CN109650504A - Ceramic tile production sewage treatment method and the method for making ceramic tile powder with recycling pug - Google Patents
Ceramic tile production sewage treatment method and the method for making ceramic tile powder with recycling pug Download PDFInfo
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- CN109650504A CN109650504A CN201910087199.9A CN201910087199A CN109650504A CN 109650504 A CN109650504 A CN 109650504A CN 201910087199 A CN201910087199 A CN 201910087199A CN 109650504 A CN109650504 A CN 109650504A
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- ceramic tile
- sewage
- pug
- precipitating
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Classifications
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/52—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
- C02F1/54—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using organic material
- C02F1/56—Macromolecular compounds
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/52—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
- C02F1/5236—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using inorganic agents
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F11/00—Treatment of sludge; Devices therefor
- C02F11/12—Treatment of sludge; Devices therefor by de-watering, drying or thickening
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/13—Compounding ingredients
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/13—Compounding ingredients
- C04B33/132—Waste materials; Refuse; Residues
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F2001/007—Processes including a sedimentation step
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P40/00—Technologies relating to the processing of minerals
- Y02P40/60—Production of ceramic materials or ceramic elements, e.g. substitution of clay or shale by alternative raw materials, e.g. ashes
Abstract
Present invention relates particularly to a kind of ceramic tile production sewage treatment method and the methods for making ceramic tile powder with recycling pug, belong to technical field of tile production.The present invention is by handling ceramic tile production waste, treated sewage and gained sediment recycling and reusing has been subjected to, recovery efficiency is high, wherein, gained sediment is used to make ceramic tile powder according to following mass fraction: according to 10-20 parts of the washing soil of mass fraction meter, imperial 2-9 parts of tiny stream kaolin, black earth 1-5 parts of ZhangZhou, clay 10-15 parts of Zhangpu, 0.5-2 parts of bentonite, carclazyte 2-10 parts of Guangdong, clay 6-12 parts of Xiamen, 1-5 parts of attaclay, albite 1-4 parts of Dehua, 10-15 parts of potassium feldspar, pug 10-15 parts of recycling, discarded 15-25 parts of ceramic tile blank.The performance of the ceramic tile made from above-mentioned ceramic tile powder can compare favourably with ceramic tile performance made from unused recycling pug.
Description
Technical field
The invention belongs to technical field of tile production, and in particular to a kind of ceramic tile production sewage treatment method and with recycling mud
The method of material production ceramic tile powder.
Background technique
Water consumption is very large in ceramic tile production process, and entire polish line is equal from preceding grinder sequence to rear grinder sequence whole process
It is be unable to do without water, kiln workshop and glaze preparation section are also required to a large amount of water, have in the production waste of ceramic tile more
Solid particle, and concentration is higher, if being discharged without handling, it will cause biggish harm to environment.
Therefore most ceramic tiles manufacturing enterprise can carry out ceramic tile sewage to handle and recycle to sewage, and treated
The recovery utilization rate of sediment is relatively low, and because sediment some contains glaze, some is free of glaze, therefore recycles purposes also not phase
Together, this just causes certain difficulty to the recycling and reusing of sediment to enterprise, can if all sediments are all made same purposes
The performance decline that ceramic tile can be will lead to, is not achieved standard.
Therefore the processing method of ceramic tile production waste is improved, and the recycling and reusing of sediment is studied,
The technical problem urgently to be resolved as this field.
Summary of the invention
A kind of ceramic tile production sewage treatment method is provided the purpose of the present invention is overcome the deficiencies in the prior art and with returning
The method for receiving pug production ceramic tile powder, it is sharp again that this method can carry out all recycling to the sewage generated in ceramic tile production process
With, waste residue in sewage can also whole recycling and reusings, at the same time it can also be carried out to the ceramic tile waste material generated in production process
Whole recycling and reusings, really realize zero-emission.
