CN109694093A - A kind of heavy alkali high-efficiency production technology - Google Patents

A kind of heavy alkali high-efficiency production technology Download PDF

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Publication number
CN109694093A
CN109694093A CN201811527919.0A CN201811527919A CN109694093A CN 109694093 A CN109694093 A CN 109694093A CN 201811527919 A CN201811527919 A CN 201811527919A CN 109694093 A CN109694093 A CN 109694093A
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CN
China
Prior art keywords
axis
steam
soda ash
reaction chamber
rope
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CN201811527919.0A
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Chinese (zh)
Inventor
余小海
王慧丽
蔡素真
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Individual
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    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01DCOMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D7/00Carbonates of sodium, potassium or alkali metals in general
    • C01D7/22Purification
    • C01D7/24Crystallisation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D9/00Crystallisation
    • B01D9/0059General arrangements of crystallisation plant, e.g. flow sheets
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D9/00Crystallisation
    • B01D9/0063Control or regulation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/0066Stirrers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B08CLEANING
    • B08BCLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
    • B08B9/00Cleaning hollow articles by methods or apparatus specially adapted thereto 
    • B08B9/08Cleaning containers, e.g. tanks
    • B08B9/087Cleaning containers, e.g. tanks by methods involving the use of tools, e.g. brushes, scrapers
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01DCOMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D7/00Carbonates of sodium, potassium or alkali metals in general
    • C01D7/22Purification
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D9/00Crystallisation
    • B01D2009/0086Processes or apparatus therefor

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Mechanical Engineering (AREA)
  • Processing Of Solid Wastes (AREA)

Abstract

The invention belongs to heavy alkali production technical field, specifically a kind of heavy alkali high-efficiency production technology, the technique uses crystallization reactor, including cabinet;It further include driving unit, auxiliary unit, collector unit, cleaning unit, No.1 air bag, spiral steam pipe, reaction chamber, generator, motor and controller.Technique one side, by the way that the temperature of steam is maintained 100-400 DEG C, so that soda ash liquid is adequately crystallized in reaction chamber, to improve the production efficiency of heavy alkali;On the other hand, the steam by temperature at 200-600 DEG C is passed into steam dryer, passes through the mutual cooperation between steam and steam dryer, heavy alkali crystal grain is dried, it avoids increase process that heavy alkali crystal grain is dried, technique is shortened, to improve heavy alkali production efficiency.

Description

A kind of heavy alkali high-efficiency production technology
Technical field
The invention belongs to heavy alkali production technical field, specifically a kind of heavy alkali high-efficiency production technology.
Background technique
Heavy soda ash is divided into common heavy soda ash and high-quality dense soda ash with the superiority and inferiority of chemical analysis, with physical property difference (referring mainly to severe) is divided into common heavy soda ash and super heavy soda ash, and heavy soda ash is compared with light soda ash, heavy soda ash due to Its severe is big, therefore packaging material saves, and transport, storage cost are low, and in use, alkali dirt is not easy to fly upward, and significantly reduces Dust collector and environmental pollution, if chemical analysis enters high-quality dense soda ash class, moreover it is possible to mitigate equipment corrosion, increase equipment Exchange capability of heat and receive praises from customers.
In the production of existing heavy alkali, need it is subsequent the heavy alkali crystal grain produced is dried, increase work Skill process;So that the technical solution is restricted.
Summary of the invention
In order to make up for the deficiencies of the prior art, it solves the problems, such as subsequent heavy alkali crystal grain to be dried;The present invention proposes A kind of heavy alkali high-efficiency production technology.
The technical solution adopted by the present invention to solve the technical problems is: a kind of heavy alkali high-efficiency production of the present invention Technique, the technique the following steps are included:
S1: heating water by heating device, so that water vapor, becomes steam, and makes the vapor (steam) temperature of steam Reach 400 DEG C, gas pressure 0.01-0.6MPa;
S2: on the basis of S1, by cooling down to steam, so that the temperature of steam maintains 100-400 DEG C, gas Pressure is 0.01-0.6MPa;
S3: on the basis of S2, steam dryer being mounted on wall box, and steam dryer is used for heavy alkali crystal grain Drying;
S4: on the basis of S1, S2 and S3, starting crystallization reactor, the crystallization of heavy alkali carried out by crystallization reactor, Ten minutes later to the crystallization of heavy alkali, by temperature at 200-600 DEG C, gas pressure is that the steam of 0.01-0.6MPa is passed into steam In drier, by the mutual cooperation between steam dryer and steam, heavy alkali crystal grain is dried;
The crystallization reactor that the present invention uses includes cabinet;It further include driving unit, auxiliary unit, collector unit, cleaning Unit, No.1 air bag, spiral steam pipe, reaction chamber, generator, motor and controller;The controller is for controlling heavy The work of alkali crystallization reactor;The wall box is equipped with steam port and gas outlet, and top of the box is equipped with inlet, alkali inlet With No.1 hole, the bottom of box is symmetrically arranged with discharge port;The spiral steam pipe is fixedly mounted on wall box, spiral to steam Steam pipe one end is connected to steam port, and the spiral steam pipe other end is located at below No.1 hole;The quantity of the No.1 air bag is two, Two No.1 air bag one end are interconnected, wherein a No.1 air bag is connected in the bottom of box, another No.1 air bag and reaction chamber are connected, Reaction chamber uncovered, reaction chamber are soda ash crystal region;The driving unit is mounted on top of the box, and driving unit includes shell, turns Dynamic fan, No.1 axis, No. two axis, No.1 helical gear, No. two helical gears, No. three helical gears and No. three axis;The shell is connected in case At the top of body;In the rotational installation on the inner wall of the housing of No.1 axis one end, the No.1 axis other end and rotation fan are connected, and rotate fan position At No.1 hole;The No.1 helical gear is set on No.1 axis;No. two helical gear quantity is two, No. two helical teeth wheel cases It is located on No. two axis outer rings and is connected in No. two shaft ends portion;Described No. two axis one end are rotatably installed on shell, and No. two axis are another End is connected with No. two helical gears, No.1 helical gear and No. two helical gear engaged transmissions;Described No. three axis one end are protruded into cabinet, and three Number axis one end and auxiliary unit are connected, and No. three axis outer rings and cabinet contact position are rotatablely installed, and No. three axis other ends are oblique with No. three Gear engagement, No. three helical gears and No. two helical gear engaged transmissions;The auxiliary unit is located in reaction chamber, and auxiliary unit is used for Soda ash crystallization is assisted, auxiliary unit includes No.1 cylinder, No. four axis, fixed pulley, blender and No.1 rope;The No.1 cylinder with The connection of two No.1 air bags, No.1 cylinder one end are connected with No. three axis, and the No.1 cylinder other end and No. four axis are connected, and No. four axis are by two Part is spliced, and forms No.1 channel after No. four axis splicings;The quantity of the fixed pulley is two, and two fixed pulleys are located at one number service At road, and two fixed pulleys pass through shaft and are rotatably installed on No. four axis;The quantity of the blender is two, and blender is along No. four Axial symmetry setting, blender are made of No.1 spring and several box bodies;The framed lid in box body on the outermost side side, is located at Innermost box body is connected on No. four axis outer rings, is interconnected between box body, and be slidably connected to each other, and pagoda is formed Shape;The No.1 spring one end is connected on outermost