CN109646981A - A kind of acetic acid rectifying and dewatering Tower System - Google Patents

A kind of acetic acid rectifying and dewatering Tower System Download PDF

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Publication number
CN109646981A
CN109646981A CN201811407917.8A CN201811407917A CN109646981A CN 109646981 A CN109646981 A CN 109646981A CN 201811407917 A CN201811407917 A CN 201811407917A CN 109646981 A CN109646981 A CN 109646981A
Authority
CN
China
Prior art keywords
tower body
stainless steel
tower
steel wire
automatic washing
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201811407917.8A
Other languages
Chinese (zh)
Inventor
田翠香
齐彬
李海峰
周湘衡
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
JEREH (TIANJIN) PETROLEUM ENGINEERING & TECHNOLOGIES Co Ltd
Original Assignee
JEREH (TIANJIN) PETROLEUM ENGINEERING & TECHNOLOGIES Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by JEREH (TIANJIN) PETROLEUM ENGINEERING & TECHNOLOGIES Co Ltd filed Critical JEREH (TIANJIN) PETROLEUM ENGINEERING & TECHNOLOGIES Co Ltd
Priority to CN201811407917.8A priority Critical patent/CN109646981A/en
Publication of CN109646981A publication Critical patent/CN109646981A/en
Pending legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14Fractional distillation or use of a fractionation or rectification column
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • C07C51/47Separation; Purification; Stabilisation; Use of additives by solid-liquid treatment; by chemisorption

Abstract

The invention discloses a kind of acetic acid rectifying and dewatering Tower Systems, cold blowing gas air inlet pipe and regeneration gas escape pipe, the bottom of the process equipment is equipped with the second blow vent, clean gas escape pipe, cold blowing gas escape pipe and regeneration gas air inlet pipe, this molecular sieve water separation tower, the equal face tower body setting in the outlet side of gas distributor are installed at second blow vent, make gas being distributed in tower body more evenly, keep the intracorporal molecular sieve water sucting degree of tower roughly the same, extend dewatering time, improves dehydration efficiency.

Description

A kind of acetic acid rectifying and dewatering Tower System
Technical field
The present invention relates to molecular sieve dehydration technical field, specially a kind of acetic acid rectifying and dewatering Tower System.
Background technique
Existing molecular sieve water separation tower, it cannot be guaranteed that gas uniformly divides not in tower body, is led in dehydration, regenerative process It causes the intracorporal molecular sieve water suction of tower, degree of dehydration different, causes regenerated frequency to improve, increase production cost;Some molecules Sieve dehydrating tower molecular sieve is only laid in stainless steel wire, and online, molecular sieve water swelling is reduced since the number of molecular sieve is more The influence that molecular sieve gravity expands molecular sieve.For this purpose, it is proposed that a kind of acetic acid rectifying and dewatering Tower System.
Summary of the invention
It is mentioned above in the background art to solve the purpose of the present invention is to provide a kind of acetic acid rectifying and dewatering Tower System Problem.
To achieve the above object, the invention provides the following technical scheme: a kind of acetic acid rectifying and dewatering Tower System, including tower Body, upper cover, process equipment and molecular sieve, are respectively and fixedly provided with positive flange at the top and bottom of the tower body, the bottom of the upper cover and Anti- flange is respectively and fixedly provided at the top of process equipment, the positive flange at the top and bottom of the tower body pass through bolt respectively with upper base Portion is fixedly connected with the anti-flange at the top of process equipment, and the top of the upper cover is equipped with the first blow vent, first blow vent Place is equipped with wet purification gas air inlet pipe, cold blowing gas air inlet pipe and regeneration gas escape pipe, and the bottom of the process equipment is equipped with second Blow vent is equipped with clean gas escape pipe, cold blowing gas escape pipe and regeneration gas air inlet pipe at second blow vent, described Stainless steel wire filter is fixed at tower body medial center, the surface that stainless steel wire filter is located on the inside of the tower body is fixed in parallel There are two automatic washing brush device, the underface of stainless steel wire filter is located on the inside of the tower body, and fixed in parallel there are three full-automatic Cleaning machine between the automatic washing brush device, is filled with porcelain ball, is located at not on the inside of the tower body between automatic washing machine The two sides of rust steel wire spacer are symmetrically fixed with third stainless steel cloth, be located on the inside of the tower body stainless steel wire filter and it is complete from Molecular sieve is filled between stainless steel wire filter and automatic washing machine between dynamic washing and brushing device and on the inside of tower body.
Specific embodiment
Below in conjunction with the embodiment of the present invention, technical scheme in the embodiment of the invention is clearly and completely described, Obviously, described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Based in the present invention Embodiment, every other embodiment obtained by those of ordinary skill in the art without making creative efforts, all Belong to the scope of protection of the invention.
Including tower body, upper cover, process equipment and molecular sieve, positive flange, institute are respectively and fixedly provided at the top and bottom of the tower body It states and is respectively and fixedly provided with anti-flange at the top of the bottom and process equipment of upper cover, the positive flange at the top and bottom of the tower body passes through spiral shell Bolt is fixedly connected with the anti-flange at the top of upper cover bottom and process equipment respectively, and the top of the upper cover is equipped with the first blow vent, Wet purification gas air inlet pipe, cold blowing gas air inlet pipe and regeneration gas escape pipe, the process equipment are installed at first blow vent Bottom be equipped with the second blow vent, clean gas escape pipe, cold blowing gas escape pipe and again are installed at second blow vent Angry air inlet pipe is fixed with stainless steel wire filter at the tower body medial center, is located at stainless steel wire filter on the inside of the tower body Surface it is fixed there are two automatic washing brush device in parallel, the underface that stainless steel wire filter is located on the inside of the tower body is parallel It is fixed there are three automatic washing machine, between the automatic washing brush device, porcelain ball, institute are filled between automatic washing machine It states the two sides on the inside of tower body positioned at stainless steel wire filter and is symmetrically fixed with third stainless steel cloth, be located at not on the inside of the tower body It becomes rusty between steel wire spacer and automatic washing brush device and tower body inside is equal between stainless steel wire filter and automatic washing machine Filled with molecular sieve.
It should be noted that, in this document, relational terms such as first and second and the like are used merely to a reality Body or operation are distinguished with another entity or operation, are deposited without necessarily requiring or implying between these entities or operation In any actual relationship or order or sequence.Moreover, the terms "include", "comprise" or its any other variant are intended to Non-exclusive inclusion, so that the process, method, article or equipment including a series of elements is not only wanted including those Element, but also including other elements that are not explicitly listed, or further include for this process, method, article or equipment Intrinsic element.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with A variety of variations, modification, replacement can be carried out to these embodiments without departing from the principles and spirit of the present invention by understanding And modification, the scope of the present invention is defined by the appended.