The present invention adopts the following technical scheme:
The present invention provides a kind of ceramic tile production sewage treatment method, includes the following steps:
Polish line sewage treatment:
The sewage that polish line is generated enters in the first sedimentation basin, and the first precipitating reagent is added and carries out first time precipitating；
Sewage is entered into the second sedimentation basin, second of precipitating of the second precipitating reagent progress is added；
Sewage is entered into third sedimentation basin, third precipitating reagent is added and carries out third time precipitating, by the clear water by precipitating three times
It is directly evacuated to polish line and carries out secondary use, each pug clearing and retrieving for precipitating bottom of pond portion is used as ceramic body to the storage of material library
Raw material；
Sewage, drying tower sewage treatment between kiln workshop sewage, glaze waterwheel:
The sewage that above-mentioned each production process generates is entered in the first sedimentation basin, the first precipitating reagent is added and carries out first time precipitating；
Sewage is entered into the second sedimentation basin, second of precipitating of the second precipitating reagent progress is added；
Sewage is entered in third sedimentation basin and is squeezed, the clear water obtained after processing is stored, as ball milling water；
First sedimentation basin, the pug in the second sedimentation basin and the pug clearing and retrieving after squeezing are used as ceramic blank to the storage of material library
Body raw material.
Further, first precipitating reagent is aluminium polychloride, and additive amount is the 0.08%- of sewage gross mass
0.12%。
Further, second precipitating reagent is polyacrylamide, and additive amount is the 0.05%- of sewage gross mass
0.10%。
Further, the third precipitating reagent is aluminium polychloride or polyacrylamide, and additive amount is sewage gross mass
0.05%-0.08%.
The present invention also provides the recycling pugs handled with the ceramic tile production sewage treatment method to make tile powder
The method of material, includes the following steps:
Step 1: will be according to 10-20 parts of the washing soil of mass fraction meter, imperial 2-9 parts of tiny stream kaolin, black earth 1-5 parts of ZhangZhou, Zhangpu
10-15 parts of clay, 0.5-2 parts of bentonite, carclazyte 2-10 parts of Guangdong, clay 6-12 parts of Xiamen, 1-5 parts of attaclay, Dehua sodium
1-4 parts of feldspar, 10-15 parts of potassium feldspar, recycling pug 10-15 parts and 15-25 parts of discarded ceramic tile blank, mixing and water adding ball milling, mistake
Sieve, discharging, material moisture 34%-36%；
Step 2: the material that step 1 obtains is sieved after except iron, and dry to water content 7.0%-8.0%, obtains powder.
Further, Ball-milling Time described in step 1 is 12-14h, and the water that when ball milling is added is the 30%- of blank
40%, the sieving is to sieve with 100 mesh sieve.
Further, sieving described in step 2 was 80 meshes.
Compared with the prior art, the present invention has the following beneficial effects:
The present invention utilizes two sewage treatment lines, has carried out recycling and reusing to the whole sewage generated in ceramic tile production process,
Waste residue in sewage can also be completely recovered as blank raw material, meanwhile, the ceramic tile waste material generated in production process can also be complete
Portion's recycling and reusing, really realizes zero-emission.
Meanwhile the ceramic tile made from ceramic tile powder of the present invention, performance can be with ceramic tile performances made from unused recycling pug
It compares favourably.
Specific embodiment
Below by specific embodiment, invention is further described in detail, but those skilled in the art will manage
Solution, the following example is merely to illustrate the present invention, and should not be taken as limiting the scope of the invention.
