CN109813581A - The mobile semi-automatic sampling car of chemical method the escaping of ammonia - Google Patents

The mobile semi-automatic sampling car of chemical method the escaping of ammonia Download PDF

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Publication number
CN109813581A
CN109813581A CN201910113525.9A CN201910113525A CN109813581A CN 109813581 A CN109813581 A CN 109813581A CN 201910113525 A CN201910113525 A CN 201910113525A CN 109813581 A CN109813581 A CN 109813581A
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solenoid valve
way solenoid
bottle
pipeline
connect
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CN201910113525.9A
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CN109813581B (en
Inventor
崔海斌
蔡旭明
刘勤潭
王兰凤
于晓游
胡明明
马德海
陈鹏
李江国
胡国柱
岑岭山
张朝阳
李健
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Jingxi District Beijing Combustion Gas Thermal Power Co Ltd
BEIJING YUANSHEN ENERGY SAVING TECHNOLOGY Co Ltd
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Jingxi District Beijing Combustion Gas Thermal Power Co Ltd
BEIJING YUANSHEN ENERGY SAVING TECHNOLOGY Co Ltd
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Publication of CN109813581A publication Critical patent/CN109813581A/en
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Abstract

The embodiment of the present invention provides a kind of mobile semi-automatic sampling car of chemical method the escaping of ammonia, it is characterized in that, the mobile semi-automatic sampling car of the chemical method the escaping of ammonia includes: the sampling Integrated power control module of smoke absorption cleaning module and connection smoke absorption cleaning module;The smoke absorption cleaning module includes smoke inlet, and exhanst gas outlet, described smoke outlet setting total three-way solenoid valve one, two lines in parallel road between smoke inlet and exhanst gas outlet, every route includes: the first three-way solenoid valve;Sample absorption bottle, the sample absorption bottle are connect by pipeline with the first three-way solenoid valve;Second three-way solenoid valve, second three-way solenoid valve are connect by pipeline with sample absorption bottle;Anti-suck bottle, the anti-suck bottle are connect by pipeline with the second three-way solenoid valve;Acid solution purification bottle, the acid solution purification bottle are connect by pipeline with anti-suck bottle;Third three-way solenoid valve, the third three-way solenoid valve are connect by pipeline with acid solution purification bottle.