box body, and the No.1 spring other end is connected in innermost box body On;The quantity of the No.1 rope is two, and two No.1 rope one end are connected on No.1 spring, and the two No.1 rope other ends pass through hook It is connected in reaction chamber bottom, and two No.1 ropes are through two fixed pulley transition;Steam is passed through from steam port, so that driving unit drives Soda ash crystallization is accelerated in auxiliary unit rotation, meanwhile, with the reduction of soda ash liquid in reaction chamber, No.1 air bag inspiration No.1 cylinder Interior gas, No.1 cylinder drive No. four axis to rise, and by fixed pulley, No.1 spring and the effect of No.1 rope, so that blender It shrinks;The collector unit is fixedly mounted on top of the box, and collector unit is arranged along No. three axial symmetry, and collector unit is for collecting Soda ash crystalline particle, collector unit include fixed column, fixed link and collecting board;The fixed column is fixedly mounted on top of the box, No.1 slot is offered in fixed column;Described fixed link one end is located at No.1 slot, and fixed link one end is connected in No.1 by spring In slot, the fixed link other end and collecting board are connected;The quantity of the motor is two, and motor is fixedly mounted in fixed column;It is described The quantity of generator is two, and generator is used to for motor provide power source, and generator is mounted on top of the box, by by fixed link The gas generated in movement acts on generator, so that generator rotation power generation;The cleaning unit is mounted on motor output shaft On, for cleaning unit for clearing up the inner sidewall of reaction chamber, cleaning unit includes cleaning annulus and No. two ropes;The cleaning Annulus is contacted with reaction chamber side wall;The quantity of No. two ropes is two, and No. two rope one end are wrapped on motor output shaft, No. two The other end of restricting is connected with cleaning annulus, and controller is equipped at the top and bottom of reaction chamber, is used to control motor just using controller Reversion, is rotated by generator drive motor, so that cleaning annulus moves up and down in reaction chamber.Soda ash is tied Crystalline substance avoids in use and a large amount of alkali dirt occurs, reduces dust collector;There is also a kind of crystallizers in the prior art, still, Crystallizer Shortcomings in the prior art, on the one hand, crystallizer in the prior art soda ash is crystallized it is ineffective, and Soda ash crystalline particle after crystallization mixes with soda ash liquid, meanwhile, the crystallization to soda ash liquid cannot be adjusted according to actual needs, To influence the practicability of crystallization;On the other hand, it after not to soda ash crystallization, reacts the crystalline particle adhered on chamber interior wall and carries out clearly Reason, to influence the crystallization effect of soda ash;The present invention passes through driving unit, auxiliary unit, cleaning unit, collector unit, No.1 Air bag, spiral steam pipe, reaction chamber, generator, motor and controller;On the one hand, it realizes the multiple utilization to steam, utilizes Steam makes rotation fan rotation, so that driving unit driving auxiliary unit rotation, the crystallization of soda ash is assisted by auxiliary unit, and Soda ash liquid and soda ash crystal grain are separated, avoids soda ash liquid and soda ash crystalline particle from mixing, influences the crystallization of soda ash liquid, from And improve soda ash crystallization effect;Meanwhile driving collecting board to move up and down by fixed link, collecting board is few by soda ash liquid measure When soda ash crystal grain be collected, avoid crystallization after soda ash crystal grain mixed with soda ash liquid, thus improve soda ash crystallization imitate Fruit;On the other hand, the pneumatic power source generated when fixed link being moved acts on generator, is turned by generator drive motor Dynamic, so that cleaning annulus moves up and down in reaction chamber, cleaning annulus clears up reaction chamber interior wall, avoids reaction chamber The soda ash crystal grain adhered on inner wall influences soda ash crystallization, to improve soda ash crystallization effect.
Firstly, steam is passed through from steam port, the steam being passed through is entered in cabinet by spiral steam pipe, to steam After being passed through a period of time, at this point, soda ash and water are entered in reaction chamber from alkali inlet and inlet respectively, with soda ash and water Be constantly passed through, the overall weight of reaction chamber becomes weight, and reaction chamber squeezes No.1 air bag, and No.1 air bag is squeezed outside air-blowing, drum Gas out transfers to No.1 cylinder, and No.1 cylinder pushes No. four axis to move downward, since the whole air content of No.1 air bag is greater than The whole air content of No.1 cylinder, so that No.1 cylinder pushes the displacement of No. four axis decline greater than the decrement of No.1 air bag, Blender flexes outward;Meanwhile the intracorporal steam impringement rotation fan of case, rotation fan rotation, and No.1 axis is driven to rotate, pass through one The mutual cooperation of number helical gear, No. two helical gears, No. three helical gears, No. two axis and No. three between centers, so that No. three axis drive No. four Axis rotation, and blender is correspondingly rotated, the blender auxiliary soda ash of rotation is crystallized;Soda ash knot is assisted in blender During crystalline substance, the soda ash crystalline substance paddle of suspension is moved upwards under the action of blender in reaction chamber with certain speed, to soda ash crystalline substance When paddle is higher than reaction chamber height, the soda ash crystal grain of bulky grain or the particle of expectation partial size fall to the bottom of box, bulky grain crystal grain Or cabinet is discharged from discharge port in the particle of expectation partial size, it is expected the soda ash crystalline substance paddle that is raised of particle less than diameter grain is carried secretly, soda ash Paddle liquid constantly follows bad, and soda ash crystal grain constantly increases, and falls to the bottom of box;Meanwhile with the continuous crystallization of soda ash, reaction chamber Overall weight mitigates, and No.1 air bag absorbs the gas in No.1 cylinder, air-breathing expansion, so that reaction chamber is transported to far from cabinet side It is dynamic;Simultaneously as the gas in No.1 cylinder is siphoned away by No.1 air bag, No.1 cylinder drives No. four axis to move upwards, and reacts Case is less than the displacement that No.1 cylinder drives No. four axis to move upwards to the displacement moved far from cabinet side, in fixed pulley Under cooperation, rope pulls No.1 spring to shrink to close to No. four axis sides, since No.1 spring one end is connected in outermost side In framework, the No.1 spring other end is connected on innermost box body, during No.1 spring contraction, so that Pagoda-shaped Blender is shunk to close to No. four axis sides, and the length of blender is shortened by length, and the speed of blender rotation becomes faster, and is increased pair The crystallization of soda ash, so that the crystalline rate of soda ash is improved, soda ash liquid is reduced in reaction chamber, the soda ash crystal grain of crystallization It is collected by collecting board;In the crystallization process of soda ash, by blender lasting contraction and stretching, extension, cooperate soda ash knot Crystalline substance, the gas that soda ash crystallization generates are discharged by gas outlet;Meanwhile with the reduction of soda ash amount in reaction chamber, fixed link is driven Collecting board moves downward, and the pneumatic power source generated in fixed link movement acts on generator, to send out by pneumatic power source Electric power generation, the electric power that generator issues act on motor, so that motor rotates;In motor rotates clockwise, No. two ropes are not Disconnected to be wound by motor output shaft, the dynamic cleaning annulus of No. two rope bands moves upwards, and the cleaning annulus of movement is to reaction chamber interior wall attachment Soda ash crystal grain be purged, when annulus for clearance is reached at the top of reaction chamber, pass through controller and control motor reversal, motor inverse time Needle rotation, No. two ropes being wrapped on motor output shaft unclamp, and cleaning annulus moves downward;By constantly controlling the positive and negative of motor Turn, so that cleaning annulus moves up and down in reaction chamber body, cleaning annulus sufficiently clears up reaction chamber interior wall, thus Improve the cleannes of reaction chamber interior wall.
