CN109626325A - A kind of energy conservation and environmental protection chlorination apparatus for forming hydrogen - Google Patents
A kind of energy conservation and environmental protection chlorination apparatus for forming hydrogen Download PDFInfo
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- CN109626325A CN109626325A CN201811525989.2A CN201811525989A CN109626325A CN 109626325 A CN109626325 A CN 109626325A CN 201811525989 A CN201811525989 A CN 201811525989A CN 109626325 A CN109626325 A CN 109626325A
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- cabinet
- concentrated sulfuric
- hydrochloric acid
- sulfuric acid
- elastic slice
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B7/00—Halogens; Halogen acids
- C01B7/01—Chlorine; Hydrogen chloride
- C01B7/03—Preparation from chlorides
- C01B7/035—Preparation of hydrogen chloride from chlorides
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B7/00—Halogens; Halogen acids
- C01B7/01—Chlorine; Hydrogen chloride
- C01B7/07—Purification ; Separation
- C01B7/0706—Purification ; Separation of hydrogen chloride
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/10—Process efficiency
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Abstract
The invention belongs to chlorination apparatus for forming hydrogen technical field, specifically a kind of energy conservation and environmental protection chlorination apparatus for forming hydrogen, including cabinet；Cabinet is equipped with gas vent；Air pump is connected on the outside of gas vent；Air pump is connected with helix tube by hose；Top of the box is connected with material spray disk；Regulator is equipped between material spray disk；Regulator includes shaft, rotor plate and support plate；The lower section of material spray disk is equipped with horizontal positioned partition；Partition is equipped with several through-holes；Pressing plate is connected with by No. three springs above through-hole；The bottom of box is equipped with discharge gate, and controller is additionally provided on cabinet, and controller is used to control the ejection of hydrochloric acid and the concentrated sulfuric acid；By the present invention in that the contact area of hydrochloric acid and the concentrated sulfuric acid becomes larger, increase the dynamics of hydrochloric acid and the concentrated sulfuric acid mutually hit, so that hydrochloric acid and concentrated sulfuric acid mixing generate more hydrogen chloride gas, improves the utilization rate of hydrochloric acid and concentrated sulfuric acid raw material.
Description
Technical field
The invention belongs to chlorination apparatus for forming hydrogen technical field, specifically a kind of energy conservation and environmental protection hydrogen chloride is filled
It sets.
Background technique
The common method of hydrogen chloride preparation is added in concentrated hydrochloric acid with the concentrated sulfuric acid, dense because the concentrated sulfuric acid has water imbibition
Aqueous solvent can be reduced in hydrochloric acid, and solute HCl can be evaporated, while temperature increases, and the solubility of HCl reduces, and also promote HCl's
Volatilization, produces HCl gas to reach.However the efficiency that existing chlorination apparatus for forming hydrogen prepares hydrogen chloride gas is lower, pole
The supply of hydrogen chloride gas applicable situation is affected greatly；Chlorination apparatus for forming hydrogen generates during preparing hydrogen chloride gas simultaneously
A large amount of heat can not utilize waste of resource.
Summary of the invention
In order to make up for the deficiencies of the prior art, a kind of energy conservation and environmental protection chlorination apparatus for forming hydrogen proposed by the present invention, the present invention
Be mainly used for solving existing hydrogen chloride generator prepare hydrogen chloride gas efficiency is lower and preparation process in output heat
Unserviceable problem.
