CN109761640A - A kind of porous ceramics fever core material and preparation method - Google Patents
A kind of porous ceramics fever core material and preparation method Download PDFInfo
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- CN109761640A CN109761640A CN201910239570.9A CN201910239570A CN109761640A CN 109761640 A CN109761640 A CN 109761640A CN 201910239570 A CN201910239570 A CN 201910239570A CN 109761640 A CN109761640 A CN 109761640A
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- pore creating
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- creating material
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Abstract
The invention discloses a kind of porous ceramics fever core material and preparation methods, specifically it is made of major ingredient and pore creating material, the major ingredient and pore creating material are respectively major ingredient 55%-65% according to quality specific gravity, pore creating material 35%-45%, the major ingredient includes silicon-dioxide powdery, schmigel and cryogenic glass powder, is respectively silicon-dioxide powdery 30%-40%, schmigel 35%-40%, cryogenic glass powder 25%-30% according to quality specific gravity.The present invention is using silicon-dioxide powdery, schmigel, cryogenic glass powder and pore creating material mixed sintering at porous ceramics heat generating core, it is used as using the powder of sand-like and holds burning body, good fluidity, high temperature resistant itself, it is not sticky, adhesion will not be generated during the sintering process with fever core assembly, it does not need manually to put simultaneously, batch sinter in a saggar can be in high volume placed in, finished product yield is high, the pottery manufactured with porous ceramics, can be used to do atomizer, filter, sensor etc., it is widely used, it is practical.
Description
Technical field
The present invention relates to a kind of heat generating core, specifically a kind of porous ceramics fever core material and preparation method.
Background technique
Electronic cigarette is a kind of electronic product for imitating cigarette, there is appearance, smog, taste and the feeling as cigarette.
General electronic cigarette is mainly made of the smoke pipe, vaporising device and battery three parts that hold nicotine solution.There is hair in vaporising device
Hot core, is battery powered, and the liquid nicotine in smoke grenade can be transformed into fog, so that user be allowed to have one kind when inhaling
The feeling of similar smoking.It can add the fragrance of the various tastes such as chocolate, peppermint into smoke pipe according to personal preference.Electricity
Sub- cigarette is a kind of instead of cigarette or the utensil of quitting tobacco dependency.
There are many materials for the production of heat generating core in electronic cigarette, are had using the heat generating core that porous ceramic film material makes fine
Atomizing effect.But current porous ceramics yield when making heat generating core is not high, cannot high-volume one-pass molding, limitation
Its use.
Summary of the invention
The purpose of the present invention is to provide a kind of porous ceramics fever core material and preparation methods, to solve above-mentioned background skill
The problem of being proposed in art.
To achieve the above object, the invention provides the following technical scheme:
A kind of porous ceramics fever core material, is specifically made of major ingredient and pore creating material, the major ingredient and pore creating material are according to mass ratio
It is respectively again major ingredient 55%-65%, pore creating material 35%-45%, the major ingredient includes silicon-dioxide powdery, schmigel and low temperature glass
Powder is respectively silicon-dioxide powdery 30%-40%, schmigel 35%-40%, cryogenic glass powder 25%-30% according to quality specific gravity.
As a further solution of the present invention: the major ingredient and pore creating material are respectively major ingredient 60%, pore-creating according to quality specific gravity
Agent 40%.
As the present invention further scheme: the major ingredient includes silicon-dioxide powdery, schmigel and cryogenic glass powder,
It is respectively silicon-dioxide powdery 35%, schmigel 35%, cryogenic glass powder 30% according to quality specific gravity.
As further scheme of the invention: the pore creating material specifically uses organic starch, organic corn powder, has machine side
One of powder.
As further scheme of the invention: the particle of the silicon-dioxide powdery, schmigel and cryogenic glass powder is big
It is small between 70-90 mesh, silicon-dioxide powdery, schmigel and cryogenic glass powder are sand-like.
As further scheme of the invention: for the pore creating material granular size between 40-60 mesh, pore creating material is fine sand
Shape.
In addition, the porous ceramics heat generating core is by the heat generating core the present invention also provides a kind of porous ceramics heat generating core
Material is made.
