CN109680479A - A kind of stamp pre-treating technology of cotton fabric - Google Patents
A kind of stamp pre-treating technology of cotton fabric Download PDFInfo
- Publication number
- CN109680479A CN109680479A CN201811603525.9A CN201811603525A CN109680479A CN 109680479 A CN109680479 A CN 109680479A CN 201811603525 A CN201811603525 A CN 201811603525A CN 109680479 A CN109680479 A CN 109680479A
- Authority
- CN
- China
- Prior art keywords
- fabric
- parts
- cotton fabric
- kiering
- desizing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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- 239000004744 fabric Substances 0.000 title claims abstract description 121
- 229920000742 Cotton Polymers 0.000 title claims abstract description 49
- 238000005516 engineering process Methods 0.000 title claims abstract description 21
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims abstract description 42
- 238000009990 desizing Methods 0.000 claims abstract description 36
- 239000000126 substance Substances 0.000 claims abstract description 33
- 239000012752 auxiliary agent Substances 0.000 claims abstract description 23
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 19
- 239000000203 mixture Substances 0.000 claims abstract description 18
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 17
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims abstract description 14
- 238000005517 mercerization Methods 0.000 claims abstract description 14
- 235000011121 sodium hydroxide Nutrition 0.000 claims abstract description 14
- 238000002203 pretreatment Methods 0.000 claims abstract description 11
- 239000002270 dispersing agent Substances 0.000 claims abstract description 10
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 10
- 239000011265 semifinished product Substances 0.000 claims abstract description 7
- 230000000740 bleeding effect Effects 0.000 claims abstract description 4
- FRPJTGXMTIIFIT-UHFFFAOYSA-N tetraacetylethylenediamine Chemical compound CC(=O)C(N)(C(C)=O)C(N)(C(C)=O)C(C)=O FRPJTGXMTIIFIT-UHFFFAOYSA-N 0.000 claims abstract description 4
- -1 sucrose ester Chemical class 0.000 claims description 12
- 108010005400 cutinase Proteins 0.000 claims description 10
- 150000001412 amines Chemical class 0.000 claims description 8
- 239000003760 tallow Substances 0.000 claims description 8
- 125000001301 ethoxy group Chemical group [H]C([H])([H])C([H])([H])O* 0.000 claims description 7
- RPNUMPOLZDHAAY-UHFFFAOYSA-N Diethylenetriamine Chemical compound NCCNCCN RPNUMPOLZDHAAY-UHFFFAOYSA-N 0.000 claims description 6
- 229930182470 glycoside Natural products 0.000 claims description 6
- 238000009992 mercerising Methods 0.000 claims description 6
- 239000004094 surface-active agent Substances 0.000 claims description 6
- 229930006000 Sucrose Natural products 0.000 claims description 5
- 239000005720 sucrose Substances 0.000 claims description 5
- 229920001214 Polysorbate 60 Polymers 0.000 claims description 4
- 108010019077 beta-Amylase Proteins 0.000 claims description 4
- 150000003242 quaternary ammonium salts Chemical class 0.000 claims description 4
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 claims description 3
- 108090000604 Hydrolases Proteins 0.000 claims description 3
- 102000004157 Hydrolases Human genes 0.000 claims description 3
- 239000001110 calcium chloride Substances 0.000 claims description 3
- 229910001628 calcium chloride Inorganic materials 0.000 claims description 3
- 239000003093 cationic surfactant Substances 0.000 claims description 3
- MOTZDAYCYVMXPC-UHFFFAOYSA-N dodecyl hydrogen sulfate Chemical compound CCCCCCCCCCCCOS(O)(=O)=O MOTZDAYCYVMXPC-UHFFFAOYSA-N 0.000 claims description 3
- 229940043264 dodecyl sulfate Drugs 0.000 claims description 3
- YWNYZQTZOONLGU-UHFFFAOYSA-N C(CC)Cl.[O] Chemical compound C(CC)Cl.[O] YWNYZQTZOONLGU-UHFFFAOYSA-N 0.000 claims 1
- OURRXQUGYQRVML-AREMUKBSSA-N [4-[(2s)-3-amino-1-(isoquinolin-6-ylamino)-1-oxopropan-2-yl]phenyl]methyl 2,4-dimethylbenzoate Chemical compound CC1=CC(C)=CC=C1C(=O)OCC1=CC=C([C@@H](CN)C(=O)NC=2C=C3C=CN=CC3=CC=2)C=C1 OURRXQUGYQRVML-AREMUKBSSA-N 0.000 claims 1
- 125000001931 aliphatic group Chemical group 0.000 claims 1
- 238000000034 method Methods 0.000 abstract description 12
- 230000000694 effects Effects 0.000 abstract description 10
- 230000008569 process Effects 0.000 abstract description 9