The technical solution adopted by the present invention to solve the technical problems is: a kind of energy conservation and environmental protection hydrogen chloride of the present invention
Generating device, including cabinet；The upper end middle position of the cabinet is equipped with gas vent, and top of the box is symmetrically tilted about gas vent
Setting；Air pump is connected on the outside of the gas vent；One end of the air pump is connected with hose, and the lower end of hose is connected with spiral
Pipe；The helix tube is wrapped on the outside of lower box, and one end of helix tube is equipped with exhaust outlet, and exhaust outlet is connect with air accumulator；Institute
It states and is symmetrically arranged with two sliding slots on the inside of top of the box, a material spray disk is slidably connected in two sliding slots；The material spray disk
Inside be equipped with cavity, connected between material spray disk lower end and sliding slot lower end by No.1 spring, material spray disk far from top of the box one
Side is equipped with spray material port, and the cavity of a material spray disk is connected to hydrochloric acid feed pipe, the cavity and the concentrated sulfuric acid of another material spray disk into
Expects pipe is connected to, and regulator is equipped between two material spray disk upper ends；The regulator is mounted on gas vent by holder pivots
Lower section, and regulator is symmetrical arranged about bracket, regulator includes shaft, rotor plate and support plate；The shaft is fixed
On bracket；There are two the rotor plate settings, and two rotor plates are symmetrically hinged in shaft about bracket, in two rotor plates
No. two springs are connected between portion, the upper end of two rotor plates is contacted with cabinet；One end of the support plate is fixed in rotation
The middle part of plate, the other end of support plate and the upper-end contact of material spray disk；The lower section of the material spray disk is equipped with horizontal positioned partition；
The partition is equipped with several through-holes；Pressing plate is connected with by No. three springs above the through-hole；The bottom of box is equipped with
Discharge gate, controller is additionally provided on cabinet, and controller is used to control the ejection of hydrochloric acid and the concentrated sulfuric acid；
When work, hydrochloric acid and the concentrated sulfuric acid respectively enter corresponding material spray by hydrochloric acid feed pipe and concentrated sulfuric acid feed pipe and circle or whirl in the air
It in chamber, and is sprayed by spray material port, the hydrochloric acid and the concentrated sulfuric acid of ejection rebound under the action of No. three springs after hitting pressing plate, make salt
Acid and the concentrated sulfuric acid mutually hit to be mixed, and the liquid after pressing plate is hit using hydrochloric acid and the concentrated sulfuric acid is spread, and recycle pressure
Plate compresses the bounce obtained after No. three springs, so that the contact area of hydrochloric acid and the concentrated sulfuric acid is become larger, makes the phase of hydrochloric acid and the concentrated sulfuric acid
The dynamics mutually hit increases, so that hydrochloric acid and concentrated sulfuric acid mixing generate more hydrogen chloride gas, improves hydrochloric acid and the concentrated sulfuric acid
The utilization rate of raw material；Hydrochloric acid and the concentrated sulfuric acid can generate hydrogen chloride gas when mixing and a large amount of heat of release, hydrogen chloride gas exist
After case cylinder accumulation is excessive, pushes rotor plate rotation to open gas vent, hydrogen chloride gas is discharged by air pump, works as rotation
When plate rotates, support plate is rotated also with rotor plate, at this point, two material spray disks upward sliding under the thrust of No.1 spring, leads to
The ejection time for crossing controller control hydrochloric acid and the concentrated sulfuric acid achievees the effect that hydrochloric acid and concentrated sulfuric acid interval spray, when hydrochloric acid and dense
When sulfuric acid does not spray, rotor plate is because the reduction of air pressure is resetted by the elasticity of No. two springs in cabinet, and again by controlling
Device control hydrochloric acid and the concentrated sulfuric acid processed spray, and make rotor plate repeated rotation, reset, realize that the repetition of material spray disk slides up and down with this,
It is just being slided in the material spray disk of material spray by regulator promotion, so that the track that hydrochloric acid and the concentrated sulfuric acid spray is more chaotic,
So that the number of contact of the hydrochloric acid with the concentrated sulfuric acid is more, improves hydrochloric acid and the concentrated sulfuric acid contacts mixed degree, to improve hydrochloric acid
The efficiency for generating hydrogen chloride gas is mixed with the concentrated sulfuric acid；With the lasting progress of reaction, the mixed solution on partition is more, passes through
Mixed liquor is patted in pressing plate pushing, in addition screw pitch changes the extruding carried out to mixed liquor, stirs during No. three spring springing
It is dynamic, the mixability of mixed liquor is further increased, the utilization rate of hydrochloric acid and concentrated sulfuric acid raw material is improved；Simultaneously with No. three springs
Springing screw pitch increases, and liquid flows into cabinet internal partition lower space by through-hole from the gap between No. three springs；It is taken away by air pump
The hydrogen chloride gas with heat by helix tube be discharged, and gas be discharged during, heat acts on cabinet internal partition
Mixed liquor in lower space, heats mixed liquor, so that mixed liquor is generated hydrogen chloride gas again, further improves
The utilization rate of hydrochloric acid and concentrated sulfuric acid raw material；Last hydrogen chloride gas enters air accumulator storage.
Preferably, elastic slice is equipped between the gas vent and rotor plate on the cabinet；The elastic slice is connected in arc-shaped
On cabinet, elastic slice is replaceable；When work, by selecting different elastic slices, it is subject to when changing rotor plate rotating opening gas vent
Active force to control air pressure when hydrogen chloride gas discharge, and then controls the interval time that hydrochloric acid and the concentrated sulfuric acid spray into, improves
The amount of hydrochloric acid and concentrated sulfuric acid mixing, improves hydrochloric acid and concentrated sulfuric acid mixing generates the working efficiency of hydrogen chloride gas；With rotor plate
Dynamic friction elastic slice is ceaselessly scraped, elastic slice generates abrasion, since elastic slice is conveniently replaceable, maintenance time is saved, to improve hydrogen chloride
The efficiency of gas preparation work.
