CN109706016A - Whole wheat light flavour dark beer malt formula, gained beer and preparation method thereof - Google Patents

Whole wheat light flavour dark beer malt formula, gained beer and preparation method thereof Download PDF

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Publication number
CN109706016A
CN109706016A CN201910188863.9A CN201910188863A CN109706016A CN 109706016 A CN109706016 A CN 109706016A CN 201910188863 A CN201910188863 A CN 201910188863A CN 109706016 A CN109706016 A CN 109706016A
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China
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malt
beer
whole wheat
coloration
dark
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Inventor
尹花
董建军
邢磊
常宗明
钱中华
黄树丽
胡孝丛
岳杰
刘晓琳
陈华磊
王剑锋
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Tsingtao Brewery Co Ltd
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Tsingtao Brewery Co Ltd
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Priority to CN201910188863.9A priority Critical patent/CN109706016A/en
Publication of CN109706016A publication Critical patent/CN109706016A/en
Priority to PCT/CN2019/104131 priority patent/WO2020181743A1/en
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    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12CBEER; PREPARATION OF BEER BY FERMENTATION; PREPARATION OF MALT FOR MAKING BEER; PREPARATION OF HOPS FOR MAKING BEER
    • C12C12/00Processes specially adapted for making special kinds of beer
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12CBEER; PREPARATION OF BEER BY FERMENTATION; PREPARATION OF MALT FOR MAKING BEER; PREPARATION OF HOPS FOR MAKING BEER
    • C12C7/00Preparation of wort
    • C12C7/04Preparation or treatment of the mash
    • C12C7/047Preparation or treatment of the mash part of the mash being unmalted cereal mash

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Biochemistry (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • General Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • Food Science & Technology (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Microbiology (AREA)
  • Distillation Of Fermentation Liquor, Processing Of Alcohols, Vinegar And Beer (AREA)
  • Alcoholic Beverages (AREA)

Abstract

The present invention proposes a kind of whole wheat light flavour dark beer malt formula, gained beer and preparation method thereof, belongs to beer technical field, is able to solve the domestic status without whole wheat light flavour dark beer at present.Selected malt using Ai Er malt collocation chocolate malt and bakes barley in whole wheat light flavour dark beer malt formula, wherein Ai Er malt coloration 5.5-7.5EBC, saccharifying power >=220WK;Chocolate malt coloration 900-1100EBC bakes barley coloration 1100-1300EBC;It is 10-12 ° of P, the limit degree of fermentation >=68%, amaroid 20-35EBC, coloration 100-150EBC by the wort concentration for being formulated the wheat juice being prepared.Malt formula provided by the present invention can be applied in the production of whole wheat light flavour dark beer.

