CN109833238A - A kind of extracting method of black fruit fructus lycii active matter used for cosmetic - Google Patents
A kind of extracting method of black fruit fructus lycii active matter used for cosmetic Download PDFInfo
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- CN109833238A CN109833238A CN201711205889.7A CN201711205889A CN109833238A CN 109833238 A CN109833238 A CN 109833238A CN 201711205889 A CN201711205889 A CN 201711205889A CN 109833238 A CN109833238 A CN 109833238A
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- fructus lycii
- black fruit
- fruit fructus
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Abstract
The invention discloses a kind of extracting methods of black fruit fructus lycii active matter used for cosmetic, specifically includes the following steps: (1) mixes black fruit fructus lycii in the ratio that the mass ratio of water is 1:10 ~ 30, constant temperature stirring is filtered after extracting 0.5 ~ 3h in 30 ~ 70 DEG C of water-bath；(2) after filtered filtrate is concentrated into 5 ~ 20 times of black fruit fructus lycii quality after being centrifuged, the polyalcohol that equal quality is added is stirred evenly；(3) preservative is added in the mixing liquid for obtaining step (2), stirs evenly, final extracting solution is made.The residual of the nonirritant substance of the extracting solution that the present invention obtains, and stability of the extracting solution in storing process is improved, and be easily added in cosmetics.
Description
Technical field
The present invention relates to a Plant Extracts fields, specifically, being related to a kind of black fruit fructus lycii in cosmetics
The extracting method of active matter.
Background technique
Black fruit fructus lycii belongs to Solanaceae Lycium, is distributed in high mountain sarin, salinization sand ground, river and lake bank, dry wash, famine
It is a kind of distinctive plant resources in northwest China Desert Area in unconcerned riparian forest, berry is spherical, is atropurpureus, taste after mature
It is sweet.It is recorded in " Uygur medicine will ", lycium ruthenicum fruit has the effects that improving eyesight, moistens dry, stomach invigorating, anti-aging." brilliant pearl sheet
Grass " it is also on the books, black fruit fructus lycii is for treating irregular menstruation, heart disease, cardiopyretic disease etc. and significant in efficacy.Therefore, black fruit fructus lycii
Be commonly applied to medicine, health care etc., the beauty industries such as cosmetics utilization seldom, however they rich in various active at
Point, such as procyanidine, anthocyanin, polysaccharide, flavones and amino acid are all with good cosmetic result.Therefore, how by black fruit
Fructus lycii is applied to cosmetic field, retains a variety of active ingredients, realizes that comprehensive utilization just becomes particularly significant.
China applies for a patent 105218695 A of CN and passes through cleaning, dry, broken, removal of impurities, extraction, decoloration, removing protein, dense
The lycium ruthenicum polysaccharide for the single component that the preparation methods such as contracting, purifying obtain.For cosmetic field, this extracting method makes
A variety of beauty and skin care ingredients in black fruit fructus lycii are not comprehensively utilized.
103082291 A of Chinese patent application CN is by lycium ruthenicum ethyl alcohol pre-treatment, 70-90 DEG C of hot water extraction in three times
It is made, which has easily residual using organic solvent pre-treatment, is unsuitable for being added in cosmetics.
China applies for a patent 101991709 A of CN and discloses a kind of method for preparing antioxidant lycium ruthenicum extract, should
Method is using black fruit fructus lycii dry fruit as raw material, and through flooding, colloid mill grinding and high-pressure homogeneous then is removed with microfiltration ceramic membrane
Impurity obtains anti-oxidant black fruit fructus lycii extract, the patent application by macroreticular resin separation, spray drying or freeze-drying
The disadvantages of complex process, equipment requirement are high, at high cost.
101982192 A of Chinese patent application CN is using black fruit lyceum juice or black fruit fructus lycii concentrate as raw material, through non-pole
Property macroporous absorbent resin separation after, be washed with deionized water and take off to sugar-free, then eluted with ethanol solution, eluent is dense through vacuum decompression
Contracting or nanofiltration membrane concentration after, finally by concentrate it is spray-dried or freeze-drying.The extract of this method preparation is solid powder
End is added into the cosmetics that cosmetics have insoluble granule, especially water aqua type with liquid extraction liquid phase ratio, is also easy to be precipitated
Form precipitating.
Summary of the invention
The object of the present invention is to provide a kind of extracting method of black fruit fructus lycii active matter used for cosmetic, which simply may be used
It leans on, is avoided that related substance is precipitated to form precipitating, improves the quality of such cosmetics.The extracting solution that this method obtains is suitable for
The cosmetics of the dosage forms such as cream, lotion, aqua are particularly suitable for the cosmetics of water aqua type.