Preferably, the wire cross sectional of the No.1 spring is rectangle, and wire cross sectional is that the No.1 spring of rectangle cooperates Box body, for improving stability when box body is shunk.The present invention by the way that the wire cross sectional of No.1 spring is set as rectangle, It is moved by the No.1 spring that cross section is rectangle with square frame, on the one hand, improve the intensity of blender;Another party Face improves the stability of blender auxiliary soda ash crystallization.
Preferably, sealing unit is equipped at the No.1 channel;The sealing unit is for avoiding soda ash liquid from entering one At number channel, sealing unit is high temperature resistant elastomeric bladder;The high temperature resistant elastomeric bladder is rectangle capsule, and high temperature resistant elastomeric bladder is along No.1 rope It is symmetrical arranged, high temperature resistant elastomeric bladder is provided with mercury, by mercury expanded by heating, so that high temperature resistant elastomeric bladder is to close to No.1 rope Side expansion, the high temperature resistant elastomeric bladder of expansion seals No.1 rope.In the crystallization of soda ash, soda ash liquid is easy from No.1 channel It enters in No. four axis, influences soda ash crystalline rate;For the present invention by setting sealing unit, sealing unit is high temperature resistant elasticity Capsule, and the built-in full water silver of high temperature resistant elastomeric bladder;On the one hand, due to the continuous crystallization of soda ash, so that the temperature in reaction chamber increases, Mercury expanded by heating in high temperature resistant elastomeric bladder, the two high temperature resistant elastomeric bladders and No.1 rope of expanded by heating are in close contact, and are avoided anti- The soda ash liquid in case is answered to enter No.1 channel, to improve the crystallization effect of soda ash;On the other hand, continuous by blender It is flexible, gas is generated in blender, the gas generated in blender generates compressing to soda ash liquid, soda ash liquid is avoided to enter No.1 Channel, to improve the sealing effect in No.1 channel.
Preferably, No. four axis are equipped with rotating bar;The rotating bar is symmetrical arranged along No.1 rope, and rotating bar one end is hinged On No. four axis, the rotating bar other end is arc-shaped, and the rotating bar other end is contacted with No.1 rope, drives four by No.1 cylinder Number axis rises, and the soda ash crystal grain adhered on No.1 rope outer ring is struck off in the cooperation of two rotating bars.In the crystallization process of soda ash, The soda ash crystal grain of crystallization is liable to stick on No.1 rope, to influence the flexible of No.1 rope;The present invention is led to by setting rotating bar Rotating bar is crossed, in No. four axis move upwards, since two rotation boom ends are contacted with No.1 rope, is generated between rotating bar and No.1 rope Relative motion, and No.1 rope is straightened, the rotating bar of movement strikes off the soda ash adhered on No.1 rope crystallization, to improve No.1 The cleannes of rope;In No. four axis move downward, rotating bar is not acted on No.1 rope generation.
Preferably, the cleaning annulus lateral wall is equipped with cleaning brush, is carried out by cleaning brush to reaction chamber interior wall Cleaning.The present invention clears up reaction chamber interior wall by the cleaning brush of up and down motion by setting cleaning brush, thus Improve the cleannes of reaction chamber interior wall.
Preferably, the cleaning brush is made of No.1 bar, No. two bars and bristle;The No.1 bar and No. two bar one end phases It is mutually hinged, and be hinged on cleaning annulus, No.1 bar and No. two bar other ends are arc-shaped, and No.1 bar and No. two bars pass through Spring is connected on cleaning annulus;The bristle is mounted on No.1 bar and No. two bars, by No.1 bar and No. two bar effects, is made Bristle straighten to reaction chamber interior wall clear up.The present invention by the way that cleaning brush is made of No.1 bar, No. two bars and bristle, When cleaning brush moves upwards, No.1 bar is rotated to close to No. two bar sides, so that the bristle on No. two bars is in reaction chamber Wall is cleared up, and when cleaning brush moves downward, No. two bars are moved to close to No.1 bar side, and No.1 bar is under the action of the spring It resets, the bristle on No.1 bar clears up reaction chamber interior wall;According to the movement that cleaning brush carries out, so that corresponding bristle Reaction chamber interior wall is cleared up, and corresponding bristle is protected, to improve the service life of bristle.
Beneficial effects of the present invention are as follows:
1. a kind of heavy alkali high-efficiency production technology of the present invention, technique one side, by tieing up the temperature of steam It holds at 100-400 DEG C, so that soda ash liquid is adequately crystallized in reaction chamber, to improve the production efficiency of heavy alkali; On the other hand, the steam by temperature at 200-600 DEG C is passed into steam dryer, passes through the phase between steam and steam dryer Mutually cooperation, is dried heavy alkali crystal grain, avoids increase process that heavy alkali crystal grain is dried, shortens technique, To improve heavy alkali production efficiency.
2. a kind of heavy alkali high-efficiency production technology of the present invention, which is closed using the scientific structure of crystallization reactor It is reason, easily operated, it is vdiverse in function, avoid increasing extra power equipment, but using soda ash crystallize in the pneumatic power source that generates, With huge economic benefit and the extensive market demand, it is worthy to be popularized.
3. a kind of heavy alkali high-efficiency production technology of the present invention, which uses crystallization reactor, and fixed link is transported The pneumatic power source generated when dynamic acts on generator, is rotated by generator drive motor, so that cleaning annulus is in reaction chamber It inside moves up and down, cleaning annulus clears up reaction chamber interior wall, avoids the soda ash crystal grain shadow adhered on reaction chamber interior wall Soda ash crystallization is rung, to improve soda ash crystallization effect.
Detailed description of the invention
The present invention will be further explained below with reference to the attached drawings.
Fig. 1 is process flow chart of the invention;
Fig. 2 is the main view of crystallization reactor;
Fig. 3 is the cross-sectional view of crystallization reactor when soda ash liquid is reduced;
Fig. 4 is the partial enlarged view in Fig. 2 at A;
Fig. 5 is the cross-sectional view for clearing up annulus;
In figure: cabinet 1, No.1 air bag 11, spiral steam pipe 12, reaction chamber 13, generator 14, motor 15, driving are single Member 2, shell 21, rotation fan 22,23, No. two axis 24 of No.1 axis, the helical gear 26, three of No.1 helical gear 25, two helical gear 27, No. three axis 28, auxiliary unit 3, No.1 cylinder 31, No. four axis 32, No.1 channel 321, rotating bar 322, fixed pulleys 33, blender 34, No.1 spring 341, box body 342, No.1 rope 35, collector unit 4, fixed column 41, fixed link 42, collecting board 43, sealing are single Member 5, high temperature resistant elastomeric bladder 51, cleaning unit 6, cleaning annulus 61, two ropes 62,631, No. two cleaning brush 63, No.1 bar bars 632, bristle 633.
Specific embodiment
In order to be easy to understand the technical means, the creative features, the aims and the efficiencies achieved by the present invention, tie below Specific embodiment is closed, the present invention is further explained.