- 238000009991 scouring Methods 0.000 abstract description 4
- 239000002585 base Substances 0.000 description 9
- 230000000052 comparative effect Effects 0.000 description 9
- 238000000354 decomposition reaction Methods 0.000 description 6
- 239000000975 dye Substances 0.000 description 6
- 239000000835 fiber Substances 0.000 description 6
- 150000002148 esters Chemical class 0.000 description 5
- 238000002834 transmittance Methods 0.000 description 5
- LRWZZZWJMFNZIK-UHFFFAOYSA-N 2-chloro-3-methyloxirane Chemical compound CC1OC1Cl LRWZZZWJMFNZIK-UHFFFAOYSA-N 0.000 description 4
- 229920002472 Starch Polymers 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- 239000008107 starch Substances 0.000 description 4
- 235000019698 starch Nutrition 0.000 description 4
- 239000003513 alkali Substances 0.000 description 3
- 238000004043 dyeing Methods 0.000 description 3
- 108090000790 Enzymes Proteins 0.000 description 2
- 102000004190 Enzymes Human genes 0.000 description 2
- GUBGYTABKSRVRQ-PICCSMPSSA-N Maltose Natural products O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@@H](CO)OC(O)[C@H](O)[C@H]1O GUBGYTABKSRVRQ-PICCSMPSSA-N 0.000 description 2
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 2
- 238000002835 absorbance Methods 0.000 description 2
- 238000004090 dissolution Methods 0.000 description 2
- 230000007062 hydrolysis Effects 0.000 description 2
- 238000006460 hydrolysis reaction Methods 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 230000008595 infiltration Effects 0.000 description 2
- 238000001764 infiltration Methods 0.000 description 2
- 229960002160 maltose Drugs 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- 230000001590 oxidative effect Effects 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- 239000002002 slurry Substances 0.000 description 2
- OWEGMIWEEQEYGQ-UHFFFAOYSA-N 100676-05-9 Natural products OC1C(O)C(O)C(CO)OC1OCC1C(O)C(O)C(O)C(OC2C(OC(O)C(O)C2O)CO)O1 OWEGMIWEEQEYGQ-UHFFFAOYSA-N 0.000 description 1
- 239000004382 Amylase Substances 0.000 description 1
- 108010065511 Amylases Proteins 0.000 description 1
- 102000013142 Amylases Human genes 0.000 description 1
- 229920000856 Amylose Polymers 0.000 description 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- BHPQYMZQTOCNFJ-UHFFFAOYSA-N Calcium cation Chemical compound [Ca+2] BHPQYMZQTOCNFJ-UHFFFAOYSA-N 0.000 description 1
- KZBUYRJDOAKODT-UHFFFAOYSA-N Chlorine Chemical compound ClCl KZBUYRJDOAKODT-UHFFFAOYSA-N 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 229920001503 Glucan Polymers 0.000 description 1
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 1
- 235000017858 Laurus nobilis Nutrition 0.000 description 1
- DKXNBNKWCZZMJT-UHFFFAOYSA-N O4-alpha-D-Mannopyranosyl-D-mannose Natural products O=CC(O)C(O)C(C(O)CO)OC1OC(CO)C(O)C(O)C1O DKXNBNKWCZZMJT-UHFFFAOYSA-N 0.000 description 1
- 229920003171 Poly (ethylene oxide) Polymers 0.000 description 1
- HVUMOYIDDBPOLL-XWVZOOPGSA-N Sorbitan monostearate Chemical compound CCCCCCCCCCCCCCCCCC(=O)OC[C@@H](O)[C@H]1OC[C@H](O)[C@H]1O HVUMOYIDDBPOLL-XWVZOOPGSA-N 0.000 description 1
- 235000005212 Terminalia tomentosa Nutrition 0.000 description 1
- 244000125380 Terminalia tomentosa Species 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000003213 activating effect Effects 0.000 description 1
- 230000004913 activation Effects 0.000 description 1
- 239000012190 activator Substances 0.000 description 1
- 235000019418 amylase Nutrition 0.000 description 1
- 239000003945 anionic surfactant Substances 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- GUBGYTABKSRVRQ-QUYVBRFLSA-N beta-maltose Chemical compound OC[C@H]1O[C@H](O[C@H]2[C@H](O)[C@@H](O)[C@H](O)O[C@@H]2CO)[C@H](O)[C@@H](O)[C@@H]1O GUBGYTABKSRVRQ-QUYVBRFLSA-N 0.000 description 1
- 238000004061 bleaching Methods 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 229910001424 calcium ion Inorganic materials 0.000 description 1
- 150000001768 cations Chemical class 0.000 description 1
- 239000003518 caustics Substances 0.000 description 1
- 239000000460 chlorine Substances 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 239000003599 detergent Substances 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- NLEBIOOXCVAHBD-QKMCSOCLSA-N dodecyl beta-D-maltoside Chemical compound O[C@@H]1[C@@H](O)[C@H](OCCCCCCCCCCCC)O[C@H](CO)[C@H]1O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 NLEBIOOXCVAHBD-QKMCSOCLSA-N 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 239000003792 electrolyte Substances 0.000 description 1
