CN109778332A - A kind of preparation method of mascara regenerated celulose fibre - Google Patents
A kind of preparation method of mascara regenerated celulose fibre Download PDFInfo
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- CN109778332A CN109778332A CN201910004916.7A CN201910004916A CN109778332A CN 109778332 A CN109778332 A CN 109778332A CN 201910004916 A CN201910004916 A CN 201910004916A CN 109778332 A CN109778332 A CN 109778332A
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Abstract
A kind of preparation method of mascara regenerated celulose fibre, the preparation method comprises the following steps: preparation washing tow；Tow cutting；Fiber drying；Fiber screening；Pack: it packs the staple fiber that screening finishes to obtain finished product, packaging bag is Double-layer packaging bag, and first layer is nylon braided bag, and the second layer is plastic film bag.The present invention provides a kind of staple fiber for stretching no curling, fibrous raw material is wood pulp cellulose, and good water absorption is good with agreeing with property of mascara, and skin-friendly is good, is not stimulated skin, makeup removing abandon after can natural degradation, it is free from environmental pollution.Mascara fiber anti-corrosive properties prepared by the present invention are good, can store for a long time under hygrometric state, up to 18 months.Good dispersion under mascara fiber hygrometric state prepared by the present invention, adhesion, not obvolvent.
Description
Technical field
The invention belongs to cosmetic field more particularly to a kind of preparation methods of mascara regenerated celulose fibre.
Background technique
Mascara is the cosmetics for being applied to eyelashes, it is therefore intended that keeps eyelashes dense, fibre is long, and volume is stuck up, and deepens eyelashes
Color.Mascara be applied alone that eyelashes can be allowed to become fine length, but tends not to become dense, or have the mascara of dense effect,
Fine long effect is again not satisfactory.For the demand for cooperating the Ms that likes to be beautiful, mascara fiber comes into being, and mascara fiber is called lengthening
Fiber, grafting fiber, are popular eye make-up products in recent years.Mascara fiber can allow eyelashes to become dense, then eyelash
Hair cream is attached on fiber, and eyelashes is made to become not only fine long but also dense.
Mascara fiber is generally there are two types of usage: cream when production with (being added in mascara Material, fiber and eyelashes when use
Cream paints eyelashes together), be applied alone (when production after oil spout directly it is filling, use when directly paint eyelashes).
Mascara is divided into natural fiber and artificial fiber with fiber, and artificial fiber is mainly nylon material, and natural fiber has
Cotton fiber, bamboo fibre, tea fiber.Natural fiber agrees with advocates natural prevailing custom now, advantage be exactly it is natural, be easy to win and disappear
The good psychological hint of the person of expense, the disadvantage is that effect is straight not as good as artificial fiber, relatively easy curling, winding.Nylon fiber hygroscopicity
Difference, regain is low, poor with agreeing with property of mascara.And regenerated celulose fibre is a kind of novel mascara fiber, though belong to
Artificial fiber scope, fiber also straight no curling, but performance, close to natural cotton fiber, skin-friendly is good, can drop naturally after discarding
Solution.Regenerated celulose fibre is applied to the research of mascara fiber at present and is had not been reported.
Summary of the invention
The purpose of the present invention is to provide a kind of preparation method of mascara regenerated celulose fibre, fiber is straight no volume
Song, fineness is uniform, and skin-friendly is good, good dispersion, after discarding can natural degradation, and have preferable anti-corrosion effect.
To achieve the above object, the invention provides the following technical scheme: a kind of system of mascara regenerated celulose fibre
Preparation Method:
(1) preparation washing tow: wood pulp cellulose pulp is passed through into dipping, squeezing, crushing, sulfonation, dissolution, filtering, is taken off
After bubble, maturation, spinning, drawing-off, tow is made, uses concentration to carry out desulfurization to tow for the sodium sulfite of 20g-35g/L, then
Tow is washed using 50-70 DEG C of hot water, all to remove sodium sulfite, then tow will carry out oiling treatment, adopt
The finish for being 10-20g/L with concentration carries out oiling treatment to tow and uses concentration for 1-3g/L's during oiling treatment
Strong oxidizer is to tow row preservative treatment.
(2) tow is cut off: tow is cut to the staple fiber of 1-5mm long using the reciprocating cutting machine of chopper；
(3) fiber is dried, and is dried using electric oven chamber typed drying-machine to fiber；
(4) fiber screens: since tow is not to be completely in straight configuration, inevitably having in cutting super
The fiber for crossing specific length exists, and needs to carry out fiber the tow that screening meets specific length, uses sieve mesh number for 5-10
Purpose screening machine is screened, and screening number is 3 times, and sieve material is 304 stainless steels；
(5) it packs: packing the staple fiber that screening finishes to obtain finished product, packaging bag is Double-layer packaging bag, and first layer is Buddhist nun
Imperial woven bag, the second layer are plastic film bag.