Embodiment 1
The present invention provides a kind of ceramic tile production sewage treatment method, includes the following steps:
Polish line sewage treatment:
The sewage that polish line is generated enters in the first sedimentation basin, and the aluminium polychloride that sewage gross mass 0.10% is added carries out the
Primary sedimentation；
Sewage is entered into second of precipitating of polyacrylamide progress that sewage gross mass 0.08% is added in the second sedimentation basin；
Sewage is entered into third sedimentation basin, the aluminium polychloride or polyacrylamide that sewage gross mass 0.06% is added carry out the
It precipitates three times, carries out secondary use for polish line is directly evacuated to by the clear water precipitated three times, each pug for precipitating bottom of pond portion is clear
Reason is recycled to the storage of material library, is used as ceramic body raw material；
Sewage, drying tower sewage treatment between kiln workshop sewage, glaze waterwheel:
The sewage that above-mentioned each production process generates is entered in the first sedimentation basin, the polyaluminium of sewage gross mass 0.10% is added
Aluminium carries out first time precipitating；
Sewage is entered into second of precipitating of polyacrylamide progress that sewage gross mass 0.08% is added in the second sedimentation basin；
Sewage is entered in third sedimentation basin and is squeezed, the clear water obtained after processing is stored, as ball milling water；
First sedimentation basin, the pug in the second sedimentation basin and the pug clearing and retrieving after squeezing are used as ceramic blank to the storage of material library
Body raw material.
With the method for the recycling pug production ceramic tile powder that above-mentioned sewage treatment obtains, include the following steps:
Step 1: by 15 parts of washing soil, imperial 5 parts of the tiny stream kaolin, 5 parts of ZhangZhou black earth, Zhangpu clay 13 according to mass fraction meter
Part, 1 part of bentonite, 6 parts of Guangdong carclazyte, 9 parts of Xiamen clay, 2.5 parts of attaclay, 2 parts of Dehua albite, potassium feldspar 13.5
Part, recycling 12 parts of pug and 20 parts of discarded ceramic tile blank, mixing and water adding ball milling 3h, the water that when ball milling is added is the 30%- of blank
40%, it sieves with 100 mesh sieve, discharges, material moisture 34%-36%；
Step 2: the material that step 1 obtains is sieved with 100 mesh sieve after except iron, and dry to water content 7.0%-8.0%, obtains powder
Material.
Embodiment 2
The present invention provides a kind of ceramic tile production sewage treatment method, includes the following steps:
Polish line sewage treatment:
The sewage that polish line is generated enters in the first sedimentation basin, and the aluminium polychloride that sewage gross mass 0.08% is added carries out the
Primary sedimentation；
Sewage is entered into second of precipitating of polyacrylamide progress that sewage gross mass 0.10% is added in the second sedimentation basin；
Sewage is entered into third sedimentation basin, the aluminium polychloride or polyacrylamide that sewage gross mass 0.08% is added carry out the
It precipitates three times, carries out secondary use for polish line is directly evacuated to by the clear water precipitated three times, each pug for precipitating bottom of pond portion is clear
Reason is recycled to the storage of material library, is used as ceramic body raw material；
Sewage, drying tower sewage treatment between kiln workshop sewage, glaze waterwheel:
The sewage that above-mentioned each production process generates is entered in the first sedimentation basin, the polyaluminium of sewage gross mass 0.08% is added
Aluminium carries out first time precipitating；
Sewage is entered into second of precipitating of polyacrylamide progress that sewage gross mass 0.10% is added in the second sedimentation basin；
Sewage is entered in third sedimentation basin and is squeezed, the clear water obtained after processing is stored, as ball milling water；
First sedimentation basin, the pug in the second sedimentation basin and the pug clearing and retrieving after squeezing are used as ceramic blank to the storage of material library
Body raw material.
With the method for the recycling pug production ceramic tile powder that above-mentioned sewage treatment obtains, include the following steps:
Step 1: by 10 parts of washing soil, imperial 2 parts of the tiny stream kaolin, 1 part of ZhangZhou black earth, Zhangpu clay 10 according to mass fraction meter
Part, 0.5 part of bentonite, 2 parts of Guangdong carclazyte, 6 parts of Xiamen clay, 1 part of attaclay, 1 part of Dehua albite, 10 parts of potassium feldspar,
Recycle 15 parts of 10 parts of pug and discarded ceramic tile blank, mixing and water adding ball milling 12h, the water that when ball milling is added is the 30%- of blank
40%, it sieves with 100 mesh sieve, discharges, material moisture 34%-36%；
Step 2: the material that step 1 obtains is sieved with 100 mesh sieve after except iron, and dry to water content 7.0%-8.0%, obtains powder
Material.