Description

The mobile semi-automatic sampling car of chemical method the escaping of ammonia
Technical field
The present invention relates to the mobile semi-automatic sampling car of chemical field more particularly to a kind of chemical method the escaping of ammonia,
Background technique
Nitrogen oxides is one of primary pollution source of atmosphere, generallys use catalysts selective reduction method both at home and abroad at present Removing nitrogen oxides is carried out with nonselective catalyst reduction method.Both methods is required to plus NH3Participate in reaction, a large amount of ammonia A small amount of the escaping of ammonia is had after addition to go out into air, pollutes environment, therefore China puts into effect relevant laws and regulations, stringent limitation Amount of ammonia slip.
NH3Detection method mainly has laser method and chemical method, and wherein laser method is to low concentration NH3Detection has certain office Sex-limited, inaccurate, laboratory generally uses chemical method analysis detection low concentration NH3, due to NH3Content is lower and easily inhales Attached, manually sampling easily causes NH3Loss, to cause detected value relatively low.
In realizing process of the present invention, at least there are the following problems in the prior art for inventor's discovery: laser method is to low dense Spend NH3Detection has certain limitation, and inaccurate, laboratory generally uses chemical method analysis detection low concentration NH3, due to NH3Content is lower and easily adsorbs, and manually sampling easily causes NH3Loss, to cause detected value relatively low.
Summary of the invention
The present invention relates to a kind of sampling car, especially a kind of mobile semi-automatic sampling car of chemical method the escaping of ammonia, to improve Working efficiency enhances detection accuracy.
A kind of mobile semi-automatic sampling car of chemical method the escaping of ammonia, the mobile semi-automatic sampling car of the chemical method the escaping of ammonia It include: the sampling Integrated power control module of smoke absorption cleaning module and connection smoke absorption cleaning module;
The smoke absorption cleaning module includes smoke inlet, exhanst gas outlet, the total electromagnetism three of the smoke outlet setting Port valve one, two lines in parallel road, every route include: between smoke inlet and exhanst gas outlet
First three-way solenoid valve;
Sample absorption bottle, the sample absorption bottle are connect by pipeline with the first three-way solenoid valve;
Second three-way solenoid valve, second three-way solenoid valve are connect by pipeline with sample absorption bottle;
Anti-suck bottle, the anti-suck bottle are connect by pipeline with the second three-way solenoid valve;
Acid solution purification bottle, the acid solution purification bottle are connect by pipeline with anti-suck bottle;
Third three-way solenoid valve, the third three-way solenoid valve are connect by pipeline with acid solution purification bottle;
Drying bottle, the drying bottle include the first drying bottle, the second drying bottle, third drying bottle, first drying bottle It is connect by pipeline with third three-way solenoid valve;
4th three-way solenoid valve, the 4th three-way solenoid valve are connect by pipeline with the first drying bottle;
Acid solution purification bottle, the acid solution purification bottle are connect by pipeline with the 4th three-way solenoid valve;
5th three-way solenoid valve, the 5th three-way solenoid valve are connect by pipeline with acid solution purification bottle;
Second drying bottle, second drying bottle are connect by pipeline with the 5th three-way solenoid valve;
6th three-way solenoid valve, the 6th three-way solenoid valve are connect by pipeline with the second drying bottle;
Third drying bottle, the third drying bottle are connect by pipeline with the 6th three-way solenoid valve;
The sampling Integrated power control module includes:
Filter, the filter are connect by pipeline with total three-way solenoid valve;
Suspended body flowmeter, the suspended body flowmeter are connected to the filter by pipeline;
Temperature sensor, the temperature sensor are connect by pipeline with suspended body flowmeter;
Pressure sensor, the pressure sensor are connect by pipeline with temperature sensor;
Blast volume controller, the blast volume controller are connect by pipeline with pressure sensor;
Vacuum pump, the vacuum pump are connect by pipeline with blast volume controller;
Signal integrated control device, the signal integrated control device by circuit respectively with temperature sensor, air quantity control Device processed, vacuum pump, pressure sensor, total three-way solenoid valve, the first three-way solenoid valve, the second three-way solenoid valve, third electromagnetism three Port valve, the 4th three-way solenoid valve, the 5th three-way solenoid valve, the connection of the 6th three-way solenoid valve.
Preferably, the mobile semi-automatic sampling car of the chemical method the escaping of ammonia includes 3 layers, and upper layer arrangement samples Integrated power Smoke absorption cleaning module, the spare bottle of lower layer arrangement smoke absorption cleaning module are arranged in control module, middle layer.
Preferably, the mobile semi-automatic sampling car of the chemical method the escaping of ammonia further include: sampling car skeleton, the sampling car Skeleton includes vehicle general frame and wheel, and sampling Integrated power control module is provided in the vehicle general frame and flue gas is inhaled Cleaning module is received, the wheel is located under vehicle general frame.
