CN109694093A - A kind of heavy alkali high-efficiency production technology - Google Patents
A kind of heavy alkali high-efficiency production technology Download PDFInfo
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- CN109694093A CN109694093A CN201811527919.0A CN201811527919A CN109694093A CN 109694093 A CN109694093 A CN 109694093A CN 201811527919 A CN201811527919 A CN 201811527919A CN 109694093 A CN109694093 A CN 109694093A
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D7/00—Carbonates of sodium, potassium or alkali metals in general
- C01D7/22—Purification
- C01D7/24—Crystallisation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D9/0059—General arrangements of crystallisation plant, e.g. flow sheets
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D9/0063—Control or regulation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/0066—Stirrers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B08—CLEANING
- B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
- B08B9/00—Cleaning hollow articles by methods or apparatus specially adapted thereto
- B08B9/08—Cleaning containers, e.g. tanks
- B08B9/087—Cleaning containers, e.g. tanks by methods involving the use of tools, e.g. brushes, scrapers
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D7/00—Carbonates of sodium, potassium or alkali metals in general
- C01D7/22—Purification
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D2009/0086—Processes or apparatus therefor
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Inorganic Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Mechanical Engineering (AREA)
- Processing Of Solid Wastes (AREA)
Abstract
The invention belongs to heavy alkali production technical field, specifically a kind of heavy alkali high-efficiency production technology, the technique uses crystallization reactor, including cabinet;It further include driving unit, auxiliary unit, collector unit, cleaning unit, No.1 air bag, spiral steam pipe, reaction chamber, generator, motor and controller.Technique one side, by the way that the temperature of steam is maintained 100-400 DEG C, so that soda ash liquid is adequately crystallized in reaction chamber, to improve the production efficiency of heavy alkali;On the other hand, the steam by temperature at 200-600 DEG C is passed into steam dryer, passes through the mutual cooperation between steam and steam dryer, heavy alkali crystal grain is dried, it avoids increase process that heavy alkali crystal grain is dried, technique is shortened, to improve heavy alkali production efficiency.
Description
Technical field
The invention belongs to heavy alkali production technical field, specifically a kind of heavy alkali high-efficiency production technology.
Background technique
Heavy soda ash is divided into common heavy soda ash and high-quality dense soda ash with the superiority and inferiority of chemical analysis, with physical property difference
(referring mainly to severe) is divided into common heavy soda ash and super heavy soda ash, and heavy soda ash is compared with light soda ash, heavy soda ash due to
Its severe is big, therefore packaging material saves, and transport, storage cost are low, and in use, alkali dirt is not easy to fly upward, and significantly reduces
Dust collector and environmental pollution, if chemical analysis enters high-quality dense soda ash class, moreover it is possible to mitigate equipment corrosion, increase equipment
Exchange capability of heat and receive praises from customers.
In the production of existing heavy alkali, need it is subsequent the heavy alkali crystal grain produced is dried, increase work
Skill process;So that the technical solution is restricted.
Summary of the invention
In order to make up for the deficiencies of the prior art, it solves the problems, such as subsequent heavy alkali crystal grain to be dried;The present invention proposes
A kind of heavy alkali high-efficiency production technology.
The technical solution adopted by the present invention to solve the technical problems is: a kind of heavy alkali high-efficiency production of the present invention
Technique, the technique the following steps are included:
S1: heating water by heating device, so that water vapor, becomes steam, and makes the vapor (steam) temperature of steam
Reach 400 DEG C, gas pressure 0.01-0.6MPa;
S2: on the basis of S1, by cooling down to steam, so that the temperature of steam maintains 100-400 DEG C, gas
Pressure is 0.01-0.6MPa;
S3: on the basis of S2, steam dryer being mounted on wall box, and steam dryer is used for heavy alkali crystal grain
Drying;
S4: on the basis of S1, S2 and S3, starting crystallization reactor, the crystallization of heavy alkali carried out by crystallization reactor,
Ten minutes later to the crystallization of heavy alkali, by temperature at 200-600 DEG C, gas pressure is that the steam of 0.01-0.6MPa is passed into steam
In drier, by the mutual cooperation between steam dryer and steam, heavy alkali crystal grain is dried;
The crystallization reactor that the present invention uses includes cabinet;It further include driving unit, auxiliary unit, collector unit, cleaning
Unit, No.1 air bag, spiral steam pipe, reaction chamber, generator, motor and controller;The controller is for controlling heavy
The work of alkali crystallization reactor;The wall box is equipped with steam port and gas outlet, and top of the box is equipped with inlet, alkali inlet
With No.1 hole, the bottom of box is symmetrically arranged with discharge port;The spiral steam pipe is fixedly mounted on wall box, spiral to steam
Steam pipe one end is connected to steam port, and the spiral steam pipe other end is located at below No.1 hole;The quantity of the No.1 air bag is two,
Two No.1 air bag one end are interconnected, wherein a No.1 air bag is connected in the bottom of box, another No.1 air bag and reaction chamber are connected,
Reaction chamber uncovered, reaction chamber are soda ash crystal region;The driving unit is mounted on top of the box, and driving unit includes shell, turns
Dynamic fan, No.1 axis, No. two axis, No.1 helical gear, No. two helical gears, No. three helical gears and No. three axis;The shell is connected in case
At the top of body;In the rotational installation on the inner wall of the housing of No.1 axis one end, the No.1 axis other end and rotation fan are connected, and rotate fan position
At No.1 hole;The No.1 helical gear is set on No.1 axis;No. two helical gear quantity is two, No. two helical teeth wheel cases
It is located on No. two axis outer rings and is connected in No. two shaft ends portion;Described No. two axis one end are rotatably installed on shell, and No. two axis are another
End is connected with No. two helical gears, No.1 helical gear and No. two helical gear engaged transmissions;Described No. three axis one end are protruded into cabinet, and three
Number axis one end and auxiliary unit are connected, and No. three axis outer rings and cabinet contact position are rotatablely installed, and No. three axis other ends are oblique with No. three
Gear engagement, No. three helical gears and No. two helical gear engaged transmissions;The auxiliary unit is located in reaction chamber, and auxiliary unit is used for
Soda ash crystallization is assisted, auxiliary unit includes No.1 cylinder, No. four axis, fixed pulley, blender and No.1 rope;The No.1 cylinder with
The connection of two No.1 air bags, No.1 cylinder one end are connected with No. three axis, and the No.1 cylinder other end and No. four axis are connected, and No. four axis are by two
Part is spliced, and forms No.1 channel after No. four axis splicings;The quantity of the fixed pulley is two, and two fixed pulleys are located at one number service
At road, and two fixed pulleys pass through shaft and are rotatably installed on No. four axis;The quantity of the blender is two, and blender is along No. four
Axial symmetry setting, blender are made of No.1 spring and several box bodies;The framed lid in box body on the outermost side side, is located at
Innermost box body is connected on No. four axis outer rings, is interconnected between box body, and be slidably connected to each other, and pagoda is formed
Shape;The No.1 spring one end is connected on outermost box body, and the No.1 spring other end is connected in innermost box body
On;The quantity of the No.1 rope is two, and two No.1 rope one end are connected on No.1 spring, and the two No.1 rope other ends pass through hook
It is connected in reaction chamber bottom, and two No.1 ropes are through two fixed pulley transition;Steam is passed through from steam port, so that driving unit drives
