CN109761507A - High transflection light coated glass and preparation method thereof - Google Patents
High transflection light coated glass and preparation method thereof Download PDFInfo
- Publication number
- CN109761507A CN109761507A CN201910188840.8A CN201910188840A CN109761507A CN 109761507 A CN109761507 A CN 109761507A CN 201910188840 A CN201910188840 A CN 201910188840A CN 109761507 A CN109761507 A CN 109761507A
- Authority
- CN
- China
- Prior art keywords
- film layer
- glass
- film
- coated glass
- transflection
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Surface Treatment Of Glass (AREA)
- Surface Treatment Of Optical Elements (AREA)
- Physical Vapour Deposition (AREA)
Abstract
The invention belongs to coated glass technical fields, more particularly to high transflection light coated glass, it is sequentially deposited on a side surface of substrate of glass including substrate of glass, film layer 1, membrane system 1, film layer 1 and film 1 according to number order, film layer 1 is oxidation stainless steel bottoming film layer, and membrane system 1 is titanium oxide membrane system.The present invention also provides the preparation methods of above-mentioned high transflection light coated glass.The reflective characteristic of the high existing mirror surface of transflection light coated glass of the invention has the characteristic of high light transmission, light transmittance 66% again；Preparation method provided by the invention reduces the cost of high transflection light coated glass, and improves its production efficiency.
Description
Technical field
The invention belongs to coated glass technical fields, and in particular to high transflection light coated glass and preparation method thereof.
Background technique
Coated glass is also referred to as reflecting glass.Coated glass is in glass surface coating one or more layers metal, alloy or gold
Belong to compound film, with optical property, the electric conductivity etc. for changing glass, to meet corresponding particular requirement.High-transparency glass
Transmission of visible light, higher solar energy transmitance and far infrared emissivity with higher, so daylighting is splendid, penetrates
The sun heat radiation of glass is more, heat-proof quality is excellent, prominent natural lighting effect, and application is relatively broad.It exists in the prior art
The problem of be: normal device production high-transparency coated glass can not guarantee high light transmission characteristic simultaneously have plated film mirror surface imitate
Fruit；And high thoroughly high anti-coated glass needs particular device solely to provide this kind of glass or similar production for oneself due to its special performance
Product, this particular device can not prepare the other coated glasses of production, cause high thoroughly high anti-glass at high cost, production efficiency is low.
Summary of the invention
In view of the deficiency of the prior art, the present invention provides high transflection light coated glass, the technology solved is asked
The high-transparency coated glass of the entitled production of normal device in the prior art can not have simultaneously plated film in the characteristic for guaranteeing high light transmission
The problem of mirror effect；The present invention provides the preparation method of high transflection light coated glass, it is solved the technical issues of for need
Particular device preparation manufacture has the high-transparency coated glass of high reflective property.
High transflection light coated glass provided by the invention, specific technical solution are as follows:
High transflection light coated glass, including substrate of glass, film layer 1, membrane system 1, the film layer 1 and the film 1 are according to number
Sequence is sequentially deposited on a side surface of substrate of glass,
The film layer 1 is oxidation stainless steel bottoming film layer, and the membrane system 1 is titanium oxide membrane system.
In some embodiments, the substrate of glass is ultra-white float glass, with a thickness of 3~10mm.
In some embodiments, the film layer 1 with a thickness of 0.5~1 μm.
In some embodiments, the membrane system 1 include film layer 2, film layer 3 and film layer 4, the film layer 2 with a thickness of 45-
60nm, the film layer 3 with a thickness of 30-50nm, the film layer 4 with a thickness of 50~70nm.
