CN109626652A - A kind of Integrated Processing Unit for Chemical Manufacture waste material - Google Patents

A kind of Integrated Processing Unit for Chemical Manufacture waste material Download PDF

Info

Publication number
CN109626652A
CN109626652A CN201910040934.0A CN201910040934A CN109626652A CN 109626652 A CN109626652 A CN 109626652A CN 201910040934 A CN201910040934 A CN 201910040934A CN 109626652 A CN109626652 A CN 109626652A
Authority
CN
China
Prior art keywords
reaction kettle
tube
waste material
processing unit
chemical manufacture
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
CN201910040934.0A
Other languages
Chinese (zh)
Inventor
黄婷静
卢清伟
卢静馨
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Priority to CN201910040934.0A priority Critical patent/CN109626652A/en
Publication of CN109626652A publication Critical patent/CN109626652A/en
Withdrawn legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/001Processes for the treatment of water whereby the filtration technique is of importance
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B11/00Oxides or oxyacids of halogens; Salts thereof
    • C01B11/04Hypochlorous acid
    • C01B11/06Hypochlorites
    • C01B11/062Hypochlorites of alkali metals
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01DCOMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D3/00Halides of sodium, potassium or alkali metals in general
    • C01D3/04Chlorides
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2101/00Nature of the contaminant
    • C02F2101/10Inorganic compounds
    • C02F2101/16Nitrogen compounds, e.g. ammonia
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/10Process efficiency

Abstract

The invention discloses a kind of Integrated Processing Units for Chemical Manufacture waste material, including collecting pit, pump, drinking-water pipe, filter device, first hydrops slot, first inlet tube, feeding device, inlet duct, outlet tube, exhaust apparatus, supercharging device, refrigerating plant, collecting tank and reaction kettle, reaction kettle is connected with the first inlet tube, feeding device, inlet duct, exhaust apparatus and outlet tube, the other end of exhaust apparatus is connected with supercharging device, the other end of supercharging device is connected with refrigerating plant, the lower end of refrigerating plant is connected with collecting tank, the reaction kettle and filter device are supported by support leg, the waste material that the present invention will generate in two kinds of common chemical production process, in a manner of NaOH solution is added, make its mutual absorbing reaction, make available Chemical Manufacture raw material, realization is turned waste into wealth, energy-saving and emission-reduction Target is suitble to promote the use of in chemical spent material processing system.