As a further solution of the present invention: a kind of preparation method of porous ceramics heat generating core, the specific steps are as follows:
S1: prepare raw material
(1) it uses sander to crush respectively material each in major ingredient and pore creating material, grinding, obtains powdered granule；
(2) by strainer, to filter out granular size respectively be the major ingredient and granular size between 70-90 mesh is between 40-60 mesh again
Pore creating material particle；
(3) each material utilization amount is weighed by the mass ratio of ingredient each in major ingredient, determines pore creating material dosage further according to the dosage of major ingredient, claimed
Pore creating material is taken, it is spare；
S2: it is stirred, is granulated
(1) powder raw material ready in S1 is respectively put into blender and is stirred, agitating mode is to stir in batches；
(2) after dry powder raw material is uniformly mixed, obtained mixed material is granulated using screw pelletizer, it is mixed obtains graininess
Close material；
S3: production idiosome
Granular mixture material obtained in S2 is used into hot press compression moulding, it is cooling, idiosome is obtained, idiosome is put into saggar
Interior, using low temperature drying, temperature is maintained at 50-60 DEG C, time 68-75h；
S4: idiosome kiln is burnt
Idiosome after drying in S3 is put into fire in kiln together with saggar and obtains ceramic wafer, firing time 30-40h, temperature by
160-1430, which is gradually warmed up, heats idiosome；
S5: will on ceramic wafer obtained in S4 print or etch heating circuit, then by ceramic plate surface successively spray insulation coating,
Corrosion-resistant finishes, antioxidant coating, welding electrode, then by monolithic ceramic plate cut separate, finally with porcelain bucket assembled formation, thus
Obtain porous ceramics heat generating core finished product.
As further scheme of the invention: stirring concrete mode in batches in the S2 are as follows: silica in major ingredient
Powder, schmigel and cryogenic glass powder sequentially add in blender, first stir and evenly mix major ingredient, add pore creating material and are stirred
It mixes.
Compared with prior art, the beneficial effects of the present invention are:
The present invention using silicon-dioxide powdery, schmigel, cryogenic glass powder and pore creating material mixed sintering at porous ceramics heat generating core,
Powder using sand-like is as burning body is held, and good fluidity, high temperature resistant itself is not sticky, with fever core assembly sintered
Adhesion will not be generated in journey, while not needing manually to put, and can in high volume be placed in batch sinter in a saggar, finished product yield
Height, the pottery manufactured with porous ceramics can be used to do atomizer, filter, sensor etc., widely used, practical.
Specific embodiment
Technical solution of the present invention is described in more detail With reference to embodiment.
Embodiment 1
A kind of porous ceramic film material, is specifically made of major ingredient and pore creating material, and the major ingredient and pore creating material are distinguished according to quality specific gravity
For major ingredient 55%, pore creating material 45%, the major ingredient includes silicon-dioxide powdery, schmigel and cryogenic glass powder, according to quality specific gravity
Respectively silicon-dioxide powdery 30%, schmigel 40%, cryogenic glass powder 30%, the pore creating material specifically uses organic starch, described
The granular size of silicon-dioxide powdery, schmigel and cryogenic glass powder is 70 mesh, and pore creating material granular size is 40 mesh, titanium dioxide
Silicon powder, schmigel, cryogenic glass powder and pore creating material are sand-like.
The present invention also provides a kind of methods for preparing porous ceramics heat generating core using porous ceramic film material, and specific steps are such as
Under:
S1: prepare raw material
(1) it uses sander to crush respectively material each in major ingredient and pore creating material, grinding, obtains powdered granule；
(2) major ingredient that granular size is 70 mesh and the pore creating material particle that granular size is 40 mesh are filtered out by strainer respectively again；
(3) each material utilization amount is weighed by the mass ratio of ingredient each in major ingredient, determines pore creating material dosage further according to the dosage of major ingredient, claimed
Pore creating material is taken, it is spare；
S2: it is stirred, is granulated
(1) powder raw material ready in S1 is respectively put into blender and is stirred, agitating mode is to stir in batches；
(2) after dry powder raw material is uniformly mixed, obtained mixed material is granulated using screw pelletizer, it is mixed obtains graininess
Close material；
S3: production idiosome
Granular mixture material obtained in S2 is used into hot press compression moulding, it is cooling, idiosome is obtained, idiosome is put into saggar
Interior, using low temperature drying, temperature is maintained at 50 DEG C, time 68h；
S4: idiosome kiln is burnt
Idiosome after drying in S3 is put into fire in kiln together with saggar and obtains ceramic wafer, firing time 30h, temperature is by 160-
1430 are gradually warmed up to idiosome heating；
S5: will on ceramic wafer obtained in S4 print or etch heating circuit, then by ceramic plate surface successively spray insulation coating,
Corrosion-resistant finishes, antioxidant coating, welding electrode, then by monolithic ceramic plate cut separate, finally with porcelain bucket assembled formation, thus
Obtain porous ceramics heat generating core finished product.