Further, raw material of the finish comprising following mass percent in the step (1): sodium alkyl sulfonate 45%,
Smear the mixture of fragrant sulfated oil 45%, ethyl alcohol 10%.
Further, the strong oxidizer in the step (1) is hydrogen peroxide, active constituent content 25%.
Compared with prior art, beneficial effects of the present invention are as follows:
(1) the present invention provides a kind of staple fiber for stretching no curling, fibrous raw material is wood pulp cellulose, good water absorption,
Good with agreeing with property of mascara, skin-friendly is good, does not stimulate skin, makeup removing abandon after can natural degradation, it is free from environmental pollution.
(2) mascara fiber anti-corrosive properties prepared by the present invention are good, can store for a long time under hygrometric state, up to 18 months.
(3) good dispersion under mascara fiber hygrometric state prepared by the present invention, adhesion, not obvolvent.
Specific embodiment
Technical solution of the present invention is clearly and completely described below in conjunction in the embodiment of the present invention, it is clear that institute
The embodiment of description is only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention,
Every other embodiment obtained by those of ordinary skill in the art without making creative efforts, belongs to this hair
The range of bright protection.
Embodiment 1
A kind of preparation method of mascara regenerated celulose fibre, includes the following steps:
(1) wood pulp cellulose pulp is passed through dipping, squeezing, crushing, sulfonation, dissolution, filtering, taken off by preparation washing tow
After bubble, maturation, spinning, drawing-off, without cutting machine enter washing silk processing system, tow by desulfurization, wash, oil after
To washing tow, desulfurization uses sodium sulfite, concentration 20g/L；50 DEG C of hot water are washed, all to remove sodium sulfite；On
Oily process oil concentration 10g/L, temperature 50 C；Strong oxidizer concentration is 1g/L, temperature 50 C；
(2) tow is cut off: tow is cut to the staple fiber of 1.5mm long using the reciprocating cutting machine of chopper；
(3) fiber is dried: being dried, can not be dried, only air draft to fiber using electric oven chamber typed drying-machine, prevented short
It splashes after fiber drying and causes fire；
(4) fiber screens: the mesh number of screening machine sieve is 10 mesh, and screening number is 3 times, and sieve material is 304 stainless steels；
(5) pack: packaging bag is Double-layer packaging bag, and first layer is nylon braided bag, and the second layer is plastic film bag.
The dry and cracked intensity of mascara manufactured in the present embodiment regenerated celulose fibre is 2.5cN/dtex, wet breaking strength
For 1.32cN/dtex, dry elongation at break is 18%, line density 2.22dtex.
Embodiment 2
A kind of preparation method of mascara regenerated celulose fibre includes the following steps: preparation washing tow:
(1) wood pulp cellulose pulp passes through dipping, squeezing, crushing, sulfonation, dissolution, filtering, deaeration, maturation, spinning, leads
After stretching, without cutting machine enter washing silk processing system, tow by desulfurization, wash, oil after obtain washing tow, desulfurization
With sodium sulfite, concentration 25g/L；60 DEG C of hot water are washed, all to remove sodium sulfite；The process that oils oil concentration 15g/
L, temperature 50 C；Strong oxidizer concentration is 2g/L, temperature 50 C.
(2) tow is cut off: tow is cut to the staple fiber of 2mm long using the reciprocating cutting machine of chopper.
(3) fiber is dried: being dried, can not be dried, only air draft to fiber using electric oven chamber typed drying-machine, prevented short
It splashes after fiber drying and causes fire.
(4) fiber screens: the mesh number of screening machine sieve is 9 mesh, and screening number is 3 times, and sieve material is 304 stainless steels.
(5) pack: packaging bag is Double-layer packaging bag, and first layer is nylon braided bag, and the second layer is plastic film bag.
The dry and cracked intensity of mascara manufactured in the present embodiment regenerated celulose fibre is 2.4cN/dtex, wet breaking strength
For 1.25cN/dtex, dry elongation at break is 19%, line density 2.22dtex.
Embodiment 3
A kind of preparation method of mascara regenerated celulose fibre, includes the following steps:
(1) preparation washing tow: wood pulp cellulose pulp by dipping, squeezing, crushing, sulfonation, dissolution, filtering, deaeration,
After maturation, spinning, drawing-off, without cutting machine enter washing silk processing system, tow by desulfurization, wash, oil after obtain
Wash tow.Desulfurization sodium sulfite, concentration 30g/L；70 DEG C of hot water are washed, all to remove sodium sulfite；Oil work
Sequence oil concentration 20g/L, temperature 70 C；Strong oxidizer concentration is 3g/L, temperature 50 C.