Description

A kind of Integrated Processing Unit for Chemical Manufacture waste material
Technical field
The present invention relates to field of chemical equipment, specifically a kind of Integrated Processing Unit for Chemical Manufacture waste material.
Background technique
Nitrogen is the nutritional ingredient in water body, but when ammonia nitrogen concentration increases in water, will cause the richness in nutrition of water body Pollution, consequence are the growth of aquatile madness, are decomposed by the microorganisms after dead and consume a large amount of oxygen, to keep water body tight Weight anoxic, leads to aquatile mortality, corrupt dead body leads to the mass propagation of anerobe again, finally makes Water body muddiness, stench, cause serious water pollution.Ammonia-nitrogen content is no more than 25mg/L in national regulation waste discharge, Steel, oil refining, chemical fertilizer, inorganic chemical industry, ferroalloy, glass manufacture, meat packing and Feed Manufacturing etc. are industrial, discharge high concentration Ammonia nitrogen waste water.
Nitrogen oxides can stimulate lung, make one the more difficult respiratory disease for resisting flu etc, and respiratory system is problematic Personage such as asthmatics, can be influenced compared with vulnerable to nitrogen dioxide, for children, nitrogen oxides be likely to result in lung development It is impaired.Research points out that sucking nitrogen oxides for a long time may result in lung's structural change, but still not can determine leads to this consequence Amount of nitrogen oxides and sucking gas time.
Excessive ammonia nitrogen, which is discharged into water body, will lead to water eutrophication, reduce water body ornamental value, and be oxidized generation NO3-N and NO2-N also will affect the aquatile even health of the mankind.Therefore, extensive pass of the wastewater treatment by people Note.Currently, requirement of the main processing method to equipment is very high, cost is excessively high, while can not be to the generation of ammonium ion It is recycled, for thorough pollution administration, it is necessary to find suitable ammonia nitrogen sewage treatment equipment, solve to produce in Chemical Manufacture The pollution problem of the ammonia nitrogen waste water generated in the raw mix waste gas containing chlorine and oxynitrides and industrial production.
Summary of the invention
The purpose of the present invention is to provide a kind of Integrated Processing Units for Chemical Manufacture waste material, to solve above-mentioned background The problem of being proposed in technology.
To achieve the above object, the invention provides the following technical scheme:
A kind of Integrated Processing Unit for Chemical Manufacture waste material, including collecting pit, pump, drinking-water pipe, filter device, first Hydrops slot, the first inlet tube, feeding device, inlet duct, outlet tube, exhaust apparatus, supercharging device, refrigerating plant, collecting tank And reaction kettle, the top and bottom of reaction kettle are pyramidal structure, upper position is connected with the first inlet tube on the left of reaction kettle, described The first inlet tube other end is connected with the first hydrops slot, is fixedly connected with filter device, the mistake above the first hydrops slot It filters the position that keeps left at the top of device and is connected with drinking-water pipe, the other end of the drinking-water pipe is connected with pump, and the pump is set in collecting pit In chamber, the pump is driven by external power supply, and the reaction kettle top left hand is connected with feeding device, among the reaction kettle top Position is connected with inlet duct, and exhaust apparatus, the other end connection of the exhaust apparatus are connected on the right side of the reaction kettle top There is supercharging device, the other end of the supercharging device is connected with refrigerating plant, and the lower end of the refrigerating plant is connected with collecting tank, Reaction kettle bottom end middle position is connected with outlet tube, and the reaction kettle and filter device are supported by support leg.
As a further solution of the present invention: the filter device includes filter device shell, the filter device shell Top side and drinking-water pipe are connected, and the filter device housing bottom is equipped with the second filter screen, the filter device shell lower section Equipped with the first hydrops slot, punching press room is equipped in the filter device shell, the punching press room is equipped with first close to two sides of the bottom and inhales Liquid mouth, first liquid sucting port are equipped with the first filter screen, and punching press room bottom is equipped with the first liquid outlet, second filtering Net is located on the first liquid outlet, and punching press indoor activity is equipped with piston, the sectional dimension and the sectional dimension phase of punching press room of piston Cooperate, push rod is fixed on the piston, the end of the push rod passes through punching press ceiling portion and extends to outside filter device shell, institute Filter device case top is stated equipped with linear bearing, the pushing rod sleeve is in linear bearing, and the push rod is in linear bearing Do straight reciprocating motion.
