CN109772478A - A kind of equipment reducing the loss of mixed bed regenerating resin - Google Patents

A kind of equipment reducing the loss of mixed bed regenerating resin Download PDF

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Publication number
CN109772478A
CN109772478A CN201910120474.2A CN201910120474A CN109772478A CN 109772478 A CN109772478 A CN 109772478A CN 201910120474 A CN201910120474 A CN 201910120474A CN 109772478 A CN109772478 A CN 109772478A
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CN
China
Prior art keywords
mixed bed
resin
strainer
loss
equipment
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201910120474.2A
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Chinese (zh)
Inventor
李峰
王汉生
徐延培
张伟
张新士
陈浩
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
HENAN YONGYIN CHEMICAL ENGINEERING INDUSTRIAL Co Ltd
Original Assignee
HENAN YONGYIN CHEMICAL ENGINEERING INDUSTRIAL Co Ltd
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Publication date
Application filed by HENAN YONGYIN CHEMICAL ENGINEERING INDUSTRIAL Co Ltd filed Critical HENAN YONGYIN CHEMICAL ENGINEERING INDUSTRIAL Co Ltd
Priority to CN201910120474.2A priority Critical patent/CN109772478A/en
Publication of CN109772478A publication Critical patent/CN109772478A/en
Pending legal-status Critical Current

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Abstract

The invention discloses the equipment that one kind can reduce the loss of mixed bed regenerating resin, including mixed bed, view cup is installed on the middle discharge pipe of mixed bed, parallel laid is equipped with strainer on the small flange lower end surface of view cup lower part.By adding view cup on middle discharge pipe, and strainer is arranged on the small flange lower end surface of view cup lower part, and the aperture of strainer is not more than the diameter of resin particle, operator is in regenerative process, can observe directly discharge acid-base waste fluid when whether there is or not resin presence, to find whether strainer is broken in time, reduces resin and be lost.