Preferably, the both ends that elastic slice is corresponded on the cabinet are equipped with No.1 groove and No. two grooves；One end of the elastic slice
Be connected in No.1 groove by No. four springs, the other end of elastic slice is slidably connected in No. two grooves, elastic slice end with No. two
Filled with oil liquid between bottom portion of groove；It is additionally provided with the counter sink of No. two grooves of perforation on the cabinet, is equipped with screw, spiral shell in counter sink
One end of nail is contacted with oil liquid；The coefficient of elasticity of elastic slice lower end to the elastic slice upper end is gradually reduced；When work, rotor plate is squeezed
When elastic slice, one end by compressing elastic slice compresses No. four springs and reduces the abrasion of elastic slice to be buffered, and then extends elastic slice
Service life；Meanwhile when the abrasion of a position of elastic slice, the depth of counter sink is screwed in by adjusting screw, squeezes screw
The space in No. two grooves is pressed, oil liquid is squeezed and elastic slice is pushed to change the position that rotor plate is contacted with elastic slice, make elastic slice even wearing,
Under conditions of guaranteeing that the operation is stable carries out, the replacement number of elastic slice is reduced, further extends the service life of elastic slice, improves work
The stability of work；Since each point coefficient of elasticity is different on elastic slice, elastic slice change rotor plate is pushed to connect with elastic slice by squeezing oil liquid
The position of touching, adjustment rotor plate pushes the pressure of elastic slice, to change pressure required when gas is discharged in cabinet, improves work
Efficiency.
Preferably, No. three springs select helical spring, and the both ends of No. three springs are scabbled；Two adjacent pressing plates
Between gap be not more than 3mm；When work, by that will select helical spring and scabble helical spring both ends, make pressing plate
It is more steady when being connected on partition, so that hydrochloric acid is sprayed on the angle being repelled on pressing plate with the concentrated sulfuric acid more stable consistent, in turn
It ensure that hydrochloric acid and the concentrated sulfuric acid contact mixed degree, guarantee that the operation is stable carries out, and then improve hydrogen chloride gas preparation work
Efficiency；Meanwhile the gap between two adjacent pressing plates is not more than 3mm, effectively avoids hydrochloric acid and the concentrated sulfuric acid in sprinkling process
In, it directly falls on partition, improves hydrochloric acid and the concentrated sulfuric acid contacts composite rate, improve hydrogen chloride preparation efficiency.
Preferably, the spring ring diameter of No. three springs is 2-3mm, and the screw pitch of No. three springs is not more than 4mm；When work,
The screw pitch of No. three springs and the difference of diameter of section are smaller, so that the rate that mixed liquor flows through No. three springs is slower, so that pressing plate is clapped
The number for hitting mixed liquor increases, and mixes hydrochloric acid and the concentrated sulfuric acid more adequately, to release more hydrogen chloride
Gas improves the utilization rate of hydrochloric acid and the concentrated sulfuric acid.
Preferably, the both ends of the pressing plate are equipped with magnet, and the magnet polarities on the adjacent one end of two pressing plates are identical；Work
When making, hydrochloric acid and the concentrated sulfuric acid hit pressing plate and pressing plate are made to generate shaking, pass through the magnet polarities phase on the adjacent one end of two pressing plates
Together, so that repelling each other between two pressing plates so that pressing plate when being knocked downward springing it is more stable, and then guarantee dilute hydrochloric acid and
The registration in the path after concentrated hydrochloric acid reflection, further ensures the mixability that hydrochloric acid and the concentrated sulfuric acid are mutually hit, Jin Erti
The efficiency of high hydrogen chloride gas preparation work.
Beneficial effects of the present invention are as follows:
1. making the power of hydrochloric acid and the concentrated sulfuric acid mutually hit by the present invention in that the contact area of hydrochloric acid and the concentrated sulfuric acid becomes larger
Degree increases, so that hydrochloric acid and concentrated sulfuric acid mixing generate more hydrogen chloride gas, improves the utilization of hydrochloric acid and concentrated sulfuric acid raw material
Rate.