As a further solution of the present invention: the top middle portion of the filter device shell is equipped with driving wheel, the drive Driving wheel and external motor are drivingly connected, and are hinged with connecting rod on driving wheel wheel face, the other end and push rod of connecting rod are hinged.
As a further solution of the present invention: first inlet tube is equipped with first pressure valve.
As a further solution of the present invention: the inlet duct includes third pressure valve, air inlet buffer unit, central tube And branch pipe, the third pressure valve and air inlet buffer unit are set to one end that central tube stretches out reaction kettle, the central tube is another End is passed down through reaction kettle and extend into reactor bottom, and the central tube lower end is equipped with branch pipe.
As a further solution of the present invention: the branch pipe is helical structure, the branch pipe be equipped with it is several obliquely Tap, endcapped of the branch pipe far from central tube.
As a further solution of the present invention: the air inlet buffer unit includes annular chamber, buffers filler and sieve, described Annular chamber is connected with third pressure valve one end, the other end of the annular chamber is connected with central tube, is equipped in the annular chamber Heart pipe, the central tube are located in the middle part of annular chamber, are equipped with buffering filler on annular chamber top.
As a further solution of the present invention: the buffering filler is steel wool.
As a further solution of the present invention: the feeding device includes the second hydrops slot, second pressure valve, the second feed liquor Feeding device is fixed on reaction kettle by pipe and feeding device support frame, the feeding device support frame, second inlet tube One end extend into reactor bottom obliquely through reaction kettle, and the other end of second inlet tube is connected with second pressure valve, the The other end of two pressure valve is connected with the second hydrops slot.
As a further solution of the present invention: the bottom middle position of the reaction kettle is equipped with the second fluid hole, institute It states and is connected with outlet tube on the second fluid hole, be additionally provided with flapper valve on outlet tube.
As a further solution of the present invention: the exhaust apparatus includes venthole, desiccant and check valve, the outlet Hole is set on the right side of reaction kettle top, and exhaust apparatus is provided with one section of U-tube, is supported by U-tube support frame, be filled in U-tube Desiccant.
As a further solution of the present invention: several groups blower is in series in the supercharging device.
As a further solution of the present invention: the refrigerating plant is circumscribed with refrigeration controler, the refrigeration in refrigerating plant Refrigeration controler outside element and refrigerating plant is electrically connected.
As a further solution of the present invention: the U-tube support frame includes support ring and chassis, and the support ring is half Circular configuration, support ring have top pillar, and top pillar lower end is equipped with thread groove, is equipped with threaded hole and thread groove spiral shell in the middle part of the chassis Conjunction is screwed, the tray bottom is additionally provided with chassis mounting hole.
Compared with prior art, the beneficial effects of the present invention are: the ammonia nitrogen waste water generated in industrial production is collected into receipts Collect in pond, into after crossing filter device suction filtration, into reaction kettle, when solution did not had branch pipe, is passed through into inlet duct The mix waste gas containing chlorine and oxynitrides generated in the Chemical Manufacture being passed through, while NaOH is passed through into feeding device Solution, the ammonia for reacting generation are discharged from exhaust apparatus, liquefy into the pressurization of supercharging device and refrigerating plant excessively and after cooling down Collected in into collecting tank, the solution after fully reacting is discharged through outlet tube, the main component in solution after reaction be sodium chloride and Sodium hypochlorite ingredient can be used as the use of chemical reaction raw material.Reaction principle is as follows:
NH4 ++3Cl2=NCl3+3HC1+H+
NH3+ 3H ClO=NCl3+3H20
3NaOH+NCl3=NH3↑+3NaClO
NaOH+HC1=NaC1+H20
NO+NO2+2NH3·H2O=2NH4 +++2NO2 -+2H2O
NH4 ++OH-=NH3↑+H20
In conclusion the present invention is by the waste material that will generate in two kinds of common chemical production process, it is molten NaOH is added The mode of liquid makes its mutual absorbing reaction, makes available Chemical Manufacture raw material, and realization is turned waste into wealth, energy-saving and emission-reduction Target, be suitble to chemical spent material processing system promote the use of.
Detailed description of the invention
Fig. 1 is the structural diagram of the present invention.
Fig. 2 is the structural schematic diagram of reaction kettle in the present invention.
Fig. 3 is the structural schematic diagram of U-tube support frame of the present invention.