Stir concrete mode in batches in the S2 are as follows: in major ingredient silicon-dioxide powdery, schmigel and cryogenic glass powder according to
In secondary addition blender, first major ingredient is stirred and evenly mixed, pore creating material is added and is stirred.
Embodiment 2
A kind of porous ceramic film material, is specifically made of major ingredient and pore creating material, and the major ingredient and pore creating material are distinguished according to quality specific gravity
For major ingredient 60%, pore creating material 40%, the major ingredient includes silicon-dioxide powdery, schmigel and cryogenic glass powder, according to quality specific gravity
Respectively silicon-dioxide powdery 35%, schmigel 35%, cryogenic glass powder 30%, the pore creating material specifically use organic corn powder, institute
The granular size for stating silicon-dioxide powdery, schmigel and cryogenic glass powder is 80 mesh, and pore creating material granular size is 50 mesh, dioxy
SiClx powder, schmigel, cryogenic glass powder and pore creating material are sand-like.
The present invention also provides a kind of methods for preparing porous ceramics heat generating core using porous ceramics fever core material, specifically
Steps are as follows:
S1: prepare raw material
(1) it uses sander to crush respectively material each in major ingredient and pore creating material, grinding, obtains powdered granule；
(2) major ingredient that granular size is 80 mesh and the pore creating material particle that granular size is 50 mesh are filtered out by strainer respectively again；
(3) each material utilization amount is weighed by the mass ratio of ingredient each in major ingredient, determines pore creating material dosage further according to the dosage of major ingredient, claimed
Pore creating material is taken, it is spare；
S2: it is stirred, is granulated
(1) powder raw material ready in S1 is respectively put into blender and is stirred, agitating mode is to stir in batches；
(2) after dry powder raw material is uniformly mixed, obtained mixed material is granulated using screw pelletizer, it is mixed obtains graininess
Close material；
S3: production idiosome
Granular mixture material obtained in S2 is used into hot press compression moulding, it is cooling, idiosome is obtained, idiosome is put into saggar
Interior, using low temperature drying, temperature is maintained at 55 DEG C, time 72h；
S4: idiosome kiln is burnt
Idiosome after drying in S3 is put into fire in kiln together with saggar and obtains ceramic wafer, firing time 36h, temperature is by 160-
1430 are gradually warmed up to idiosome heating；
S5: will on ceramic wafer obtained in S4 print or etch heating circuit, then by ceramic plate surface successively spray insulation coating,
Corrosion-resistant finishes, antioxidant coating, welding electrode, then by monolithic ceramic plate cut separate, finally with porcelain bucket assembled formation, thus
Obtain porous ceramics heat generating core finished product.
Stir concrete mode in batches in the S2 are as follows: in major ingredient silicon-dioxide powdery, schmigel and cryogenic glass powder according to
In secondary addition blender, first major ingredient is stirred and evenly mixed, pore creating material is added and is stirred.
Embodiment 3
A kind of porous ceramic film material, is specifically made of major ingredient and pore creating material, and the major ingredient and pore creating material are distinguished according to quality specific gravity
For major ingredient 65%, pore creating material 35%, the major ingredient includes silicon-dioxide powdery, schmigel and cryogenic glass powder, according to quality specific gravity
Respectively silicon-dioxide powdery 40%, schmigel 35%, cryogenic glass powder 25%, the pore creating material specifically use organic corn powder, institute
The granular size for stating silicon-dioxide powdery, schmigel and cryogenic glass powder is 90 mesh, and pore creating material granular size is 60 mesh, dioxy
SiClx powder, schmigel, cryogenic glass powder and pore creating material are sand-like.
The present invention also provides a kind of methods for preparing porous ceramics heat generating core using porous ceramics fever core material, specifically
Steps are as follows:
S1: prepare raw material
(1) it uses sander to crush respectively material each in major ingredient and pore creating material, grinding, obtains powdered granule；
(2) major ingredient that granular size is 90 mesh and the pore creating material particle that granular size is 60 mesh are filtered out by strainer respectively again；
(3) each material utilization amount is weighed by the mass ratio of ingredient each in major ingredient, determines pore creating material dosage further according to the dosage of major ingredient, claimed
Pore creating material is taken, it is spare；
S2: it is stirred, is granulated
(1) powder raw material ready in S1 is respectively put into blender and is stirred, agitating mode is to stir in batches；
(2) after dry powder raw material is uniformly mixed, obtained mixed material is granulated using screw pelletizer, it is mixed obtains graininess
Close material；
S3: production idiosome
Granular mixture material obtained in S2 is used into hot press compression moulding, it is cooling, idiosome is obtained, idiosome is put into saggar
Interior, using low temperature drying, temperature is maintained at 60 DEG C, time 75h；
S4: idiosome kiln is burnt
Idiosome after drying in S3 is put into fire in kiln together with saggar and obtains ceramic wafer, firing time 40h, temperature is by 160-
1430 are gradually warmed up to idiosome heating；
S5: will on ceramic wafer obtained in S4 print or etch heating circuit, then by ceramic plate surface successively spray insulation coating,
Corrosion-resistant finishes, antioxidant coating, welding electrode, then by monolithic ceramic plate cut separate, finally with porcelain bucket assembled formation, thus
Obtain porous ceramics heat generating core finished product.