Embodiment 3
The present invention provides a kind of ceramic tile production sewage treatment method, includes the following steps:
Polish line sewage treatment:
The sewage that polish line is generated enters in the first sedimentation basin, and the aluminium polychloride that sewage gross mass 0.12% is added carries out the
Primary sedimentation；
Sewage is entered into second of precipitating of polyacrylamide progress that sewage gross mass 0.05% is added in the second sedimentation basin；
Sewage is entered into third sedimentation basin, the aluminium polychloride or polyacrylamide that sewage gross mass 0.05% is added carry out the
It precipitates three times, carries out secondary use for polish line is directly evacuated to by the clear water precipitated three times, each pug for precipitating bottom of pond portion is clear
Reason is recycled to the storage of material library, is used as ceramic body raw material；
Sewage, drying tower sewage treatment between kiln workshop sewage, glaze waterwheel:
The sewage that above-mentioned each production process generates is entered in the first sedimentation basin, the polyaluminium of sewage gross mass 0.12% is added
Aluminium carries out first time precipitating；
Sewage is entered into second of precipitating of polyacrylamide progress that sewage gross mass 0.10% is added in the second sedimentation basin；
Sewage is entered in third sedimentation basin and is squeezed, the clear water obtained after processing is stored, as ball milling water；
First sedimentation basin, the pug in the second sedimentation basin and the pug clearing and retrieving after squeezing are used as ceramic blank to the storage of material library
Body raw material.
With the method for the recycling pug production ceramic tile powder that above-mentioned sewage treatment obtains, include the following steps:
Step 1: by 20 parts of washing soil, imperial 9 parts of the tiny stream kaolin, 5 parts of ZhangZhou black earth, Zhangpu clay 15 according to mass fraction meter
Part, 2 parts of bentonite, 10 parts of Guangdong carclazyte, 12 parts of Xiamen clay, 5 parts of attaclay, 4 parts of Dehua albite, 15 parts of potassium feldspar,
Recycle 25 parts of 15 parts of pug and discarded ceramic tile blank, mixing and water adding ball milling 14h, the water that when ball milling is added is the 30%- of blank
40%, it sieves with 100 mesh sieve, discharges, material moisture 34%-36%；
Step 2: the material that step 1 obtains is sieved with 100 mesh sieve after except iron, and dry to water content 7.0%-8.0%, obtains powder
Material.
Reference examples
The difference from embodiment 1 is that the recycling pug in ceramic tile powder is replaced with potassium feldspar.
In the same manner, it is fabricated to unglazed marble respectively with embodiment 1 to 3, the resulting powder of reference examples
Adobe body, and 60min is fired at 1150 DEG C, the wear-resistant volume of unglazed tile is tested ,≤175mm is met3Requirement, test
Method is GB/T 3810.6, as a result as shown in table 1 below:
1 test result of table
| Test item | Embodiment 1 | Embodiment 2 | Embodiment 3 | Reference examples |
| The wear volume of resistance to depth, mm3 | 50 | 54 | 50 | 55 |
The basic principles and main features and advantages of the present invention of the invention, the technology of the industry has been shown and described above
Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the above embodiments and description only describe this
The principle of invention, under the premise of not departing from the inventive spirit of the present invention and range, various changes and improvements may be made to the invention, this
A little changes and improvements all fall within the protetion scope of the claimed invention, and the claimed scope of the invention is by appended claims
And its equivalent thereof.