In figure: 1- collecting pit, 2- pump, 3- drinking-water pipe, 4- filter device, 41- driving wheel, 42- connecting rod, 43- push rod, 431- Piston, 44- linear bearing, 45- filter device shell, the first liquid outlet of 451-, 46- punching press room, the first liquid sucting port of 461-, 47- First filter screen, 5- the first hydrops slot, the second filter screen of 51-, the first inlet tube of 6-, 61- first pressure valve, 7- feeding device, 71- the second hydrops slot, 72- second pressure valve, the second inlet tube of 73-, 74- feeding device support frame, 8- inlet duct, 81- Three pressure valve, 82- air inlet buffer unit, 821- annular chamber, 822- buffering filler, 823- sieve, 83- central tube, 84- branch pipe, 841- tap, 9- outlet tube, the second fluid hole of 91-, 92- flapper valve, 10- exhaust apparatus, 101- venthole, 102- are dry Agent, 103- check valve, 11- supercharging device, 111- blower, 12- refrigerating plant, 121- refrigeration controler, 13- collecting tank, 14-U Type pipe support frame, 141- support ring, 142- thread groove, the chassis 143-, the chassis 144- mounting hole, 15- reaction kettle.
Specific embodiment
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete Site preparation description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts every other Embodiment shall fall within the protection scope of the present invention.
Embodiment 1
Please refer to Fig. 1~3, in the embodiment of the present invention, a kind of Integrated Processing Unit for Chemical Manufacture waste material, including receive Collect pond 1, pump 2, drinking-water pipe 3, filter device 4, the first hydrops slot 5, the first inlet tube 6, feeding device 7, inlet duct 8, go out liquid Pipe 9, exhaust apparatus 10, supercharging device 11, refrigerating plant 12, collecting tank 13 and reaction kettle 15, the top and bottom of reaction kettle 15 For pyramidal structure, 15 left side upper position of reaction kettle is connected with the first inlet tube 6, and 6 other end of the first inlet tube is connected with First hydrops slot 5, filter device 4 is fixedly connected with above the first hydrops slot 5, and the filter device 4 is used for chemical industry is raw Solid impurity filtering in the ammonia nitrogen waste water generated during producing, prevents occurring uncontrollable situation in subsequent reactions, described The position that keeps left at the top of filter device 4 is connected with drinking-water pipe 3, and the other end of the drinking-water pipe 3 is connected with pump 2, and the pump 2, which is set to, to be received Collect in 1 inner cavity of pond, the pump 2 is driven by external power supply, is not pointed out on figure, and the collecting pit 1 is arranged for accepting in Chemical Manufacture Ammonia nitrogen waste water out, 15 top left hand of reaction kettle are connected with feeding device 7, and the feeding device 7 is used for reaction kettle 15 In be passed through suitable NaOH solution, the 15 top middle position of reaction kettle is connected with inlet duct 8, and the inlet duct 8 is used In being passed through the mix waste gas containing chlorine and oxynitrides generated in Chemical Manufacture, the reaction kettle 15 into reaction solution It is connected with exhaust apparatus 10 on the right side of top, goes out reaction kettle 15 for generating ammonia emission after reacting, the exhaust apparatus 10 The other end is connected with supercharging device 11, and the other end of the supercharging device 11 is connected with refrigerating plant 12, the refrigerating plant 12 Lower end be connected with collecting tank 13, the supercharging device 11 and refrigerating plant 12 are by way of pressurizeing and cooling down by the ammonia of generation Gas liquefaction is collected into collecting tank 13, is used as industrial chemicals, the 15 bottom end middle position of reaction kettle is connected with outlet tube 9, institute Outlet tube 9 is stated by the waste water discharge after reaction as Chemical Manufacture raw material, the reaction kettle 15 and filter device 4 are by support leg Support, the present invention is by the waste material that will generate in two kinds of common chemical production process, in a manner of NaOH solution is added, mutually Absorbing reaction makes available Chemical Manufacture raw material, and realization is turned waste into wealth, and the target of energy-saving and emission-reduction is suitble in chemical industry Waste disposal system is promoted the use of.
Please refer to Fig. 1~3, in the embodiment of the present invention, a kind of Integrated Processing Unit for Chemical Manufacture waste material, the mistake Filtering device 4 includes filter device shell 45, and 45 top side of filter device shell and drinking-water pipe 3 are connected, the filtering dress It sets 45 bottom of shell and is equipped with the second filter screen 51, the first hydrops slot 5, the filtering dress are equipped with below the filter device shell 45 It sets and is equipped with punching press room 46 in shell 45, the punching press room 46 is equipped with the first liquid sucting port 461, first imbibition close to two sides of the bottom Mouth 461 is equipped with the first filter screen 47, and 46 bottom of punching press room is equipped with the first liquid outlet 451, and second filter screen 51 is set On the first liquid outlet 451, piston 431, the