Preferably, two lines road in parallel between the smoke inlet and exhanst gas outlet is generally aligned in the same plane, the filtering Device is generally aligned in the same plane with suspended body flowmeter, and two lines road in parallel between smoke inlet and exhanst gas outlet is vertical.
Preferably, total three-way solenoid valve includes three ports, and first port and second port are separately connected two lines Road, third port connection are connected to the filter by pipeline.
Preferably, in parallel with the second drying bottle the is arranged between the 5th three-way solenoid valve and the 6th three-way solenoid valve Three parallel lines.
Preferably, in parallel with the first drying bottle the is arranged between the third three-way solenoid valve and the 4th three-way solenoid valve Two parallel lines.
Preferably, in parallel with sample absorption bottle the is arranged between first three-way solenoid valve and the second three-way solenoid valve One parallel line.
Preferably, the signal control device includes the display screen being arranged on sampling car skeleton.
Above-mentioned technical proposal has the following beneficial effects: because using anti-suck bottle and the technology hand of sampling car skeleton Section, so having reached, mechanism is simple, easy to use, work efficiency is high, improves the technical effect of detection accuracy.
Detailed description of the invention
In order to more clearly explain the embodiment of the invention or the technical proposal in the existing technology, to embodiment or will show below There is attached drawing needed in technical description to be briefly described, it should be apparent that, the accompanying drawings in the following description is only this Some embodiments of invention for those of ordinary skill in the art without creative efforts, can be with It obtains other drawings based on these drawings.
Fig. 1 is the operation principle schematic diagram of the mobile semi-automatic sampling car of chemical method the escaping of ammonia
Fig. 2 is the structural schematic diagram of the mobile semi-automatic sampling car of chemical method the escaping of ammonia
Detailed description of the invention
1, the first three-way solenoid valve;2, sample absorption bottle;3, the second three-way solenoid valve;4, anti-suck bottle;5, acid solution purifies Bottle;6, third three-way solenoid valve;7, the first drying bottle;8, the 4th three-way solenoid valve;9, solution purification bottle;10, the 5th electromagnetism three Port valve;11, the second drying bottle;12, the 6th three-way solenoid valve;13, third drying bottle;14, total three-way solenoid valve;15, filter; 16, suspended body flowmeter;17, temperature sensor;18, pressure sensor;19, blast volume controller;20, vacuum pump;21, signal is integrated Control device;22, the first parallel line;23, the second parallel line;24, third parallel line;25, upper layer arrangement samples power Integrated control module;26, smoke absorption cleaning module is arranged in middle layer;27, the lower spare bottle of layer arrangement smoke absorption cleaning module; 28, sampling car skeleton.
Specific embodiment
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete Site preparation description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts every other Embodiment shall fall within the protection scope of the present invention.
The present invention provides a kind of mobile semi-automatic sampling car of chemical method the escaping of ammonia, as shown in Figure 1, chemical method the escaping of ammonia moves The semi-automatic sampling car of dynamic formula include in parallel two lines road and connect total three-way solenoid valve 14 on two lines road, filter 15, Suspended body flowmeter 16, temperature sensor 17, pressure sensor 18, blast volume controller 19, vacuum pump 20.
Every route includes that sequence is the first three-way solenoid valve 1, sample absorption bottle 2, the second three-way solenoid valve 3, anti-suck Bottle 4, acid solution purification bottle 5, third three-way solenoid valve 6, the first drying bottle 7, the 4th three-way solenoid valve 8, solution purification bottle the 9, the 5th Three-way solenoid valve 10, the second drying bottle 11, the 6th three-way solenoid valve 12, third drying bottle 13.
Signal integrated control device 21 by circuit respectively with temperature sensor 17, blast volume controller 19, vacuum pump 20, pressure Force snesor 18, total three-way solenoid valve 14, the first three-way solenoid valve 1, the second three-way solenoid valve 3, third three-way solenoid valve 6, Four three-way solenoid valves 8, the 5th three-way solenoid valve 10, the 6th three-way solenoid valve 12;Ammonia can be effectively avoided by various elements The escape of gas, and improve detection accuracy.Integrated power control module is sampled, specifically using vacuum pump as power source.
Smoke absorption cleaning module, two lines road in parallel, that is, take the using and the reserved to arrange, flue gas passes sequentially through sample suction Receive bottle 2, anti-suck bottle 4, solution purification bottle 9, the first drying bottle 7, diluted acid purification bottle, the second drying bottle 11, third drying bottle 13; Three-way solenoid valve is arranged in the sample absorption bottle 2, the first drying bottle 7 and 11 two sides of the second drying bottle;Flue gas is through filter, floating After subflow meter, flowmeter, vacuum pump, it is discharged into atmosphere.