The present invention also provides the preparation methods of high transflection light coated glass, are used to prepare above-mentioned high transflection light coated glass
Method, include the following steps:
Pretreatment: S1 cuts glass, edging processing, obtains pretreated glass；
S2, tempering processing: carrying out tempering processing for the pretreated glass in step S1, obtains tempering and handles glass；
Cleaning treatment: S3 the tempering processing glass in step S2 is started the cleaning processing, and is dried, is obtained
Substrate of glass；
S4, magnetron sputtering aoxidize stainless steel bottoming film: the substrate of glass in step S3 being sent into plated film cabinet, opens 1
Number operating current injects argon gas and oxygen working gas in Xiang Suoshu plated film cabinet, sputters stainless target, form film layer 1, institute
It states film layer 1 and aoxidizes stainless steel bottoming film；
S5, magnetron sputtering multilayer oxidation titanium film: opening No. 2 operating currents, in Xiang Suoshu plated film cabinet injection argon gas and
Oxygen working gas, sputtered titanium target form film layer 2, and the film layer 2 is oxidation titanium film；No. 3 operating currents are opened, to the plating
Argon gas and oxygen working gas are injected in film cabinet, sputtered titanium target forms film layer 3, and the film layer 3 is oxidation titanium film；Open 4
Number titanium target operating current injects argon gas and oxygen working gas in Xiang Suoshu plated film cabinet, and sputtered titanium target forms film layer 4, institute
Stating film layer 4 is oxidation titanium film, obtains high transflection light coated glass.
In some embodiments, the step of cleaning treatment in step S3 is as follows: the glass that the tempering is handled according to
Secondary progress first time hairbrush scrub, level-one pure water rinsing, second of hairbrush scrub, second level pure water rinsing and the punching of three-level ionized water
It washes.
In some embodiments, the mode of the drying process in step S3 is air knife drying process.
In some embodiments, in step S4, sputtering formed in the film layer 1, No. 1 operating current be 40~
The ratio of 90mA, the argon gas and oxygen is 5:1；
In step S5, sputtering is formed in the film layer 2, and No. 2 operating currents are 60~75mA, the argon gas and oxygen
Ratio be 2:1；
Sputtering is formed in the film layer 3, and No. 3 operating currents are 60~90mA, and the ratio of the argon gas and oxygen is
2:1；
Sputtering is formed in the film layer 4, and No. 4 operating currents are 60~100mA, and the ratio of the argon gas and oxygen is
2:1。
The invention has the following advantages: there are four film layer, film layers 1 for high transflection light coated glass tool provided by the invention
To aoxidize stainless steel bottoming film layer, film layer 2, film layer 3 and film layer 2 are all titanium oxide layer, and four film layers pass through magnetron sputtering
Method is deposited on the surface of substrate of glass, so that the characteristic for keeping the existing mirror surface of final finished glass reflective has the spy of high light transmission again
Property, high transflection light coated glass light transmittance provided by the invention is 66%.
Detailed description of the invention
Fig. 1 is the flow chart of the preparation method of high transflection light coated glass of the invention.
Specific embodiment
To make the objectives, technical solutions, and advantages of the present invention clearer, below in conjunction with specific embodiment, and reference
Attached drawing 1, the present invention is described in more detail.
High transflection light coated glass provided by the invention, specific technical solution are as follows:
High transflection light coated glass, including substrate of glass, film layer 1, membrane system 1, film layer 1 and film 1 according to number order successively
It is deposited on a side surface of substrate of glass, film layer 1 is oxidation stainless steel bottoming film layer, and membrane system 1 is titanium oxide membrane system.Further
Ground, substrate of glass is ultra-white float glass, with a thickness of 3~10mm.In the present embodiment, ultra-white float glass with a thickness of 5mm.
Further, film layer 1 with a thickness of 0.5~1 μm.In the present embodiment, film layer 1 with a thickness of 0.6 μm.
Further, membrane system 1 include film layer 2, film layer 3 and film layer 4, film layer 2 with a thickness of 45-60nm, the thickness of film layer 3
For 30-50nm, film layer 4 with a thickness of 50~70nm.In the present embodiment, film layer 2 with a thickness of 50nm, film layer 3 with a thickness of
40nm, film layer 4 with a thickness of 65nm.