sectional dimension of piston 431 and cutting for punching press room 46 are movably installed in punching press room 46 Face size matches, and push rod 43 is fixed on the piston 431, and the end of the push rod 43 passes through to be extended at the top of punching press room 46 Outside filter device shell 45, linear bearing 44 is equipped at the top of the filter device shell 45, the push rod 43 is sleeved on linear axis It holds in 44, the push rod 43 does straight reciprocating motion in linear bearing 44, when piston 431 moves upwards, by ammonia nitrogen waste water It sucks in punching press room 46, ammonia nitrogen waste water is through 47 first heavy filtration of the first filter screen at the first liquid sucting port 461, the piston 431 Ammonia nitrogen waste water is squeezed when moving downward and enters the first hydrops slot 5, and ammonia nitrogen waste water passes through the second filter screen 51 of 46 bottom of punching press room The fine degree of second heavy filtration, double filtration, filtering steps up, and filter effect is good, and under mechanical driving, crosses filtering velocity Degree is obviously improved, and 5 inner cavity of the first hydrops slot is squeezed when piston 431 moves downward, and the ammonia nitrogen waste water by filtering is logical The first inlet tube 6 is crossed to enter in reaction kettle 15.
Please refer to Fig. 1~3, in the embodiment of the present invention, a kind of Integrated Processing Unit for Chemical Manufacture waste material, the mistake The top middle portion of filter device housing 45 is equipped with driving wheel 41, and the driving wheel 41 is drivingly connected with external motor, driving wheel 41 Connecting rod 42 is hinged on wheel face, the other end and push rod 43 of connecting rod 42 are hinged, and whole device is slider-crank mechanism, passes through driving The rotation of wheel 41 drives the piston 431 being fixedly connected with push rod 43 to do straight reciprocating motion in punching press room 46.
Please refer to Fig. 1~3, in the embodiment of the present invention, a kind of Integrated Processing Unit for Chemical Manufacture waste material, described One inlet tube 6 is equipped with first pressure valve 61, and first pressure valve 61 is opened after by certain pressure, prevents the ammonia generated from returning It flow in the first inlet tube 6.
Please refer to Fig. 1~3, in the embodiment of the present invention, a kind of Integrated Processing Unit for Chemical Manufacture waste material, it is described into Device of air 8 include third pressure valve 81, air inlet buffer unit 82, central tube 83 and branch pipe 84, the third pressure valve 81 by It is opened after to certain pressure, prevents reaction solution from occurring flowing backward phenomenon, it is raw that the air inlet buffer unit 82 buffers the chemical industry being passed through The mix waste gas containing chlorine and oxynitrides generated in production prevents air pressure is excessive from causing reaction incomplete.
Please refer to Fig. 1~3, in the embodiment of the present invention, a kind of Integrated Processing Unit for Chemical Manufacture waste material, described Three pressure valve 81 and air inlet buffer unit 82 are set to one end that central tube 83 stretches out reaction kettle 15,83 other end of central tube to Under across reaction kettle 15 extend into 15 bottom of reaction kettle, 83 lower end of central tube is equipped with branch pipe 84.
Please refer to Fig. 1~3, in the embodiment of the present invention, a kind of Integrated Processing Unit for Chemical Manufacture waste material, the branch Pipe 84 is helical structure, and the branch pipe 84 is equipped with several taps 841 obliquely, and the branch pipe 84 is far from central tube 83 Endcapped, what the tap 841 dispersed to generate from the Chemical Manufacture being passed through in inlet duct 8 contains chlorine and nitrogen oxidation The direction closing the mix waste gas of object, and being arranged obliquely by tap 841, which plays the role of stirring reaction solution, to be made to react More sufficiently.
Please refer to Fig. 1~3, in the embodiment of the present invention, a kind of Integrated Processing Unit for Chemical Manufacture waste material, it is described into Gas buffer unit 82 includes annular chamber 821, buffers filler 822 and sieve 823, the annular chamber 821 and third pressure valve 81 1 End is connected, and the other end of the annular chamber 821 is connected with central tube 83, and the annular chamber 821 is interior equipped with central tube 83, it is described in Heart pipe 83 is located at 821 middle part of annular chamber, is equipped with buffering filler 822 on 821 top of annular chamber.
Further, the buffering filler 822 is preferably steel wool.
Please refer to Fig. 1~3, in the embodiment of the present invention, a kind of Integrated Processing Unit for Chemical Manufacture waste material, it is described into Liquid device 7 includes the second hydrops slot 71, second pressure valve 72, the second inlet tube 73 and feeding device support frame 74, the feed liquor Feeding device 7 is fixed on reaction kettle 15 by device support stand 74, and described second inlet tube, 73 one end is obliquely through reaction kettle 15 It is extend into 15 bottom of reaction kettle, the other end of second inlet tube 73 is connected with second pressure valve 72, second pressure valve 72 The other end is connected with the second hydrops slot 71, and NaOH solution is held in the second hydrops slot 71, and the second pressure valve 72 is reaching The phenomenon that opening when to certain pressure, feeding device 7 made to be passed through NaOH solution into reaction kettle 15, prevent reverse irrigation.