2. the present invention is just being slided in the material spray disk of material spray by regulator promotion, spray hydrochloric acid and the concentrated sulfuric acid
Track is more chaotic, so that the number of contact of the hydrochloric acid with the concentrated sulfuric acid is more, improves hydrochloric acid and the concentrated sulfuric acid contacts mixed degree,
The efficiency of hydrogen chloride gas is generated to improve hydrochloric acid and concentrated sulfuric acid mixing.
3. the present invention is further increased the mixability of mixed liquor, is improved by the extruding, the agitation that carry out to mixed liquor
The utilization rate of hydrochloric acid and concentrated sulfuric acid raw material；High-temp chlorination hydrogen is discharged by helix tube, is heated to mixed liquor, again
So that mixed liquor is generated hydrogen chloride gas, further improves the utilization rate of hydrochloric acid and concentrated sulfuric acid raw material.
Detailed description of the invention
The present invention will be further explained below with reference to the attached drawings.
Fig. 1 is main view of the invention；
Fig. 2 is partial enlarged view at A in Fig. 1；
Fig. 3 is partial enlarged view at B in Fig. 2
In figure: cabinet 1, gas vent 2, helix tube 3, material spray disk 4, No.1 spring 5, regulator 6, shaft 61, rotor plate
62, support plate 63,7, No. three springs 8 of partition, pressing plate 9, elastic slice 10, No.1 groove 11, No. two grooves 12, counter sinks 13, screw
14, magnet 15.
Specific embodiment
It is said as follows using a kind of energy conservation and environmental protection chlorination apparatus for forming hydrogen of the Fig. 1 to Fig. 3 to an embodiment of the present invention
It is bright.
As shown in Figure 1, a kind of energy conservation and environmental protection chlorination apparatus for forming hydrogen of the present invention, including cabinet 1；The cabinet 1
Upper end middle position be equipped with gas vent 2, the top of cabinet 1 is symmetrically obliquely installed about gas vent 2；The outside of the gas vent 2
It is connected with air pump；One end of the air pump is connected with hose, and the lower end of hose is connected with helix tube 3；The helix tube 3 is wrapped in
One end of 1 lower outside of cabinet, helix tube 3 is equipped with exhaust outlet, and exhaust outlet is connect with air accumulator；1 inside top pair of cabinet
Title is set there are two sliding slot, slidably connects a material spray disk 4 in two sliding slots；The inside of the material spray disk 4 is equipped with cavity, spray
It is connected between 4 lower end of charging tray and sliding slot lower end by No.1 spring 5, material spray disk 4 is equipped with material spray far from the side at 1 top of cabinet
Mouthful, the cavity of a material spray disk 4 is connected to hydrochloric acid feed pipe, and the cavity of another material spray disk 4 is connected to concentrated sulfuric acid feed pipe, and two
Regulator 6 is equipped between a 4 upper end of material spray disk；The regulator 6 is mounted on 2 lower section of gas vent by holder pivots, and
Regulator 6 is symmetrical arranged about bracket, and regulator 6 includes shaft 61, rotor plate 62 and support plate 63；The shaft 61 is solid
It is scheduled on bracket；There are two the settings of rotor plate 62, and two rotor plates 62 are symmetrically hinged in shaft 61 about bracket, and two
Rotor plate is connected with No. two springs between 62 middle part, and the upper end of two rotor plates 62 is contacted with cabinet 1；The support plate 63
One end is fixed in the middle part of rotor plate 62, the other end of support plate 63 and the upper-end contact of material spray disk 4；Under the material spray disk 4
Side is equipped with horizontal positioned partition 7；The partition 7 is equipped with several through-holes；It is connected above the through-hole by No. three springs 8
There is pressing plate 9；1 bottom of cabinet is equipped with discharge gate, controller is additionally provided on cabinet 1, controller is for controlling hydrochloric acid and dense sulphur
The ejection of acid；
When work, hydrochloric acid and the concentrated sulfuric acid respectively enter corresponding material spray disk 4 by hydrochloric acid feed pipe and concentrated sulfuric acid feed pipe
In cavity, and being sprayed by spray material port, the hydrochloric acid and the concentrated sulfuric acid of ejection rebound under the action of No. three spring 8 after hitting pressing plate 9,