As shown in Figures 1 to 5, a kind of heavy alkali high-efficiency production technology of the present invention, the technique the following steps are included:
S1: heating water by heating device, so that water vapor, becomes steam, and makes the vapor (steam) temperature of steam Reach 400 DEG C, gas pressure 0.01-0.6MPa;
S2: on the basis of S1, by cooling down to steam, so that the temperature of steam maintains 100-400 DEG C, gas Pressure is 0.01-0.6MPa;
S3: on the basis of S2, steam dryer being mounted on wall box, and steam dryer is used for heavy alkali crystal grain Drying;
S4: on the basis of S1, S2 and S3, starting crystallization reactor, the crystallization of heavy alkali carried out by crystallization reactor, Ten minutes later to the crystallization of heavy alkali, by temperature at 200-600 DEG C, gas pressure is that the steam of 0.01-0.6MPa is passed into steam In drier, by the mutual cooperation between steam dryer and steam, heavy alkali crystal grain is dried;
The crystallization reactor that the present invention uses includes cabinet 1;Further include driving unit 2, auxiliary unit 3, collector unit 4, Clear up unit 6, No.1 air bag 11, spiral steam pipe 12, reaction chamber 13, generator 14, motor 15 and controller;The control Device is used to control the work of heavy alkali crystallization reactor;1 side wall of cabinet is equipped with steam port and gas outlet, 1 top of cabinet Equipped with inlet, alkali inlet and No.1 hole, 1 bottom symmetrical of cabinet is equipped with discharge port;The spiral steam pipe 12 is fixedly mounted On 1 side wall of cabinet, spiral 12 one end of steam pipe is connected to steam port, and spiral 12 other end of steam pipe is located under No.1 hole Side;The quantity of the No.1 air bag 11 is two, and two No.1 air bags, 11 one end is interconnected, wherein a No.1 air bag 11 is connected in case 1 bottom of body, another No.1 air bag 11 are connected with reaction chamber 13, and 13 uncovered of reaction chamber, reaction chamber 13 is soda ash crystal region;The drive Moving cell 2 is mounted on 1 top of cabinet, and driving unit 2 is oblique including 23, No. two shell 21, rotation fan 22, No.1 axis axis 24, No.1s The helical gear 27 of helical gear 26, three of gear 25, two and No. three axis 28;The shell 21 is connected in 1 top of cabinet;The No.1 23 one end of axis is rotatably installed on 21 inner wall of shell, and 23 other end of No.1 axis and rotation fan 22 are connected, and rotate fan 22 and be located at one At number hole;The No.1 helical gear 25 is set on No.1 axis 23;The quantity of No. two helical gears 26 is two, No. two helical gears 26 are set on No. two 24 outer rings of axis and are connected in No. two 24 ends of axis;24 one end of No. two axis is rotatably installed in shell 21 On, No. two 24 other ends of axis and No. two helical gears 26 are connected, No.1 helical gear 25 and No. two 26 engaged transmissions of helical gear;Described three Number 28 one end of axis is protruded into cabinet 1, and No. three 28 one end of axis and auxiliary unit 3 are connected, and No. three 28 outer rings of axis and 1 contact position of cabinet Rotational installation, No. three 28 other ends of axis are engaged with No. three helical gears 27, No. three helical gears 27 and No. two 26 engaged transmissions of helical gear; The auxiliary unit 3 is located in reaction chamber 13, and for auxiliary unit 3 for assisting soda ash to crystallize, auxiliary unit 3 includes No.1 cylinder 31, No. four axis 32, fixed pulley 33, blender 34 and No.1 rope 35;The No.1 cylinder 31 is connected to two No.1 air bags 11, No.1 31 one end of cylinder is connected with No. three axis 28, and 31 other end of No.1 cylinder and No. four axis 32 are connected, and No. four axis 32 are spliced by two parts It forms, No. four axis 32 form No.1 channel 321 after splicing;The quantity of the fixed pulley 33 is two, and two fixed pulleys 33 are located at No.1 At channel 321, and two fixed pulleys 33 are rotatably installed on No. four axis 32 by shaft;The quantity of the blender 34 is two, Blender 34 is symmetrical arranged along No. four axis 32, and blender 34 is made of No.1 spring 341 and several box bodies 342;Positioned at outermost The framed lid in 342 side of box body of side, is connected on No. four 32 outer rings of axis, between box body 342 positioned at innermost box body 342 It is interconnected, and is slidably connected to each other, form Pagoda-shaped;Described 341 one end of No.1 spring is connected in outermost box body On 342,341 other end of No.1 spring is connected on innermost box body 342;The quantity of the No.1 rope 35 is two, two 1 Number rope 35 one end be connected on No.1 spring 341, two No.1 ropes, 35 other end by hook is connected in 13 bottom of reaction chamber, and Two No.1 ropes 35 are through two fixed pulleys, 33 transition;Steam is passed through from steam port, so that driving unit 2 drives auxiliary unit 3 to rotate, Accelerate soda ash crystallization, meanwhile, the gas with the reduction of soda ash liquid in reaction chamber 13, in 11 inspiration No.1 cylinder 31 of No.1 air bag Body, No.1 cylinder 31 drive No. four axis 32 to rise, and are acted on by fixed pulley 33, No.1 spring 341 and No.1 rope 35, so that stirring Mix the contraction of device 34;The collector unit 4 is fixedly mounted on 1 top of cabinet, and collector unit 4 is symmetrical arranged along No. three axis 28, collects Unit 4 includes fixed column 41, fixed link 42 and collecting board 43 for collecting soda ash crystalline particle, collector unit 4;The fixed column 41 are fixedly mounted on 1 top of cabinet, offer No.1 slot in fixed column 41;Described 42 one end of fixed link is located at No.1 slot, Gu 42 one end of fixed pole is connected in No.1 slot by spring, and 42 other end of fixed link and collecting board 43 are connected;The number of the motor 15 Amount is two, and motor 15 is fixedly mounted in fixed column 41;The quantity of the generator 14 is two, and generator 14 is used to be motor 15 Power source is provided, generator 14 is mounted on 1 top of cabinet, by the way that the gas generated in the movement of fixed link 42 is acted on generator 14, so that the rotation power generation of generator 14;The cleaning unit 6 is mounted on 15 output shaft of motor, and cleaning unit 6 is used for reaction The inner sidewall of case 13 is cleared up, and cleaning unit 6 includes cleaning annulus 61 and No. two ropes 62;The cleaning annulus 61 and reaction chamber The contact of 13 side walls;The quantity of No. two ropes 62 is two, and No. two 62 one end of rope are wrapped on 15 output shaft of motor, No. two ropes 62 The other end and cleaning annulus 61 are connected, and controller are equipped at the top and bottom of reaction chamber 13, using controller for controlling motor 15 Positive and negative rotation, by 14 driving motor 15 of generator rotate so that cleaning annulus 61 move up and down in reaction chamber 13.It will Soda ash is crystallized, and avoids in use and a large amount of alkali dirt occurs, reduces dust collector;There is also a kind of knots in the prior art Brilliant device, still, crystallizer Shortcomings in the prior art, on the one hand, crystallizer in the prior art crystallizes soda ash It is ineffective, and the soda ash crystalline particle after crystallization mixes with soda ash liquid, meanwhile, it cannot adjust according to actual needs to pure The crystallization of lye, to influence the practicability of crystallization;On the other hand, after not to soda ash crystallization, adhere on 13 inner wall of reaction chamber Crystalline particle is cleared up, to influence the crystallization effect of soda ash;The present invention is single by driving unit 2, auxiliary unit 3, cleaning Member 6, collector unit 4, No.1 air bag 11, spiral steam pipe 12, reaction chamber 13, generator 14, motor 15 and controller;One side The multiple utilization to steam is realized in face, makes 22 rotation of rotation fan using steam, so that driving unit 2 drives 3 turns of auxiliary unit It is dynamic, the crystallization of soda ash is assisted by auxiliary unit 3, and soda ash liquid and soda ash crystal grain are separated, avoid soda ash liquid and soda ash knot Brilliant particle mixes, and influences the crystallization of soda ash liquid, to improve soda ash crystallization effect;Meanwhile it being driven by fixed link 42 Collecting board 43 moves up and down, and soda ash crystal grain of soda ash liquid measure when few is collected by collecting board 43, pure after avoiding crystallization Alkali crystal grain is mixed with soda ash liquid, to improve the crystallization effect of soda ash;On the other hand, the gas generated when fixed link 42 being moved Body power source acts on generator 14, is rotated by 14 driving motor 15 of generator, so that cleaning annulus 61 is in reaction chamber 13 It moves up and down, cleaning annulus 61 clears up 13 inner wall of reaction chamber, avoids the soda ash adhered on 13 inner wall of reaction chamber brilliant Grain influences soda ash crystallization, to improve soda ash crystallization effect.