Soda ash crystallization is accelerated in auxiliary unit rotation, meanwhile, with the reduction of soda ash liquid in reaction chamber, No.1 air bag inspiration No.1 cylinder
Interior gas, No.1 cylinder drive No. four axis to rise, and by fixed pulley, No.1 spring and the effect of No.1 rope, so that blender
It shrinks;The collector unit is fixedly mounted on top of the box, and collector unit is arranged along No. three axial symmetry, and collector unit is for collecting
Soda ash crystalline particle, collector unit include fixed column, fixed link and collecting board;The fixed column is fixedly mounted on top of the box,
No.1 slot is offered in fixed column;Described fixed link one end is located at No.1 slot, and fixed link one end is connected in No.1 by spring
In slot, the fixed link other end and collecting board are connected;The quantity of the motor is two, and motor is fixedly mounted in fixed column;It is described
The quantity of generator is two, and generator is used to for motor provide power source, and generator is mounted on top of the box, by by fixed link
The gas generated in movement acts on generator, so that generator rotation power generation;The cleaning unit is mounted on motor output shaft
On, for cleaning unit for clearing up the inner sidewall of reaction chamber, cleaning unit includes cleaning annulus and No. two ropes;The cleaning
Annulus is contacted with reaction chamber side wall;The quantity of No. two ropes is two, and No. two rope one end are wrapped on motor output shaft, No. two
The other end of restricting is connected with cleaning annulus, and controller is equipped at the top and bottom of reaction chamber, is used to control motor just using controller
Reversion, is rotated by generator drive motor, so that cleaning annulus moves up and down in reaction chamber.Soda ash is tied
Crystalline substance avoids in use and a large amount of alkali dirt occurs, reduces dust collector;There is also a kind of crystallizers in the prior art, still,
Crystallizer Shortcomings in the prior art, on the one hand, crystallizer in the prior art soda ash is crystallized it is ineffective, and
Soda ash crystalline particle after crystallization mixes with soda ash liquid, meanwhile, the crystallization to soda ash liquid cannot be adjusted according to actual needs,
To influence the practicability of crystallization;On the other hand, it after not to soda ash crystallization, reacts the crystalline particle adhered on chamber interior wall and carries out clearly
Reason, to influence the crystallization effect of soda ash;The present invention passes through driving unit, auxiliary unit, cleaning unit, collector unit, No.1
Air bag, spiral steam pipe, reaction chamber, generator, motor and controller;On the one hand, it realizes the multiple utilization to steam, utilizes
Steam makes rotation fan rotation, so that driving unit driving auxiliary unit rotation, the crystallization of soda ash is assisted by auxiliary unit, and
Soda ash liquid and soda ash crystal grain are separated, avoids soda ash liquid and soda ash crystalline particle from mixing, influences the crystallization of soda ash liquid, from
And improve soda ash crystallization effect;Meanwhile driving collecting board to move up and down by fixed link, collecting board is few by soda ash liquid measure
When soda ash crystal grain be collected, avoid crystallization after soda ash crystal grain mixed with soda ash liquid, thus improve soda ash crystallization imitate
Fruit;On the other hand, the pneumatic power source generated when fixed link being moved acts on generator, is turned by generator drive motor
Dynamic, so that cleaning annulus moves up and down in reaction chamber, cleaning annulus clears up reaction chamber interior wall, avoids reaction chamber
The soda ash crystal grain adhered on inner wall influences soda ash crystallization, to improve soda ash crystallization effect.
Firstly, steam is passed through from steam port, the steam being passed through is entered in cabinet by spiral steam pipe, to steam
After being passed through a period of time, at this point, soda ash and water are entered in reaction chamber from alkali inlet and inlet respectively, with soda ash and water
Be constantly passed through, the overall weight of reaction chamber becomes weight, and reaction chamber squeezes No.1 air bag, and No.1 air bag is squeezed outside air-blowing, drum
Gas out transfers to No.1 cylinder, and No.1 cylinder pushes No. four axis to move downward, since the whole air content of No.1 air bag is greater than
The whole air content of No.1 cylinder, so that No.1 cylinder pushes the displacement of No. four axis decline greater than the decrement of No.1 air bag,
Blender flexes outward;Meanwhile the intracorporal steam impringement rotation fan of case, rotation fan rotation, and No.1 axis is driven to rotate, pass through one
The mutual cooperation of number helical gear, No. two helical gears, No. three helical gears, No. two axis and No. three between centers, so that No. three axis drive No. four
Axis rotation, and blender is correspondingly rotated, the blender auxiliary soda ash of rotation is crystallized;Soda ash knot is assisted in blender
During crystalline substance, the soda ash crystalline substance paddle of suspension is moved upwards under the action of blender in reaction chamber with certain speed, to soda ash crystalline substance
When paddle is higher than reaction chamber height, the soda ash crystal grain of bulky grain or the particle of expectation partial size fall to the bottom of box, bulky grain crystal grain
Or cabinet is discharged from discharge port in the particle of expectation partial size, it is expected the soda ash crystalline substance paddle that is raised of particle less than diameter grain is carried secretly, soda ash
Paddle liquid constantly follows bad, and soda ash crystal grain constantly increases, and falls to the bottom of box;Meanwhile with the continuous crystallization of soda ash, reaction chamber
Overall weight mitigates, and No.1 air bag absorbs the gas in No.1 cylinder, air-breathing expansion, so that reaction chamber is transported to far from cabinet side
It is dynamic;Simultaneously as the gas in No.1 cylinder is siphoned away by No.1 air bag, No.1 cylinder drives No. four axis to move upwards, and reacts
Case is less than the displacement that No.1 cylinder drives No. four axis to move upwards to the displacement moved far from cabinet side, in fixed pulley
Under cooperation, rope pulls No.1 spring to shrink to close to No. four axis sides, since No.1 spring one end is connected in outermost side
In framework, the No.1 spring other end is connected on innermost box body, during No.1 spring contraction, so that Pagoda-shaped
Blender is shunk to close to No. four axis sides, and the length of blender is shortened by length, and the speed of blender rotation becomes faster, and is increased pair
The crystallization of soda ash, so that the crystalline rate of soda ash is improved, soda ash liquid is reduced in reaction chamber, the soda ash crystal grain of crystallization
It is collected by collecting board;In the crystallization process of soda ash, by blender lasting contraction and stretching, extension, cooperate soda ash knot
Crystalline substance, the gas that soda ash crystallization generates are discharged by gas outlet;Meanwhile with the reduction of soda ash amount in reaction chamber, fixed link is driven
Collecting board moves downward, and the pneumatic power source generated in fixed link movement acts on generator, to send out by pneumatic power source
Electric power generation, the electric power that generator issues act on motor, so that motor rotates;In motor rotates clockwise, No. two ropes are not
Disconnected to be wound by motor output shaft, the dynamic cleaning annulus of No. two rope bands moves upwards, and the cleaning annulus of movement is to reaction chamber interior wall attachment
Soda ash crystal grain be purged, when annulus for clearance is reached at the top of reaction chamber, pass through controller and control motor reversal, motor inverse time
Needle rotation, No. two ropes being wrapped on motor output shaft unclamp, and cleaning annulus moves downward;By constantly controlling the positive and negative of motor
Turn, so that cleaning annulus moves up and down in reaction chamber body, cleaning annulus sufficiently clears up reaction chamber interior wall, thus
Improve the cleannes of reaction chamber interior wall.