The present invention also provides the preparation methods of high transflection light coated glass, are used to prepare above-mentioned high transflection light coated glass
Method, the specific steps are as follows:
Pretreatment: S1 by glass-cutting at edging processing is carried out after required size, obtains pretreated glass；
S2, tempering processing: carrying out tempering processing for the pretreated glass in step S1, obtains tempering and handles glass；
The step of S3, cleaning treatment: the tempering processing glass in step S2 is started the cleaning processing, cleaning treatment are as follows: will
The glass of tempering processing successively carries out first time hairbrush scrub, level-one pure water rinsing, second hairbrush scrub, second level pure water rinsing
It is rinsed with three-level ionized water；The dust box spot on cleaning treatment removal tempered glass surface；The glass of cleaning treatment is adopted later
With air knife be dried removal it is water stain, to guarantee that glass basic surface is completely smooth；
S4, magnetron sputtering aoxidize stainless steel bottoming film: the substrate of glass in step S3 being sent into plated film cabinet, opens 1
Number operating current (control electric current is 40~90mA), argon gas and oxygen are injected into plated film cabinet, and (ratio of argon gas and oxygen is
5:1) working gas sputters stainless target, forms film layer 1, and film layer 1 is oxidation stainless steel protection film layer；Oxidation stainless steel is beaten
Counterdie can make glass substrate generate meeting effect；
Magnetron sputtering multilayer oxidation titanium film: S5 opens No. 2 operating currents (control 60~75mA of electric current), to plated film case
Argon gas and oxygen working gas (ratio of argon gas and oxygen is 2:1) are injected in body, sputtered titanium target forms film layer 2；Open No. 3
Operating current (control 60~90mA of electric current), argon gas and the oxygen working gas (ratio of argon gas and oxygen are injected into plated film cabinet
Example is 2:1), sputtered titanium target forms film layer 3；No. 4 titanium target operating currents (control 60~100mA of electric current) is opened, to plated film case
Argon gas and oxygen working gas (ratio of argon gas and oxygen is 2:1) are injected in body, sputtered titanium target forms film layer 4, obtains high
Transflection light coated glass.Multilayer titanium oxide layer forms fine and close film plating layer, and final glass finished-product is effectively made to have translucency.
In conclusion high transflection light coated glass tool provided by the invention, there are four film layer, film layer 1 is that oxidation stainless steel is beaten
Bottom membrane, film layer 2, film layer 3 and film layer 2 are all titanium oxide layer, and four film layers are deposited on glass by the method for magnetron sputtering
The surface of substrate, so that the characteristic for keeping the existing mirror surface of final finished glass reflective has the characteristic of high light transmission again, it is provided by the invention
High transflection light coated glass light transmittance is 66%；High transflection light coated glass preparation method provided by the invention is not necessarily to particular device
It manufactures, to reduce the production cost of high transflection light coated glass, improves its production efficiency.
Above-mentioned preferable possible embodiments only of the invention, are not limitations of the present invention, the present invention is also not limited to above-mentioned
Citing, those skilled in the art, within the essential scope of the present invention, made variations, modifications, additions or substitutions,
Also it should belong to protection scope of the present invention.
Claims (8)
1. high transflection light coated glass, which is characterized in that including substrate of glass, film layer 1, membrane system 1, the film layer 1 and the film 1
It is sequentially deposited on a side surface of substrate of glass according to number order,
The film layer 1 is oxidation stainless steel bottoming film layer, and the membrane system 1 is titanium oxide membrane system.
2. high transflection light coated glass according to claim 1, which is characterized in that the substrate of glass is ultrawhite float glass process glass
Glass, with a thickness of 3~10mm.
3. high transflection light coated glass according to claim 1, which is characterized in that the film layer 1 with a thickness of 0.5~1 μ
m。
4. high transflection light coated glass according to claim 1, which is characterized in that the membrane system includes film layer 2, film layer 3
With film layer 4, the film layer 2 with a thickness of 45-60nm, the film layer 3 with a thickness of 30-50nm, the film layer 4 with a thickness of 50
~70nm.