Description

A kind of equipment reducing the loss of mixed bed regenerating resin
Technical field
The present invention relates to mixed bed equipment technical field, more particularly to one kind can reduce the loss of mixed bed regenerating resin Equipment.
Background technique
Mixed bed is the abbreviation of hybrid ionic exchange column, is for equipment designed by ion exchange technique.So-called mixed bed, just It is that a certain proportion of cationic, anionic exchange resin is mixed loaded in same switch, the ion in fluid is handed over It changes, remove.As shown in Figure 1, mixed bed generally comprises water inlet, inlet valve, upper valve, exhaust valve, upper water distributing plate, alkali-feeding valve, tree Rouge loading port, middle valve, middle row mouth, acid inlet valve, resin discharge outlet, lower water distributing plate, just washing drain valve, discharge outlet, water outlet and Outlet valve etc..Domestic mixed bed treatment process main feature is embodied in resin separation regeneration technology, when mixed bed produces water through examining not When qualified, regeneration treatment must be carried out to it, regeneration method is Synchronos method regeneration.
Mixed bed regeneration step is usual are as follows: 1) prepares before regeneration: checking that failure each valve of mixed bed is fastened;Regenerate water tank Gao Shui Position, mixed bed acid, alkali batch meter liquid level are high;Primary demineralixation system normal operation, compressed air is sufficient, and prepares to use with long contact of value Gas;The normal operation inputs such as pressure gauge, flowmeter, thermometer;2) it is layered: opening backwash inlet valve (HV5917A/B/C), upper row Valve (HV5915A/B/C), exhaust valve control 10 ms/hour of backwash flow velocity, the backwash time about 30-45 minutes, generally use resin layer Expansion rate controls backwash flow, notices that centre cannot have bulky grain resin to run out of, and at the end of backwash, slowly closing backwash is answered to intake Whether valve (HV5917A/B/C), settles resin particle gradually, clear with positive and negative resin boundary surface after sedimentation, differentiates layering effect Fruit repeats operation if once-through operation does not reach requirement to obtain satisfied layered effect;3) it regenerates: being first turned on lower valve (HV5916A/B/C), column internal water accumulation is drained at the above 100-200 ㎜ of resin level, avoid it is unnecessary dilute again, then close It closes lower valve (HV5916A/B/C), opens acid inlet valve (HV5921A/B/C), alkali-feeding valve (HV5920A/B/C), middle valve HV5918A/B/C starts regeneration pump (P4508A/B), with identical regenerant flow simultaneously in lower part into acid, top into alkali, regenerates Raffinate is discharged by middle comb, and 2-5 ms/hour of regeneration velocity, with 45 minutes by required soda acid even suction, and valve in controlling (HV5918A/B/C) opening degree remains stationary liquid level in column;4) it cleans: after regenerated liquid sucks, closing injector into acid HV5927A/B/C, alkali valve HV5930A/B/C enter mixed bed with pure water with 2-5 ms/hour of flow velocity simultaneously up and down, are arranged by middle row Out, to wash away remaining regenerated liquid in pipeline and resin, and regenerated liquid is made to be reused, cleaning reaches defined acid to drain Basicity is terminal, and general PH reaches 7-8;5) mix layer: after resin cleaning is qualified, valve (HV5915A/B/C) in opening is closed Middle valve (HV5918A/B/C), alkali-feeding valve (HV5920A/B/C) are closed, is rinsed with back-washing method, loosens resin layer, then closed It closes acid inlet valve (HV5919A/B/C), opens lower valve (HV5916A/B/C), column internal water accumulation is drained into the above 100- of resin level At 150 ㎜, resin layer is made to have sufficient activity space, then opens intake valve (HV5921A/B/C) and mixed into compressed air It closes, admission pressure 0.1-0.15Mpa, incorporation time is 3-5 minutes general, 2.5-3.0 ms/min of air inflow, abundant with resin in column It is mixed into terminal, is then shut off intake valve (HV5921A/B/C), opens simultaneously inlet valve (HV5913A/B/ with most fast speed C) and lower valve (HV5916A/B/C), valve (HV5915A/B/C) in closing, settles resin rapidly, prevents resin from settling It separates again in the process, while to prevent resin from exposing the surface, aeration effluent quality otherwise can be generated between resin;6) just It washes: closing lower valve (HV5916A/B/C), exhaust valve is closed when water is full of equipment, open lower valve (HV5916A/B/C), It is positive with water flow processed and washes flow, into operating condition is just washed, just washed flow velocity and be generally 15-30 ms/hour, after water outlet is qualified, under closing Valve (HV5916A/B/C) is opened outlet valve (HV5914A/B/C), is put into operation.
But in mixed bed pickling, alkaline cleaning procedure, comb primarily serves the effect of filtering resin, and middle comb in mixed bed Interior strainer is often broken, so that resin will flow out together with acid-base waste fluid, is not easy to be found, is caused resin stream It loses.
Therefore, the equipment that the loss of mixed bed regenerating resin can be reduced by how providing one kind is those skilled in the art's urgent need to resolve The problem of.
Summary of the invention
In view of this, being able to observe that discharge the present invention provides the equipment that one kind can reduce the loss of mixed bed regenerating resin Whether there is or not resin presence when acid-base waste fluid, and whether comb internal screen is broken in discovery in time, reduce because finding to generate not in time Resin number of dropouts.