Preferably, as shown in Fig. 2, the mobile semi-automatic sampling car of the chemical method the escaping of ammonia includes 3 layers, upper layer arrangement is taken Sample Integrated power control module 25, middle layer arrange that smoke absorption cleaning module 26, lower layer arrangement smoke absorption cleaning module are spare Bottle 27, the various bottles used for replacing middle layer smoke absorption cleaning module;Sampling car is divided into multilayer, the division of labor is clear, The simplicity that ensure that operation avoids interfering with each other.
Preferably, as shown in Fig. 2, the mobile semi-automatic sampling car of the chemical method the escaping of ammonia further include: sampling car skeleton 28, it plays a supportive role;Sampling car skeleton, is specifically welded with stainless steel tube and stainless steel plate;The sampling car skeleton includes, Vehicle general frame, wheel are provided with sampling Integrated power control module and smoke absorption cleaning module in the vehicle general frame, The wheel is located under vehicle general frame;The setting of sampling car skeleton can be such that the sampling car is moved easily, and can be formed Confined space.
Preferably, as shown in Figure 1, two lines road in parallel between the smoke inlet and exhanst gas outlet is located at same put down Face, the filter 15 are generally aligned in the same plane with suspended body flowmeter 16, and in parallel two between smoke inlet and exhanst gas outlet Route is vertical, avoids interfering with each other;Two parallel lines are set in this way, and wherein A route samples, and B connection new sample is inhaled Bottle is received, terminates to switch to the second route by sampling Integrated power control module when first line samples, increases sampling car Capacity.
Preferably, as shown in Figure 1, total three-way solenoid valve includes three ports, first port and second port difference Two lines road is connected, third port connection is connected to the filter by pipeline;Setting can be by sampling Integrated power mould in this way Block controls the switching on two lines road, also can control smoke absorption cleaning module switch.
Preferably, as shown in Figure 1, setting and second between the 5th three-way solenoid valve 10 and the 6th three-way solenoid valve 12 The third parallel line 24 in parallel of drying bottle 11;When the second drying bottle saturation, part route where making the second drying bottle The replacement that short circuit, in this way setting facilitate the second drying bottle.
Preferably, as shown in Figure 1, setting and first dry between the third three-way solenoid valve 6 and the 4th three-way solenoid valve 8 Second parallel line 23 of dry bottle parallel connection;When the first drying bottle 7 saturation, keep partial line where the first drying bottle short out Road, in this way setting facilitate the replacement of the first drying bottle, and do not have ammonia escape.
Preferably, as shown in Figure 1, setting and sample suction between first three-way solenoid valve 1 and the second three-way solenoid valve 3 Receive the first parallel line 22 of bottle parallel connection;When sample absorption bottle needs replacing time, part line short where making sample absorption bottle, Setting in this way facilitates the replacement of sample absorption bottle, and does not have ammonia escape.Sample absorption bottle inlet end three-way solenoid valve is adopted With silica coating spool
Preferably, as shown in Fig. 2, display screen is arranged in the signal control module;Setting can more intuitively be seen in this way Valid data.
The sampling car connects flue gas source, controls the second three-way solenoid valve short circuit sample by sampling Integrated power control module Product absorption bottle persistently takes gas 15 minutes, controls the second three-way solenoid valve again by sampling Integrated power control module and connects sample Product absorption bottle, samples according to demand.
The smoke absorption cleaning module arranges AB two-way, and wherein the road A samples, and the road B connects new sample absorption bottle, when the road A Sampling terminates to switch to the road B by sampling Integrated power control module.
Further, temperature sensor 17, suspended body flowmeter 16, pressure sensor 18 monitor smoke behavior.
Further, by sampling Integrated power control when the first drying bottle 7 and 11 desiccant of the second drying bottle absorb saturation Module short circuit processed, with renewing drying bottle.
Further, filter 15 prevents desiccant dust from entering vacuum pump;
Further, acid solution purification bottle 5 is added reindeer moss and monitors acid solution acidity.
The present invention is convenient and efficient, persistently extracts fresh smoke, and ammonia loss amount reduces deviation caused by sampling manually, improves DATA REASONING precision.
Above-described specific embodiment has carried out further the purpose of the present invention, technical scheme and beneficial effects It is described in detail, it should be understood that being not intended to limit the present invention the foregoing is merely a specific embodiment of the invention Protection scope, all within the spirits and principles of the present invention, any modification, equivalent substitution, improvement and etc. done should all include Within protection scope of the present invention.