5. the preparation method of high transflection light coated glass, which is characterized in that be used to prepare described in claim 1-4 any one
The method of high transflection light coated glass, includes the following steps:
Pretreatment: S1 cuts glass, edging processing, obtains pretreated glass；
S2, tempering processing: carrying out tempering processing for the pretreated glass in step S1, obtains tempering and handles glass；
Cleaning treatment: S3 the tempering processing glass in step S2 is started the cleaning processing, and is dried, glass is obtained
Substrate；
S4, magnetron sputtering aoxidize stainless steel bottoming film: the substrate of glass in step S3 being sent into plated film cabinet, opens No. 1 work
Make electric current, injects argon gas and oxygen working gas in Xiang Suoshu plated film cabinet, sputter stainless target, form film layer 1, the film
Layer 1 aoxidizes stainless steel bottoming film；
Magnetron sputtering multilayer oxidation titanium film: S5 opens No. 2 operating currents, injects argon gas and oxygen in Xiang Suoshu plated film cabinet
Working gas, sputtered titanium target form film layer 2, and the film layer 2 is oxidation titanium film；Open No. 3 operating currents, Xiang Suoshu plated film case
Argon gas and oxygen working gas are injected in body, sputtered titanium target forms film layer 3, and the film layer 3 is oxidation titanium film；Open No. 4 titaniums
Target operating current, argon gas and oxygen working gas are injected in Xiang Suoshu plated film cabinet, and sputtered titanium target forms film layer 4, the film
Layer 4 is oxidation titanium film, obtains high transflection light coated glass.
6. the preparation method of high transflection light coated glass according to claim 5, which is characterized in that the cleaning in step S3
The step of processing is as follows: the glass that the tempering is handled successively carries out first time hairbrush scrub, level-one pure water rinsing, second
Hairbrush scrub, second level pure water rinsing and three-level ionized water rinse.
7. the preparation method of high transflection light coated glass according to claim 5, which is characterized in that the drying in step S3
The mode of processing is air knife drying process.
8. the preparation method of high transflection light coated glass according to claim 5, which is characterized in that in step S4, sputtering
It is formed in the film layer 1, No. 1 operating current is 40~90mA, and the ratio of the argon gas and oxygen is 5:1；
Sputtering is formed in the film layer 2, and No. 2 operating currents are 60~75mA, and the ratio of the argon gas and oxygen is 2:1；
In step S5, sputtering is formed in the film layer 3, and No. 3 operating currents are 60~90mA, the ratio of the argon gas and oxygen
Example is 2:1；
Sputtering is formed in the film layer 4, and No. 4 operating currents are 60~100mA, and the ratio of the argon gas and oxygen is 2:1.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910188840.8A CN109761507B (en) | 2019-03-13 | 2019-03-13 | High-transmittance reflective coated glass and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910188840.8A CN109761507B (en) | 2019-03-13 | 2019-03-13 | High-transmittance reflective coated glass and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN109761507A true CN109761507A (en) | 2019-05-17 |
| CN109761507B CN109761507B (en) | 2022-02-11 |
Family
ID=66458884
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201910188840.8A Active CN109761507B (en) | 2019-03-13 | 2019-03-13 | High-transmittance reflective coated glass and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109761507B (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115016163A (en) * | 2022-07-22 | 2022-09-06 | 悦创显视科技(深圳)有限公司 | Side light leakage prevention structure of liquid crystal display screen |
| CN115093130A (en) * | 2022-06-17 | 2022-09-23 | 安徽思楠电子科技有限公司 | Multifunctional mirror surface composite processing method |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1246547A (en) * | 1999-09-09 | 2000-03-08 | 苏州华东镀膜玻璃有限公司 | Process for coating on glass to simulate low-radiation film and able to be thermally treated |
| US6142642A (en) * | 1995-06-29 | 2000-11-07 | Cardinal Ig Company | Bendable mirrors and method of manufacture |