In order to achieve the above objectives, the present invention provides a kind of preparation method of black fruit fructus lycii extracting solution used for cosmetic, include
Following steps:
(1) black fruit fructus lycii is mixed in the ratio that the mass ratio of water is 1:10 ~ 30, constant temperature stirs in 30 ~ 70 DEG C of water-bath
It is filtered after extracting 0.5 ~ 3h；
(2) after filtered filtrate is concentrated into 5 ~ 20 times of black fruit fructus lycii quality after being centrifuged, the polyalcohol of equal quality is added
It stirs evenly；
(3) preservative is added in the mixing liquid for obtaining step (2), stirs evenly, final extracting solution is made.
In some embodiments, the revolving speed of step (2) centrifugation is 6000~12000r/min.
In some embodiments, the polyalcohol of step (2) can be glycerol, 1,3-PD, 1,3-BDO, dipropyl
One of glycol.
In some embodiments, the preservative of step (3) can be potassium sorbate, sodium benzoate, Phenoxyethanol etc..
Main advantages of the present invention are as follows:
The black fruit fructus lyciis main component such as amino acid, polysaccharide, anthocyanidin and procyanidine is extracted from black fruit fructus lycii by this method
Comprehensive recovery rate maintains higher level.Furthermore method provided by the invention is used, black fruit fructus lycii in extracting solution is not only increased
The solubility of each active matter, and solve black fruit fructus lycii extracting solution refrigeration, in heating process due to activity concentration is excessively high
The FAQs of precipitating and color change etc. is precipitated, and under 4 DEG C, 25 DEG C, 45 DEG C of room temperature and subzero 18 DEG C of temperature constant states all
It can stablize 3 months or more, solution keeps clear, and no precipitating and macroscopic foreign matter are precipitated, with other raw materials of cosmetics
Compatibility it is good, be suitble to cosmetics in as raw material add.
Specific embodiment
As described below is the preferred embodiment of the present invention, and what the present invention was protected is not limited to following preferred implementation side
Formula.It should be pointed out that for those skilled in the art on the basis of the inventive concept, several deformations for making and
It improves, belongs to protection scope of the present invention.
Black fruit fructus lycii is obtained from commercially available in the embodiment of the present invention.It is realized in the embodiment of the present invention by the following conditions:
Experiment condition: after black fruit fructus lycii is extracted with water, extracting solution is after filtering, centrifugation, concentration, by extracting solution and glycerol, 1,3-
One of polyalcohols such as butanediol, 1,3- propylene glycol, dipropylene glycol, be statically placed in 45 DEG C, 4 DEG C, it is 18 DEG C and 25 DEG C of room temperature subzero
In the environment of, the smell of observation extracting solution, color change, pH value change and whether have substance precipitation under the corresponding period
Etc. judge the stability of extracting solution.
Embodiment 1
The dry black fruit fructus lycii of 20.0g is weighed, the ratio that black fruit fructus lycii and water are 1:10 in mass ratio is mixed, in 30 DEG C of water
Constant temperature stirring is filtered after extracting 0.5h in bath；
(2) filtered filtrate is concentrated into 5 times of black fruit fructus lycii quality after 12000r/min is centrifuged 20min, and same matter is added
The glycerol of amount stirs evenly；
(3) Phenoxyethanol is added in the mixing liquid for obtaining step (2), stirs evenly, final extracting solution is made.By extracting solution into
Row stability test.Water consumption substitution glycerol is tested as a comparison, and the result is shown in tables 1.
1 stability test result of table
Embodiment 2
The dry black fruit fructus lycii of 20.0g is weighed, the ratio that black fruit fructus lycii and water are 1:15 in mass ratio is mixed, in 40 DEG C of water
Constant temperature stirring is filtered after extracting 1h in bath；
(2) filtered filtrate is concentrated into 8 times of black fruit fructus lycii quality after 6000r/min is centrifuged 20min, and equal quality is added
1,3-BDO stir evenly；
(3) sodium benzoate is added in the mixing liquid for obtaining step (2), stirs evenly, final extracting solution is made.By extracting solution into
Row stability test.Water consumption substitution 1,3-BDO is tested as a comparison, and the result is shown in tables 2.