Hit hydrochloric acid and the concentrated sulfuric acid mutually to be mixed, the liquid after pressing plate 9 is hit using hydrochloric acid and the concentrated sulfuric acid is spread, then benefit
The bounce obtained after compressing No. three springs 8 with pressing plate 9, makes the contact area of hydrochloric acid and the concentrated sulfuric acid become larger, makes hydrochloric acid and dense sulphur
The dynamics mutually hit of acid increases so that hydrochloric acid and concentrated sulfuric acid mixing generate more hydrogen chloride gas, improve hydrochloric acid and
The utilization rate of concentrated sulfuric acid raw material；Hydrochloric acid and the concentrated sulfuric acid can generate hydrogen chloride gas and a large amount of heat of release, hydrogen chloride when mixing
After gas accumulates excessively in cabinet 1, pushes the rotation of rotor plate 62 to open gas vent 2, hydrogen chloride gas is made to pass through air pump
Discharge, when rotor plate 62 rotates, support plate 63 is rotated also with rotor plate 62, at this point, two material spray disks 4 are in No.1 spring 5
Thrust under upward sliding, by controller control hydrochloric acid and the concentrated sulfuric acid the ejection time, reach hydrochloric acid and the concentrated sulfuric acid interval spray
Effect out, when hydrochloric acid and the concentrated sulfuric acid do not spray, rotor plate 62 is because the reduction of air pressure passes through the bullet of No. two springs in cabinet 1
Property resetted, and hydrochloric acid and the concentrated sulfuric acid are controlled by controller again and sprayed, made 62 repeated rotation of rotor plate, reset, with this reality
The repetition of existing material spray disk 4 slides up and down, and is just being slided in the material spray disk 4 of material spray by the promotion of regulator 6 so that hydrochloric acid with
The track that the concentrated sulfuric acid sprays is more chaotic, so that the number of contact of the hydrochloric acid with the concentrated sulfuric acid is more, improves hydrochloric acid and the concentrated sulfuric acid connects
Mixed degree is touched, to improve the efficiency of hydrochloric acid and concentrated sulfuric acid mixing generation hydrogen chloride gas；With the lasting progress of reaction,
Mixed solution on partition 7 is more, is patted by the pushing of pressing plate 9 mixed liquor, in addition spiral shell during No. three 8 springing of spring
Away from extruding, the agitation carried out to mixed liquor is changed, the mixability of mixed liquor is further increased, hydrochloric acid is improved and the concentrated sulfuric acid is former
The utilization rate of material；Simultaneously as No. three 8 springing screw pitch of spring increase, liquid is flowed into from the gap between No. three springs 8 by through-hole
1 internal partition of cabinet, 7 lower space；It is discharged by the hydrogen chloride gas with heat that air pump is taken away by helix tube 3, and gas is arranged
During out, heat acts on the mixed liquor in 1 internal partition of cabinet, 7 lower space, heats to mixed liquor, makes again
Mixed liquor generates hydrogen chloride gas, further improves the utilization rate of hydrochloric acid and concentrated sulfuric acid raw material；Last hydrogen chloride gas enters
Air accumulator storage.
As shown in Fig. 2, being equipped with elastic slice 10 between gas vent 2 and rotor plate 62 on the cabinet 1；The elastic slice 10 is in circle
Arcuation is connected on cabinet 1, and elastic slice 10 is replaceable；When work, by selecting different elastic slices 10, changes the rotation of rotor plate 62 and beat
Begin to rehearse stomata 2 when the active force that is subject to, to control air pressure when hydrogen chloride gas discharge, and then control hydrochloric acid and concentrated sulfuric acid spray
The interval time entered improves the amount of hydrochloric acid and concentrated sulfuric acid mixing, improves hydrochloric acid and concentrated sulfuric acid mixing generates the work of hydrogen chloride gas
Make efficiency；As rotor plate 62 ceaselessly scrapes dynamic friction elastic slice 10, elastic slice 10 generates abrasion, since elastic slice 10 is conveniently replaceable, section
About maintenance time, to improve the efficiency of hydrogen chloride gas preparation work.