Firstly, steam is passed through from steam port, the steam being passed through is entered in cabinet 1 by spiral steam pipe 12, to After steam is passed through a period of time, at this point, soda ash and water are entered in reaction chamber 13 from alkali inlet and inlet respectively, with pure Alkali and the continuous of water are passed through, and the overall weight of reaction chamber 13 becomes weight, and reaction chamber 13 squeezes No.1 air bag 11, and No.1 air bag 11 is by crowded Outer air-blowing is pressed to, the gas of bulging transfers to No.1 cylinder 31, and No.1 cylinder 31 pushes No. four axis 32 to move downward, due to No.1 gas The whole air content of capsule 11 is greater than the whole air content of No.1 cylinder 31, so that No.1 cylinder 31 pushes the position of No. four axis 32 decline Shifting amount is greater than the decrement of No.1 air bag 11, and blender 34 flexes outward;Meanwhile the steam impringement rotation fan 22 in cabinet 1, turn Dynamic 22 rotation of fan, and No.1 axis 23 is driven to rotate, pass through the helical gear 26, three helical gear 27, two of No.1 helical gear 25, two Mutual cooperation between axis 24 and No. three axis 28, so that No. three axis 28 drive No. four axis 32 to rotate, and blender 34 carries out accordingly The blender 34 of rotation, rotation assists soda ash to be crystallized;It is assisted in soda ash crystallization process in blender 34, the soda ash of suspension is brilliant Paddle is moved upwards under the action of blender 34 in reaction chamber 13 with certain speed, is higher than 13 height of reaction chamber to soda ash crystalline substance paddle When, the soda ash crystal grain of bulky grain or the particle of expectation partial size fall to 1 bottom of cabinet, bulky grain crystal grain or the particle for it is expected partial size Cabinet 1 is discharged from discharge port, it is expected the soda ash crystalline substance paddle that is raised of particle less than diameter grain is carried secretly, soda ash paddle liquid constantly follow it is bad, it is pure Alkali crystal grain constantly increases, and falls to 1 bottom of cabinet;Meanwhile with the continuous crystallization of soda ash, the overall weight of reaction chamber 13 subtracts Gently, No.1 air bag 11 absorbs the gas in No.1 cylinder 31, air-breathing expansion, so that reaction chamber 13 is moved to far from 1 side of cabinet; Simultaneously as the gas in No.1 cylinder 31 is siphoned away by No.1 air bag 11, No.1 cylinder 31 drives No. four axis 32 to move upwards, and Reaction chamber 13 is less than the displacement that No.1 cylinder 31 drives No. four axis 32 to move upwards to the displacement moved far from 1 side of cabinet Amount, under the cooperation of fixed pulley 33, rope pulls No.1 spring 341 to shrink to close to No. four 32 sides of axis, due to No.1 spring 341 one end are connected on outermost box body 342, and 341 other end of No.1 spring is connected on innermost box body 342, In 341 contraction process of No.1 spring, so that the blender 34 of Pagoda-shaped is shunk to close to No. four 32 sides of axis, blender 34 Length is shortened by length, and the speed that blender 34 rotates becomes faster, and increases the crystallization to soda ash, to improve the crystallization effect of soda ash Rate, soda ash liquid is reduced in reaction chamber 13, the soda ash crystal grain of crystallization is collected by collecting board 43;In the knot of soda ash During crystalline substance, by blender 34 lasting contraction and stretching, extension, cooperate soda ash crystallization, the gas that soda ash crystallization generates passes through outlet Mouth discharge;Meanwhile with the reduction of soda ash amount in reaction chamber 13, fixed link 42 drives collecting board 43 to move downward, fixed link 42 The pneumatic power source generated in movement acts on generator 14, by pneumatic power source generator 14 is generated electricity, generator 14 The electric power of sending acts on motor 15, so that motor 15 rotates;In motor 15 rotates clockwise, No. two ropes 62 are constantly by motor The winding of 15 output shafts, No. two ropes 62 drive cleaning annulus 61 to move upwards, and the cleaning annulus 61 of movement is attached to 13 inner wall of reaction chamber Soda ash crystal grain be purged, when annulus 61 for clearance reaches 13 top of reaction chamber, motor 15 is controlled by controller and is inverted, Motor 15 rotates counterclockwise, and No. two ropes 62 being wrapped on 15 output shaft of motor unclamp, and cleaning annulus 61 moves downward;By not The positive and negative rotation of disconnected control motor 15 clears up annulus 61 to anti-so that cleaning annulus 61 moves up and down in 13 body 1 of reaction chamber 13 inner wall of case is answered sufficiently to be cleared up, to improve the cleannes of 13 inner wall of reaction chamber.
As one embodiment of the present invention, the wire cross sectional of the No.1 spring 341 is rectangle, wire cross sectional Cooperate box body 342 for the No.1 spring 341 of rectangle, for improving stability when box body 342 is shunk.The present invention pass through by The wire cross sectional of No.1 spring 341 is set as rectangle, is transported by the No.1 spring 341 that cross section is rectangle with square frame It is dynamic, on the one hand, to improve the intensity of blender 34;On the other hand, the stability that blender 34 assists soda ash crystallization is improved.
As one embodiment of the present invention, sealing unit 5 is equipped at the No.1 channel 321;The sealing unit 5 For avoiding soda ash liquid from entering at No.1 channel 321, sealing unit 5 is high temperature resistant elastomeric bladder 51;The high temperature resistant elastomeric bladder 51 be rectangle capsule, and high temperature resistant elastomeric bladder 51 is symmetrical arranged along No.1 rope 35, and high temperature resistant elastomeric bladder 51 is provided with mercury, passes through mercury Expanded by heating, so that high temperature resistant elastomeric bladder 51 is expanded to the side close to No.1 rope 35, the high temperature resistant elastomeric bladder 51 of expansion is to one Number rope 35 sealing.In the crystallization of soda ash, soda ash liquid is easy to enter in No. four axis 32 from No.1 channel 321, influences soda ash knot Brilliant efficiency;The present invention is by setting sealing unit 5, and sealing unit 5 is high temperature resistant elastomeric bladder 51, and high temperature resistant elastomeric bladder 51 is built-in Full water silver;On the one hand, due to the continuous crystallization of soda ash, so that the temperature in reaction chamber 13 increases, in high temperature resistant elastomeric bladder 51 Mercury expanded by heating, two high temperature resistant elastomeric bladders 51 and the No.1 rope 35 of expanded by heating are in close contact, avoid pure in reaction chamber 13 Lye enters No.1 channel 321, to improve the crystallization effect of soda ash;It is on the other hand, constantly flexible by blender 34, Gas is generated in blender 34, the gas generated in blender 34 generates compressing to soda ash liquid, soda ash liquid is avoided to enter No.1 Channel 321, to improve the sealing effect in No.1 channel 321.