- 238000004945 emulsification Methods 0.000 description 1
- 230000002255 enzymatic effect Effects 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 150000004665 fatty acids Chemical class 0.000 description 1
- 239000008103 glucose Substances 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 239000007800 oxidant agent Substances 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 125000001453 quaternary ammonium group Chemical group 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 230000003014 reinforcing effect Effects 0.000 description 1
- 239000013049 sediment Substances 0.000 description 1
- 238000004513 sizing Methods 0.000 description 1
- 229910052938 sodium sulfate Inorganic materials 0.000 description 1
- 235000011152 sodium sulphate Nutrition 0.000 description 1
- 238000005063 solubilization Methods 0.000 description 1
- 230000007928 solubilization Effects 0.000 description 1
- 230000008961 swelling Effects 0.000 description 1
- 230000002195 synergetic effect Effects 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
- 238000009988 textile finishing Methods 0.000 description 1
- 238000009941 weaving Methods 0.000 description 1
- 239000002759 woven fabric Substances 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
- D06M11/38—Oxides or hydroxides of elements of Groups 1 or 11 of the Periodic Table
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06L—DRY-CLEANING, WASHING OR BLEACHING FIBRES, FILAMENTS, THREADS, YARNS, FABRICS, FEATHERS OR MADE-UP FIBROUS GOODS; BLEACHING LEATHER OR FURS
- D06L1/00—Dry-cleaning or washing fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods
- D06L1/12—Dry-cleaning or washing fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods using aqueous solvents
- D06L1/14—De-sizing
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/50—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with hydrogen peroxide or peroxides of metals; with persulfuric, permanganic, pernitric, percarbonic acids or their salts
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/11—Compounds containing epoxy groups or precursors thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/165—Ethers
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/325—Amines
- D06M13/332—Di- or polyamines
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/388—Amine oxides
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/46—Compounds containing quaternary nitrogen atoms
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
- D06M16/003—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic with enzymes or microorganisms
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
- D06M2101/06—Vegetal fibres cellulosic
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Biochemistry (AREA)
- Microbiology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
Abstract
The invention discloses a kind of stamp pre-treating technologies of cotton fabric.A kind of stamp pre-treating technology of cotton fabric: the pre-treating technology is the following steps are included: S1: cotton fabric fabric is carried out processing of singing；S2: it singes that treated by above-mentioned cotton fabric fabric carries out desizing treatment；S3: the cotton fabric fabric after above-mentioned desizing treatment is subjected to kiering processing, each chemical composition of the kiering substance added in the kiering is based on parts by weight are as follows: dilute caustic soda 3-5 parts, 10-20 parts of emulsifier, 15-20 parts of dispersing agent, 5-10 parts of chelated dispersants, 5-8 parts of bleeding agent, 50-60 parts of the first auxiliary agent, 30-40 parts of hydrogen peroxide, 3-5 parts of tetraacetyl ethylene diamine and 150-200 parts of water；S4: above-mentioned kiering treated cotton fabric fabric is subjected to mercerization finish；S5: the cotton fabric fabric after mercerization finish is subjected to thermal finalization processing；Cotton fabric semi-finished product cloth by above-mentioned five steps, after obtaining pre-treatment.The present invention has the dosage for reducing caustic soda, and fabric is made more to handle milder effect in scouring process again.
