CN109793111A - A kind of preparation method of the threonine chelated ferrous iron of feed - Google Patents

A kind of preparation method of the threonine chelated ferrous iron of feed Download PDF

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Publication number
CN109793111A
CN109793111A CN201711147917.4A CN201711147917A CN109793111A CN 109793111 A CN109793111 A CN 109793111A CN 201711147917 A CN201711147917 A CN 201711147917A CN 109793111 A CN109793111 A CN 109793111A
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China
Prior art keywords
threonine
iron
ferrous iron
feed
ferrous
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CN201711147917.4A
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Chinese (zh)
Inventor
孙继安
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Xinyi Yixin Biotechnology Co Ltd
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Xinyi Yixin Biotechnology Co Ltd
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Priority to CN201711147917.4A priority Critical patent/CN109793111A/en
Publication of CN109793111A publication Critical patent/CN109793111A/en
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Abstract

The invention discloses a kind of feed preparation method of threonine chelated ferrous iron, this method belongs to feed additive field, and producing the raw material that the product uses includes: threonine, ferrous sulfate, 10% sodium hydrate aqueous solution;Product is made by techniques such as the chelatropic reaction of the production of aqueous solution, threonine and ferrous sulfate, separation drying, technological advantage is: the threonine chelated ferrous iron of industrialized production, simple process, manufacturing cost is low, it is easy to operate without increasing important equipment, it is easy to spread;Threonine chelated ferrous iron sufficiently plays the effect of growth of animal, iron is one of indispensable microelement in animal feed, during executing oxygen carrier and storage oxygen, iron plays highly important role, ferro element is with hematopoiesis function, the synthesis of hemalbumin, cytochromes and various enzymes is participated in, iron also starts shipment oxygen therapy and the effect of nutriment in blood and the absorptivity of threonine chelated rear animal greatly increases.

Description

A kind of preparation method of the threonine chelated ferrous iron of feed
Technical field
The invention belongs to feed additive fields, and in particular to a kind of preparation method of the threonine chelated ferrous iron of feed.
Background technique
Microelement is one of essential nutrient during growth of animal, and initial microelement is with inorganic salts Form is introduced directly into feed, such as ferrous sulfate, although inorganic salts are water-soluble very well, in animal alimentary canal easily with feeding Common phytate anion, oxalate anion form corresponding solubility very little by the intracorporal biochemical reaction form of animal in material Salt, be not easy by intestinal absorption.With the development of feed industry, trace mineral supplement amino-acid trace element chelate etc. is gradually It is developed, its feature is stable, efficient, small toxicity, and the absorption easy to digest in enteron aisle is conducive to growth of animal, energy Prevent and treat trace element deficiency, improve the immunity of organisms of animal, and in feed nutrition composition using beneficial, it is also simultaneous There is high-protein agent.The present invention is the chelate of threonine and ferrous sulfate, and threonine is the second or of livestock and poultry Three limiting amino acids have promotion growth, improve immunity function, lack threonine, and can lead to animal feed intake reduces, grows It is obstructed, the symptoms such as efficiency of feed utilization decline, immunity function inhibit, and threonine is that animal itself cannot synthesize, but extremely need The amino acid wanted can only be entered in animal body by feed, and addition threonine also can reduce tryptophan or methionine excessively causes Growth inhibition.Trace elements iron be to the life of animal it is extremely important, iron is present among hemoglobin and myoglobins, During they execute oxygen carrier and storage oxygen, iron plays highly important role, and ferro element is participated in hematopoiesis function The synthesis of hemalbumin, cytochromes and various enzymes promotes growth;Iron also starts shipment oxygen therapy and the effect of nutriment in blood; Iron is that the absorptivity of one of indispensable microelement and threonine chelated rear animal greatly increases in animal feed.
Summary of the invention
Present invention mainly solves the problem of be to provide a kind of with threonine and ferrous chelate, produce what the product used Raw material includes: threonine, ferrous sulfate, 10% sodium hydrate aqueous solution.
The present invention can be achieved through the following technical solutions:
A kind of preparation method of the threonine chelated ferrous iron of feed, it is characterized in that being made of following steps:
(1) threonine: ferrous sulfate: the ratio of water 19-21:11:68-70 in molar ratio is sent into chemical reaction kettle, keeps normal Temperature starts blender, monitors pH value at any time, is 7.0-7.2, reaction time 0.8-1.0 with 10% sodium hydrate aqueous solution tune pH value Hour.
(2) reactant is sent into centrifugal separator separation, removing the solid obtained after moisture removal is threonine chelated ferrous iron, will Threonine chelated ferrous be sent into after drying machine sealing is dried 1.0-1.2 hours obtains finished product.
Threonine purity described in above-mentioned steps (1) is 90%.
Ferrous sulfate purity described in above-mentioned steps (1) is 70%.
The drying temperature of drying machine described in above-mentioned steps (2) is 50 DEG C -60 DEG C.
The beneficial effects of the present invention are:
(1) the threonine chelated ferrous iron of industrialized production, simple process, manufacturing cost is low, without increasing important equipment, operation side Just, easy to spread;
(2) the feed palatability of product configuration is good, and absorptivity is high, easily transports, the threonine chelated ferrous effect to growth of animal Sufficiently being played, iron is one of indispensable microelement in animal feed, during executing oxygen carrier and storage oxygen, iron Highly important role is played, ferro element participates in the synthesis of hemalbumin, cytochromes and various enzymes with hematopoiesis function, Iron also starts shipment oxygen therapy and the effect of nutriment in blood and the absorptivity of threonine chelated rear animal greatly increases.
Specific embodiment
Below with reference to specific embodiment, the present invention is described in further detail.
Embodiment 1
Threonine: ferrous sulfate: water in molar ratio 19:11:70 ratio be sent into chemical reaction kettle, the temperature remains within the normal range, starts and stirs Mix device, monitor pH value at any time, with 10% sodium hydrate aqueous solution tune pH value be 7.0, the reaction time 0.8 hour;Reactant is sent into Centrifugal separator separation, removing the solid obtained after moisture removal is threonine chelated ferrous iron, by threonine chelated ferrous feeding drying Secret envelope obtains finished product after drying 1.0 hours.
Embodiment 2
Threonine: ferrous sulfate: water in molar ratio 20:11:69 ratio be sent into chemical reaction kettle, the temperature remains within the normal range, starts and stirs Mix device, monitor pH value at any time, with 10% sodium hydrate aqueous solution tune pH value be 7.1, the reaction time 0.9 hour;Reactant is sent into Centrifugal separator separation, removing the solid obtained after moisture removal is threonine chelated ferrous iron, by threonine chelated ferrous feeding drying Secret envelope obtains finished product after drying 1.1 hours.
Embodiment 3
Threonine: ferrous sulfate: water in molar ratio 21:11:70 ratio be sent into chemical reaction kettle, the temperature remains within the normal range, starts Blender monitors pH value at any time, with 10% sodium hydrate aqueous solution tune pH value be 7.2, the reaction time 1.0 hours;Reactant is sent Enter centrifugal separator separation, removing the solid obtained after moisture removal is threonine chelated ferrous iron, and threonine chelated ferrous be sent into is done Dry secret envelope obtains finished product after drying 1.2 hours.