Preferably, the wire cross sectional of the No.1 spring is rectangle, and wire cross sectional is that the No.1 spring of rectangle cooperates
Box body, for improving stability when box body is shunk.The present invention by the way that the wire cross sectional of No.1 spring is set as rectangle,
It is moved by the No.1 spring that cross section is rectangle with square frame, on the one hand, improve the intensity of blender;Another party
Face improves the stability of blender auxiliary soda ash crystallization.
Preferably, sealing unit is equipped at the No.1 channel;The sealing unit is for avoiding soda ash liquid from entering one
At number channel, sealing unit is high temperature resistant elastomeric bladder;The high temperature resistant elastomeric bladder is rectangle capsule, and high temperature resistant elastomeric bladder is along No.1 rope
It is symmetrical arranged, high temperature resistant elastomeric bladder is provided with mercury, by mercury expanded by heating, so that high temperature resistant elastomeric bladder is to close to No.1 rope
Side expansion, the high temperature resistant elastomeric bladder of expansion seals No.1 rope.In the crystallization of soda ash, soda ash liquid is easy from No.1 channel
It enters in No. four axis, influences soda ash crystalline rate;For the present invention by setting sealing unit, sealing unit is high temperature resistant elasticity
Capsule, and the built-in full water silver of high temperature resistant elastomeric bladder;On the one hand, due to the continuous crystallization of soda ash, so that the temperature in reaction chamber increases,
Mercury expanded by heating in high temperature resistant elastomeric bladder, the two high temperature resistant elastomeric bladders and No.1 rope of expanded by heating are in close contact, and are avoided anti-
The soda ash liquid in case is answered to enter No.1 channel, to improve the crystallization effect of soda ash;On the other hand, continuous by blender
It is flexible, gas is generated in blender, the gas generated in blender generates compressing to soda ash liquid, soda ash liquid is avoided to enter No.1
Channel, to improve the sealing effect in No.1 channel.
Preferably, No. four axis are equipped with rotating bar;The rotating bar is symmetrical arranged along No.1 rope, and rotating bar one end is hinged
On No. four axis, the rotating bar other end is arc-shaped, and the rotating bar other end is contacted with No.1 rope, drives four by No.1 cylinder
Number axis rises, and the soda ash crystal grain adhered on No.1 rope outer ring is struck off in the cooperation of two rotating bars.In the crystallization process of soda ash,
The soda ash crystal grain of crystallization is liable to stick on No.1 rope, to influence the flexible of No.1 rope;The present invention is led to by setting rotating bar
Rotating bar is crossed, in No. four axis move upwards, since two rotation boom ends are contacted with No.1 rope, is generated between rotating bar and No.1 rope
Relative motion, and No.1 rope is straightened, the rotating bar of movement strikes off the soda ash adhered on No.1 rope crystallization, to improve No.1
The cleannes of rope;In No. four axis move downward, rotating bar is not acted on No.1 rope generation.
Preferably, the cleaning annulus lateral wall is equipped with cleaning brush, is carried out by cleaning brush to reaction chamber interior wall
Cleaning.The present invention clears up reaction chamber interior wall by the cleaning brush of up and down motion by setting cleaning brush, thus
Improve the cleannes of reaction chamber interior wall.
Preferably, the cleaning brush is made of No.1 bar, No. two bars and bristle;The No.1 bar and No. two bar one end phases
It is mutually hinged, and be hinged on cleaning annulus, No.1 bar and No. two bar other ends are arc-shaped, and No.1 bar and No. two bars pass through
Spring is connected on cleaning annulus;The bristle is mounted on No.1 bar and No. two bars, by No.1 bar and No. two bar effects, is made
Bristle straighten to reaction chamber interior wall clear up.The present invention by the way that cleaning brush is made of No.1 bar, No. two bars and bristle,
When cleaning brush moves upwards, No.1 bar is rotated to close to No. two bar sides, so that the bristle on No. two bars is in reaction chamber
Wall is cleared up, and when cleaning brush moves downward, No. two bars are moved to close to No.1 bar side, and No.1 bar is under the action of the spring
It resets, the bristle on No.1 bar clears up reaction chamber interior wall;According to the movement that cleaning brush carries out, so that corresponding bristle
Reaction chamber interior wall is cleared up, and corresponding bristle is protected, to improve the service life of bristle.
Beneficial effects of the present invention are as follows:
1. a kind of heavy alkali high-efficiency production technology of the present invention, technique one side, by tieing up the temperature of steam
It holds at 100-400 DEG C, so that soda ash liquid is adequately crystallized in reaction chamber, to improve the production efficiency of heavy alkali;
On the other hand, the steam by temperature at 200-600 DEG C is passed into steam dryer, passes through the phase between steam and steam dryer
Mutually cooperation, is dried heavy alkali crystal grain, avoids increase process that heavy alkali crystal grain is dried, shortens technique,
To improve heavy alkali production efficiency.
2. a kind of heavy alkali high-efficiency production technology of the present invention, which is closed using the scientific structure of crystallization reactor
It is reason, easily operated, it is vdiverse in function, avoid increasing extra power equipment, but using soda ash crystallize in the pneumatic power source that generates,
With huge economic benefit and the extensive market demand, it is worthy to be popularized.
3. a kind of heavy alkali high-efficiency production technology of the present invention, which uses crystallization reactor, and fixed link is transported
The pneumatic power source generated when dynamic acts on generator, is rotated by generator drive motor, so that cleaning annulus is in reaction chamber
It inside moves up and down, cleaning annulus clears up reaction chamber interior wall, avoids the soda ash crystal grain shadow adhered on reaction chamber interior wall
Soda ash crystallization is rung, to improve soda ash crystallization effect.
Detailed description of the invention
The present invention will be further explained below with reference to the attached drawings.
Fig. 1 is process flow chart of the invention;
Fig. 2 is the main view of crystallization reactor;
Fig. 3 is the cross-sectional view of crystallization reactor when soda ash liquid is reduced;
Fig. 4 is the partial enlarged view in Fig. 2 at A;
Fig. 5 is the cross-sectional view for clearing up annulus;
In figure: cabinet 1, No.1 air bag 11, spiral steam pipe 12, reaction chamber 13, generator 14, motor 15, driving are single
Member 2, shell 21, rotation fan 22,23, No. two axis 24 of No.1 axis, the helical gear 26, three of No.1 helical gear 25, two helical gear 27,
No. three axis 28, auxiliary unit 3, No.1 cylinder 31, No. four axis 32, No.1 channel 321, rotating bar 322, fixed pulleys 33, blender
34, No.1 spring 341, box body 342, No.1 rope 35, collector unit 4, fixed column 41, fixed link 42, collecting board 43, sealing are single
Member 5, high temperature resistant elastomeric bladder 51, cleaning unit 6, cleaning annulus 61, two ropes 62,631, No. two cleaning brush 63, No.1 bar bars
632, bristle 633.
Specific embodiment
In order to be easy to understand the technical means, the creative features, the aims and the efficiencies achieved by the present invention, tie below
Specific embodiment is closed, the present invention is further explained.