Description
Technical field
The present invention relates to dyeing and printing process field more particularly to a kind of stamp pre-treating technologies of cotton fabric.
Background technique
Cotton fabric is also known as cotton, is using cotton yarn as the woven fabric of raw material.Cotton fabric is become most with excellent wearability
One of common fabric, is widely used in garment material, drapery and TECHNICAL FABRIC.
The production technology of cotton fabric generally include the pre-treatment of fabric, dyeing, tentering, preshrunk, stamp, at steps such as product examine dresses
Suddenly.The pre-treatment of cotton fabric can remove natural impurity, slurry and greasy dirt on fiber etc., and fiber is made to give full play to its excellent product
Matter.And make fabric that there is pure white, soft, good infiltration and processing performance, the appearance and inherent quality of fabric are improved, after providing
The qualified semi-finished product of road processing.The pre-treatment production technology of pure cotton fabric traditionally uses always the chemical method of high temperature highly basic,
This technique consumes mass energy, and generates a large amount of environmentally harmful substances.
A large amount of caustic scourings are used in pre-treatment, be also easy to produce the air-dried print of alkaline spot, alkali or refuse specking, and when semi-products are examined
It is not easy to find, influences the quality of dye product.
Summary of the invention
In view of the deficiencies of the prior art, the present invention intends to provide a kind of stamp pre-treatment work of cotton fabric
Skill carries out kiering to fabric by adding the first auxiliary agent and hydrogen peroxide oxidant in kiering, reduces the dosage of caustic soda, make base
Cloth more handles in scouring process more mild again.
Above-mentioned purpose of the invention has the technical scheme that
A kind of stamp pre-treating technology of cotton fabric, the pre-treating technology the following steps are included:
S1: cotton fabric fabric is subjected to processing of singing；
S2: it singes that treated by above-mentioned cotton fabric fabric carries out desizing treatment；
S3: the cotton fabric fabric after above-mentioned desizing treatment is subjected to kiering processing, the kiering substance added in the kiering
Each chemical composition based on parts by weight are as follows: dilute caustic soda 3-5 parts, 10-20 parts of emulsifier, 10-20 parts of dispersing agent, chelated dispersants
5-10 parts, 5-8 parts of bleeding agent, 50-60 parts of the first auxiliary agent, 30-40 parts of hydrogen peroxide, 3-5 parts of tetraacetyl ethylene diamine and water 150-
200 parts；
S4: above-mentioned kiering treated cotton fabric fabric is subjected to mercerization finish；
S5: the cotton fabric fabric after mercerization finish is subjected to thermal finalization processing；
Cotton fabric semi-finished product cloth by above-mentioned five steps, after obtaining pre-treatment.
By using above-mentioned technical proposal, cotton fabric fabric is first singed the villus burn off on fabric surface, makes cloth
Surface becomes smooth；Then the fabric after singing carries out desizing treatment, and the starch size having on fabric in weaving is removed
It goes；Then kiering is carried out in kiering substance again, a small amount of dilute caustic soda is used to increase the hydrolysis to the aliphatic ester substance on fabric
Effect, chelated dispersants can prevent beavy metal impurity and slurry to be deposited on fiber again so that fabric again after kiering more
It is pure white.Hydrogen peroxide plays the role of to fabric oxidation bleaching, and strong oxidizing property can also play certain bactericidal effect, tetrem
Acyl ethylenediamine is a kind of oxide activator, can be further improved the oxidation efficiency of hydrogen peroxide.Emulsifier, dispersing agent and infiltration
Agent synergistic effect plays the role of reinforcing fabric wetability.Fabric after kiering passes through mercerization finish again, further increases fabric
Dimensional stability, by thermal finalization cloth outputting sizing after becoming semi-finished product cloth, be used for subsequent printing technology.Entire pre-treatment
The dosage of caustic soda is very small when kiering in the process, efficiently avoids a possibility that alkaline spot occurs after kiering for fabric, pre-treatment
Process is more green mild.First auxiliary agent plays main function for the kiering of cotton fabric, by the fatty acid on cotton-textile fibres
Esters and waxy substance etc. carry out decomposition removal, instead of the effect of sodium hydroxide in the prior art.