Please refer to Fig. 1~3, in the embodiment of the present invention, a kind of Integrated Processing Unit for Chemical Manufacture waste material is described anti- It answers the bottom middle position of kettle 15 to be equipped with the second fluid hole 91, is connected with outlet tube 9, outlet tube 9 on second fluid hole 91 On be additionally provided with flapper valve 92, the mixed solution after reaction is collected, be can be used as by the solution after opening the discharge reaction of flapper valve 92 The raw material of Chemical Manufacture.
Please refer to Fig. 1~3, in the embodiment of the present invention, a kind of Integrated Processing Unit for Chemical Manufacture waste material, the row Device of air 10 includes venthole 101, desiccant 102 and check valve 103, and the venthole 101 is set on the right side of 15 top of reaction kettle, Collecting pit 1 is provided with one section of U-tube, is supported by U-tube support frame 14, and desiccant 102 is filled in U-tube, and desiccant 102 is used In removing the aqueous vapor in the ammonia generated, the check valve 103 only unilaterally connected from left to right.
Please refer to Fig. 1~3, in the embodiment of the present invention, a kind of Integrated Processing Unit for Chemical Manufacture waste material, the increasing It is in series with several groups blower 111 in pressure device 11, for low pressure ammonia to be pressurized, makes it easier to liquefy.
Please refer to Fig. 1~3, in the embodiment of the present invention, a kind of Integrated Processing Unit for Chemical Manufacture waste material, the system Device for cooling 12 is circumscribed with refrigeration controler 121, the cooling module in refrigerating plant 12 and the refrigeration controler outside refrigerating plant 12 121 are electrically connected, and the cooling module that refrigerating plant 12 controls in refrigerating plant 12 makes pressurized ammonia liquefy, and make it more It is easy to be collected utilization.
Please refer to Fig. 1~3, in the embodiment of the present invention, a kind of Integrated Processing Unit for Chemical Manufacture waste material, the U Type pipe support frame 14 includes support ring 141 and chassis 143, and the support ring 141 is semicircular structure, it is easier to support tubes, Support ring 141 has top pillar, and top pillar lower end is equipped with thread groove 142, is equipped with threaded hole and thread groove in the middle part of the chassis 143 142 threaded engagements, 143 bottom of chassis are additionally provided with chassis mounting hole 144 for U-tube support frame 14 to be fixed on fixing piece On, keep pipe fitting support more stable.
Reaction principle of the invention is:
NH4 ++3Cl2=NCl3+3HC1+H+
NH3+ 3H ClO=NCl3+3H20
3NaOH+NCl3=NH3↑+3NaClO
NaOH+HC1=NaC1+H20
NO+NO2+2NH3·H2O=2NH4 +++2NO2 -+2H2O
NH4 ++OH-=NH3↑+H20
Workflow of the invention are as follows: the ammonia nitrogen waste water generated in industrial production is collected into collecting pit 1, is filtered into crossing After device 4 is filtered by suction, into reaction kettle 15, when solution did not had branch pipe 84, the chemical industry that is passed through into inlet duct 8 The mix waste gas containing chlorine and oxynitrides generated in production, while it being passed through NaOH solution into feeding device 7, it reacts The ammonia of generation is discharged from exhaust apparatus 10, enters into the pressurization for crossing supercharging device 11 and refrigerating plant 12 with liquefaction after cooling Collect in collecting tank 13, the solution after fully reacting is discharged through outlet tube 9, the main component in solution after reaction be sodium chloride and time Sodium chlorate ingredient can be used as the use of chemical reaction raw material.
In conclusion the present invention is by the waste material that will generate in two kinds of common chemical production process, it is molten NaOH is added The mode of liquid makes its mutual absorbing reaction, makes available Chemical Manufacture raw material, and realization is turned waste into wealth, energy-saving and emission-reduction Target, be suitble to chemical spent material processing system promote the use of.
Embodiment 2
A kind of chemical spent material processing system, the integrated treatment including being used for Chemical Manufacture waste material as described in Example 1 fill It sets.
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie In the case where without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power Benefit requires rather than above description limits, it is intended that all by what is fallen within the meaning and scope of the equivalent elements of the claims Variation is included within the present invention.Any reference signs in the claims should not be construed as limiting the involved claims.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art The other embodiments being understood that.