Claims (7)
1. ceramic tile production sewage treatment method, which comprises the steps of:
Polish line sewage treatment:
The sewage that polish line is generated enters in the first sedimentation basin, and the first precipitating reagent is added and carries out first time precipitating；
Sewage is entered into the second sedimentation basin, second of precipitating of the second precipitating reagent progress is added；
Sewage is entered into third sedimentation basin, third precipitating reagent is added and carries out third time precipitating, by the clear water by precipitating three times
It is directly evacuated to polish line and carries out secondary use, each pug clearing and retrieving for precipitating bottom of pond portion is used as ceramic body to the storage of material library
Raw material；
Sewage, drying tower sewage treatment between kiln workshop sewage, glaze waterwheel:
The sewage that above-mentioned each production process generates is entered in the first sedimentation basin, the first precipitating reagent is added and carries out first time precipitating；
Sewage is entered into the second sedimentation basin, second of precipitating of the second precipitating reagent progress is added；
Sewage is entered in third sedimentation basin and is squeezed, the clear water obtained after processing is stored, as ball milling water；
First sedimentation basin, the pug in the second sedimentation basin and the pug clearing and retrieving after squeezing are used as ceramic blank to the storage of material library
Body raw material.
2. ceramic tile production sewage treatment method according to claim 1, which is characterized in that first precipitating reagent is polymerization
Aluminium chloride, additive amount are the 0.08%-0.12% of sewage gross mass.
3. ceramic tile production sewage treatment method according to claim 1, which is characterized in that second precipitating reagent is poly- third
Acrylamide, additive amount are the 0.05%-0.10% of sewage gross mass.
4. ceramic tile production sewage treatment method according to claim 1, which is characterized in that the third precipitating reagent is polymerization
Aluminium chloride or polyacrylamide, additive amount are the 0.05%-0.08% of sewage gross mass.
5. with the side for the recycling pug production ceramic tile powder that ceramic tile production sewage treatment method described in claim 1 is handled
Method, which comprises the steps of:
Step 1: will be according to 10-20 parts of the washing soil of mass fraction meter, imperial 2-9 parts of tiny stream kaolin, black earth 1-5 parts of ZhangZhou, Zhangpu
10-15 parts of clay, 0.5-2 parts of bentonite, carclazyte 2-10 parts of Guangdong, clay 6-12 parts of Xiamen, 1-5 parts of attaclay, Dehua sodium
1-4 parts of feldspar, 10-15 parts of potassium feldspar, recycling pug 10-15 parts and 15-25 parts of discarded ceramic tile blank, mixing and water adding ball milling, mistake
Sieve, discharging, material moisture 34%-36%；
Step 2: the material that step 1 obtains is sieved after except iron, and dry to water content 7.0%-8.0%, obtains powder.
6. the recycling pug production ceramic tile powder according to claim 5 handled with ceramic tile production sewage treatment method
Method, which is characterized in that Ball-milling Time described in step 1 is 12-14h, and the water that when ball milling is added is the 30%- of blank
40%, the sieving is to sieve with 100 mesh sieve.
7. the recycling pug production ceramic tile powder according to claim 5 handled with ceramic tile production sewage treatment method
Method, which is characterized in that described in step 2 sieving be 80 meshes.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201910087199.9A CN109650504A (en) | 2019-01-29 | 2019-01-29 | Ceramic tile production sewage treatment method and the method for making ceramic tile powder with recycling pug |
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| CN201910087199.9A CN109650504A (en) | 2019-01-29 | 2019-01-29 | Ceramic tile production sewage treatment method and the method for making ceramic tile powder with recycling pug |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110451926A (en) * | 2019-07-04 | 2019-11-15 | 东莞市唯美装饰材料有限公司 | A method of using building site waste mud for Ceramic Tiles |
| CN115124321A (en) * | 2022-06-10 | 2022-09-30 | 东莞市唯美陶瓷工业园有限公司 | Sewage sludge for preparing ceramic tiles, antique tiles and preparation method of sewage sludge |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110451926A (en) * | 2019-07-04 | 2019-11-15 | 东莞市唯美装饰材料有限公司 | A method of using building site waste mud for Ceramic Tiles |
| CN115124321A (en) * | 2022-06-10 | 2022-09-30 | 东莞市唯美陶瓷工业园有限公司 | Sewage sludge for preparing ceramic tiles, antique tiles and preparation method of sewage sludge |
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Application publication date: 20190419 |
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