The present invention is further arranged to: first auxiliary agent is made of by percentage to the quality following chemical composition: angle
Matter enzyme 20%-25%, two (ethoxy) tallow base amine oxide 0.1%-0.3%, dodecyl-β-D-Maltose glycosides
0.1%-0.3%, surplus are water.
By using above-mentioned technical proposal, the cutinase in the first auxiliary agent can effectively increase to aliphatic ester on fabric
Decomposition efficiency, and the decomposable process of cutinase more it is mild thoroughly.Two (ethoxy) tallow base amine oxides are a kind of both sexes
Surfactant plays solubilization for cutinase and the dissolution of dodecyl-β-D-Maltose glycosides, and in kiering by
In being in alkaline condition, two (ethoxy) tallow base amine oxides are in nonionic, and stability is high, not vulnerable to pH and electrolyte
The influence of salt.And two (ethoxy) tallow base amine oxide it is biodegradable, pollution is almost nil.Dodecyl-β-D-
Maltoside is a kind of Nonionic Detergents, can stablize Cutinase activity.
The present invention is further arranged to: the emulsifier consists of the following mass percentage components: polyoxyethylene removes water
Span 60%-70%, sldium lauryl sulfate 10%-20% and sucrose ester 17%-19%.
By using above-mentioned technical proposal, polyoxyethylene sorbitan aliphatic ester is used for as a kind of emulsifier to two
(ethoxy) tallow base amine oxide and dodecyl-β-D-Maltose glycosides solubilising, sldium lauryl sulfate are a kind of anion
Surfactant, sucrose ester are that a kind of nonionic surface active agent is all used to enhance cutinase in the first auxiliary agent, two (hydroxyl second
Base) tallow base amine oxide, the dodecyl-β-solvability of D-Maltose glycosides in water, apparent activation energy is reduced, in diluted alkaline
Under conditions of property, sucrose ester is more stable, and nonionic surface active agent has preferable emulsification to oil and to water.
The present invention is further arranged to: each chemical composition of the desizing substance added in desizing treatment in the S2 is with quality
Percentages are as follows: 1,4- α-D- glucan hydrolase 30%-40%, beta amylase %10%-20%, calcium chloride 1%-5%, table
Face activating agent 5%-10%, surplus are water.
By using above-mentioned technical proposal, Isosorbide-5-Nitrae-α-D- glucan hydrolase plays main point to the starch size on fabric
Solution effect, beta amylase play auxiliary decomposition, amylose can be completely decomposed into maltose and a small amount of glucose.Chlorine
The calcium ion changed in calcium plays facilitation to the hydrolysis of starch for amylase, so that the efficiency decomposed more is increased.
The present invention is further arranged to: fabric carries out desizing treatment by the way of padding in the S2, desizing treatment
Temperature control is 50-60 DEG C, and the control of desizing time is 1-2h, and the complete fabric of desizing is washed again, dried.
By using above-mentioned technical proposal, when the temperature of desizing treatment is lower than 50 DEG C, the activity of enzyme used in desizing treatment
It is very low, decomposition is carried out to the starch on fabric and needs to take a substantial amount of time.And when the temperature of desizing treatment is higher than 50 DEG C, it forms sediment
Powder enzymatic activity, which can also reduce, possibly even to fail, and hands over reduction for the desizing of fabric.
The present invention is further arranged to: each chemical composition of the mercerising substance added in mercerization finish in the S4 is with quality
Percentages are as follows: sodium hydroxide 10%-20%, the second auxiliary agent 5%-10%, surplus are water.
By using above-mentioned technical proposal, in sodium hydroxide solution, violent swelling can occur for cotton fiber, and longitudinal is natural
Distortion disappears, and imposing tension appropriate can make fiber be stretched or not shunk, and such fiber longitudinally becomes very smooth
Cylindrical body, the regular reflection of incident light is enhanced, i.e., lustrous surface improves；After mercerising, fiber amorphous region increases, adsorptivity
It can improve,；The dimensional stability of fabric improves simultaneously.
The present invention is further arranged to: second auxiliary agent by following chemical composition by percentage to the quality are as follows: cation
Surfactant 30%-40%, diethylenetriamine 5%-10%, epoxychloropropane 5%-10%, quaternary ammonium salt etherifying agent 3%-
5%, surplus is water.