Stir concrete mode in batches in the S2 are as follows: in major ingredient silicon-dioxide powdery, schmigel and cryogenic glass powder according to
In secondary addition blender, first major ingredient is stirred and evenly mixed, pore creating material is added and is stirred.
The present invention is sent out using silicon-dioxide powdery, schmigel, cryogenic glass powder and pore creating material mixed sintering at porous ceramics
Hot core, the powder using sand-like is as burning body is held, and good fluidity, high temperature resistant itself is not sticky, is burning with fever core assembly
Adhesion will not be generated during knot, while not needing manually to put, and can in high volume be placed in batch sinter in a saggar, finished product
Yield is high, the pottery manufactured with porous ceramics, can be used to do atomizer, filter, sensor etc., widely used, practical
Property is strong.
Better embodiment of the invention is explained in detail above, but the present invention is not limited to above-mentioned embodiment party
Formula within the knowledge of one of ordinary skill in the art can also be without departing from the purpose of the present invention
Various changes can be made.
Claims (9)
1. a kind of porous ceramic film material, which is characterized in that be specifically made of major ingredient and pore creating material, the major ingredient and pore creating material according to
Quality specific gravity is respectively major ingredient 55%-65%, and pore creating material 35%-45%, the major ingredient includes silicon-dioxide powdery, schmigel and low temperature
Glass powder is respectively silicon-dioxide powdery 30%-40%, schmigel 35%-40%, cryogenic glass powder 25%-30% according to quality specific gravity.
2. a kind of porous ceramic film material according to claim 1, which is characterized in that the major ingredient and pore creating material are according to quality
Specific gravity is respectively major ingredient 60%, pore creating material 40%.
3. a kind of porous ceramic film material according to claim 1, which is characterized in that the major ingredient includes silicon dioxide powder
Body, schmigel and cryogenic glass powder are respectively silicon-dioxide powdery 35%, schmigel 35%, cryogenic glass powder according to quality specific gravity
30%。
4. a kind of porous ceramic film material according to claim 1, which is characterized in that the pore creating material specifically uses organic shallow lake
One of powder, organic corn powder, organic flour.
5. a kind of porous ceramic film material according to claim 1, which is characterized in that the silicon-dioxide powdery, schmigel
And the granular size of cryogenic glass powder, between 70-90 mesh, silicon-dioxide powdery, schmigel and cryogenic glass powder are fine sand
Shape.
6. a kind of porous ceramic film material according to claim 1, which is characterized in that the pore creating material granular size is in 40-
Between 60 mesh, pore creating material is sand-like.
7. a kind of porous ceramics heat generating core, which is characterized in that the porous ceramics heat generating core is by any one of such as claim 1-6 institute
The fever core material stated is made.
8. a kind of preparation method of porous ceramics heat generating core, which is characterized in that specific step is as follows:
S1: prepare raw material
(1) it uses sander to crush respectively material each in major ingredient and pore creating material, grinding, obtains powdered granule；
(2) by strainer, to filter out granular size respectively be the major ingredient and granular size between 70-90 mesh is between 40-60 mesh again
Pore creating material particle；
(3) each material utilization amount is weighed by the mass ratio of ingredient each in major ingredient, determines pore creating material dosage further according to the dosage of major ingredient, claimed
Pore creating material is taken, it is spare；
S2: it is stirred, is granulated
(1) powder raw material ready in S1 is respectively put into blender and is stirred, agitating mode is to stir in batches；
(2) after dry powder raw material is uniformly mixed, obtained mixed material is granulated using screw pelletizer, it is mixed obtains graininess
Close material；
S3: production idiosome
Granular mixture material obtained in S2 is used into hot press compression moulding, it is cooling, idiosome is obtained, idiosome is put into saggar
Interior, using low temperature drying, temperature is maintained at 50-60 DEG C, time 68-75h；
S4: idiosome kiln is burnt
Idiosome after drying in S3 is put into fire in kiln together with saggar and obtains ceramic wafer, firing time 30-40h, temperature by
160-1430, which is gradually warmed up, heats idiosome；
S5: will on ceramic wafer obtained in S4 print or etch heating circuit, then by ceramic plate surface successively spray insulation coating,
Corrosion-resistant finishes, antioxidant coating, welding electrode, then by monolithic ceramic plate cut separate, finally with porcelain bucket assembled formation, thus
Obtain porous ceramics heat generating core finished product.