Description

Whole wheat light flavour dark beer malt formula, gained beer and preparation method thereof
Technical field
The invention belongs to beer technical field more particularly to a kind of whole wheat light flavour dark beer malt formulas, gained beer And preparation method thereof.
Background technique
Dark beer enjoys the good reputation of " black milk ".National standard defines the beer of beer color 41EBC or more mainly point three classes: The black beer of German-style (Schwarzbier), baud (Porter) He Shitao (Stout).The black beer of German-style (Schwarzbier) is lower leaven Mother's fermentation, taste are thin refreshing;English black beer baud (Porter) He Shitao (Stout) is top yeast fermentation, and taste is more mellow. Under normal conditions, dark beer is aterrimus, 12 ° of P-20 ° of P of original wort concentration, alcoholic strength >=4.5%vol, mellow in taste, slightly Sweet taste.
Black beer why burnt odor it is prominent, with taste, mellow in taste, slightly sweet taste is charred, main reason is that black beer exists In manufacturing process largely use burnt malt and black malt, and both malt be during wheat processed high temperature drying and obtain , therefore the product of Maillard reaction is more compared with common malt, coloration is deep, so as to bring deep color and coke to dark beer Flavor that is fragrant, being charred;But high temperature drying simultaneously also destroys the enzyme material in malt, therefore without using the black of external source carbohydrase The usual degree of fermentation of beer is lower, residual sugar is higher, therefore black beer has the characteristics that slightly sweet taste, mellow in taste.Based on this, one kind is developed In the case where not adding external source carbohydrase, both there is the typical burnt odor of black beer, chocolate, coffee flavor, while again without being charred Taste, the degree of fermentation is high, and residual sugar is low, and the light black beer of feeling well of mouthfeel can not only enrich the type of black beer in this way, while it is black also to can solve tradition Beer flavor and taste lay particular stress on, are not suitable for the problem of more drinks, provide more more options to consumer.
Summary of the invention
The present invention proposes a kind of whole wheat light flavour dark beer malt formula, gained beer and preparation method thereof, this beer Both there is the typical burnt odor of black beer, chocolate, coffee flavor, while again without taste is charred, the degree of fermentation is high, residual sugar is low, and mouthfeel is light to feel well, Solves the domestic status without whole wheat light flavour dark beer at present.
In order to achieve the above object, the present invention provides a kind of whole wheat light flavour dark beer malt formula, in the formula Selected malt is using Ai Er malt collocation chocolate malt and bakes barley, wherein Ai Er malt coloration 5.5-7.5EBC, saccharification Power >=220WK;Chocolate malt coloration 900-1100EBC bakes barley coloration 1100-1300EBC;It is prepared by the formula The wort concentration of the wheat juice arrived is 10-12 ° of P, the limit degree of fermentation >=68%, amaroid 20-35EBC, coloration 100-150EBC.
Preferably, the additive amount of the Ai Er malt accounts for the 89-93% of selected malt total amount, the addition of chocolate malt Amount accounts for the 1%-8% of selected malt total amount, and the additive amount for baking barley accounts for the 1%-8% of selected malt total amount.
It is prepared the present invention also provides a kind of using whole wheat light flavour dark beer malt formula described in above-mentioned technical proposal The method of whole wheat light flavour dark beer, includes the following steps:
Selecting Ai Er malt collocation chocolate malt and baking barley, water is primary raw material, after malt raw material is crushed, with Material-water ratio 1:3-1:4 is mixed with water, and in 62-73 DEG C of progress two-period form saccharification, saccharifying does not add exogenous enzyme preparations;
After saccharification, mellow solution of saccharification is filtered in 76 ± 1 DEG C, is boiled after obtaining clarification wheat juice, in boiling part by several times Hops or hop product are added, convolution precipitating is carried out after boiling, is cooled to 16-18 DEG C, while being oxygenated access top yeast and carrying out Fermentation, obtains beer fermentation liquid;
10-12 ° of P, packaging sterilization are diluted or be not diluted to after beer fermentation liquid is filtered, and obtain the black beer of whole wheat light flavour Wine.
Preferably, two-period form saccharification is included in 62-65 DEG C, the first segment saccharification of 80-100min and in 71-73 DEG C, the saccharification of the second segment of 20-40min, wherein do not add exogenous enzyme preparations in entire saccharifying.
Preferably, adding hops by several times in boiling part or hop product specifically includes:
Hops or hop product are added respectively when boiling beginning, boiling 15min and boil 60min.
Preferably, the hops or hop product are bitter flower, fragrant flower or bitter fragrant inclusive type.
Preferably, the oxygenation access top yeast carries out fermentation and specifically includes:
To convolution precipitating, Wort oxygenating after cooling, wheat juice dissolved oxygen 8-10mg/L is controlled, while accessing top yeast, Canful yeast number controls ten thousand/ml of 600-1500, and main 16-20 DEG C of ferment temperature, 16-20 DEG C of reduction temperature are down to biacetyl 0.05mg/L or less is cooled to -2 DEG C -0 DEG C, cold storage time >=4 day.
The present invention also provides a kind of black beers of whole wheat light flavour that the method according to the above technical scheme is prepared Wine.
Preferably, the original wort concentration of the beer is 10-12 ° of P, amaroid 15-25EBC, coloration 80- 140EBC, RDF >=66%, appearance pol≤2.4 ° P.
Compared with prior art, the advantages and positive effects of the present invention are:
Composition of raw materials is optimized in whole wheat light flavour dark beer malt formula provided by the present invention, is adding it not Under the premise of adding any external source carbohydrase, can reach with black beer typical case flavor camerlsed, chocolate, coffee flavor and Show without the tasty and refreshing feature of taste, mouthfeel is charred, has solved the black beer flavor of tradition and taste is laid particular stress on, be not suitable for the statuses drunk more.
Specific embodiment
The technical scheme in the embodiments of the invention will be clearly and completely described below, it is clear that described implementation Example is only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, this field is common Technical staff's every other embodiment obtained without making creative work belongs to the model that the present invention protects It encloses.
The embodiment of the invention provides a kind of whole wheat light flavour dark beer malt formula, selected malt is used in the formula Ai Er malt collocation chocolate malt and baking barley, wherein Ai Er malt coloration 5.5-7.5EBC, saccharifying power >=220WK;Ingeniously Gram force malt coloration 900-1100EBC bakes barley coloration 1100-1300EBC;By the wheat for being formulated the wheat juice being prepared Juice concentration is 10-12 ° of P, the limit degree of fermentation >=68%, amaroid 20-35EBC, coloration 100-150EBC.
Pilsen provided by the above embodiment is made of whole wheat, accounts for main coin in selected malt with Ai Er malt Kind, collocation chocolate malt and baking barley, wherein the additive amount of Ai Er malt accounts for the 89-93% of selected malt total amount, chalk The additive amount of power malt accounts for the 1%-8% of selected malt total amount, and the additive amount for baking barley accounts for the 1%- of selected malt total amount 8%.This mainly considers that the more common malt coloration of Ai Er malt is high, and saccharifying power, can using Ai Er malt close to common malt To reduce the usage amount of black malt, reduction is charred taste, while the dark beer wheat juice limit degree of fermentation can be improved;Collocation uses high The chocolate malt of coloration and baking barley, it is possible to reduce the usage amount of burnt malt improves formula saccharifying power, it is ensured that wheat The limit degree of fermentation >=68% of juice, while the distinctive chocolate of black beer, coffee flavor can be contributed.In addition, this beer formula In without using auxiliary materials such as rice, corns, and exogenous enzyme preparations are not added, in conjunction with the ingredient requirement that specifically limits and last To wort concentration, amaroid, coloration and the limit degree of fermentation require preparation-obtained beer that there is black beer typical case flavor simultaneously Camerlsed, chocolate, coffee flavor, and realize without the tasty and refreshing feature of taste, mouthfeel is charred, solve the black beer flavor of tradition and mouth Taste is laid particular stress on, and the statuses drunk are not suitable for more.
Whole wheat light flavour dark beer malt formula described in above-described embodiment is utilized the embodiment of the invention also provides a kind of The method for preparing whole wheat light flavour dark beer, includes the following steps:
S1: selecting Ai Er malt collocation chocolate malt and bakes barley, water is primary raw material, and malt raw material is crushed Afterwards, it is mixed with material-water ratio 1:3-1:4 with water, in 62-73 DEG C of progress two-period form saccharification, saccharifying does not add exogenous enzyme preparations;
In the step, mixed again with water with the ratio of 1:3-1:4 after need to sufficiently crushing each malt, to ensure wheat Bud makes full use of.In addition, saccharifying is optimized for two-period form saccharification in this step, the decomposition of starch both can guarantee in this way, Be conducive to the control of the wheat juice limit degree of fermentation again.
S2: after saccharification, mellow solution of saccharification being filtered in 76 ± 1 DEG C, is boiled after obtaining clarification wheat juice, is divided in boiling part Secondary addition hops or hop product carry out convolution precipitating after boiling, are cooled to 16-18 DEG C, at the same be oxygenated access top yeast into Row fermentation, obtains beer fermentation liquid.
In the step, mellow solution of saccharification is filtered, guarantees the suspended material in mellow solution of saccharification by abundant precipitating, separation.In addition, In order to ensure making full use of for hops substance, gradation addition manner is used for the addition of hops or hop product, is preferably being boiled Boiling starts, boils 15min and add hops or hop product respectively when boiling 60min, in addition after hops add, in order to As much as possible retain hops Studies of The Aromatic Substances, one 0-10min boiling pot of optional addition is stopped the supple of gas or steam after reflux technique, then is carried out convolution and sunk It forms sediment, swing time can may be, for example, 20min-30min according to boomerang effect appropriate adjustment, at this time the wort concentration of gained wheat juice For 10-12 ° of P.
S3: it is diluted to 10-12 ° of P, packaging sterilization after beer fermentation liquid is filtered, obtains whole wheat light flavour dark beer.
In a preferred embodiment, two-period form saccharification be included in 62-65 DEG C, the first segment saccharification of 80-100min and It is saccharified in the second segment of 71-73 DEG C, 20-40min, wherein do not add exogenous enzyme preparations in entire saccharifying.The present embodiment In, it not only can guarantee the decomposition of starch after optimizing two-period form Mashing process, but also be conducive to the control of the wheat juice limit degree of fermentation.