By using above-mentioned technical proposal, there is the diethylenetriamine being added during mercerising the arrangement to fabric to imitate
Fruit, diethylenetriamine and epoxychloropropane, which can react, is etherified available quaternized color fixing agent by quaternary ammonium salt etherifying agent again, right
Tint retention is played in the subsequent stamp of fabric.Cationic surfactant increases diethylenetriamine, epoxychloropropane and quaternary ammonium
The dissolution of salt etherifying agent, and can be with the wetability of fabric.
The present invention is further arranged to: temperature control when kiering is handled is 50-60 DEG C, and the kiering time is 2-3h.
By using above-mentioned technical proposal, when the temperature of kiering processing is lower than 50 DEG C, kiering processing cutinase used
Activity is very low, carries out decomposition to the esters on fabric and needs to take a substantial amount of time.And when the temperature of kiering processing is higher than 50 DEG C
When, Cutinase activity, which can also reduce, possibly even to fail, and it is lower for the esters decomposition efficiency on fabric, or even hardly decompose
Esters.
Compared with prior art, the beneficial effects of the present invention are:
1, by the way that the first auxiliary agent is added in scouring process, so that fabric is during kiering to the rouge adhered on fabric
Fat acid esters is decomposed, and the use of alkali is reduced, and keeps the kiering treatment process of fabric milder, and will not generate alkali on fabric
Spot；
2, by adding the second auxiliary agent during mercerising, the ingredient in the second auxiliary agent is playing the effect to textile finishing
While can also generate color fixing agent, for improving in the processing of subsequent stamp to the fixation ability of colorant.
Detailed description of the invention
Fig. 1 is process flow chart of the invention.
Specific embodiment
With reference to the accompanying drawings and examples, the present invention will be described in detail.
Embodiment 1:
A kind of stamp pre-treating technology of cotton fabric disclosed by the invention, comprises the following steps that:
The configuration of first auxiliary agent: by mass percentage by cutinase 20%, two (ethoxy) tallow base amine oxide
0.1%, dodecyl-β-D-Maltose glycosides 0.1%, water 79.8% are uniformly mixed spare；
The configuration of second auxiliary agent: by mass percentage by cationic surfactant 30%, diethylenetriamine 5%, epoxy
Chloropropane 5%, quaternary ammonium salt etherifying agent 3%, water 57% are uniformly mixed spare；
The configuration of emulsifier: by mass percentage by polyoxyethylene sorbitan aliphatic ester (tween) 60%, laurel
Alcohol sodium sulphate 20%, sucrose ester 20% mix it is equal with it is spare.
S1: cotton fabric fabric is subjected to processing of singing；
S2: carrying out desizing treatment for above-mentioned cotton fabric fabric of singing that treated, and the Portugal Isosorbide-5-Nitrae-α-D- is added in when desizing treatment
Endohydrolase 30%, beta amylase 10%, calcium chloride 1%, surfactant 5%, water 54% desizing substance, the temperature of desizing
At 50 DEG C, the desizing time is controlled in 1h for degree control；
S3: the cotton fabric fabric after above-mentioned desizing treatment is subjected to kiering processing, the kiering substance weight added in kiering
Number are as follows: 3 parts of dilute caustic soda, 10 parts of emulsifier, 10 parts of dispersing agent, 5 parts of chelated dispersants, 5 parts of bleeding agent, 50 parts of the first auxiliary agent,
The temperature control of 30 parts of hydrogen peroxide, 3 parts of tetraacetyl ethylene diamine and 150 parts of water, kiering is 50 DEG C, and the time control of kiering is 2h；
S4: carrying out mercerization finish for above-mentioned kiering treated cotton fabric fabric, first by sodium hydroxide when mercerization finish
10%, the second auxiliary agent 5% and water 85% are uniformly mixed, and then the fabric after kiering, which is put into mixed liquor, carries out mercerization finish；
S5: the cotton fabric fabric after mercerization finish is subjected to thermal finalization processing.