As one embodiment of the present invention, No. four axis 32 are equipped with rotating bar 322;The rotating bar 322 is along one Number rope 35 is symmetrical arranged, and 322 one end of rotating bar is hinged on No. four axis 32, and 322 other end of rotating bar is arc-shaped, and rotating bar 322 other ends are contacted with No.1 rope 35, drive No. four axis 32 to rise by No.1 cylinder 31, two rotating bars 322 cooperate to No.1 The soda ash crystal grain adhered on 35 outer rings of restricting is struck off.In the crystallization process of soda ash, the soda ash crystal grain of crystallization is liable to stick to On No.1 rope 35, to influence the flexible of No.1 rope 35;The present invention is by setting rotating bar 322, by rotating bar 322, four Number axis 32, since two rotating bars, 322 end is contacted with No.1 rope 35, generates in moving upwards between rotating bar 322 and No.1 rope 35 Relative motion, and No.1 rope 35 is straightened, the rotating bar 322 of movement strikes off the soda ash adhered on No.1 rope 35 crystallization, to mention The high cleannes of No.1 rope 35;In No. four axis 32 move downward, rotating bar 322 is not acted on 35 generation of No.1 rope.
As one embodiment of the present invention, 61 lateral wall of cleaning annulus is equipped with cleaning brush 63, by clear Reason hairbrush 63 clears up 13 inner wall of reaction chamber.The present invention passes through the cleaning hair of up and down motion by setting cleaning brush 63 Brush 63, clears up 13 inner wall of reaction chamber, to improve the cleannes of 13 inner wall of reaction chamber.
As one embodiment of the present invention, the cleaning brush 63 is by 631, No. two bars 632 of No.1 bar and bristle 633 Composition;The No.1 bar 631 and No. two 632 one end of bar are hinged, and are hinged on cleaning annulus 61, No.1 bar 631 and two Number 632 other end of bar is arc-shaped, and No.1 bar 631 and No. two bars 632 are connected in by spring and are cleared up on annulus 61;It is described Bristle 633 is mounted on No.1 bar 631 and No. two bars 632, is acted on by No.1 bar 631 and No. two bars 632, so that bristle 633 It straightens and 13 inner wall of reaction chamber is cleared up.The present invention by by cleaning brush 63 by No.1 bar 631, No. two bars 632 and bristles 633 compositions, when cleaning brush 63 moves upwards, No.1 bar 631 is rotated to close to No. two 632 sides of bar, so that No. two bars 632 On bristle 633 13 inner wall of reaction chamber is cleared up, when cleaning brush 63 moves downward, No. two bars 632 are to close to No.1 The movement of 631 side of bar, No.1 bar 631 resets under the action of the spring, the bristle 633 on No.1 bar 631 to 13 inner wall of reaction chamber into Row cleaning;According to the movement that cleaning brush 63 carries out, so that corresponding bristle 633 clears up 13 inner wall of reaction chamber, and it is right The bristle 633 answered is protected, to improve the service life of bristle 633.
In use, the steam being passed through is by spirally steaming firstly, temperature is passed through in 100-400 DEG C of steam from steam port Steam pipe 12 enters in cabinet 1, after steam is passed through a period of time, at this point, by soda ash and water respectively from alkali inlet and inlet It enters in reaction chamber 13, as soda ash and the continuous of water are passed through, the overall weight of reaction chamber 13 becomes weight, and reaction chamber 13 squeezes one Number air bag 11, No.1 air bag 11 are squeezed outside air-blowing, and the gas of bulging transfers to No.1 cylinder 31, and No.1 cylinder 31 pushes No. four Axis 32 moves downward, since the whole air content of No.1 air bag 11 is greater than the whole air content of No.1 cylinder 31, so that No.1 gas Cylinder 31 pushes the displacement of No. four axis 32 decline greater than the decrement of No.1 air bag 11, and blender 34 flexes outward;Meanwhile cabinet Steam impringement rotation in 1 fans 22, and rotation fan 22 rotates, and No.1 axis 23 is driven to rotate, oblique by No.1 helical gear 25, two Mutual cooperation between the axis 24 of helical gear 27, two of gear 26, three and No. three axis 28, so that No. three axis 28 drive No. four 32 turns of axis It is dynamic, and blender 34 is correspondingly rotated, the blender 34 of rotation assists soda ash to be crystallized;Soda ash is assisted in blender 34 In crystallization process, the soda ash crystalline substance paddle of suspension is moved upwards under the action of blender 34 in reaction chamber 13 with certain speed, to When soda ash crystalline substance paddle is higher than 13 height of reaction chamber, the soda ash crystal grain of bulky grain or the particle of expectation partial size fall to 1 bottom of cabinet, greatly Grain it is expected that cabinet 1 is discharged from discharge port in the particle of partial size, less than the soda ash crystalline substance paddle that is raised of particle of desired diameter grain Entrainment, soda ash paddle liquid constantly follow bad, and soda ash crystal grain constantly increases, and falls to 1 bottom of cabinet;Meanwhile with the continuous knot of soda ash The overall weight of crystalline substance, reaction chamber 13 mitigates, and No.1 air bag 11 absorbs the gas in No.1 cylinder 31, air-breathing expansion, so that reaction Case 13 is moved to far from 1 side of cabinet;Simultaneously as the gas in No.1 cylinder 31 is siphoned away by No.1 air bag 11, No.1 cylinder 31 No. four axis 32 of drive move upwards, and reaction chamber 13 is less than 31 band of No.1 cylinder to the displacement moved far from 1 side of cabinet The displacement that dynamic No. four axis 32 move upwards, under the cooperation of fixed pulley 33, rope pulls No.1 spring 341 to close to No. four axis 32 sides are shunk, and since 341 one end of No.1 spring is connected on outermost box body 342,341 other end of No.1 spring is connected On innermost box body 342, in 341 contraction process of No.1 spring, so that the blender 34 of Pagoda-shaped is to close to No. four 32 side of axis is shunk, and the length of blender 34 is shortened by length, and the speed that blender 34 rotates becomes faster, and increases the knot to soda ash Crystalline substance, to improve the crystalline rate of soda ash, soda ash liquid is reduced in reaction chamber 13, the soda ash crystal grain of crystallization passes through receipts Collection plate 43 is collected;In the crystallization process of soda ash, by blender 34 lasting contraction and stretching, extension, cooperate soda ash crystallization, The gas that soda ash crystallization generates is discharged by gas outlet;Meanwhile with the reduction of soda ash amount in reaction chamber 13, fixed link 42 is driven Collecting board 43 moves downward, and the pneumatic power source generated in the movement of fixed link 42 acts on generator 14, passes through pneumatic power source So that generator 14 generates electricity, the electric power that generator 14 issues acts on motor 15, so that motor 15 rotates;When motor 15 is clockwise In rotation, No. two rope 62 constantly by 15 output shaft of motor wind, No. two rope 62 drive cleaning annulus 61 move upwards, movement it is clear The soda ash crystal grain that reason annulus 61 adheres to 13 inner wall of reaction chamber is purged, when annulus 61 for clearance reaches 13 top of reaction chamber, Motor 15 being controlled by controller to invert, motor 15 rotates counterclockwise, and No. two ropes 62 being wrapped on 15 output shaft of motor unclamp, Cleaning annulus 61 moves downward;By constantly controlling the positive and negative rotation of motor 15 so that cleaning annulus 61 in 13 body 1 of reaction chamber into Row moves up and down, and cleaning annulus 61 sufficiently clears up 13 inner wall of reaction chamber, to improve the cleaning of 13 inner wall of reaction chamber Degree;Meanwhile the steam by temperature at 200-600 DEG C is passed into steam dryer, is cooperated by steam and steam dryer, it is right Heavy alkali crystal grain is dried.