In a preferred embodiment, the hops or hop product be bitter flower, fragrant flower or bitter fragrant inclusive type it is understood that As long as it is good that the hop varieties of the present embodiment selection meet hops hardship sense harmony, facilitate final beer product with burnt odor, nothing Nothing is charred the light refreshing feature of taste, mouthfeel.
In a preferred embodiment, the oxygenation access top yeast, which ferment, specifically includes:
To convolution precipitating, Wort oxygenating after cooling, wheat juice dissolved oxygen 8-10mg/L is controlled, while accessing top yeast, Canful yeast number controls ten thousand/ml of 600-1500, and main 16-20 DEG C of ferment temperature, 16-20 DEG C of reduction temperature are down to biacetyl 0.05mg/L or less is cooled to -2 DEG C -0 DEG C, cold storage time >=4 day.It ferments in the present embodiment to oxygenation access top yeast The step of involved in Parameter Conditions be defined, it is ensured that after fermentation products obtained therefrom be desired product.It is understood that right It can slightly be adjusted in the range of above-mentioned restriction according to practical condition in the restriction of above-mentioned parameter condition.
The embodiment of the invention also provides a kind of whole wheat light flavour dark beer being prepared according to the above method, the beers The original wort concentration of wine be 10-12 ° of P, amaroid 15-25EBC, coloration 80-140EBC, RDF >=66%, appearance pol≤ 2.4 ° of P reach it can and be charred taste, mouth with black beer typical case flavor camerlsed, chocolate, coffee flavor and nothing Feel tasty and refreshing feature, solves the black beer flavor of tradition and taste is laid particular stress on, be not suitable for the statuses drunk more.
Whole wheat light flavour dark beer malt formula, gained provided by the embodiment of the present invention are introduced in detail in order to become apparent from Beer and preparation method thereof is described below in conjunction with specific embodiment.
Embodiment 1
With Ai Er malt 92%, chocolate malt 3.5%, bake barley 4.5%), water be raw material through crushing → saccharification → Filter → boil (addition hops by several times, boil 10 ° of P of whole wort concentration) → convolution precipitating → cooling → oxygenation → addition top yeast → fermentation → filtering → sterilization → up to 10 ° of P whole wheat light flavour dark beer.
Embodiment 2
With Ai Er malt 91%, chocolate malt 1%, bake barley 8%), water be raw material through crushing → saccharification → filtering → boil (addition hops by several times, boil 10 ° of P of whole wort concentration) → convolution precipitating → cooling → oxygenation → addition top yeast → hair Ferment → filtering → sterilization → up to 10 ° of P whole wheat light flavour dark beer.
Embodiment 3
With Ai Er malt 91%, chocolate malt 8%, bake barley 1%), water be raw material through crushing → saccharification → filtering → boil (addition hops by several times, boil 10 ° of P of whole wort concentration) → convolution precipitating → cooling → oxygenation → addition top yeast → hair Ferment → filtering → sterilization → up to 10 ° of P whole wheat light flavour dark beer.
Embodiment 4
With Ai Er malt 93%, chocolate malt 2%, bake barley 5%), water be raw material through crushing → saccharification → filtering → boil (addition hops by several times, boil 12 ° of P of whole wort concentration) → convolution precipitating → cooling → oxygenation → addition top yeast → hair Ferment → filtering → sterilization → up to 12 ° of P whole wheat light flavour dark beer.
Embodiment 5
With Ai Er malt 89%, chocolate malt 7%, bake barley 4%), water be raw material through crushing → saccharification → filtering → boil (addition hops by several times, boil 12 ° of P of whole wort concentration) → convolution precipitating → cooling → oxygenation → addition top yeast → hair Ferment → filtering → sterilization → up to 12 ° of P whole wheat light flavour dark beer.
Whole wheat light flavour dark beer Physico-chemical tests
The part Physico-chemical tests result of 1 the used raw material of embodiment 1-5 of table
Detection project Ai Er malt Chocolate malt Bake barley
Coloration EBC 7.0 950 1150
Saccharifying power WK 235 / /
The Physico-chemical tests result of wheat juice obtained by 2 embodiment 1-5 of table
Detection project Embodiment 1 Embodiment 2 Embodiment 3 Embodiment 4 Embodiment 5
Limit degree of fermentation % 68.3 68.1 68.8 69 68
Wort concentration ° P 10 10 10 12 12
Coloration EBC 110 125 100 123 128
The testing result of the preparation-obtained whole wheat light beer of 3 embodiment 1-5 of table
From the data in table 1, it can be seen that right in whole wheat light flavour dark beer that 1-5 is met using malt of embodiment of the present invention formula In the established standards of malt, and by table 2-3 data it is found that based on the setting to component selected in formula, so that prepared obtain The wort concentration of the wheat juice arrived is 10-12 ° of P, the limit degree of fermentation >=68%, amaroid 20-35EBC, coloration 100-150EBC; Preparation-obtained whole wheat light flavour dark beer original wort concentration is 10-12 ° of P, amaroid 15-25EBC, coloration 80- 140EBC, RDF >=66%, appearance pol≤2.4 ° P meet the desired black beer flavor and taste requirement prepared.
Flavor evaluation
Flavor evaluation measurement is carried out to the obtained whole wheat light flavour dark beer of above-described embodiment 1-5, the results are shown in Table 4.
The obtained whole wheat light flavour dark beer product special flavour of 4 embodiment 1-5 of table judges result
As seen from the results in Table 4, whole wheat light flavour dark beer provided in an embodiment of the present invention had both had black beer typical case flavor burnt Sugared perfume, chocolate, coffee flavor, and have without taste is charred, the tasty and refreshing feature of mouthfeel, solves the black beer flavor of tradition and taste is inclined Weight is not suitable for the statuses drunk more.