Embodiment 2 to embodiment 14 the difference from example 2 is that, the in the kiering substance added in S3 kiering processing
Each chemical composition of two auxiliary agents is as follows: by percentage to the quality
Embodiment 15 to embodiment 34 the difference from example 2 is that, in S3 kiering each chemical composition of kiering substance with
Parts by weight meter is as follows:
Embodiment 34 to embodiment 42 the difference from example 2 is that, eachization of desizing treatment substance in S2 desizing treatment
Composition is learned to be as follows: by percentage to the quality
Embodiment 43 to embodiment 50 the difference from example 2 is that, each chemistry of mercerizing agent in S4 mercerization finish
Composition is as follows: by percentage to the quality
Embodiment 51 to embodiment 62 the difference from example 2 is that, second helped in mercerizing agent in S4 mercerization finish
Each chemical composition of agent is as follows: by percentage to the quality
Embodiment 62 to embodiment 66 the difference from embodiment 1 is that, each chemical composition of emulsifier in S3 kiering processing
It is as follows: by percentage to the quality
Embodiment 66 to embodiment 70 the difference from embodiment 1 is that, the temperature of kiering is as follows: in S3 kiering processing
| Group | Embodiment 67 | Embodiment 68 | Embodiment 69 | Embodiment 70 |
| Temperature | 52.5 | 55 | 57.5 | 60 |
Embodiment 71 to embodiment 74 the difference from embodiment 1 is that, the desizing temperature of desizing treatment is as follows: in S2
| Group | Embodiment 71 | Embodiment 72 | Embodiment 73 | Embodiment 74 |
| Temperature | 52.5 | 55 | 57.5 | 60 |
Embodiment 75 to embodiment 78 the difference from embodiment 1 is that, the kiering time in S3 kiering processing is as follows:
| Group | Embodiment 75 | Embodiment 76 | Embodiment 77 | Embodiment 78 |
| The kiering time | 2.25 | 2.5 | 2.75 | 3 |
Embodiment 79 to embodiment 82 the difference from embodiment 1 is that, the desizing time in S2 desizing treatment is as follows:
| Group | Embodiment 79 | Embodiment 80 | Embodiment 81 | Embodiment 82 |
| The desizing time | 1.25 | 1.5 | 1.75 | 2 |
Comparative example
Comparative example 1: the difference from embodiment 1 is that the second auxiliary agent is not added；
Comparative example 2: the difference from embodiment 1 is that kiering is using concentrated sodium hydroxide progress kiering in S3.
Detection method
Alkaline spot test
Cloth after pre-treatment detects the cloth of different parts under Mingguang City, tests average transmittance.
| Embodiment | Light transmittance % |
| Embodiment 1 | 70 |
| Embodiment 2 | 71 |
| Embodiment 3 | 73 |
| Embodiment 4 | 71 |
| Embodiment 5 | 69 |
| Embodiment 6 | 72 |
| Embodiment 7 | 72 |
| Embodiment 8 | 73 |
| Embodiment 9 | 71 |
| Embodiment 10 | 72 |
| Embodiment 11 | 73 |
| Embodiment 12 | 68 |
| Embodiment 13 | 69 |
| Embodiment 14 | 72 |
| Comparative example 2 | 53 |
Conclusion: as seen from the above table, the light transmittance of comparative example 1 is far below embodiment 1-14, it can be seen that kiering in comparative example 2
Alkaline spot is had on cloth afterwards, so that the cutinase that the light transmittance of cloth is substantially reduced, and utilized in embodiment 1-14
Replace main kiering substance, effect is better, and the cloth handled is also more thoroughly, and light transmittance is higher.
Dye-uptake test
Comparative example 1, embodiment 51 to the cloth that the semi-finished product cloth in embodiment 62 cuts same size are put into identical
In dye liquor, upper dye 60min.Cloth is then taken out, then measures the suction of dye liquor in maximum absorption wave strong point with 722S spectrophotometer
Luminosity calculates dye-uptake with following formula:
Dye-uptake/%=(1-I/I °) × 100
In formula: I is raffinate absorbance after dyeing；I ° is dye liquor initial concentration absorbance.
| I | I° | Dye-uptake % | |
| Embodiment 51 | 0.525 | 0.824 | 36.28641 |
| Embodiment 52 | 0.523 | 0.824 | 36.52913 |
| Embodiment 53 | 0.526 | 0.824 | 36.16505 |
| Embodiment 54 | 0.522 | 0.824 | 36.65049 |
| Embodiment 55 | 0.415 | 0.824 | 49.63592 |
| Embodiment 56 | 0.387 | 0.824 | 53.03398 |
| Embodiment 57 | 0.256 | 0.824 | 68.93204 |
| Embodiment 58 | 0.235 | 0.824 | 71.48058 |
| Embodiment 59 | 0.503 | 0.824 | 38.95631 |
| Embodiment 60 | 0.496 | 0.824 | 39.80583 |
| Embodiment 61 | 0.486 | 0.824 | 41.01942 |
| Embodiment 62 | 0.473 | 0.824 | 42.59709 |
| Comparative example 1 | 0.585 | 0.824 | 29.00485 |
Conclusion: embodiment 51 to 62 can be seen that by upper table and the dye-uptake comparison of comparative example 1 finds out that addition second helps
The dye-uptake of agent treated semi-finished product cloth obviously rises, and illustrates that the second auxiliary agent enhances the fixation ability of cloth, so that dyestuff
Preferably it is attached on cloth.
