CN109619475A - A kind of preparation method of fresh black fruit Sorbus alnifloria powder - Google Patents

A kind of preparation method of fresh black fruit Sorbus alnifloria powder Download PDF

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Publication number
CN109619475A
CN109619475A CN201811560414.4A CN201811560414A CN109619475A CN 109619475 A CN109619475 A CN 109619475A CN 201811560414 A CN201811560414 A CN 201811560414A CN 109619475 A CN109619475 A CN 109619475A
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black fruit
sorbus alnifloria
fruit sorbus
powder
fresh black
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丁传波
赵婷
程志强
刘文丛
郑毅男
刘兴龙
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L19/00Products from fruits or vegetables; Preparation or treatment thereof
    • A23L19/01Instant products; Powders; Flakes; Granules
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23BPRESERVING, e.g. BY CANNING, MEAT, FISH, EGGS, FRUIT, VEGETABLES, EDIBLE SEEDS; CHEMICAL RIPENING OF FRUIT OR VEGETABLES; THE PRESERVED, RIPENED, OR CANNED PRODUCTS
    • A23B7/00Preservation or chemical ripening of fruit or vegetables
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L33/00Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L5/00Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L5/00Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
    • A23L5/30Physical treatment, e.g. electrical or magnetic means, wave energy or irradiation
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Polymers & Plastics (AREA)
  • Food Science & Technology (AREA)
  • Nutrition Science (AREA)
  • Health & Medical Sciences (AREA)
  • Mycology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Medicines Containing Plant Substances (AREA)
  • Coloring Foods And Improving Nutritive Qualities (AREA)

Abstract

The present invention relates to the field of Chinese medicines, and in particular to a kind of fresh black fruit Sorbus alnifloria powder and preparation method thereof.The fresh black fruit Sorbus alnifloria powder is made of a variety of or a kind of raw material, by weight percentage, above-mentioned plurality of raw materials includes fresh black fruit Sorbus alnifloria powder 60-100%, water-soluble cellulose 0-10%, corrigent 0-1% or more, vegetable fat powder 0-40%, citric acid 0-2%, white granulated sugar 0-2%, plant polyose 0-10%, then by adding the processes such as water grinding, homogeneous, spray drying to be prepared into fresh black fruit Sorbus alnifloria powder, with can directly enter capsule, in tablet, conducive to carry, it is in good taste, conveniently take, loss of effective components is few, absorption is fast, bioavilability is high the features such as.