As shown in Figures 1 to 5, a kind of heavy alkali high-efficiency production technology of the present invention, the technique the following steps are included:
S1: heating water by heating device, so that water vapor, becomes steam, and makes the vapor (steam) temperature of steam
Reach 400 DEG C, gas pressure 0.01-0.6MPa;
S2: on the basis of S1, by cooling down to steam, so that the temperature of steam maintains 100-400 DEG C, gas
Pressure is 0.01-0.6MPa;
S3: on the basis of S2, steam dryer being mounted on wall box, and steam dryer is used for heavy alkali crystal grain
Drying;
S4: on the basis of S1, S2 and S3, starting crystallization reactor, the crystallization of heavy alkali carried out by crystallization reactor,
Ten minutes later to the crystallization of heavy alkali, by temperature at 200-600 DEG C, gas pressure is that the steam of 0.01-0.6MPa is passed into steam
In drier, by the mutual cooperation between steam dryer and steam, heavy alkali crystal grain is dried;
The crystallization reactor that the present invention uses includes cabinet 1;Further include driving unit 2, auxiliary unit 3, collector unit 4,
Clear up unit 6, No.1 air bag 11, spiral steam pipe 12, reaction chamber 13, generator 14, motor 15 and controller;The control
Device is used to control the work of heavy alkali crystallization reactor;1 side wall of cabinet is equipped with steam port and gas outlet, 1 top of cabinet
Equipped with inlet, alkali inlet and No.1 hole, 1 bottom symmetrical of cabinet is equipped with discharge port;The spiral steam pipe 12 is fixedly mounted
On 1 side wall of cabinet, spiral 12 one end of steam pipe is connected to steam port, and spiral 12 other end of steam pipe is located under No.1 hole
Side;The quantity of the No.1 air bag 11 is two, and two No.1 air bags, 11 one end is interconnected, wherein a No.1 air bag 11 is connected in case
1 bottom of body, another No.1 air bag 11 are connected with reaction chamber 13, and 13 uncovered of reaction chamber, reaction chamber 13 is soda ash crystal region;The drive
Moving cell 2 is mounted on 1 top of cabinet, and driving unit 2 is oblique including 23, No. two shell 21, rotation fan 22, No.1 axis axis 24, No.1s
The helical gear 27 of helical gear 26, three of gear 25, two and No. three axis 28;The shell 21 is connected in 1 top of cabinet;The No.1
23 one end of axis is rotatably installed on 21 inner wall of shell, and 23 other end of No.1 axis and rotation fan 22 are connected, and rotate fan 22 and be located at one
At number hole;The No.1 helical gear 25 is set on No.1 axis 23;The quantity of No. two helical gears 26 is two, No. two helical gears
26 are set on No. two 24 outer rings of axis and are connected in No. two 24 ends of axis;24 one end of No. two axis is rotatably installed in shell 21
On, No. two 24 other ends of axis and No. two helical gears 26 are connected, No.1 helical gear 25 and No. two 26 engaged transmissions of helical gear;Described three
Number 28 one end of axis is protruded into cabinet 1, and No. three 28 one end of axis and auxiliary unit 3 are connected, and No. three 28 outer rings of axis and 1 contact position of cabinet
Rotational installation, No. three 28 other ends of axis are engaged with No. three helical gears 27, No. three helical gears 27 and No. two 26 engaged transmissions of helical gear;
The auxiliary unit 3 is located in reaction chamber 13, and for auxiliary unit 3 for assisting soda ash to crystallize, auxiliary unit 3 includes No.1 cylinder
31, No. four axis 32, fixed pulley 33, blender 34 and No.1 rope 35;The No.1 cylinder 31 is connected to two No.1 air bags 11, No.1
31 one end of cylinder is connected with No. three axis 28, and 31 other end of No.1 cylinder and No. four axis 32 are connected, and No. four axis 32 are spliced by two parts
It forms, No. four axis 32 form No.1 channel 321 after splicing;The quantity of the fixed pulley 33 is two, and two fixed pulleys 33 are located at No.1
At channel 321, and two fixed pulleys 33 are rotatably installed on No. four axis 32 by shaft;The quantity of the blender 34 is two,
Blender 34 is symmetrical arranged along No. four axis 32, and blender 34 is made of No.1 spring 341 and several box bodies 342;Positioned at outermost
The framed lid in 342 side of box body of side, is connected on No. four 32 outer rings of axis, between box body 342 positioned at innermost box body 342
It is interconnected, and is slidably connected to each other, form Pagoda-shaped;Described 341 one end of No.1 spring is connected in outermost box body
On 342,341 other end of No.1 spring is connected on innermost box body 342;The quantity of the No.1 rope 35 is two, two 1
Number rope 35 one end be connected on No.1 spring 341, two No.1 ropes, 35 other end by hook is connected in 13 bottom of reaction chamber, and
Two No.1 ropes 35 are through two fixed pulleys, 33 transition;Steam is passed through from steam port, so that driving unit 2 drives auxiliary unit 3 to rotate,
Accelerate soda ash crystallization, meanwhile, the gas with the reduction of soda ash liquid in reaction chamber 13, in 11 inspiration No.1 cylinder 31 of No.1 air bag
Body, No.1 cylinder 31 drive No. four axis 32 to rise, and are acted on by fixed pulley 33, No.1 spring 341 and No.1 rope 35, so that stirring
Mix the contraction of device 34;The collector unit 4 is fixedly mounted on 1 top of cabinet, and collector unit 4 is symmetrical arranged along No. three axis 28, collects
Unit 4 includes fixed column 41, fixed link 42 and collecting board 43 for collecting soda ash crystalline particle, collector unit 4;The fixed column
41 are fixedly mounted on 1 top of cabinet, offer No.1 slot in fixed column 41;Described 42 one end of fixed link is located at No.1 slot, Gu
42 one end of fixed pole is connected in No.1 slot by spring, and 42 other end of fixed link and collecting board 43 are connected;The number of the motor 15
Amount is two, and motor 15 is fixedly mounted in fixed column 41;The quantity of the generator 14 is two, and generator 14 is used to be motor 15
Power source is provided, generator 14 is mounted on 1 top of cabinet, by the way that the gas generated in the movement of fixed link 42 is acted on generator
14, so that the rotation power generation of generator 14;The cleaning unit 6 is mounted on 15 output shaft of motor, and cleaning unit 6 is used for reaction
The inner sidewall of case 13 is cleared up, and cleaning unit 6 includes cleaning annulus 61 and No. two ropes 62;The cleaning annulus 61 and reaction chamber
The contact of 13 side walls;The quantity of No. two ropes 62 is two, and No. two 62 one end of rope are wrapped on 15 output shaft of motor, No. two ropes 62
The other end and cleaning annulus 61 are connected, and controller are equipped at the top and bottom of reaction chamber 13, using controller for controlling motor 15
Positive and negative rotation, by 14 driving motor 15 of generator rotate so that cleaning annulus 61 move up and down in reaction chamber 13.It will
Soda ash is crystallized, and avoids in use and a large amount of alkali dirt occurs, reduces dust collector;There is also a kind of knots in the prior art
Brilliant device, still, crystallizer Shortcomings in the prior art, on the one hand, crystallizer in the prior art crystallizes soda ash
It is ineffective, and the soda ash crystalline particle after crystallization mixes with soda ash liquid, meanwhile, it cannot adjust according to actual needs to pure
The crystallization of lye, to influence the practicability of crystallization;On the other hand, after not to soda ash crystallization, adhere on 13 inner wall of reaction chamber
Crystalline particle is cleared up, to influence the crystallization effect of soda ash;The present invention is single by driving unit 2, auxiliary unit 3, cleaning
Member 6, collector unit 4, No.1 air bag 11, spiral steam pipe 12, reaction chamber 13, generator 14, motor 15 and controller;One side
The multiple utilization to steam is realized in face, makes 22 rotation of rotation fan using steam, so that driving unit 2 drives 3 turns of auxiliary unit
It is dynamic, the crystallization of soda ash is assisted by auxiliary unit 3, and soda ash liquid and soda ash crystal grain are separated, avoid soda ash liquid and soda ash knot
Brilliant particle mixes, and influences the crystallization of soda ash liquid, to improve soda ash crystallization effect;Meanwhile it being driven by fixed link 42
Collecting board 43 moves up and down, and soda ash crystal grain of soda ash liquid measure when few is collected by collecting board 43, pure after avoiding crystallization
Alkali crystal grain is mixed with soda ash liquid, to improve the crystallization effect of soda ash;On the other hand, the gas generated when fixed link 42 being moved
Body power source acts on generator 14, is rotated by 14 driving motor 15 of generator, so that cleaning annulus 61 is in reaction chamber 13
It moves up and down, cleaning annulus 61 clears up 13 inner wall of reaction chamber, avoids the soda ash adhered on 13 inner wall of reaction chamber brilliant
Grain influences soda ash crystallization, to improve soda ash crystallization effect.
