC, phenolic resin, lecithin and medical stone are added in blender and are uniformly mixed by step a, obtain material a,
It is respectively as follows: PVC30 parts by weight；10 parts of phenolic resin；5 parts of lecithin；1 part of medical stone；
Material a is transferred in reaction kettle by step b, and melamine and hydroxypropyl methyl cellulose is added, and is added under condition of negative pressure
Heat stirs 10 minutes to 65 DEG C, obtains material b, and the parts by weight of melamine are 3 parts, the weight of hydroxypropyl methyl cellulose
Number is 4 parts；
Antioxidant, barium stearate and sodium benzoate are added in material b, is uniformly mixed, obtains material c, antioxygen by step c
The parts by weight of agent are 1 part, and the parts by weight of barium stearate are 3 parts, and the parts by weight of sodium benzoate are 4 parts；
Step d, by material c in double screw extruder extruding pelletization, obtain master batch, by master batch using plastic film blowing machine extrusion blow
Film obtains the preventing atomization medical films with sterilization functions；
The beneficial effects of the present invention are: the medical atomized film is with good performance, heat distortion temperature has reached 160 DEG C or more,
Preventing atomization performance has reached level-one, has good thermal stability and preventing atomization performance, while having the effect of antibacterial, meets need
It asks.
Embodiment 2
A kind of preparation method of the sprayed film with bactericidal effect, comprising the following steps:
PVC, phenolic resin, lecithin and medical stone are added in blender and are uniformly mixed by step a, obtain material a,
It is respectively as follows: PVC35 parts by weight；13 parts of phenolic resin；7 parts of lecithin；3 parts of medical stone；
Material a is transferred in reaction kettle by step b, and melamine and hydroxypropyl methyl cellulose is added, and is added under condition of negative pressure
Heat stirs 13 minutes to 67 DEG C, obtains material b, and the parts by weight of melamine are 4 parts, the weight of hydroxypropyl methyl cellulose
Number is 6 parts；
Antioxidant, barium stearate and sodium benzoate are added in material b, is uniformly mixed, obtains material c, antioxygen by step c
The parts by weight of agent are 2 parts, and the parts by weight of barium stearate are 5 parts, and the parts by weight of sodium benzoate are 6 parts；
Step d, by material c in double screw extruder extruding pelletization, obtain master batch, by master batch using plastic film blowing machine extrusion blow
Film obtains the preventing atomization medical films with sterilization functions；
The beneficial effects of the present invention are: the medical atomized film is with good performance, heat distortion temperature has reached 160 DEG C or more,
Preventing atomization performance has reached level-one, has good thermal stability and preventing atomization performance, while having the effect of antibacterial, meets need
It asks.
Embodiment 3
A kind of preparation method of the sprayed film with bactericidal effect, comprising the following steps:
PVC, phenolic resin, lecithin and medical stone are added in blender and are uniformly mixed by step a, obtain material a,
It is respectively as follows: PVC40 parts by weight；15 parts of phenolic resin；10 parts of lecithin；4 parts of medical stone；
Material a is transferred in reaction kettle by step b, and melamine and hydroxypropyl methyl cellulose is added, and is added under condition of negative pressure
Heat stirs 15 minutes to 70 DEG C, obtains material b, and the parts by weight of melamine are 5 parts, the weight of hydroxypropyl methyl cellulose
Number is 8 parts；
Antioxidant, barium stearate and sodium benzoate are added in material b, is uniformly mixed, obtains material c, antioxygen by step c
The parts by weight of agent are 3 parts, and the parts by weight of barium stearate are 7 parts, and the parts by weight of sodium benzoate are 8 parts；
Step d, by material c in double screw extruder extruding pelletization, obtain master batch, by master batch using plastic film blowing machine extrusion blow
Film obtains the preventing atomization medical films with sterilization functions；
The beneficial effects of the present invention are: the medical atomized film is with good performance, heat distortion temperature has reached 160 DEG C or more,
Preventing atomization performance has reached level-one, has good thermal stability and preventing atomization performance, while having the effect of antibacterial, meets need
It asks.
The above described is only a preferred embodiment of the present invention, being not the limit for making any other form to the present invention
System, and made any modification or equivalent variations according to the technical essence of the invention, still fall within present invention model claimed
It encloses.
Claims (4)
1. a kind of preparation method of the sprayed film with bactericidal effect, it is characterised in that: the following steps are included:
PVC, phenolic resin, lecithin and medical stone are added in blender and are uniformly mixed by step a, obtain material a；
Material a is transferred in reaction kettle by step b, and melamine and hydroxypropyl methyl cellulose is added, and is added under condition of negative pressure
Heat stirs 10-15 minutes to 65-70 DEG C, obtains material b；
Antioxidant, barium stearate and sodium benzoate are added in material b, is uniformly mixed, obtains material c by step c；
Step d, by material c in double screw extruder extruding pelletization, obtain master batch, by master batch using plastic film blowing machine extrusion blow
Film obtains the preventing atomization medical films with sterilization functions.
2. a kind of preparation method of sprayed film with bactericidal effect according to claim 1, it is characterised in that: described
PVC, phenolic resin, lecithin and medical stone parts by weight be respectively as follows:
30-40 parts of PVC；
10-15 parts of phenolic resin；
5-10 parts of lecithin；
1-4 parts of medical stone.
3. a kind of preparation method of sprayed film with bactericidal effect according to claim 1, it is characterised in that: described three
The parts by weight of poly cyanamid are 3-5 parts, and the parts by weight of the hydroxypropyl methyl cellulose are 4-8 parts.
4. a kind of preparation method of sprayed film with bactericidal effect according to claim 1, it is characterised in that: described anti-
The parts by weight of oxygen agent are 1-3 parts, and the parts by weight of the barium stearate are 3-7 parts, and the parts by weight of the sodium benzoate are
4-8 parts.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711221624.6A CN109836722A (en) | 2017-11-29 | 2017-11-29 | A kind of preparation method of the sprayed film with bactericidal effect |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711221624.6A CN109836722A (en) | 2017-11-29 | 2017-11-29 | A kind of preparation method of the sprayed film with bactericidal effect |
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| CN109836722A true CN109836722A (en) | 2019-06-04 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201711221624.6A Pending CN109836722A (en) | 2017-11-29 | 2017-11-29 | A kind of preparation method of the sprayed film with bactericidal effect |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS62257953A (en) * | 1986-05-01 | 1987-11-10 | Mitsubishi Kasei Vinyl Co | Production of vinyl chloride resin composition |
| CN103571014A (en) * | 2013-10-13 | 2014-02-12 | 甘春丽 | Composition as well as functional film and preparation method thereof |
| CN105131472A (en) * | 2015-09-23 | 2015-12-09 | 江苏蓝湾生物科技有限公司 | Preparation method of anti-fogging medical film having sterilizing function |
-
2017
- 2017-11-29 CN CN201711221624.6A patent/CN109836722A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS62257953A (en) * | 1986-05-01 | 1987-11-10 | Mitsubishi Kasei Vinyl Co | Production of vinyl chloride resin composition |
| CN103571014A (en) * | 2013-10-13 | 2014-02-12 | 甘春丽 | Composition as well as functional film and preparation method thereof |
| CN105131472A (en) * | 2015-09-23 | 2015-12-09 | 江苏蓝湾生物科技有限公司 | Preparation method of anti-fogging medical film having sterilizing function |
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Application publication date: 20190604 |