To achieve the goals above, the present invention adopts the following technical scheme:
A kind of equipment reducing the loss of mixed bed regenerating resin, including mixed bed are equipped on the middle discharge pipe of the mixed bed Depending on cup, parallel laid is equipped with strainer on the small flange lower end surface of the view cup lower part.
Further, the nominal diameter for regarding cup is 100mm.
Further, the aperture of the strainer is not more than the diameter of resin particle.
Further, the aperture of the strainer is 0.15mm, and the diameter of the resin particle is 0.3-1.2mm.
Further, the material of the strainer is 316L stainless steel.
Further, the strainer is welded as a whole with the small flange lower end surface depending on cup lower part.
By taking above scheme, the beneficial effects of the present invention are:
It is arranged on the small flange lower end surface of view cup lower part by adding view cup on middle discharge pipe, and by strainer, and filters The aperture of net is not more than the diameter of resin particle, and operator can observe directly discharge acid-base waste fluid in regenerative process Shi Youwu resin exists, and to find whether strainer is broken in time, reduces resin and is lost.
Detailed description of the invention
In order to more clearly explain the embodiment of the invention or the technical proposal in the existing technology, to embodiment or will show below There is attached drawing needed in technical description to be briefly described, it should be apparent that, the accompanying drawings in the following description is only this The embodiment of invention for those of ordinary skill in the art without creative efforts, can also basis The attached drawing of offer obtains other attached drawings.
Fig. 1 attached drawing is the overall structure diagram of mixed bed equipment in the prior art;
Fig. 2 attached drawing is the overall structure diagram for the equipment that one kind of the present invention can reduce the loss of mixed bed regenerating resin.
In figure: 1- water inlet, 2- inlet valve, the upper valve of 3-, 4- exhaust valve, the upper water distributing plate of 5-, 6- alkali-feeding valve, 7- resin dress Entrance, valve in 8- arrange mouth in 9-, 10- acid inlet valve, 11- resin discharge outlet, and water distributing plate under 12-, 13- just washes drain valve, 14- Discharge outlet, 15- water outlet, 16- outlet valve, 17- regard cup, 18- strainer.
Specific embodiment
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete Site preparation description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts every other Embodiment shall fall within the protection scope of the present invention.
As shown in Fig. 2, the embodiment of the invention discloses the equipment that one kind can reduce the loss of mixed bed regenerating resin, including it is mixed Bed, view cup 17 is installed, parallel laid is equipped with strainer on the small flange lower end surface of view 17 lower part of cup on the middle discharge pipe of mixed bed 18.It is arranged on the small flange lower end surface of view 17 lower part of cup by adding view cup 17 on middle discharge pipe, and by strainer 18, and filters The aperture of net 18 is not more than the diameter of resin particle, and it is useless can to observe directly discharge soda acid in regenerative process by operator Whether there is or not resin presence when liquid, to find whether strainer 18 is broken in time, reduce resin and are lost.
Specifically, regarding the nominal diameter of cup 17 as 100mm.
Specifically, the aperture of strainer 18 is not more than the diameter of resin particle.
Specifically, the aperture of strainer 18 is 0.15mm, the diameter of resin particle is 0.3-1.2mm.
Specifically, the material of strainer 18 is 316L stainless steel.
Specifically, strainer 18 is welded as a whole with the small flange lower end surface depending on 17 lower part of cup.
The present invention regard the large flange of cup 17 including top, two stainless steel pipes, the small flange on top, glass tube view cup, Large flange and the small flange of lower part of lower part etc., and the large flange on top, stainless steel pipes, the small flange on top, glass tube regard It is all conventional setting that cup, the small flange of lower part, stainless steel pipes and the sequential connection of the large flange of lower part, which are integrated, is not this The emphasis of invention, details are not described herein.
Each embodiment in this specification is described in a progressive manner, the highlights of each of the examples are with other The difference of embodiment, the same or similar parts in each embodiment may refer to each other.For device disclosed in embodiment For, since it is corresponded to the methods disclosed in the examples, so being described relatively simple, related place is said referring to method part It is bright.
The foregoing description of the disclosed embodiments enables those skilled in the art to implement or use the present invention. Various modifications to these embodiments will be readily apparent to those skilled in the art, as defined herein General Principle can be realized in other embodiments without departing from the spirit or scope of the present invention.Therefore, of the invention It is not intended to be limited to the embodiments shown herein, and is to fit to and the principles and novel features disclosed herein phase one The widest scope of cause.