Claims (9)

1. whole wheat light flavour dark beer malt formula, which is characterized in that selected malt is arranged in pairs or groups using Ai Er malt in the formula Chocolate malt and baking barley, wherein Ai Er malt coloration 5.5-7.5EBC, saccharifying power >=220WK;Chocolate malt coloration 900-1100EBC bakes barley coloration 1100-1300EBC;It is 10- by the wort concentration for being formulated the wheat juice being prepared 12 ° of P, the limit degree of fermentation >=68%, amaroid 20-35EBC, coloration 100-150EBC.
2. whole wheat light flavour dark beer malt formula according to claim 1, which is characterized in that the Ai Er malt adds Dosage accounts for the 89-93% of selected malt total amount, and the additive amount of chocolate malt accounts for the 1%-8% of selected malt total amount, bakes big The additive amount of wheat accounts for the 1%-8% of selected malt total amount.
3. preparing the side of whole wheat light flavour dark beer using whole wheat light flavour dark beer malt formula described in as claimed in claim 1 or 22 Method, which comprises the steps of:
It selects Ai Er malt collocation chocolate malt and bakes barley, water for primary raw material, after malt raw material is crushed, to expect water It is mixed than 1:3-1:4 with water, in 62-73 DEG C of progress two-period form saccharification, saccharifying does not add exogenous enzyme preparations;
After saccharification, mellow solution of saccharification is filtered in 76 ± 1 DEG C, boils after obtaining clarification wheat juice, added by several times in boiling part Hops or hop product carry out convolution precipitating after boiling, are cooled to 16-18 DEG C, while being oxygenated access top yeast and fermenting, Obtain beer fermentation liquid;
10-12 ° of P, packaging sterilization are diluted or be not diluted to after beer fermentation liquid is filtered, and obtain whole wheat light flavour dark beer.
4. according to the method described in claim 3, it is characterized in that, two-period form saccharification is included in 62-65 DEG C, 80- The first segment of 100min is saccharified and is saccharified in the second segment of 71-73 DEG C, 20-40min, wherein does not add in entire saccharifying Add exogenous enzyme preparations.
5. according to the method described in claim 3, it is characterized in that, adding hops by several times in boiling part or hop product is specific Include:
Hops or hop product are added respectively when boiling beginning, boiling 15min and boil 60min.
6. the method according to claim 3 or 5, which is characterized in that the hops or hop product are bitter flower, fragrant flower or hardship Fragrant inclusive type.
7. according to the method described in claim 3, it is characterized in that, oxygenation access top yeast carries out the specific packet that ferments It includes:
To convolution precipitating, Wort oxygenating after cooling, wheat juice dissolved oxygen 8-10mg/L is controlled, while accessing top yeast, canful Yeast number controls ten thousand/ml of 600-1500, and main 16-20 DEG C of ferment temperature, 16-20 DEG C of reduction temperature are down to 0.05mg/ to biacetyl L or less is cooled to -2 DEG C -0 DEG C, cold storage time >=4 day.
8. the whole wheat light flavour dark beer being prepared according to the described in any item methods of claim 3-7.
9. whole wheat light flavour dark beer according to claim 8, which is characterized in that the original wort concentration of the beer is 10-12 ° of P, amaroid 15-25EBC, coloration 80-140EBC, RDF >=66%, appearance pol≤2.4 ° P.
CN201910188863.9A 2019-03-13 2019-03-13 Whole wheat light flavour dark beer malt formula, gained beer and preparation method thereof Pending CN109706016A (en)