Above-mentioned front, back, left, right, up, down is mark according to personage's observation visual angle on the basis of Fig. 2 in Figure of description Standard, device surface are defined as a left side on the left of observer to before being defined as on one side of observer, and so on.
In the description of the present invention, it is to be understood that, term " center ", " longitudinal direction ", " transverse direction ", "front", "rear", The orientation or positional relationship of the instructions such as "left", "right", "vertical", "horizontal", "top", "bottom" "inner", "outside" is based on attached drawing institute The orientation or positional relationship shown, is merely for convenience of description of the present invention and simplification of the description, rather than the dress of indication or suggestion meaning It sets or element must have a particular orientation, be constructed and operated in a specific orientation, therefore should not be understood as protecting the present invention The limitation of range.
Finally it is noted that the above embodiments are merely illustrative of the technical solutions of the present invention, rather than its limitations.To the greatest extent Present invention has been described in detail with reference to the aforementioned embodiments for pipe, those skilled in the art should understand that: it is still It is possible to modify the technical solutions described in the foregoing embodiments, or part of technical characteristic is equally replaced It changes;And these are modified or replaceed, the essence for technical solution of various embodiments of the present invention that it does not separate the essence of the corresponding technical solution Mind and range.Every other embodiment obtained by those of ordinary skill in the art without making creative efforts, It shall fall within the protection scope of the present invention.

Claims (6)

1. a kind of heavy alkali high-efficiency production technology, it is characterised in that: the technique the following steps are included:
S1: heating water by heating device, so that water vapor, becomes steam, and the vapor (steam) temperature of steam is reached 400 DEG C, gas pressure 0.01-0.6MPa;
S2: on the basis of S1, by cooling down to steam, so that the temperature of steam maintains 100-400 DEG C, gas pressure For 0.01-0.6MPa;
S3: on the basis of S2, steam dryer being mounted on wall box, and steam dryer is for the dry of heavy alkali crystal grain It is dry;
S4: on the basis of S1, S2 and S3, start crystallization reactor, the crystallization of heavy alkali is carried out by crystallization reactor, to weight Matter alkali crystallizes ten minutes later, and by temperature at 200-600 DEG C, gas pressure is that the steam of 0.01-0.6MPa is passed into steam drying In device, by the mutual cooperation between steam dryer and steam, heavy alkali crystal grain is dried;
The crystallization reactor that the present invention uses includes cabinet (1);It further include driving unit (2), auxiliary unit (3), collector unit (4), unit (6), No.1 air bag (11), spiral steam pipe (12), reaction chamber (13), generator (14), motor (15) are cleared up And controller;The controller is used to control the work of heavy alkali crystallization apparatus;Cabinet (1) side wall be equipped with steam port and Gas outlet, cabinet (1) top are equipped with inlet, alkali inlet and No.1 hole, and cabinet (1) bottom symmetrical is equipped with discharge port;The spiral shell Rotating steam pipe (12) is fixedly mounted on cabinet (1) side wall, and spiral steam pipe (12) one end is connected to steam port, spirally Steam pipe (12) other end is located at below No.1 hole;The quantity of the No.1 air bag (11) is two, two No.1 air bag (11) one end It is interconnected, wherein a No.1 air bag (11) is connected in cabinet (1) bottom, another No.1 air bag (11) and reaction chamber (13) are solid Even, reaction chamber (13) uncovered, reaction chamber (13) are soda ash crystal region;The driving unit (2) is mounted at the top of cabinet (1), drives Moving cell (2) include shell (21), rotation fan (22), No.1 axis (23), No. two axis (24), No.1 helical gear (25), No. two tiltedly Gear (26), No. three helical gears (27) and No. three axis (28);The shell (21) is connected at the top of cabinet (1);The No.1 axis (23) one end is rotatably installed on shell (21) inner wall, and No.1 axis (23) other end and rotation fan (22) are connected, and rotate fan (22) it is located at No.1 hole;The No.1 helical gear (25) is set on No.1 axis (23);The number of No. two helical gears (26) Amount is two, and No. two helical gears (26) are set on No. two axis (24) outer rings and are connected in No. two axis (24) ends;No. two axis (24) one end is rotatably installed on shell (21), and No. two axis (24) other ends and No. two helical gears (26) are connected, No.1 helical gear (25) and No. two helical gears (26) engaged transmission;Described No. three axis (28) one end is protruded into cabinet (1), No. three axis (28) one end with Auxiliary unit (3) is connected, and No. three axis (28) outer rings and cabinet (1) contact position are rotatablely installed, No. three axis (28) other ends and three The engagement of number helical gear (27), No. three helical gears (27) and No. two helical gears (26) engaged transmissions;The auxiliary unit (3) is located at anti- It answers in case (13), for auxiliary unit (3) for assisting soda ash to crystallize, auxiliary unit (3) includes No.1 cylinder (31), No. four axis (32), fixed pulley (33), blender (34) and No.1 rope (35);The No.1 cylinder (31) is connected to two No.1 air bags (11), No.1 cylinder (31) one end is connected with No. three axis (28), and No.1 cylinder (31) other end and No. four axis (32) are connected, No. four axis (32) it is spliced by two parts, forms No.1 channel (321) after No. four axis (32) splicings;The quantity of the fixed pulley (33) is Two, two fixed pulleys (33) are located at No.1 channel (321), and two fixed pulleys (33) are rotatably installed in No. four axis by shaft (32) on;The quantity of the blender (34) is two, and blender (34) is symmetrical arranged along No. four axis (32), and blender (34) is by one Number spring (341) and several box bodies (342) composition;The framed lid in box body (342) side on the outermost side is located at most inner side Box body (342) be connected on No. four axis (32) outer rings, be interconnected, and be slidably connected between box body (342) to each other, shape At Pagoda-shaped;Described No.1 spring (341) one end is connected on outermost box body (342), No.1 spring (341) other end It is connected on innermost box body (342);The quantity of the No.1 rope (35) is two, and two No.1 rope (35) one end are connected in On No.1 spring (341), two No.1 rope (35) other ends are connected in reaction chamber (13) bottom, and two No.1 ropes (35) by hook Through two fixed pulleys (33) transition;Steam is passed through from steam port, so that driving unit (2) driving auxiliary unit (3) rotation, accelerates Soda ash crystallization, meanwhile, the gas with the reduction of the interior soda ash liquid of reaction chamber (13), in No.1 air bag (11) inspiration No.1 cylinder (31) Body, No.1 cylinder (31) drive No. four axis (32) to rise, and pass through fixed pulley (33), No.1 spring (341) and No.1 rope (35) Effect, so that blender (34) is shunk;The collector unit (4) is fixedly mounted at the top of cabinet (1), and collector unit (4) is along three Number axis (28) is symmetrical arranged, and for collector unit (4) for collecting soda ash crystalline particle, collector unit (4) includes fixed column (41), solid Fixed pole (42) and collecting board (43);The fixed column (41) is fixedly mounted at the top of cabinet (1), and fixed column offers one on (41) Number slot;Described fixed link (42) one end is located at No.1 slot, and fixed link (42) one end is connected in No.1 slot by spring, fixed Bar (42) other end and collecting board (43) are connected;The quantity of the motor (15) is two, and motor (15) is fixedly mounted on fixed column (41) on;The quantity of the generator (14) is two, and generator (14) is used to provide power source, generator (14) for motor (15) It is mounted at the top of cabinet (1), by the way that the gas generated in fixed link (42) movement is acted on generator (14), so that generator (14) rotation power generation;The cleaning unit (6) is mounted on motor (15) output shaft, and cleaning unit (6) is used for reaction chamber (13) inner sidewall is cleared up, and cleaning unit (6) includes cleaning annulus (61) and No. two ropes (62);The cleaning annulus (61) It is contacted with reaction chamber (13) side wall;The quantity of No. two ropes (62) is two, and No. two rope (62) one end are wrapped in motor (15) On output shaft, No. two rope (62) other ends and cleaning annulus (61) are connected, and controller, benefit are equipped at the top and bottom of reaction chamber (13) It is used to control the positive and negative rotation of motor (15) with controller, is rotated by generator (14) driving motor (15), so that cleaning annulus (61) it moves up and down in reaction chamber (13).