2 stability test result of table
Embodiment 3
The dry black fruit fructus lycii of 20.0g is weighed, the ratio that black fruit fructus lycii and water are 1:20 in mass ratio is mixed, in 70 DEG C of water
Constant temperature stirring is filtered after extracting 2h in bath；
(2) filtered filtrate is concentrated into 20 times of black fruit fructus lycii quality after 8000r/min is centrifuged 20min, and same matter is added
The 1,3-PD of amount stirs evenly；
(3) potassium sorbate is added in the mixing liquid for obtaining step (2), stirs evenly, final extracting solution is made.By extracting solution into
Row stability test.Water consumption substitution 1,3-PD is tested as a comparison, and the result is shown in tables 3.
3 stability test result of table
Embodiment 4
The dry black fruit fructus lycii of 20.0g is weighed, the ratio that black fruit fructus lycii and water are 1:30 in mass ratio is mixed, in 50 DEG C of water
Constant temperature stirring is filtered after extracting 3h in bath；
(2) filtered filtrate is concentrated into 10 times of black fruit fructus lycii quality after 10000r/min is centrifuged 20min, and same matter is added
The dipropylene glycol of amount stirs evenly；
(3) Phenoxyethanol is added in the mixing liquid for obtaining step (2), stirs evenly, final extracting solution is made.By extracting solution into
Row stability test.Water consumption substitution dipropylene glycol is tested as a comparison, and the result is shown in tables 4.
4 stability test result of table
Claims (4)
1. a kind of extracting method of black fruit fructus lycii active matter used for cosmetic, which comprises the following steps:
(1) black fruit fructus lycii is mixed in the ratio that the mass ratio of water is 1:10 ~ 30, constant temperature stirs in 30 ~ 70 DEG C of water-bath
It is filtered after extracting 0.5 ~ 3h；
(2) after filtered filtrate is concentrated into 5 ~ 20 times of black fruit fructus lycii quality after being centrifuged, the polyalcohol of equal quality is added
It stirs evenly；
(3) preservative is added in the mixing liquid for obtaining step (2), stirs evenly, final extracting solution is made.
2. extracting method according to claim 1, it is characterised in that: step (2) centrifugation revolving speed be 6000~
12000r/min。
3. extracting method according to claim 1, it is characterised in that: the polyalcohol of step (2) can be glycerol, 1,3- third
Glycol, 1,3 butylene glycol, dipropylene glycol one of.
4. extracting method according to claim 1, it is characterised in that: the preservative of step (3) can be, potassium sorbate,
Sodium benzoate, Phenoxyethanol etc..
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711205889.7A CN109833238A (en) | 2017-11-27 | 2017-11-27 | A kind of extracting method of black fruit fructus lycii active matter used for cosmetic |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201711205889.7A CN109833238A (en) | 2017-11-27 | 2017-11-27 | A kind of extracting method of black fruit fructus lycii active matter used for cosmetic |
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| CN109833238A true CN109833238A (en) | 2019-06-04 |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101584647A (en) * | 2008-05-20 | 2009-11-25 | 赢创德固赛(中国)投资有限公司 | Polylol-in-oil composition with high vitamin C content and preparation method thereof |
| CN103446339A (en) * | 2013-08-27 | 2013-12-18 | 格尔木源鑫堂生物科技有限公司 | Preparation method of lycium ruthenicum extract |
| CN103565728A (en) * | 2013-11-06 | 2014-02-12 | 中国科学院西北高原生物研究所 | Lycium ruthenicum mill whitening and moisturizing smoothing toner and preparation method of smoothing toner |
| CN105963167A (en) * | 2016-04-11 | 2016-09-28 | 甘肃大禹黑枸杞农业科技有限公司 | Lycium ruthenicum murr toner |
-
2017
- 2017-11-27 CN CN201711205889.7A patent/CN109833238A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101584647A (en) * | 2008-05-20 | 2009-11-25 | 赢创德固赛(中国)投资有限公司 | Polylol-in-oil composition with high vitamin C content and preparation method thereof |
| CN103446339A (en) * | 2013-08-27 | 2013-12-18 | 格尔木源鑫堂生物科技有限公司 | Preparation method of lycium ruthenicum extract |
| CN103565728A (en) * | 2013-11-06 | 2014-02-12 | 中国科学院西北高原生物研究所 | Lycium ruthenicum mill whitening and moisturizing smoothing toner and preparation method of smoothing toner |
| CN105963167A (en) * | 2016-04-11 | 2016-09-28 | 甘肃大禹黑枸杞农业科技有限公司 | Lycium ruthenicum murr toner |
Non-Patent Citations (1)
| Title |
|---|
| 汪建红 等: "黑果枸杞果实多糖水浸提条件优化研究", 《新疆师范大学学报（自然科学版）》 * |
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