Firstly, steam is passed through from steam port, the steam being passed through is entered in cabinet 1 by spiral steam pipe 12, to
After steam is passed through a period of time, at this point, soda ash and water are entered in reaction chamber 13 from alkali inlet and inlet respectively, with pure
Alkali and the continuous of water are passed through, and the overall weight of reaction chamber 13 becomes weight, and reaction chamber 13 squeezes No.1 air bag 11, and No.1 air bag 11 is by crowded
Outer air-blowing is pressed to, the gas of bulging transfers to No.1 cylinder 31, and No.1 cylinder 31 pushes No. four axis 32 to move downward, due to No.1 gas
The whole air content of capsule 11 is greater than the whole air content of No.1 cylinder 31, so that No.1 cylinder 31 pushes the position of No. four axis 32 decline
Shifting amount is greater than the decrement of No.1 air bag 11, and blender 34 flexes outward;Meanwhile the steam impringement rotation fan 22 in cabinet 1, turn
Dynamic 22 rotation of fan, and No.1 axis 23 is driven to rotate, pass through the helical gear 26, three helical gear 27, two of No.1 helical gear 25, two
Mutual cooperation between axis 24 and No. three axis 28, so that No. three axis 28 drive No. four axis 32 to rotate, and blender 34 carries out accordingly
The blender 34 of rotation, rotation assists soda ash to be crystallized;It is assisted in soda ash crystallization process in blender 34, the soda ash of suspension is brilliant
Paddle is moved upwards under the action of blender 34 in reaction chamber 13 with certain speed, is higher than 13 height of reaction chamber to soda ash crystalline substance paddle
When, the soda ash crystal grain of bulky grain or the particle of expectation partial size fall to 1 bottom of cabinet, bulky grain crystal grain or the particle for it is expected partial size
Cabinet 1 is discharged from discharge port, it is expected the soda ash crystalline substance paddle that is raised of particle less than diameter grain is carried secretly, soda ash paddle liquid constantly follow it is bad, it is pure
Alkali crystal grain constantly increases, and falls to 1 bottom of cabinet;Meanwhile with the continuous crystallization of soda ash, the overall weight of reaction chamber 13 subtracts
Gently, No.1 air bag 11 absorbs the gas in No.1 cylinder 31, air-breathing expansion, so that reaction chamber 13 is moved to far from 1 side of cabinet;
Simultaneously as the gas in No.1 cylinder 31 is siphoned away by No.1 air bag 11, No.1 cylinder 31 drives No. four axis 32 to move upwards, and
Reaction chamber 13 is less than the displacement that No.1 cylinder 31 drives No. four axis 32 to move upwards to the displacement moved far from 1 side of cabinet
Amount, under the cooperation of fixed pulley 33, rope pulls No.1 spring 341 to shrink to close to No. four 32 sides of axis, due to No.1 spring
341 one end are connected on outermost box body 342, and 341 other end of No.1 spring is connected on innermost box body 342,
In 341 contraction process of No.1 spring, so that the blender 34 of Pagoda-shaped is shunk to close to No. four 32 sides of axis, blender 34
Length is shortened by length, and the speed that blender 34 rotates becomes faster, and increases the crystallization to soda ash, to improve the crystallization effect of soda ash
Rate, soda ash liquid is reduced in reaction chamber 13, the soda ash crystal grain of crystallization is collected by collecting board 43;In the knot of soda ash
During crystalline substance, by blender 34 lasting contraction and stretching, extension, cooperate soda ash crystallization, the gas that soda ash crystallization generates passes through outlet
Mouth discharge;Meanwhile with the reduction of soda ash amount in reaction chamber 13, fixed link 42 drives collecting board 43 to move downward, fixed link 42
The pneumatic power source generated in movement acts on generator 14, by pneumatic power source generator 14 is generated electricity, generator 14
The electric power of sending acts on motor 15, so that motor 15 rotates;In motor 15 rotates clockwise, No. two ropes 62 are constantly by motor
The winding of 15 output shafts, No. two ropes 62 drive cleaning annulus 61 to move upwards, and the cleaning annulus 61 of movement is attached to 13 inner wall of reaction chamber
Soda ash crystal grain be purged, when annulus 61 for clearance reaches 13 top of reaction chamber, motor 15 is controlled by controller and is inverted,
Motor 15 rotates counterclockwise, and No. two ropes 62 being wrapped on 15 output shaft of motor unclamp, and cleaning annulus 61 moves downward;By not
The positive and negative rotation of disconnected control motor 15 clears up annulus 61 to anti-so that cleaning annulus 61 moves up and down in 13 body 1 of reaction chamber
13 inner wall of case is answered sufficiently to be cleared up, to improve the cleannes of 13 inner wall of reaction chamber.
As one embodiment of the present invention, the wire cross sectional of the No.1 spring 341 is rectangle, wire cross sectional
Cooperate box body 342 for the No.1 spring 341 of rectangle, for improving stability when box body 342 is shunk.The present invention pass through by
The wire cross sectional of No.1 spring 341 is set as rectangle, is transported by the No.1 spring 341 that cross section is rectangle with square frame
It is dynamic, on the one hand, to improve the intensity of blender 34;On the other hand, the stability that blender 34 assists soda ash crystallization is improved.