2. a kind of heavy alkali high-efficiency production technology according to claim 1, it is characterised in that: the No.1 spring (341) Wire cross sectional be rectangle, wire cross sectional be rectangle No.1 spring (341) cooperate box body (342), for the side of raising Stability when framework (342) is shunk.
3. a kind of heavy alkali high-efficiency production technology according to claim 1, it is characterised in that: the No.1 channel (321) Place is equipped with sealing unit (5);The sealing unit (5) is for avoiding soda ash liquid from entering at No.1 channel (321), sealing unit (5) it is high temperature resistant elastomeric bladder (51);The high temperature resistant elastomeric bladder (51) is rectangle capsule, and high temperature resistant elastomeric bladder (51) is along No.1 rope (35) it is symmetrical arranged, high temperature resistant elastomeric bladder (51) is provided with mercury, by mercury expanded by heating, so that high temperature resistant elastomeric bladder (51) It is expanded to the side close to No.1 rope (35), the high temperature resistant elastomeric bladder (51) of expansion seals No.1 rope (35).
4. a kind of heavy alkali high-efficiency production technology according to claim 1, it is characterised in that: No. four axis (32) are equipped with Rotating bar (322);The rotating bar (322) is symmetrical arranged along No.1 rope (35), and rotating bar (322) one end is hinged on No. four axis (32) on, rotating bar (322) other end is arc-shaped, and rotating bar (322) other end is contacted with No.1 rope (35), passes through No.1 Cylinder (31) drives No. four axis (32) to rise, and two rotating bars (322) cooperate to the soda ash crystal grain adhered on No.1 rope (35) outer ring It is struck off.
5. a kind of heavy alkali high-efficiency production technology according to claim 1, it is characterised in that: the cleaning annulus (61) is outside Side wall is equipped with cleaning brush (63), is cleared up by cleaning brush (63) reaction chamber (13) inner wall.
6. a kind of heavy alkali high-efficiency production technology according to claim 5, it is characterised in that: the cleaning brush (63) by No.1 bar (631), No. two bars (632) and bristle (633) composition;The No.1 bar (631) and No. two bar (632) one end are mutually cut with scissors It connects, and is hinged in cleaning annulus (61), No.1 bar (631) and No. two bar (632) other ends are arc-shaped, and No.1 bar (631) it is connected in cleaning annulus (61) by spring with No. two bars (632);The bristle (633) is mounted on No.1 bar (631) and on No. two bars (632), by No.1 bar (631) and No. two bar (632) effects, so that bristle (633) is straightened to reaction Case (13) inner wall is cleared up.
CN201811527919.0A 2018-12-13 2018-12-13 A kind of heavy alkali high-efficiency production technology Withdrawn CN109694093A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110354786A (en) * 2019-07-31 2019-10-22 北京鼎翰科技有限公司 A kind of water treatment agent process units with organic exhaust gas detection function

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SU1637823A1 (en) * 1988-11-09 1991-03-30 Предприятие П/Я Р-6273 Crystallizer
SU845311A1 (en) * 1980-02-18 1995-02-20 Дзержинский филиал Научно-исследовательского и конструкторского института химического машиностроения Apparatus for obtaining scaly product from melt
CN104073418A (en) * 2014-06-27 2014-10-01 北京鼎盛泰来科贸有限公司 Alkali treatment device
CN104445288A (en) * 2014-12-02 2015-03-25 成都华西堂投资有限公司 Sodium hydrogen carbonate reaction crystallizer
CN204319821U (en) * 2014-12-02 2015-05-13 成都华西堂投资有限公司 A kind of sodium acid carbonate crystallizer containing central tube
CN205391791U (en) * 2016-02-24 2016-07-27 福建万科药业有限公司 Air agitation formula crystallization kettle
CN205699547U (en) * 2016-06-13 2016-11-23 信丰正天伟电子科技有限公司 A kind of backflow crystallization prevention device
CN208031959U (en) * 2018-02-28 2018-11-02 杨娜 A kind of traditional Chinese medicine extraction crystallization apparatus

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SU845311A1 (en) * 1980-02-18 1995-02-20 Дзержинский филиал Научно-исследовательского и конструкторского института химического машиностроения Apparatus for obtaining scaly product from melt
SU1637823A1 (en) * 1988-11-09 1991-03-30 Предприятие П/Я Р-6273 Crystallizer
CN104073418A (en) * 2014-06-27 2014-10-01 北京鼎盛泰来科贸有限公司 Alkali treatment device
CN104445288A (en) * 2014-12-02 2015-03-25 成都华西堂投资有限公司 Sodium hydrogen carbonate reaction crystallizer
CN204319821U (en) * 2014-12-02 2015-05-13 成都华西堂投资有限公司 A kind of sodium acid carbonate crystallizer containing central tube
CN205391791U (en) * 2016-02-24 2016-07-27 福建万科药业有限公司 Air agitation formula crystallization kettle
CN205699547U (en) * 2016-06-13 2016-11-23 信丰正天伟电子科技有限公司 A kind of backflow crystallization prevention device
CN208031959U (en) * 2018-02-28 2018-11-02 杨娜 A kind of traditional Chinese medicine extraction crystallization apparatus

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110354786A (en) * 2019-07-31 2019-10-22 北京鼎翰科技有限公司 A kind of water treatment agent process units with organic exhaust gas detection function

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