The above is only a preferred embodiment of the present invention, protection scope of the present invention is not limited merely to above-mentioned implementation
Example, all technical solutions belonged under thinking of the present invention all belong to the scope of protection of the present invention.It should be pointed out that for the art
Those of ordinary skill for, several improvements and modifications without departing from the principles of the present invention, these improvements and modifications
It should be regarded as protection scope of the present invention.
Claims (8)
1. a kind of stamp pre-treating technology of cotton fabric, it is characterised in that: the pre-treating technology the following steps are included:
S1: cotton fabric fabric is subjected to processing of singing；
S2: it singes that treated by above-mentioned cotton fabric fabric carries out desizing treatment；
S3: carrying out kiering processing for the cotton fabric fabric after above-mentioned desizing treatment, the kiering substance added in the kiering it is each
Chemical composition is based on parts by weight are as follows: dilute caustic soda 3-5 parts, 10-20 parts of emulsifier, 10-20 parts of dispersing agent, chelated dispersants 5-10
Part, 5-8 parts of bleeding agent, 50-60 parts of the first auxiliary agent, 30-40 parts of hydrogen peroxide, 3-5 parts of tetraacetyl ethylene diamine and 150-200 parts of water；
S4: above-mentioned kiering treated cotton fabric fabric is subjected to mercerization finish；
S5: the cotton fabric fabric after mercerization finish is subjected to thermal finalization processing；
Cotton fabric semi-finished product cloth by above-mentioned five steps, after obtaining pre-treatment.
2. a kind of stamp pre-treating technology of cotton fabric according to claim 1, it is characterised in that: first auxiliary agent by
Following chemical composition forms by percentage to the quality: cutinase 20%-25%, two (ethoxy) tallow base amine oxides
0.1%-0.3%, dodecyl-β-D-Maltose glycosides 0.1%-0.3%, surplus are water.
3. a kind of stamp pre-treating technology of cotton fabric according to claim 1, it is characterised in that: the emulsifier by with
The group of lower mass percent is grouped as: polyoxyethylene sorbitan aliphatic ester 60%-70%, sldium lauryl sulfate 10%-
20% and sucrose ester 15%-20%.
4. a kind of stamp pre-treating technology of cotton fabric according to claim 1, it is characterised in that: in the S2 at desizing
Each chemical composition of the desizing substance added in reason is by percentage to the quality are as follows: 1,4- α-D- glucan hydrolase 30%-40%,
Beta amylase %10%-20%, calcium chloride 1%-5%, surfactant 5%-10%, surplus are water.
5. a kind of stamp pre-treating technology of cotton fabric according to claim 1, it is characterised in that: fabric is adopted in the S2
Desizing treatment is carried out with the mode padded, the temperature control of desizing treatment is 50-60 DEG C, and the control of desizing time is 1-2h, desizing
Complete fabric is washed again, is dried.
6. a kind of stamp pre-treating technology of cotton fabric according to claim 1, it is characterised in that: in the S4 at mercerising
Each chemical composition of the mercerising substance added in reason is by percentage to the quality are as follows: sodium hydroxide 10%-20%, the second auxiliary agent 5%-
10%, surplus is water.
7. a kind of stamp pre-treating technology of cotton fabric according to claim 6, it is characterised in that: second auxiliary agent by
Following chemical composition is by percentage to the quality are as follows: cationic surfactant 30%-40%, diethylenetriamine 5%-10%, ring
Oxygen chloropropane 5%-10%, quaternary ammonium salt etherifying agent 3%-5%, surplus are water.
8. a kind of stamp pre-treating technology of cotton fabric according to claim 1, it is characterised in that: temperature when kiering is handled
Degree control is 50-60 DEG C, and the kiering time is 2-3h.
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