9. a kind of preparation method of porous ceramics heat generating core according to claim 7, which is characterized in that in the S2 in batches
Secondary stirring concrete mode are as follows: silicon-dioxide powdery, schmigel and cryogenic glass powder sequentially add in blender in major ingredient, will first lead
Material stirs and evenly mixs, and adds pore creating material and is stirred.
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| CN110105054A (en) * | 2019-05-27 | 2019-08-09 | 陈美坤 | Negative low sintering micropore oil suction/ceramic water of oxygen and its preparation method and application |
| CN110282979A (en) * | 2019-07-02 | 2019-09-27 | 湖南嘉盛电陶新材料股份有限公司 | A kind of Multi-hole ceramic heating element, preparation method and application |
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| CN110845251A (en) * | 2019-11-05 | 2020-02-28 | 深圳顺络电子股份有限公司 | Preparation method of atomization core, atomization assembly and electronic cigarette |
| CN111592332A (en) * | 2020-06-05 | 2020-08-28 | 深圳职业技术学院 | Environment-friendly heat-insulation core material and preparation method thereof |
| CN112441820A (en) * | 2019-08-27 | 2021-03-05 | 上海魅湃实业有限公司 | Porous ceramic and preparation method thereof |
| CN113102439A (en) * | 2021-03-09 | 2021-07-13 | 丁尧文 | Recycling device of ceramic heating core |
| WO2021169782A1 (en) * | 2020-02-27 | 2021-09-02 | 深圳麦克韦尔科技有限公司 | Electronic atomization device, atomization assembly, atomization element and manufacturing method therefor |
| CN113387572A (en) * | 2021-05-20 | 2021-09-14 | 深圳市基克纳科技有限公司 | Porous material containing hollow glass powder and preparation method and application thereof |
| CN116199506A (en) * | 2022-12-24 | 2023-06-02 | 深圳市吉迩科技有限公司 | Porous ceramic preparation method, porous ceramic and atomization device |
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| CN110282979A (en) * | 2019-07-02 | 2019-09-27 | 湖南嘉盛电陶新材料股份有限公司 | A kind of Multi-hole ceramic heating element, preparation method and application |
| CN110372345A (en) * | 2019-07-02 | 2019-10-25 | 湖南嘉盛电陶新材料股份有限公司 | A kind of electronic cigarette micropore ceramics atomization core and preparation method thereof |
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| CN110627519A (en) * | 2019-10-16 | 2019-12-31 | 湖南嘉盛电陶新材料股份有限公司 | Method for manufacturing porous ceramic atomizing core |
| CN110845251A (en) * | 2019-11-05 | 2020-02-28 | 深圳顺络电子股份有限公司 | Preparation method of atomization core, atomization assembly and electronic cigarette |
| CN110759717A (en) * | 2019-11-11 | 2020-02-07 | 宁波伏尔肯科技股份有限公司 | Porous corundum ceramic for heating atomizer and preparation method thereof |
| CN110759717B (en) * | 2019-11-11 | 2021-12-07 | 宁波伏尔肯科技股份有限公司 | Porous corundum ceramic for heating atomizer and preparation method thereof |
| WO2021169782A1 (en) * | 2020-02-27 | 2021-09-02 | 深圳麦克韦尔科技有限公司 | Electronic atomization device, atomization assembly, atomization element and manufacturing method therefor |
| CN111592332A (en) * | 2020-06-05 | 2020-08-28 | 深圳职业技术学院 | Environment-friendly heat-insulation core material and preparation method thereof |
| CN113102439A (en) * | 2021-03-09 | 2021-07-13 | 丁尧文 | Recycling device of ceramic heating core |
| CN113387572A (en) * | 2021-05-20 | 2021-09-14 | 深圳市基克纳科技有限公司 | Porous material containing hollow glass powder and preparation method and application thereof |
| CN116199506A (en) * | 2022-12-24 | 2023-06-02 | 深圳市吉迩科技有限公司 | Porous ceramic preparation method, porous ceramic and atomization device |
| CN116199506B (en) * | 2022-12-24 | 2024-04-05 | 深圳市吉迩科技有限公司 | Porous ceramic preparation method, porous ceramic and atomization device |
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Application publication date: 20190517 |