As shown in figure 3, the both ends for corresponding to elastic slice 10 on the cabinet 1 are equipped with No.1 groove 11 and No. two grooves 12；It is described
One end of elastic slice 10 is connected in No.1 groove 11 by No. four springs, and the other end of elastic slice 10 is slidably connected at No. two grooves 12
It is interior, filled with oil liquid between 10 end of elastic slice and No. two 12 bottoms of groove；The heavy of No. two grooves 12 of perforation is additionally provided on the cabinet 1
Head bore 13, counter sink 13 is interior to be equipped with screw 14, and one end of screw 14 is contacted with oil liquid；10 lower end of elastic slice to 10 upper end of elastic slice
Coefficient of elasticity be gradually reduced；When work, when 62 extrusion elastic 10 of rotor plate, No. four bullets are compressed in the one end for passing through compression elastic slice 10
Spring reduces the abrasion of elastic slice 10 to be buffered, and then extends the service life of elastic slice 10；Meanwhile when one of elastic slice 10
When position is worn, the depth of counter sink 13 is screwed in by adjusting screw 14, screw 14 is made to squeeze the space in No. two grooves 12, is squeezed
Pressure oil liquid pushes elastic slice 10 to change the position that rotor plate 62 is contacted with elastic slice 10, makes 10 even wearing of elastic slice, is guaranteeing that work is steady
Under conditions of fixed progress, the replacement number of elastic slice 10 is reduced, further extends the service life of elastic slice 10, improves the stabilization of work
Property；Since each point coefficient of elasticity is different on elastic slice 10, the change rotor plate 62 of elastic slice 10 is pushed to connect with elastic slice 10 by squeezing oil liquid
The position of touching, adjustment rotor plate 62 push the pressure of elastic slice 10, to change pressure required when gas is discharged in cabinet 1, mention
High working efficiency.
As shown in Figure 1, No. three springs 8 select helical spring, and the both ends of No. three springs 8 are scabbled；Adjacent two
Gap between a pressing plate 9 is not more than 3mm；When work, by that will select helical spring and scabble helical spring both ends,
Keep pressing plate 9 more steady when being connected on partition 7, so that hydrochloric acid and the concentrated sulfuric acid is sprayed on the angle being repelled on pressing plate 9 more stable
Unanimously, it and then ensure that hydrochloric acid and the concentrated sulfuric acid contact mixed degree, guarantee that the operation is stable carries out, and then improve hydrogen chloride gas
The efficiency of preparation work；Meanwhile the gap between two adjacent pressing plates 9 is not more than 3mm, effectively reduces hydrochloric acid and the concentrated sulfuric acid exists
It during sprinkling, directly falls on partition 7, improves hydrochloric acid and the concentrated sulfuric acid contacts composite rate, improve hydrogen chloride preparation efficiency.
As shown in Figure 1, the spring ring diameter of No. three springs 8 is 2-3mm, the screw pitch of No. three springs 8 is not more than 4mm；Work
When making, the screw pitch of No. three springs 8 and the difference of diameter of section are smaller, so that the rate that mixed liquor flows through No. three springs 8 is slower, so that
The number that pressing plate 9 flops mixed liquor increases, and mixes hydrochloric acid and the concentrated sulfuric acid more adequately, to release more
Hydrogen chloride gas improves the utilization rate of hydrochloric acid and the concentrated sulfuric acid.
As shown in Figure 1, the both ends of the pressing plate 9 are equipped with magnet 15, and the magnet polarity on the adjacent one end of two pressing plates 9
It is identical；When work, hydrochloric acid and the concentrated sulfuric acid hit pressing plate 9 and pressing plate 9 are made to generate shaking, by the adjacent one end of two pressing plates 9
15 polarity of magnet is identical so that repel each other between two pressing plates 9, the pressing plate 9 made when being knocked again downward springing it is more stable, into
And guarantee the registration in the path after dilute hydrochloric acid and concentrated hydrochloric acid reflection, it further ensures hydrochloric acid and that the concentrated sulfuric acid is mutually hit is mixed
Conjunction degree, and then improve the efficiency of hydrogen chloride gas preparation work.