As one embodiment of the present invention, sealing unit 5 is equipped at the No.1 channel 321;The sealing unit 5
For avoiding soda ash liquid from entering at No.1 channel 321, sealing unit 5 is high temperature resistant elastomeric bladder 51;The high temperature resistant elastomeric bladder
51 be rectangle capsule, and high temperature resistant elastomeric bladder 51 is symmetrical arranged along No.1 rope 35, and high temperature resistant elastomeric bladder 51 is provided with mercury, passes through mercury
Expanded by heating, so that high temperature resistant elastomeric bladder 51 is expanded to the side close to No.1 rope 35, the high temperature resistant elastomeric bladder 51 of expansion is to one
Number rope 35 sealing.In the crystallization of soda ash, soda ash liquid is easy to enter in No. four axis 32 from No.1 channel 321, influences soda ash knot
Brilliant efficiency;The present invention is by setting sealing unit 5, and sealing unit 5 is high temperature resistant elastomeric bladder 51, and high temperature resistant elastomeric bladder 51 is built-in
Full water silver;On the one hand, due to the continuous crystallization of soda ash, so that the temperature in reaction chamber 13 increases, in high temperature resistant elastomeric bladder 51
Mercury expanded by heating, two high temperature resistant elastomeric bladders 51 and the No.1 rope 35 of expanded by heating are in close contact, avoid pure in reaction chamber 13
Lye enters No.1 channel 321, to improve the crystallization effect of soda ash;It is on the other hand, constantly flexible by blender 34,
Gas is generated in blender 34, the gas generated in blender 34 generates compressing to soda ash liquid, soda ash liquid is avoided to enter No.1
Channel 321, to improve the sealing effect in No.1 channel 321.
As one embodiment of the present invention, No. four axis 32 are equipped with rotating bar 322;The rotating bar 322 is along one
Number rope 35 is symmetrical arranged, and 322 one end of rotating bar is hinged on No. four axis 32, and 322 other end of rotating bar is arc-shaped, and rotating bar
322 other ends are contacted with No.1 rope 35, drive No. four axis 32 to rise by No.1 cylinder 31, two rotating bars 322 cooperate to No.1
The soda ash crystal grain adhered on 35 outer rings of restricting is struck off.In the crystallization process of soda ash, the soda ash crystal grain of crystallization is liable to stick to
On No.1 rope 35, to influence the flexible of No.1 rope 35;The present invention is by setting rotating bar 322, by rotating bar 322, four
Number axis 32, since two rotating bars, 322 end is contacted with No.1 rope 35, generates in moving upwards between rotating bar 322 and No.1 rope 35
Relative motion, and No.1 rope 35 is straightened, the rotating bar 322 of movement strikes off the soda ash adhered on No.1 rope 35 crystallization, to mention
The high cleannes of No.1 rope 35;In No. four axis 32 move downward, rotating bar 322 is not acted on 35 generation of No.1 rope.
As one embodiment of the present invention, 61 lateral wall of cleaning annulus is equipped with cleaning brush 63, by clear
Reason hairbrush 63 clears up 13 inner wall of reaction chamber.The present invention passes through the cleaning hair of up and down motion by setting cleaning brush 63
Brush 63, clears up 13 inner wall of reaction chamber, to improve the cleannes of 13 inner wall of reaction chamber.
As one embodiment of the present invention, the cleaning brush 63 is by 631, No. two bars 632 of No.1 bar and bristle 633
Composition;The No.1 bar 631 and No. two 632 one end of bar are hinged, and are hinged on cleaning annulus 61, No.1 bar 631 and two
Number 632 other end of bar is arc-shaped, and No.1 bar 631 and No. two bars 632 are connected in by spring and are cleared up on annulus 61;It is described
Bristle 633 is mounted on No.1 bar 631 and No. two bars 632, is acted on by No.1 bar 631 and No. two bars 632, so that bristle 633
It straightens and 13 inner wall of reaction chamber is cleared up.The present invention by by cleaning brush 63 by No.1 bar 631, No. two bars 632 and bristles
633 compositions, when cleaning brush 63 moves upwards, No.1 bar 631 is rotated to close to No. two 632 sides of bar, so that No. two bars 632
On bristle 633 13 inner wall of reaction chamber is cleared up, when cleaning brush 63 moves downward, No. two bars 632 are to close to No.1
The movement of 631 side of bar, No.1 bar 631 resets under the action of the spring, the bristle 633 on No.1 bar 631 to 13 inner wall of reaction chamber into
Row cleaning;According to the movement that cleaning brush 63 carries out, so that corresponding bristle 633 clears up 13 inner wall of reaction chamber, and it is right
The bristle 633 answered is protected, to improve the service life of bristle 633.
In use, the steam being passed through is by spirally steaming firstly, temperature is passed through in 100-400 DEG C of steam from steam port
Steam pipe 12 enters in cabinet 1, after steam is passed through a period of time, at this point, by soda ash and water respectively from alkali inlet and inlet
It enters in reaction chamber 13, as soda ash and the continuous of water are passed through, the overall weight of reaction chamber 13 becomes weight, and reaction chamber 13 squeezes one
Number air bag 11, No.1 air bag 11 are squeezed outside air-blowing, and the gas of bulging transfers to No.1 cylinder 31, and No.1 cylinder 31 pushes No. four
Axis 32 moves downward, since the whole air content of No.1 air bag 11 is greater than the whole air content of No.1 cylinder 31, so that No.1 gas
Cylinder 31 pushes the displacement of No. four axis 32 decline greater than the decrement of No.1 air bag 11, and blender 34 flexes outward;Meanwhile cabinet
Steam impringement rotation in 1 fans 22, and rotation fan 22 rotates, and No.1 axis 23 is driven to rotate, oblique by No.1 helical gear 25, two
Mutual cooperation between the axis 24 of helical gear 27, two of gear 26, three and No. three axis 28, so that No. three axis 28 drive No. four 32 turns of axis
It is dynamic, and blender 34 is correspondingly rotated, the blender 34 of rotation assists soda ash to be crystallized;Soda ash is assisted in blender 34
In crystallization process, the soda ash crystalline substance paddle of suspension is moved upwards under the action of blender 34 in reaction chamber 13 with certain speed, to
When soda ash crystalline substance paddle is higher than 13 height of reaction chamber, the soda ash crystal grain of bulky grain or the particle of expectation partial size fall to 1 bottom of cabinet, greatly
Grain it is expected that cabinet 1 is discharged from discharge port in the particle of partial size, less than the soda ash crystalline substance paddle that is raised of particle of desired diameter grain
Entrainment, soda ash paddle liquid constantly follow bad, and soda ash crystal grain constantly increases, and falls to 1 bottom of cabinet;Meanwhile with the continuous knot of soda ash
The overall weight of crystalline substance, reaction chamber 13 mitigates, and No.1 air bag 11 absorbs the gas in No.1 cylinder 31, air-breathing expansion, so that reaction
Case 13 is moved to far from 1 side of cabinet;Simultaneously as the gas in No.1 cylinder 31 is siphoned away by No.1 air bag 11, No.1 cylinder
31 No. four axis 32 of drive move upwards, and reaction chamber 13 is less than 31 band of No.1 cylinder to the displacement moved far from 1 side of cabinet
The displacement that dynamic No. four axis 32 move upwards, under the cooperation of fixed pulley 33, rope pulls No.1 spring 341 to close to No. four axis
32 sides are shunk, and since 341 one end of No.1 spring is connected on outermost box body 342,341 other end of No.1 spring is connected
On innermost box body 342, in 341 contraction process of No.1 spring, so that the blender 34 of Pagoda-shaped is to close to No. four
32 side of axis is shunk, and the length of blender 34 is shortened by length, and the speed that blender 34 rotates becomes faster, and increases the knot to soda ash
Crystalline substance, to improve the crystalline rate of soda ash, soda ash liquid is reduced in reaction chamber 13, the soda ash crystal grain of crystallization passes through receipts
Collection plate 43 is collected;In the crystallization process of soda ash, by blender 34 lasting contraction and stretching, extension, cooperate soda ash crystallization,
The gas that soda ash crystallization generates is discharged by gas outlet;Meanwhile with the reduction of soda ash amount in reaction chamber 13, fixed link 42 is driven
Collecting board 43 moves downward, and the pneumatic power source generated in the movement of fixed link 42 acts on generator 14, passes through pneumatic power source
So that generator 14 generates electricity, the electric power that generator 14 issues acts on motor 15, so that motor 15 rotates;When motor 15 is clockwise
In rotation, No. two rope 62 constantly by 15 output shaft of motor wind, No. two rope 62 drive cleaning annulus 61 move upwards, movement it is clear
The soda ash crystal grain that reason annulus 61 adheres to 13 inner wall of reaction chamber is purged, when annulus 61 for clearance reaches 13 top of reaction chamber,
Motor 15 being controlled by controller to invert, motor 15 rotates counterclockwise, and No. two ropes 62 being wrapped on 15 output shaft of motor unclamp,
Cleaning annulus 61 moves downward;By constantly controlling the positive and negative rotation of motor 15 so that cleaning annulus 61 in 13 body 1 of reaction chamber into
Row moves up and down, and cleaning annulus 61 sufficiently clears up 13 inner wall of reaction chamber, to improve the cleaning of 13 inner wall of reaction chamber
Degree;Meanwhile the steam by temperature at 200-600 DEG C is passed into steam dryer, is cooperated by steam and steam dryer, it is right
Heavy alkali crystal grain is dried.