Claims (1)

1. a kind of acetic acid rectifying and dewatering Tower System, it is characterised in that: including tower body, upper cover, process equipment and molecular sieve, the tower It is respectively and fixedly provided with positive flange at the top and bottom of body, anti-flange, institute are respectively and fixedly provided at the top of the bottom of the upper cover and process equipment State the positive flange at the top and bottom of tower body pass through bolt respectively with the anti-flange at the top of upper cover bottom and process equipment is fixed connects Connect, the top of the upper cover is equipped with the first blow vent, be equipped at first blow vent wet purification gas air inlet pipe, cold blowing gas into Tracheae and regeneration gas escape pipe, the bottom of the process equipment are equipped with the second blow vent, are equipped at second blow vent dry Purification gas escape pipe, cold blowing gas escape pipe and regeneration gas air inlet pipe, be fixed at the tower body medial center stainless steel wire every Net, positioned at the surface of stainless steel wire filter, there are two automatic washing brush device, the tower bodies for fixation in parallel for the tower body inside It is fixed there are three automatic washing machine in parallel that inside is located at the underface of stainless steel wire filter, the automatic washing brush device it Between, porcelain ball is filled between automatic washing machine, the two sides that stainless steel wire filter is located on the inside of the tower body are symmetrically fixed There are third stainless steel cloth, tower body inside position between stainless steel wire filter and automatic washing brush device and on the inside of tower body Molecular sieve is filled between stainless steel wire filter and automatic washing machine.
CN201811407917.8A 2018-11-23 2018-11-23 A kind of acetic acid rectifying and dewatering Tower System Pending CN109646981A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201811407917.8A CN109646981A (en) 2018-11-23 2018-11-23 A kind of acetic acid rectifying and dewatering Tower System

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201811407917.8A CN109646981A (en) 2018-11-23 2018-11-23 A kind of acetic acid rectifying and dewatering Tower System

Publications (1)

Publication Number Publication Date
CN109646981A true CN109646981A (en) 2019-04-19

Family

ID=66112186

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201811407917.8A Pending CN109646981A (en) 2018-11-23 2018-11-23 A kind of acetic acid rectifying and dewatering Tower System

Country Status (1)

Country Link
CN (1) CN109646981A (en)

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2508234A (en) * 2012-11-27 2014-05-28 Endet Ltd Molecular-sieve vessel
CN204447690U (en) * 2014-12-19 2015-07-08 中国石油天然气股份有限公司 Molecular sieve water separation tower
US20150224420A1 (en) * 2014-02-07 2015-08-13 Robert Hickey Processes for the production of plural anhydrous alcohols
CN206746016U (en) * 2017-05-05 2017-12-15 西北民族大学 Novel distillation is dehydrated purifying plant
CN207047175U (en) * 2017-07-19 2018-02-27 益通天然气股份有限公司 Liquefied natural gas (LNG) production dehydration device
CN208742249U (en) * 2018-08-07 2019-04-16 杰瑞(天津)石油工程技术有限公司 A kind of novel molecular sieve dehydrating tower

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2508234A (en) * 2012-11-27 2014-05-28 Endet Ltd Molecular-sieve vessel
US20150224420A1 (en) * 2014-02-07 2015-08-13 Robert Hickey Processes for the production of plural anhydrous alcohols
CN204447690U (en) * 2014-12-19 2015-07-08 中国石油天然气股份有限公司 Molecular sieve water separation tower
CN206746016U (en) * 2017-05-05 2017-12-15 西北民族大学 Novel distillation is dehydrated purifying plant
CN207047175U (en) * 2017-07-19 2018-02-27 益通天然气股份有限公司 Liquefied natural gas (LNG) production dehydration device
CN208742249U (en) * 2018-08-07 2019-04-16 杰瑞(天津)石油工程技术有限公司 A kind of novel molecular sieve dehydrating tower

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Application publication date: 20190419