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PCT/CN2019/104131 WO2020181743A1 (en) 2019-03-13 2019-09-03 Malt formula of whole-wheat light-flavored black beer, beer obtained thereby, and preparation method thereof

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Publication number Priority date Publication date Assignee Title
WO2020181743A1 (en) * 2019-03-13 2020-09-17 青岛啤酒股份有限公司 Malt formula of whole-wheat light-flavored black beer, beer obtained thereby, and preparation method thereof
WO2020181744A1 (en) * 2019-03-13 2020-09-17 青岛啤酒股份有限公司 Whole-wheat light-flavor-type dark beer and preparation method therefor
CN110951560A (en) * 2019-12-27 2020-04-03 青岛啤酒股份有限公司 Strong IPA beer malt formula, beer obtained by same and preparation method thereof
CN112029599A (en) * 2020-09-21 2020-12-04 青岛啤酒股份有限公司 Light red ale malt formula, beer obtained by using same and preparation method of beer
CN112063463A (en) * 2020-09-21 2020-12-11 青岛啤酒股份有限公司 Light red beer and its preparing method
CN112592779A (en) * 2020-12-31 2021-04-02 青岛啤酒股份有限公司 Black wheat beer and preparation method thereof
CN112592779B (en) * 2020-12-31 2022-08-12 青岛啤酒股份有限公司 Black wheat beer and preparation method thereof
CN115232685A (en) * 2022-08-23 2022-10-25 青岛啤酒股份有限公司 Brewing method for improving wheat flavor of whole wheat beer and beer obtained by brewing method
CN116064200A (en) * 2022-12-29 2023-05-05 青岛啤酒股份有限公司 Preparation process of whole wheat sugar-free beer and obtained product

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Application publication date: 20190503