Claims (9)

1. a kind of mobile semi-automatic sampling car of chemical method the escaping of ammonia, which is characterized in that the chemical method the escaping of ammonia mobile half Automatic sampling vehicle includes: the sampling Integrated power control module of smoke absorption cleaning module and connection smoke absorption cleaning module;
The smoke absorption cleaning module includes smoke inlet, exhanst gas outlet, the total three-way solenoid valve of the smoke outlet setting One, two lines in parallel road, every route include: between smoke inlet and exhanst gas outlet
First three-way solenoid valve;
Sample absorption bottle, the sample absorption bottle are connect by pipeline with the first three-way solenoid valve;
Second three-way solenoid valve, second three-way solenoid valve are connect by pipeline with sample absorption bottle;
Anti-suck bottle, the anti-suck bottle are connect by pipeline with the second three-way solenoid valve;
Acid solution purification bottle, the acid solution purification bottle are connect by pipeline with anti-suck bottle;
Third three-way solenoid valve, the third three-way solenoid valve are connect by pipeline with acid solution purification bottle;
Drying bottle, the drying bottle include the first drying bottle, and the second drying bottle, third drying bottle, first drying bottle passes through Pipeline is connect with third three-way solenoid valve;
4th three-way solenoid valve, the 4th three-way solenoid valve are connect by pipeline with the first drying bottle;
Acid solution purification bottle, the acid solution purification bottle are connect by pipeline with the 4th three-way solenoid valve;
5th three-way solenoid valve, the 5th three-way solenoid valve are connect by pipeline with acid solution purification bottle;
Second drying bottle, second drying bottle are connect by pipeline with the 5th three-way solenoid valve;
6th three-way solenoid valve, the 6th three-way solenoid valve are connect by pipeline with the second drying bottle;
Third drying bottle, the third drying bottle are connect by pipeline with the 6th three-way solenoid valve;
The sampling Integrated power control module includes:
Filter, the filter are connect by pipeline with total three-way solenoid valve;
Suspended body flowmeter, the suspended body flowmeter are connected to the filter by pipeline;
Temperature sensor, the temperature sensor are connect by pipeline with suspended body flowmeter;
Pressure sensor, the pressure sensor are connect by pipeline with temperature sensor;
Blast volume controller, the blast volume controller are connect by pipeline with pressure sensor;
Vacuum pump, the vacuum pump are connect by pipeline with blast volume controller;And
Signal integrated control device, the signal integrated control device by circuit respectively with temperature sensor, blast volume controller, Vacuum pump, pressure sensor, total three-way solenoid valve, the first three-way solenoid valve, the second three-way solenoid valve, third three-way solenoid valve, 4th three-way solenoid valve, the 5th three-way solenoid valve, the connection of the 6th three-way solenoid valve.
2. the mobile semi-automatic sampling car of chemical method the escaping of ammonia as described in claim 1, which is characterized in that
The mobile semi-automatic sampling car of the chemical method the escaping of ammonia further include: sampling car skeleton, the sampling car skeleton includes: vehicle General frame and wheel are provided with sampling Integrated power control module and smoke absorption cleaning module in the vehicle general frame, The wheel is located under vehicle general frame.
3. the mobile semi-automatic sampling car of chemical method the escaping of ammonia as claimed in claim 2, which is characterized in that the chemical method ammonia The mobile semi-automatic sampling car of escape further include: the spare bottle of smoke absorption cleaning module, the sampling car skeleton are divided into 3 layers, on Layer arrangement samples Integrated power control module, and smoke absorption cleaning module, lower layer arrangement smoke absorption cleaning module are arranged in middle layer Spare bottle.
4. the mobile semi-automatic sampling car of chemical method the escaping of ammonia as claimed in claim 3, which is characterized in that the smoke inlet Two lines road in parallel is located at first plane in middle layer between exhanst gas outlet, and the filter and suspended body flowmeter are located at middle layer The second plane, the first plane and the second plane are vertical.
5. the mobile semi-automatic sampling car of chemical method the escaping of ammonia as described in claim 1, which is characterized in that total electromagnetism three For port valve tool there are three port, the first port and second port of total three-way solenoid valve are separately connected two lines road, third end Mouth is connected to the filter by pipeline.
6. the mobile semi-automatic sampling car of chemical method the escaping of ammonia as described in claim 1, which is characterized in that the 5th electromagnetism The third parallel line in parallel with the second drying bottle is set between triple valve and the 6th three-way solenoid valve.
7. the mobile semi-automatic sampling car of chemical method the escaping of ammonia as described in claim 1, which is characterized in that the third electromagnetism Second parallel line in parallel with the first drying bottle is set between triple valve and the 4th three-way solenoid valve.
8. the mobile semi-automatic sampling car of chemical method the escaping of ammonia as described in claim 1, which is characterized in that first electromagnetism First parallel line in parallel with sample absorption bottle is set between triple valve and the second three-way solenoid valve.
9. the mobile semi-automatic sampling car of chemical method the escaping of ammonia as claimed in claim 2, which is characterized in that the signal is integrated Control device includes the display screen being arranged on sampling car skeleton.
CN201910113525.9A 2019-02-14 2019-02-14 Movable semi-automatic sampling vehicle for ammonia escape by chemical method Active CN109813581B (en)

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Publication number Priority date Publication date Assignee Title
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CN210037349U (en) * 2019-02-14 2020-02-07 北京源深节能技术有限责任公司 Chemical method ammonia escape sampling vehicle

Patent Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1878604A (en) * 2003-09-02 2006-12-13 安格斯公司 Reactive gas filter
US20050183490A1 (en) * 2003-12-03 2005-08-25 Anatoly Grayfer Systems and methods for detecting contaminants
US20090193884A1 (en) * 2008-02-01 2009-08-06 Pearl Field Services, Llc Mobile vacuum sampling system
US20160030886A1 (en) * 2013-03-29 2016-02-04 Plastic Omnium Advanced Innovation And Research A tank for selective catalytic reduction purification of the exhaust gases of a combustion engine of a vehicle
CN103541794A (en) * 2013-10-30 2014-01-29 中国第一汽车股份有限公司 Circulation ammonia filling method for solid ammonia storing system
CN104931303A (en) * 2015-03-27 2015-09-23 北京京能电力股份有限公司石景山热电厂 Sampling device and sampling method for detecting ammonia escaping concentration of smoke denitration
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