Specific working mode:
When work, hydrochloric acid and the concentrated sulfuric acid respectively enter corresponding material spray disk 4 by hydrochloric acid feed pipe and concentrated sulfuric acid feed pipe
In cavity, and being sprayed by spray material port, the hydrochloric acid and the concentrated sulfuric acid of ejection rebound under the action of No. three spring 8 after hitting pressing plate 9,
Hit hydrochloric acid and the concentrated sulfuric acid mutually to be mixed, the liquid after pressing plate 9 is hit using hydrochloric acid and the concentrated sulfuric acid is spread, then benefit
The bounce obtained after compressing No. three springs 8 with pressing plate 9, makes the contact area of hydrochloric acid and the concentrated sulfuric acid become larger, makes hydrochloric acid and dense sulphur
The dynamics mutually hit of acid increases so that hydrochloric acid and concentrated sulfuric acid mixing generate more hydrogen chloride gas, improve hydrochloric acid and
The utilization rate of concentrated sulfuric acid raw material；Hydrochloric acid and the concentrated sulfuric acid can generate hydrogen chloride gas and a large amount of heat of release, hydrogen chloride when mixing
After gas accumulates excessively in cabinet 1, pushes the rotation of rotor plate 62 to open gas vent 2, hydrogen chloride gas is made to pass through air pump
Discharge, when rotor plate 62 rotates, support plate 63 is rotated also with rotor plate 62, at this point, two material spray disks 4 are in No.1 spring 5
Thrust under upward sliding, by controller control hydrochloric acid and the concentrated sulfuric acid the ejection time, reach hydrochloric acid and the concentrated sulfuric acid interval spray
Effect out, when hydrochloric acid and the concentrated sulfuric acid do not spray, rotor plate 62 is because the reduction of air pressure passes through the bullet of No. two springs in cabinet 1
Property resetted, and hydrochloric acid and the concentrated sulfuric acid are controlled by controller again and sprayed, made 62 repeated rotation of rotor plate, reset, with this reality
The repetition of existing material spray disk 4 slides up and down, and is just being slided in the material spray disk 4 of material spray by the promotion of regulator 6 so that hydrochloric acid with
The track that the concentrated sulfuric acid sprays is more chaotic, so that the number of contact of the hydrochloric acid with the concentrated sulfuric acid is more, improves hydrochloric acid and the concentrated sulfuric acid connects
Mixed degree is touched, to improve the efficiency of hydrochloric acid and concentrated sulfuric acid mixing generation hydrogen chloride gas；With the lasting progress of reaction,
Mixed solution on partition 7 is more, is patted by the pushing of pressing plate 9 mixed liquor, in addition spiral shell during No. three 8 springing of spring
Away from extruding, the agitation carried out to mixed liquor is changed, the mixability of mixed liquor is further increased, hydrochloric acid is improved and the concentrated sulfuric acid is former
The utilization rate of material；Simultaneously as No. three 8 springing screw pitch of spring increase, liquid is flowed into from the gap between No. three springs 8 by through-hole
1 internal partition of cabinet, 7 lower space；It is discharged by the hydrogen chloride gas with heat that air pump is taken away by helix tube 3, and gas is arranged
During out, hydrogen chloride gas body heat content acts on the mixed liquor in 1 internal partition of cabinet, 7 lower space by helix tube 3, to mixed
It closes liquid to be heated, so that mixed liquor is generated hydrogen chloride gas again, further improve the utilization of hydrochloric acid and concentrated sulfuric acid raw material
Rate, last hydrogen chloride gas enter air accumulator storage.
In the description of the present invention, it is to be understood that, term " center ", "front", "rear", "vertical", "horizontal",
The orientation or positional relationship of the instructions such as "top", "bottom" "inner", "outside" be based on the orientation or positional relationship shown in the drawings, be only for
Convenient for the description present invention and simplify description, rather than the device or element of indication or suggestion meaning there must be specific side
Position is constructed and operated in a specific orientation, therefore should not be understood as limiting the scope of the invention.
Although the present invention be illustrated by specific embodiment, it will be appreciated by those skilled in the art that, do not departing from
In the case where the scope of the invention, various transformation and equivalent substitute can also be carried out to the present invention.In addition, being directed to particular condition or material
Material, can do various modifications to the present invention, without departing from the scope of the present invention.Therefore, the present invention is not limited to disclosed tool
Body embodiment, and should include the whole embodiments fallen within the scope of the appended claims.
Claims (6)
1. a kind of energy conservation and environmental protection chlorination apparatus for forming hydrogen, including cabinet (1), it is characterised in that: among the upper end of the cabinet (1)
Position is equipped with gas vent (2), is symmetrically obliquely installed at the top of cabinet (1) about gas vent (2)；Connect on the outside of the gas vent (2)
It is connected to air pump；One end of the air pump is connected with hose, and the lower end of hose is connected with helix tube (3)；Helix tube (3) winding
It is equipped with exhaust outlet in one end of cabinet (1) lower outside, helix tube (3), exhaust outlet is connect with air accumulator；Cabinet (1) top
Two sliding slots are symmetrically arranged on the inside of portion, a material spray disk (4) is slidably connected in two sliding slots；Material spray disk (4) lower end
It being connect between sliding slot lower end by No.1 spring (5), material spray disk (4) is equipped with spray material port far from the side at the top of cabinet (1),
Regulator (6) are equipped between two material spray disk (4) upper ends；The regulator (6) is mounted on gas vent by holder pivots
(2) lower section, and regulator (6) is symmetrical arranged about bracket, regulator (6) includes shaft (61), rotor plate (62) and branch
Fagging (63)；The shaft (61) is fixed on bracket；There are two the rotor plate (62) settings, two rotor plates (62) about
Bracket is symmetrically hinged on shaft (61), is connected with No. two springs, two rotor plates (62) between two rotor plates (62) middle parts
Upper end contacted with cabinet (1)；One end of the support plate (63) is fixed in the middle part of rotor plate (62), support plate (63)
The upper-end contact of the other end and material spray disk (4)；The lower section of the material spray disk (4) is equipped with horizontal positioned partition (7)；The partition
(7) several through-holes are equipped with；Pressing plate (9) are connected with by No. three springs (8) above the through-hole；Cabinet (1) bottom
Equipped with discharge gate.