Above-mentioned front, back, left, right, up, down is mark according to personage's observation visual angle on the basis of Fig. 2 in Figure of description
Standard, device surface are defined as a left side on the left of observer to before being defined as on one side of observer, and so on.
In the description of the present invention, it is to be understood that, term " center ", " longitudinal direction ", " transverse direction ", "front", "rear",
The orientation or positional relationship of the instructions such as "left", "right", "vertical", "horizontal", "top", "bottom" "inner", "outside" is based on attached drawing institute
The orientation or positional relationship shown, is merely for convenience of description of the present invention and simplification of the description, rather than the dress of indication or suggestion meaning
It sets or element must have a particular orientation, be constructed and operated in a specific orientation, therefore should not be understood as protecting the present invention
The limitation of range.
Finally it is noted that the above embodiments are merely illustrative of the technical solutions of the present invention, rather than its limitations.To the greatest extent
Present invention has been described in detail with reference to the aforementioned embodiments for pipe, those skilled in the art should understand that: it is still
It is possible to modify the technical solutions described in the foregoing embodiments, or part of technical characteristic is equally replaced
It changes;And these are modified or replaceed, the essence for technical solution of various embodiments of the present invention that it does not separate the essence of the corresponding technical solution
Mind and range.Every other embodiment obtained by those of ordinary skill in the art without making creative efforts,
It shall fall within the protection scope of the present invention.
Claims (6)
1. a kind of heavy alkali high-efficiency production technology, it is characterised in that: the technique the following steps are included:
S1: heating water by heating device, so that water vapor, becomes steam, and the vapor (steam) temperature of steam is reached
400 DEG C, gas pressure 0.01-0.6MPa;
S2: on the basis of S1, by cooling down to steam, so that the temperature of steam maintains 100-400 DEG C, gas pressure
For 0.01-0.6MPa;
S3: on the basis of S2, steam dryer being mounted on wall box, and steam dryer is for the dry of heavy alkali crystal grain
It is dry;
S4: on the basis of S1, S2 and S3, start crystallization reactor, the crystallization of heavy alkali is carried out by crystallization reactor, to weight
Matter alkali crystallizes ten minutes later, and by temperature at 200-600 DEG C, gas pressure is that the steam of 0.01-0.6MPa is passed into steam drying
In device, by the mutual cooperation between steam dryer and steam, heavy alkali crystal grain is dried;
The crystallization reactor that the present invention uses includes cabinet (1);It further include driving unit (2), auxiliary unit (3), collector unit
(4), unit (6), No.1 air bag (11), spiral steam pipe (12), reaction chamber (13), generator (14), motor (15) are cleared up
And controller;The controller is used to control the work of heavy alkali crystallization apparatus;Cabinet (1) side wall be equipped with steam port and
Gas outlet, cabinet (1) top are equipped with inlet, alkali inlet and No.1 hole, and cabinet (1) bottom symmetrical is equipped with discharge port;The spiral shell
Rotating steam pipe (12) is fixedly mounted on cabinet (1) side wall, and spiral steam pipe (12) one end is connected to steam port, spirally
Steam pipe (12) other end is located at below No.1 hole;The quantity of the No.1 air bag (11) is two, two No.1 air bag (11) one end
It is interconnected, wherein a No.1 air bag (11) is connected in cabinet (1) bottom, another No.1 air bag (11) and reaction chamber (13) are solid
Even, reaction chamber (13) uncovered, reaction chamber (13) are soda ash crystal region;The driving unit (2) is mounted at the top of cabinet (1), drives
Moving cell (2) include shell (21), rotation fan (22), No.1 axis (23), No. two axis (24), No.1 helical gear (25), No. two tiltedly
Gear (26), No. three helical gears (27) and No. three axis (28);The shell (21) is connected at the top of cabinet (1);The No.1 axis
(23) one end is rotatably installed on shell (21) inner wall, and No.1 axis (23) other end and rotation fan (22) are connected, and rotate fan
(22) it is located at No.1 hole;The No.1 helical gear (25) is set on No.1 axis (23);The number of No. two helical gears (26)
Amount is two, and No. two helical gears (26) are set on No. two axis (24) outer rings and are connected in No. two axis (24) ends;No. two axis
(24) one end is rotatably installed on shell (21), and No. two axis (24) other ends and No. two helical gears (26) are connected, No.1 helical gear
(25) and No. two helical gears (26) engaged transmission;Described No. three axis (28) one end is protruded into cabinet (1), No. three axis (28) one end with
Auxiliary unit (3) is connected, and No. three axis (28) outer rings and cabinet (1) contact position are rotatablely installed, No. three axis (28) other ends and three
The engagement of number helical gear (27), No. three helical gears (27) and No. two helical gears (26) engaged transmissions;The auxiliary unit (3) is located at anti-
It answers in case (13), for auxiliary unit (3) for assisting soda ash to crystallize, auxiliary unit (3) includes No.1 cylinder (31), No. four axis
(32), fixed pulley (33), blender (34) and No.1 rope (35);The No.1 cylinder (31) is connected to two No.1 air bags (11),
No.1 cylinder (31) one end is connected with No. three axis (28), and No.1 cylinder (31) other end and No. four axis (32) are connected, No. four axis
(32) it is spliced by two parts, forms No.1 channel (321) after No. four axis (32) splicings;The quantity of the fixed pulley (33) is
Two, two fixed pulleys (33) are located at No.1 channel (321), and two fixed pulleys (33) are rotatably installed in No. four axis by shaft
(32) on;The quantity of the blender (34) is two, and blender (34) is symmetrical arranged along No. four axis (32), and blender (34) is by one
Number spring (341) and several box bodies (342) composition;The framed lid in box body (342) side on the outermost side is located at most inner side
Box body (342) be connected on No. four axis (32) outer rings, be interconnected, and be slidably connected between box body (342) to each other, shape
At Pagoda-shaped;Described No.1 spring (341) one end is connected on outermost box body (342), No.1 spring (341) other end
It is connected on innermost box body (342);The quantity of the No.1 rope (35) is two, and two No.1 rope (35) one end are connected in