Claims (4)

1. a kind of feed preparation method of threonine chelated ferrous iron, producing the raw material that the product uses includes: threonine, sulfuric acid Ferrous, 10% sodium hydrate aqueous solution;Its feature the following steps are included:
(1) threonine: ferrous sulfate: the ratio of water 19-21:11:68-70 in molar ratio is sent into chemical reaction kettle, keeps normal Temperature starts blender, monitors pH value at any time, is 7.0-7.2, reaction time 0.8-1.0 with 10% sodium hydrate aqueous solution tune pH value Hour;
(2) reactant is sent into centrifugal separator separation, removing the solid obtained after moisture removal is threonine chelated ferrous iron, by ammonia of reviving Acid chelating ferrous feeding drying machine sealing obtains finished product after drying 1.0-1.2 hours.
2. a kind of feed according to claim 1 preparation method of threonine chelated ferrous iron, it is characterized in that: the Soviet Union Propylhomoserin purity is 90%.
3. a kind of feed according to claim 1 preparation method of threonine chelated ferrous iron, it is characterized in that: the sulphur Sour ferrous iron purity is 70%.
4. a kind of feed according to claim 1 preparation method of threonine chelated ferrous iron, it is characterized in that: described is dry The drying temperature of dry machine is 50 DEG C -60 DEG C.
CN201711147917.4A 2017-11-17 2017-11-17 A kind of preparation method of the threonine chelated ferrous iron of feed Withdrawn CN109793111A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201711147917.4A CN109793111A (en) 2017-11-17 2017-11-17 A kind of preparation method of the threonine chelated ferrous iron of feed

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201711147917.4A CN109793111A (en) 2017-11-17 2017-11-17 A kind of preparation method of the threonine chelated ferrous iron of feed

Publications (1)

Publication Number Publication Date
CN109793111A true CN109793111A (en) 2019-05-24

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CN201711147917.4A Withdrawn CN109793111A (en) 2017-11-17 2017-11-17 A kind of preparation method of the threonine chelated ferrous iron of feed

Country Status (1)

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CN (1) CN109793111A (en)

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Application publication date: 20190524