2. a kind of energy conservation and environmental protection chlorination apparatus for forming hydrogen according to claim 1, it is characterised in that: on the cabinet (1)
Gas vent (2) and rotor plate (62) between be equipped with elastic slice (10)；The elastic slice (10) is connected on cabinet (1) in arc-shaped.
3. a kind of energy conservation and environmental protection chlorination apparatus for forming hydrogen according to claim 2, it is characterised in that: on the cabinet (1)
The both ends of corresponding elastic slice (10) are equipped with No.1 groove (11) and No. two grooves (12)；One end of the elastic slice (10) passes through No. four bullets
Spring is connected in No.1 groove (11), and the other end of elastic slice (10) is slidably connected in No. two grooves (12), elastic slice (10) end
Filled with oil liquid between No. two groove (12) bottoms；The counter sink of No. two grooves (12) of perforation is additionally provided on the cabinet (1)
(13), screw (14) are equipped in counter sink (13), one end of screw (14) is contacted with oil liquid.
4. a kind of energy conservation and environmental protection chlorination apparatus for forming hydrogen according to claim 1, it is characterised in that: No. three springs
(8) helical spring is selected, and the both ends of No. three springs (8) are scabbled；Gap between two adjacent pressing plates (9) is not more than
3mm。
5. a kind of energy conservation and environmental protection chlorination apparatus for forming hydrogen according to claim 4, it is characterised in that: No. three springs
(8) spring ring diameter is 2-3mm, and the screw pitch of No. three springs (8) is not more than 4mm.
6. a kind of energy conservation and environmental protection chlorination apparatus for forming hydrogen according to claim 1, it is characterised in that: the pressing plate (9)
Both ends are equipped with magnet (15), and magnet (15) polarity on the adjacent one end of two pressing plates (9) is identical.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811525989.2A CN109626325A (en) | 2018-12-13 | 2018-12-13 | A kind of energy conservation and environmental protection chlorination apparatus for forming hydrogen |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811525989.2A CN109626325A (en) | 2018-12-13 | 2018-12-13 | A kind of energy conservation and environmental protection chlorination apparatus for forming hydrogen |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109626325A true CN109626325A (en) | 2019-04-16 |
Family
ID=66073695
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811525989.2A Pending CN109626325A (en) | 2018-12-13 | 2018-12-13 | A kind of energy conservation and environmental protection chlorination apparatus for forming hydrogen |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109626325A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112382879A (en) * | 2020-11-04 | 2021-02-19 | 贵州航天电器股份有限公司 | Plug-resistant electric connector |
Citations (4)
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|---|---|---|---|---|
| GB688206A (en) * | 1949-05-24 | 1953-03-04 | Addage Ltd | Improvements in and relating to the production of chlorine dioxide |
| GB1037133A (en) * | 1963-01-30 | 1966-07-27 | Electro Chimie Metal | Improvements in or relating to the preparation of hydrofluoric acid |
| US20050029118A1 (en) * | 2003-07-21 | 2005-02-10 | Smartpool Incorporated | Salt chlorine generator |
| US20080099075A1 (en) * | 2006-10-31 | 2008-05-01 | Robert Lee Martrich | Leak containment apparatus for reactive gases |
-
2018
- 2018-12-13 CN CN201811525989.2A patent/CN109626325A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB688206A (en) * | 1949-05-24 | 1953-03-04 | Addage Ltd | Improvements in and relating to the production of chlorine dioxide |
| GB1037133A (en) * | 1963-01-30 | 1966-07-27 | Electro Chimie Metal | Improvements in or relating to the preparation of hydrofluoric acid |
| US20050029118A1 (en) * | 2003-07-21 | 2005-02-10 | Smartpool Incorporated | Salt chlorine generator |
| US20080099075A1 (en) * | 2006-10-31 | 2008-05-01 | Robert Lee Martrich | Leak containment apparatus for reactive gases |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112382879A (en) * | 2020-11-04 | 2021-02-19 | 贵州航天电器股份有限公司 | Plug-resistant electric connector |
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