| CN103963387A (en) * | 2014-01-15 | 2014-08-06 | 洛阳新晶润工程玻璃有限公司 | High-heat-absorption low-reflection blue film coated glass and production method thereof |
| CN106946472A (en) * | 2017-03-07 | 2017-07-14 | 江苏秀强玻璃工艺股份有限公司 | A kind of high brightness and anti-steam infiltration printed decoration glass and preparation method thereof |
-
2019
- 2019-03-13 CN CN201910188840.8A patent/CN109761507B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6142642A (en) * | 1995-06-29 | 2000-11-07 | Cardinal Ig Company | Bendable mirrors and method of manufacture |
| CN1246547A (en) * | 1999-09-09 | 2000-03-08 | 苏州华东镀膜玻璃有限公司 | Process for coating on glass to simulate low-radiation film and able to be thermally treated |
| CN103963387A (en) * | 2014-01-15 | 2014-08-06 | 洛阳新晶润工程玻璃有限公司 | High-heat-absorption low-reflection blue film coated glass and production method thereof |
| CN106946472A (en) * | 2017-03-07 | 2017-07-14 | 江苏秀强玻璃工艺股份有限公司 | A kind of high brightness and anti-steam infiltration printed decoration glass and preparation method thereof |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115093130A (en) * | 2022-06-17 | 2022-09-23 | 安徽思楠电子科技有限公司 | Multifunctional mirror surface composite processing method |
| CN115016163A (en) * | 2022-07-22 | 2022-09-06 | 悦创显视科技(深圳)有限公司 | Side light leakage prevention structure of liquid crystal display screen |
Also Published As
| Publication number | Publication date |
|---|---|
| CN109761507B (en) | 2022-02-11 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN105084778B (en) | A kind of green low radiation coated glass and preparation method thereof | |
| TR200003691T2 (en) | Multi-layer coatings with anti-solar and low emission functions. | |
| CN206553403U (en) | A kind of high infrared reflection coated glass | |
| CN109761507A (en) | High transflection light coated glass and preparation method thereof | |
| US8609253B2 (en) | Coated article and method for making the same | |
| CN106186724B (en) | A kind of high light green color bendable steel Three-silver-layer low-radiation coated glass and preparation method | |
| CN105481267A (en) | High-penetrability single-sliver low-emissivity coated glass for subsequent processing and production technology thereof | |
| CN106396425A (en) | Coated glass with dual functions of highly reflecting visible light and blocking infrared rays and preparation method thereof | |
| CN106431003A (en) | Coated glass with dual functions of visible light high reflection and blue purple light blocking and preparation method thereof | |
| CN107452818A (en) | A kind of copper-indium-galliun-selenium film solar cell back electrode and preparation method thereof | |
| CN105084781B (en) | A kind of golden low radiation film coating glass and preparation method thereof | |
| CN109136859A (en) | A method of preparing high transparency gallium oxide film | |
| CN107056084A (en) | Three-silver-layer low-radiation coated glass and manufacture method and application | |
| CN102732830A (en) | Plating method for anti-reflection film with high transmittance and low reflectivity | |
| CN211078928U (en) | Double-silver low-emissivity coated glass | |
| CN105439468A (en) | Sky blue mirror reflection coated glass and preparation method thereof | |
| CN102219396A (en) | Temperable gold low-emissivity coated glass and manufacturing method thereof | |
| CN105084779B (en) | A kind of high-transparency double-silver low-emissivity coated glass and preparation method thereof | |
| CN103895276A (en) | Silver-based low-radiation coated glass | |
| CN207047104U (en) | Three-silver-layer low-radiation coated glass | |
| WO2019157799A1 (en) | Method for preparing low-radiation coated glass | |
| CN206109216U (en) | But golden low -emissivity coated glass of tempering | |
| CN103288362A (en) | Technology for high-transmittance, high-performance and low-emissivity glass | |
| US8304100B2 (en) | Coated glass and method for making the same | |
| CN214457645U (en) | Single-silver low-emissivity glass |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: High transmittance reflective coated glass and its preparation method Effective date of registration: 20230414 Granted publication date: 20220211 Pledgee: Jiangyin branch of Bank of China Ltd. Pledgor: JIANGYIN TAIRONG PHOTOELECTRIC TECHNOLOGY Co.,Ltd. Registration number: Y2023980038166 |
|
| PE01 | Entry into force of the registration of the contract for pledge of patent right |