Claims (10)

1. a kind of Integrated Processing Unit for Chemical Manufacture waste material, including collecting pit (1), pump (2), drinking-water pipe (3), filtering dress Set (4), the first hydrops slot (5), the first inlet tube (6), feeding device (7), inlet duct (8), outlet tube (9), exhaust apparatus (10), supercharging device (11), refrigerating plant (12), collecting tank (13) and reaction kettle (15), which is characterized in that reaction kettle (15) Top and bottom are pyramidal structure, and upper position is connected with the first inlet tube (6) on the left of reaction kettle (15), the first inlet tube (6) It is equipped with first pressure valve (61), the first inlet tube (6) other end is connected with the first hydrops slot (5), first hydrops It is fixedly connected with filter device (4) above slot (5), the position that keeps left at the top of the filter device (4) is connected with drinking-water pipe (3), institute The other end for stating drinking-water pipe (3) is connected with pump (2), and the pump (2) is set in collecting pit (1) inner cavity, and the pump (2) is by external electricity Source driving, reaction kettle (15) top left hand are connected with feeding device (7), reaction kettle (15) the top middle position connection Have inlet duct (8), be connected with exhaust apparatus (10) on the right side of reaction kettle (15) top, the exhaust apparatus (10) it is another End is connected with supercharging device (11), is in series with several groups blower (111) in the supercharging device (11), the supercharging device (11) The other end be connected with refrigerating plant (12), the lower end of the refrigerating plant (12) is connected with collecting tank (13), the reaction kettle (15) bottom end middle position is connected with outlet tube (9), and the reaction kettle (15) and filter device (4) are supported by support leg.
2. the Integrated Processing Unit according to claim 1 for Chemical Manufacture waste material, which is characterized in that the filtering dress Setting (4) includes filter device shell (45), and filter device shell (45) top side and drinking-water pipe (3) are connected, the mistake It filters device housing (45) bottom and is equipped with the second filter screen (51), the first hydrops slot is equipped with below the filter device shell (45) (5), punching press room (46) are equipped in the filter device shell (45), the punching press room (46) is equipped with first close to two sides of the bottom and inhales Liquid mouth (461), first liquid sucting port (461) are equipped with the first filter screen (47), and punching press room (46) bottom is equipped with first Liquid outlet (451), second filter screen (51) are located on the first liquid outlet (451), are movably installed with work in punching press room (46) It fills in (431), the sectional dimension of piston (431) is matched with the sectional dimension of punching press room (46), is fixed on the piston (431) Push rod (43), the end of the push rod (43) pass through and extend to filter device shell (45) outside at the top of punching press room (46), the mistake It filters and is equipped with linear bearing (44) at the top of device housing (45), the push rod (43) is sleeved in linear bearing (44), the push rod (43) straight reciprocating motion is done in linear bearing (44).
3. the Integrated Processing Unit according to claim 1 or 2 for Chemical Manufacture waste material, which is characterized in that the mistake The top middle portion of filter device housing (45) is equipped with driving wheel (41), and the driving wheel (41) and external motor are drivingly connected, and is driven It is hinged with connecting rod (42) on driving wheel (41) wheel face, the other end of connecting rod (42) and push rod (43) are hinged.
4. the Integrated Processing Unit according to claim 1 for Chemical Manufacture waste material, which is characterized in that the air inlet dress Setting (8) includes third pressure valve (81), air inlet buffer unit (82), central tube (83) and branch pipe (84), the third pressure valve (81) and air inlet buffer unit (82) is set to one end that central tube (83) stretch out reaction kettle (15), central tube (83) other end It is passed down through reaction kettle (15) and extend into reaction kettle (15) bottom, central tube (83) lower end is equipped with branch pipe (84), the branch Managing (84) is helical structure, and the branch pipe (84) is equipped with several taps (841) obliquely, and the branch pipe (84) is far from The endcapped of heart pipe (83).
5. the Integrated Processing Unit according to claim 4 for Chemical Manufacture waste material, which is characterized in that the air inlet is slow Flushing device (82) includes annular chamber (821), buffering filler (822) and sieve (823), the annular chamber (821) and third pressure Valve (81) one end is connected, and the other end of the annular chamber (821) is connected with central tube (83), is equipped in the annular chamber (821) Central tube (83), the central tube (83) are located in the middle part of annular chamber (821), are equipped with buffering filler on annular chamber (821) top (822), the buffering filler (822) is steel wool.
6. the Integrated Processing Unit according to claim 1 for Chemical Manufacture waste material, which is characterized in that the feed liquor dress Setting (7) includes the second hydrops slot (71), second pressure valve (72), the second inlet tube (73) and feeding device support frame (74), institute It states feeding device support frame (74) feeding device (7) is fixed on reaction kettle (15), described second inlet tube (73) one end is oblique It is extend into reaction kettle (15) bottom to reaction kettle (15) are passed through, the other end of second inlet tube (73) is connected with second pressure Valve (72), the other end of second pressure valve (72) are connected with the second hydrops slot (71).
7. the Integrated Processing Unit according to claim 1 for Chemical Manufacture waste material, which is characterized in that the reaction kettle (15) bottom middle position is equipped with the second fluid hole (91), is connected with outlet tube (9) on second fluid hole (91), out liquid Flapper valve (92) are additionally provided on pipe (9).
8. the Integrated Processing Unit according to claim 1 for Chemical Manufacture waste material, which is characterized in that the exhaust dress Setting (10) includes venthole (101), desiccant (102) and check valve (103), and the venthole (101) is set to reaction kettle (15) On the right side of top, exhaust apparatus (10) is provided with one section of U-tube, is supported by U-tube support frame (14), and drying is filled in U-tube Agent (102).
9. the Integrated Processing Unit according to claim 8 for Chemical Manufacture waste material, which is characterized in that the U-tube Support frame (14) includes support ring (141) and chassis (143), and the support ring (141) is semicircular structure, support ring (141) Top pillar is had, top pillar lower end is equipped with thread groove (142), and threaded hole and thread groove (142) spiral shell are equipped in the middle part of the chassis (143) Conjunction is screwed, chassis (143) bottom is additionally provided with chassis mounting hole (144).
10. a kind of chemical spent material processing system, which is characterized in that including according to any one of claims 1 to 9 raw for chemical industry Produce the Integrated Processing Unit of waste material.
CN201910040934.0A 2019-01-16 2019-01-16 A kind of Integrated Processing Unit for Chemical Manufacture waste material Withdrawn CN109626652A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201910040934.0A CN109626652A (en) 2019-01-16 2019-01-16 A kind of Integrated Processing Unit for Chemical Manufacture waste material