On No.1 spring (341), two No.1 rope (35) other ends are connected in reaction chamber (13) bottom, and two No.1 ropes (35) by hook
Through two fixed pulleys (33) transition;Steam is passed through from steam port, so that driving unit (2) driving auxiliary unit (3) rotation, accelerates
Soda ash crystallization, meanwhile, the gas with the reduction of the interior soda ash liquid of reaction chamber (13), in No.1 air bag (11) inspiration No.1 cylinder (31)
Body, No.1 cylinder (31) drive No. four axis (32) to rise, and pass through fixed pulley (33), No.1 spring (341) and No.1 rope (35)
Effect, so that blender (34) is shunk;The collector unit (4) is fixedly mounted at the top of cabinet (1), and collector unit (4) is along three
Number axis (28) is symmetrical arranged, and for collector unit (4) for collecting soda ash crystalline particle, collector unit (4) includes fixed column (41), solid
Fixed pole (42) and collecting board (43);The fixed column (41) is fixedly mounted at the top of cabinet (1), and fixed column offers one on (41)
Number slot;Described fixed link (42) one end is located at No.1 slot, and fixed link (42) one end is connected in No.1 slot by spring, fixed
Bar (42) other end and collecting board (43) are connected;The quantity of the motor (15) is two, and motor (15) is fixedly mounted on fixed column
(41) on;The quantity of the generator (14) is two, and generator (14) is used to provide power source, generator (14) for motor (15)
It is mounted at the top of cabinet (1), by the way that the gas generated in fixed link (42) movement is acted on generator (14), so that generator
(14) rotation power generation;The cleaning unit (6) is mounted on motor (15) output shaft, and cleaning unit (6) is used for reaction chamber
(13) inner sidewall is cleared up, and cleaning unit (6) includes cleaning annulus (61) and No. two ropes (62);The cleaning annulus (61)
It is contacted with reaction chamber (13) side wall;The quantity of No. two ropes (62) is two, and No. two rope (62) one end are wrapped in motor (15)
On output shaft, No. two rope (62) other ends and cleaning annulus (61) are connected, and controller, benefit are equipped at the top and bottom of reaction chamber (13)
It is used to control the positive and negative rotation of motor (15) with controller, is rotated by generator (14) driving motor (15), so that cleaning annulus
(61) it moves up and down in reaction chamber (13).
2. a kind of heavy alkali high-efficiency production technology according to claim 1, it is characterised in that: the No.1 spring (341)
Wire cross sectional be rectangle, wire cross sectional be rectangle No.1 spring (341) cooperate box body (342), for the side of raising
Stability when framework (342) is shunk.
3. a kind of heavy alkali high-efficiency production technology according to claim 1, it is characterised in that: the No.1 channel (321)
Place is equipped with sealing unit (5);The sealing unit (5) is for avoiding soda ash liquid from entering at No.1 channel (321), sealing unit
(5) it is high temperature resistant elastomeric bladder (51);The high temperature resistant elastomeric bladder (51) is rectangle capsule, and high temperature resistant elastomeric bladder (51) is along No.1 rope
(35) it is symmetrical arranged, high temperature resistant elastomeric bladder (51) is provided with mercury, by mercury expanded by heating, so that high temperature resistant elastomeric bladder (51)
It is expanded to the side close to No.1 rope (35), the high temperature resistant elastomeric bladder (51) of expansion seals No.1 rope (35).
4. a kind of heavy alkali high-efficiency production technology according to claim 1, it is characterised in that: No. four axis (32) are equipped with
Rotating bar (322);The rotating bar (322) is symmetrical arranged along No.1 rope (35), and rotating bar (322) one end is hinged on No. four axis
(32) on, rotating bar (322) other end is arc-shaped, and rotating bar (322) other end is contacted with No.1 rope (35), passes through No.1
Cylinder (31) drives No. four axis (32) to rise, and two rotating bars (322) cooperate to the soda ash crystal grain adhered on No.1 rope (35) outer ring
It is struck off.
5. a kind of heavy alkali high-efficiency production technology according to claim 1, it is characterised in that: the cleaning annulus (61) is outside
Side wall is equipped with cleaning brush (63), is cleared up by cleaning brush (63) reaction chamber (13) inner wall.
6. a kind of heavy alkali high-efficiency production technology according to claim 5, it is characterised in that: the cleaning brush (63) by
No.1 bar (631), No. two bars (632) and bristle (633) composition;The No.1 bar (631) and No. two bar (632) one end are mutually cut with scissors
It connects, and is hinged in cleaning annulus (61), No.1 bar (631) and No. two bar (632) other ends are arc-shaped, and No.1 bar
(631) it is connected in cleaning annulus (61) by spring with No. two bars (632);The bristle (633) is mounted on No.1 bar
(631) and on No. two bars (632), by No.1 bar (631) and No. two bar (632) effects, so that bristle (633) is straightened to reaction
Case (13) inner wall is cleared up.
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CN110354786A (en) * | 2019-07-31 | 2019-10-22 | 北京鼎翰科技有限公司 | A kind of water treatment agent process units with organic exhaust gas detection function |
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CN205699547U (en) * | 2016-06-13 | 2016-11-23 | 信丰正天伟电子科技有限公司 | A kind of backflow crystallization prevention device |
CN208031959U (en) * | 2018-02-28 | 2018-11-02 | 杨娜 | A kind of traditional Chinese medicine extraction crystallization apparatus |
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SU1637823A1 (en) * | 1988-11-09 | 1991-03-30 | Предприятие П/Я Р-6273 | Crystallizer |
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CN104445288A (en) * | 2014-12-02 | 2015-03-25 | 成都华西堂投资有限公司 | Sodium hydrogen carbonate reaction crystallizer |
CN204319821U (en) * | 2014-12-02 | 2015-05-13 | 成都华西堂投资有限公司 | A kind of sodium acid carbonate crystallizer containing central tube |
CN205391791U (en) * | 2016-02-24 | 2016-07-27 | 福建万科药业有限公司 | Air agitation formula crystallization kettle |
CN205699547U (en) * | 2016-06-13 | 2016-11-23 | 信丰正天伟电子科技有限公司 | A kind of backflow crystallization prevention device |
CN208031959U (en) * | 2018-02-28 | 2018-11-02 | 杨娜 | A kind of traditional Chinese medicine extraction crystallization apparatus |
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Publication number | Priority date | Publication date | Assignee | Title |
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CN110354786A (en) * | 2019-07-31 | 2019-10-22 | 北京鼎翰科技有限公司 | A kind of water treatment agent process units with organic exhaust gas detection function |
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