(2) tow is cut off: tow is cut to the staple fiber of 3mm long using the reciprocating cutting machine of chopper.
(3) fiber is dried: being dried, can not be dried, only air draft to fiber using electric oven chamber typed drying-machine, prevented short
It splashes after fiber drying and causes fire.
(4) fiber screens: the mesh number of screening machine sieve is 6 mesh, and screening number is 3 times, and sieve material is 304 stainless steels.
(5) pack: packaging bag is Double-layer packaging bag, and first layer is nylon braided bag, and the second layer is plastic film bag.
The dry and cracked intensity of mascara manufactured in the present embodiment regenerated celulose fibre is 2.3cN/dtex, wet breaking strength
For 1.22cN/dtex, dry elongation at break is 19%, line density 2.22dtex.
Comparative example 1
The preparation method of the mascara regenerated celulose fibre of this comparative example is same as Example 2, difference, washing
Strong oxdiative processing and oiling treatment are not carried out during tow preparing is standby.
Under aqueous 55% hygrometric state, the dry of the mascara regenerated celulose fibre of 3 months this comparative examples preparation is placed
Resistance to spalling is 1.6cN/dtex, wet breaking strength 0.8cN/dtex, and dry elongation at break is 19%, line density 2.22dtex,
The decline of fiber index, local growth black mildew have simultaneously silk in water, are not at the state of dispersion.
It is had to pass through by mascara known to analyzing above with regenerated celulose fibre and is oiled and Strong oxdiative processing, it is not so fine
Dimension can not be stored for a long time under hygrometric state.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
A variety of variations, modification, replacement can be carried out to these embodiments without departing from the principles and spirit of the present invention by understanding
And modification, the scope of the present invention is defined by the appended.
Claims (3)
1. a kind of preparation method of mascara regenerated celulose fibre, it is characterised in that: specific the preparation method comprises the following steps: prepared by (1)
Washing tow: wood pulp cellulose pulp is passed through into dipping, squeezing, crushing, sulfonation, dissolution, filtering, deaeration, maturation, spinning, is led
After stretching, tow is made, concentration is used to carry out desulfurization to tow for the sodium sulfite of 20g-35g/L, then uses 50-70 DEG C of heat
Water washes tow, and all to remove sodium sulfite, then tow will carry out oiling treatment, use concentration for 10-20g/L
Finish, to tow carry out oiling treatment, during oiling treatment, using concentration is the strong oxidizer of 1-3g/L to tow row
Preservative treatment；
(2) tow is cut off: tow is cut to the staple fiber of 1-5mm long using the reciprocating cutting machine of chopper；
(3) fiber is dried, and is dried using electric oven chamber typed drying-machine to fiber；
(4) fiber screens: since tow is not to be completely in straight configuration, inevitably having more than rule in cutting
The fiber of measured length exists, and needs to carry out fiber the tow that screening meets specific length, uses sieve mesh number for 5-10 purpose
Screening machine is screened, and screening number is 3 times, and sieve material is 304 stainless steels；
(5) it packs: the staple fiber that screening finishes being packed to obtain finished product, packaging bag is Double-layer packaging bag, and first layer is nylon volume
Bag is knitted, the second layer is plastic film bag.
2. a kind of preparation method of mascara regenerated celulose fibre according to claim 1, it is characterised in that: described
The step of (1) in finish include following mass percent raw material: sodium alkyl sulfonate 45% smears fragrant sulfated oil 45%, ethyl alcohol
10% mixture.
3. a kind of preparation method of mascara regenerated celulose fibre according to claim 1, it is characterised in that: described
The step of (1) in strong oxidizer be hydrogen peroxide, active constituent content 25%.