Claims (6)

1. the equipment that one kind can reduce the loss of mixed bed regenerating resin, including mixed bed, which is characterized in that the middle discharge pipe of the mixed bed On view cup is installed, positioned at it is described view cup lower part small flange lower end surface on parallel laid be equipped with strainer.
2. the equipment that one kind according to claim 1 can reduce the loss of mixed bed regenerating resin, which is characterized in that the view cup Nominal diameter be 100mm.
3. the equipment that one kind according to claim 1 can reduce the loss of mixed bed regenerating resin, which is characterized in that the strainer Aperture be not more than resin particle diameter.
4. the equipment that one kind according to claim 3 can reduce the loss of mixed bed regenerating resin, which is characterized in that the strainer Aperture be 0.15mm, the diameter of the resin particle is 0.3-1.2mm.
5. the equipment that one kind according to claim 4 can reduce the loss of mixed bed regenerating resin, which is characterized in that the strainer Material be 316L stainless steel.
6. the equipment that one kind according to claim 5 can reduce the loss of mixed bed regenerating resin, which is characterized in that the strainer It is welded as a whole with the small flange lower end surface depending on cup lower part.
CN201910120474.2A 2019-02-18 2019-02-18 A kind of equipment reducing the loss of mixed bed regenerating resin Pending CN109772478A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201910120474.2A CN109772478A (en) 2019-02-18 2019-02-18 A kind of equipment reducing the loss of mixed bed regenerating resin

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201910120474.2A CN109772478A (en) 2019-02-18 2019-02-18 A kind of equipment reducing the loss of mixed bed regenerating resin

Publications (1)

Publication Number Publication Date
CN109772478A true CN109772478A (en) 2019-05-21

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110790343A (en) * 2019-11-15 2020-02-14 师宗煤焦化工有限公司 Mixed bed regeneration method for water conservation and emission reduction
CN115555055A (en) * 2021-07-01 2023-01-03 中粮糖业辽宁有限公司 Resin regeneration system and resin regeneration method

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US3316171A (en) * 1962-08-25 1967-04-25 Mastrorilli Nunzio Process for regenerating cationic resins
US4472282A (en) * 1981-12-07 1984-09-18 Crane Co. Mixed bed polishing process
CN2444936Y (en) * 2000-07-21 2001-08-29 常州新区明园电子有限公司 Resin anti-run-out and anti-block-up observing control device
CN201211476Y (en) * 2008-04-25 2009-03-25 杨马云 Multifunctional high efficiency ion exchanging apparatus
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CN203079724U (en) * 2012-12-20 2013-07-24 江西迪特科技有限公司 Industrial deionized water treatment device
CN203425600U (en) * 2013-05-31 2014-02-12 山东西奥自动化系统工程有限公司 T-shaped resin trapper
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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3316171A (en) * 1962-08-25 1967-04-25 Mastrorilli Nunzio Process for regenerating cationic resins
US4472282A (en) * 1981-12-07 1984-09-18 Crane Co. Mixed bed polishing process
CN2444936Y (en) * 2000-07-21 2001-08-29 常州新区明园电子有限公司 Resin anti-run-out and anti-block-up observing control device
CN201211476Y (en) * 2008-04-25 2009-03-25 杨马云 Multifunctional high efficiency ion exchanging apparatus
CN101780422A (en) * 2010-03-05 2010-07-21 南京中电联环保股份有限公司 Four-tower mixed ion exchanger resin external separation regeneration method
CN203079724U (en) * 2012-12-20 2013-07-24 江西迪特科技有限公司 Industrial deionized water treatment device
CN203425600U (en) * 2013-05-31 2014-02-12 山东西奥自动化系统工程有限公司 T-shaped resin trapper
CN103801411A (en) * 2014-02-19 2014-05-21 内蒙古包钢钢联股份有限公司 Demineralization water system mixed bed regeneration method

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110790343A (en) * 2019-11-15 2020-02-14 师宗煤焦化工有限公司 Mixed bed regeneration method for water conservation and emission reduction
CN115555055A (en) * 2021-07-01 2023-01-03 中粮糖业辽宁有限公司 Resin regeneration system and resin regeneration method

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