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201910040934.0A CN109626652A (en) 2019-01-16 2019-01-16 A kind of Integrated Processing Unit for Chemical Manufacture waste material

Publications (1)

Publication Number Publication Date
CN109626652A true CN109626652A (en) 2019-04-16

Family

ID=66061125

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201910040934.0A Withdrawn CN109626652A (en) 2019-01-16 2019-01-16 A kind of Integrated Processing Unit for Chemical Manufacture waste material

Country Status (1)

Country Link
CN (1) CN109626652A (en)

Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101274806A (en) * 2007-03-30 2008-10-01 北京清华紫光英力化工技术有限责任公司 Novel process for reclaiming waste water containing CN- and NH3 or NH4-
CN102688607A (en) * 2012-05-24 2012-09-26 崇义章源钨业股份有限公司 Ammonia tail gas recycling method and system
CN202717595U (en) * 2012-05-22 2013-02-06 江苏隆昌化工有限公司 Ammonia gas absorption device
CN103420398A (en) * 2012-05-25 2013-12-04 日本派欧尼株式会社 Method of recovering ammonia and method of recycling ammonia by using the same
CN104817157A (en) * 2015-05-14 2015-08-05 四川润雅环境工程有限公司 Chemical wastewater pretreatment method and sequencing-batch alkaline hydrolysis reactor
CN105597535A (en) * 2016-03-29 2016-05-25 南京工业大学 Treatment method for mixed organic waste gas containing chlorine, hydrogen chloride and oxynitride
CN206386670U (en) * 2017-01-18 2017-08-08 广州市象丰润滑油品有限公司 A kind of lubricating oil filter
CN107224846A (en) * 2017-07-12 2017-10-03 安徽弘源化工科技有限公司 A kind of air-flow buffer type liquid seal can
CN107244775A (en) * 2017-08-02 2017-10-13 郑州嘉晨化工科技有限公司 A kind of coal chemical industrial waste water processing unit

Patent Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101274806A (en) * 2007-03-30 2008-10-01 北京清华紫光英力化工技术有限责任公司 Novel process for reclaiming waste water containing CN- and NH3 or NH4-
CN202717595U (en) * 2012-05-22 2013-02-06 江苏隆昌化工有限公司 Ammonia gas absorption device
CN102688607A (en) * 2012-05-24 2012-09-26 崇义章源钨业股份有限公司 Ammonia tail gas recycling method and system
CN103420398A (en) * 2012-05-25 2013-12-04 日本派欧尼株式会社 Method of recovering ammonia and method of recycling ammonia by using the same
CN104817157A (en) * 2015-05-14 2015-08-05 四川润雅环境工程有限公司 Chemical wastewater pretreatment method and sequencing-batch alkaline hydrolysis reactor
CN105597535A (en) * 2016-03-29 2016-05-25 南京工业大学 Treatment method for mixed organic waste gas containing chlorine, hydrogen chloride and oxynitride
CN206386670U (en) * 2017-01-18 2017-08-08 广州市象丰润滑油品有限公司 A kind of lubricating oil filter
CN107224846A (en) * 2017-07-12 2017-10-03 安徽弘源化工科技有限公司 A kind of air-flow buffer type liquid seal can
CN107244775A (en) * 2017-08-02 2017-10-13 郑州嘉晨化工科技有限公司 A kind of coal chemical industrial waste water processing unit

Similar Documents

Publication Publication Date Title
CN111362345A (en) Micro-nano bubble generator
CN207680316U (en) A kind of emission-control equipment of abundant processing exhaust gas
CN207913506U (en) A kind of biological deodorizing device
CN109626652A (en) A kind of Integrated Processing Unit for Chemical Manufacture waste material
CN212016391U (en) Breathing device for cardiovascular internal medicine
CN210736380U (en) Coupling dispersion type rural domestic sewage treatment system
CN107746145A (en) A kind of Environmental Cities water supply chlorine residue secure processing device
CN208642121U (en) A kind of multistage vortex water flow formula emission-control equipment
CN208200505U (en) A kind of factory's sewage-treatment plant
CN207671808U (en) A kind of efficient plant chimney stalk processing equipment
CN207918635U (en) Sewage-treatment plant
CN217490380U (en) Novel waste gas treatment tower for coal chemical industry
CN207175661U (en) A kind of desulfurization wastewater treatment system
CN209362207U (en) A kind of chlorine dioxide denitrification apparatus
CN208791271U (en) A kind of gas-vapor mix device using ozone purification tap water
CN207385173U (en) A kind of laboratory inorganic waste gases purifier
CN207451800U (en) A kind of fish farm water-ozone purifier
CN102167287B (en) Multifunction efficient energy-saving chlorine dioxide generator
CN207079121U (en) A kind of outdoor water purifier
CN110204107A (en) Aluminium ion separation equipment and its process
CN201969386U (en) Decomposer for ozone tail gas of gas-water mixing pump
CN2507853Y (en) Simple direct drinking water sterilizing device
KR200305788Y1 (en) High performance liquid oxygenation equipment
CN206985962U (en) A kind of EGR of architecture indoor landscape water body
CN2670330Y (en) Chlorinedioxide gas multistage dissolving circulating absorber

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
WW01 Invention patent application withdrawn after publication

Application publication date: 20190416

WW01 Invention patent application withdrawn after publication