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| CN201910004916.7A CN109778332A (en) | 2019-01-03 | 2019-01-03 | A kind of preparation method of mascara regenerated celulose fibre |
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| CN201910004916.7A CN109778332A (en) | 2019-01-03 | 2019-01-03 | A kind of preparation method of mascara regenerated celulose fibre |
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Citations (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1696359A (en) * | 2005-05-09 | 2005-11-16 | 马立峰 | Method for preparing viscose stable fiber of bamboo and hemp fiber |
| CN101024907A (en) * | 2007-03-23 | 2007-08-29 | 山东海龙股份有限公司 | High-wetness modulus adhesive colloid fiber and preparing method |
| CN102787380A (en) * | 2012-08-08 | 2012-11-21 | 张家港市天一纺织有限公司 | Method for preparing straw regenerated cellulose fiber |
| CN103215679A (en) * | 2013-04-08 | 2013-07-24 | 宜宾海丝特纤维有限责任公司 | Production technology of viscose flat monofilament |
| CN103233289A (en) * | 2013-04-08 | 2013-08-07 | 宜宾海丝特纤维有限责任公司 | Viscose monofilament production process |
| CN104831387A (en) * | 2015-05-27 | 2015-08-12 | 宜宾丝丽雅集团有限公司 | Delustering high-strength low-elongation viscose fiber preparation technology |
| CN104862802A (en) * | 2015-05-27 | 2015-08-26 | 宜宾丝丽雅集团有限公司 | Process method for preparing high-tenacity and low-elongation viscose |
| CN104894670A (en) * | 2015-05-27 | 2015-09-09 | 宜宾丝丽雅集团有限公司 | High-strength viscose fibers and preparation method and application of high-strength viscose fibers |
| CN104911726A (en) * | 2015-05-27 | 2015-09-16 | 宜宾丝丽雅集团有限公司 | Flatting ultra-fine type high-strength and low-stretching viscose fibers and preparation method thereof |
| CN106435799A (en) * | 2016-08-29 | 2017-02-22 | 山东银鹰化纤有限公司 | Preparing method of high-strength regenerated cellulose fiber |
| CN106521672A (en) * | 2016-08-29 | 2017-03-22 | 山东银鹰化纤有限公司 | Preparation method of ultra-short flat fiber |
| WO2018078094A1 (en) * | 2016-10-27 | 2018-05-03 | Kelheim Fibres Gmbh | Man-made cellulosic fibre and nonwoven product or fabric comprising the cellulosic fibre |
| CN107988643A (en) * | 2016-10-26 | 2018-05-04 | 佛山源诚顺生态纺织科技有限公司 | A kind of preparation method that true qualities bamboo cellulose fibre is prepared using true qualities bamboo made fiber pulp |
-
2019
- 2019-01-03 CN CN201910004916.7A patent/CN109778332A/en active Pending
Patent Citations (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1696359A (en) * | 2005-05-09 | 2005-11-16 | 马立峰 | Method for preparing viscose stable fiber of bamboo and hemp fiber |
| CN101024907A (en) * | 2007-03-23 | 2007-08-29 | 山东海龙股份有限公司 | High-wetness modulus adhesive colloid fiber and preparing method |
| CN102787380A (en) * | 2012-08-08 | 2012-11-21 | 张家港市天一纺织有限公司 | Method for preparing straw regenerated cellulose fiber |
| CN103215679A (en) * | 2013-04-08 | 2013-07-24 | 宜宾海丝特纤维有限责任公司 | Production technology of viscose flat monofilament |
| CN103233289A (en) * | 2013-04-08 | 2013-08-07 | 宜宾海丝特纤维有限责任公司 | Viscose monofilament production process |
| CN104862802A (en) * | 2015-05-27 | 2015-08-26 | 宜宾丝丽雅集团有限公司 | Process method for preparing high-tenacity and low-elongation viscose |
| CN104831387A (en) * | 2015-05-27 | 2015-08-12 | 宜宾丝丽雅集团有限公司 | Delustering high-strength low-elongation viscose fiber preparation technology |
| CN104894670A (en) * | 2015-05-27 | 2015-09-09 | 宜宾丝丽雅集团有限公司 | High-strength viscose fibers and preparation method and application of high-strength viscose fibers |
| CN104911726A (en) * | 2015-05-27 | 2015-09-16 | 宜宾丝丽雅集团有限公司 | Flatting ultra-fine type high-strength and low-stretching viscose fibers and preparation method thereof |
| CN106435799A (en) * | 2016-08-29 | 2017-02-22 | 山东银鹰化纤有限公司 | Preparing method of high-strength regenerated cellulose fiber |
| CN106521672A (en) * | 2016-08-29 | 2017-03-22 | 山东银鹰化纤有限公司 | Preparation method of ultra-short flat fiber |
| CN107988643A (en) * | 2016-10-26 | 2018-05-04 | 佛山源诚顺生态纺织科技有限公司 | A kind of preparation method that true qualities bamboo cellulose fibre is prepared using true qualities bamboo made fiber pulp |
| WO2018078094A1 (en) * | 2016-10-27 | 2018-05-03 | Kelheim Fibres Gmbh | Man-made cellulosic fibre and nonwoven product or fabric comprising the cellulosic fibre |
Non-Patent Citations (1)
| Title |
|---|
| 张庸: "《粘胶短纤维生产》", 31 October 1984, 纺织工业出版社 * |
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