Description

A kind of preparation method of fresh black fruit Sorbus alnifloria powder
Technical field
The present invention relates to health food manufacture field, the processing method for being specifically related to a kind of fresh black fruit Sorbus alnifloria powder.
Background technique
Black fruit Sorbus alnifloria also known as Black Box Tracing, the wild cherry certain kind of berries, the not old certain kind of berries, rosaceae gland Aronia machaka both may be used It is used as medicine, and is a kind of food with very high nutritive value.Nutritional studies discovery, in black fruit Sorbus alnifloria fruit rich in anthocyanidin, The polyphenols such as flavonoids, phenolic acid, procyanidine.Wherein, the polyphenol content in fruit reaches 2051- 2556mg / kg(fresh weight), account for 99% or more of the fruit antioxidant content.Polyphenols in fresh juice and pasteurized juice is respectively 740-840mg/100mL and 630-695mg/100m L, accounts for about the 1/3 of fruit total phenol.Black fruit Sorbus alnifloria fruit has potential Liver protection, anti-oxidant, anti-inflammatory, antibacterial, it is antifatigue, delay senescence and the effects of beauty, cardioprotection, hypoglycemic and anti-mutation, It is used to develop the functional food of preventing hypertension, cardio-cerebrovascular diseases in American-European countries.At present in Chinese market, still Rarely Related product occurs.
Mechanical high-temperature squeezing or high temperature are perhaps generallyd use in juice process of manufacture in the extraction of black fruit Sorbus alnifloria The process of extraction, this is easy to cause the loss of the effective component flavone compound, Polyphenols and Anthocyanins of black fruit Sorbus alnifloria Or denaturation, therefore how to retain to greatest extent in black fruit Sorbus alnifloria in commercial process has an ingredient not broken It is bad, and remain to fresh-keeping and do not lose nutrition, but can accomplish to be convenient for carrying, convenient to take, ingredient draws are fast, biological utilisation Degree is high, and the present invention researchs and proposes in view of the deficiencies of the prior art.
Summary of the invention
It is an object of the invention to be directed to the deficiency of existing fresh black fruit Sorbus alnifloria processing method for keeping fresh, it is quick to provide a kind of energy Controlled atmosphere, and the nutriment of black fruit Sorbus alnifloria through processing is able to the method saved from damage, the method for the present invention has process letter Short, speed of production is fast, the low feature of processing cost, while black fruit Sorbus alnifloria through processing has easy to carry, in good taste, ingredient Absorb feature fast, that bioavilability is high.
The present invention provides a kind of preparation method of fresh black fruit Sorbus alnifloria powder, the weight percent of the component of fresh black fruit Sorbus alnifloria powder Are as follows: fresh black fruit Sorbus alnifloria powder 60-100%, water-soluble cellulose 0-10%, corrigent 0-1% or more, vegetable fat powder 0-40%, citric acid 0- 2%, white granulated sugar 0-20%, plant polyose 0-10%.Preparation method including the following steps:
Step 1): the full fresh black fruit Sorbus alnifloria of juice is selected, cleans spare, black fruit Sorbus alnifloria will be cleaned with enzyme according to 1:0.01- 0.05 ratio digests 1-4h at room temperature;
Step 2): the ratio of fresh black fruit Sorbus alnifloria and water after enzymatic hydrolysis is put into colloid mill according to the ratio of 1:2-8, is beaten, obtains Fresh black fruit Sorbus alnifloria slurries, such as must addition water-soluble fibre, corrigent, vegetable fat powder, citric acid, plant polyose component, can first by These component water are dissolved or are added water and stirred as uniform suspension, then are beaten together with the fresh black fruit Sorbus alnifloria after enzymatic hydrolysis;
Step 3): the fresh black fruit Sorbus alnifloria slurries in step 2 are crossed into homogenizer, homogenization pressure is that 0-10MP homogenization cycles are 2-3 It is secondary, the fresh black fruit Sorbus alnifloria slurries after obtaining homogeneous;
Step 4): black fruit Sorbus alnifloria slurries fresh in step 3 are crossed into high pressure homogenizer, it is equal that homogenization pressure is that 50-500MP obtains high pressure Fresh black fruit Sorbus alnifloria slurries after matter, fresh black fruit Sorbus alnifloria slurries obtain fresh black fruit Sorbus alnifloria powder through low temperature spray drying.
Compared with prior art, the invention has the following beneficial effects:
1. liang step homogeneous, first low pressure can guarantee the fluency in homogenizing process in high pressure, and can guarantee product particle size Uniformly, and particle diameter reaches between 10-200nm, ensure that the absorption of product spy fast, in good taste and high bioavilability Point.
2. using the method for the present invention, the distinctive many effumabilities of script in fresh black fruit Sorbus alnifloria can be made, to thermo-responsive day Right functional component remains well, and retains the shape of fresh ginseng, distinctive smell, and when being obviously shortened processing Between, processing cost is reduced, the quality guarantee period of fresh black fruit Sorbus alnifloria is extended, and can accomplish to be convenient for carrying, convenient to take, ingredient Absorb fast, bioavilability height.
Specific embodiment
The present invention is made combined with specific embodiments below and being further described through, but specific embodiment is not the present invention Any restriction.
The comparison (%) of effective component in the fresh black fruit Sorbus alnifloria of embodiment 1 and fresh black fruit Sorbus alnifloria powder
Ingredient Flavones Polyphenol Anthocyanidin Anthocyanin
Fresh black fruit Sorbus alnifloria 0.258% 2.24 1.75 0.025
Fresh black fruit Sorbus alnifloria powder 0.249% 2.35 1.66 0.027
Embodiment 2
The weight percent of the component of fresh black fruit Sorbus alnifloria powder are as follows: fresh black fruit Sorbus alnifloria 100%.Preparation method includes following step It is rapid:
Step 1): the full fresh black fruit Sorbus alnifloria of juice is selected, cleans spare, black fruit Sorbus alnifloria will be cleaned with enzyme according to 1:0.01's Ratio digests 1h at room temperature;
Step 2): the ratio of fresh black fruit Sorbus alnifloria and water after enzymatic hydrolysis is put into colloid mill according to the ratio of 1:8, is beaten, obtains fresh Black fruit Sorbus alnifloria slurries;
Step 3): the fresh black fruit Sorbus alnifloria slurries in step 2 are crossed into homogenizer, homogenization cycles are 3 times, and homogenization pressure is 10,000,000 Pa, the fresh black fruit Sorbus alnifloria slurries after obtaining homogeneous;
Step 4): black fruit Sorbus alnifloria slurries fresh in step 3 are crossed into high pressure homogenizer, homogenization pressure is 500 megapascal, and it is equal to obtain high pressure Fresh black fruit Sorbus alnifloria slurries after matter, fresh black fruit Sorbus alnifloria slurries obtain fresh black fruit Sorbus alnifloria powder, fresh black fruit Sorbus alnifloria through low temperature spray drying The diameter of powder is 10nm.
Embodiment 3
The weight percent of the component of fresh black fruit Sorbus alnifloria powder are as follows: fresh black fruit Sorbus alnifloria powder 60%, water-soluble cellulose 10%, corrigent 1% More than, vegetable fat powder 10%, citric acid 2%, white granulated sugar 10%, plant polyose 7%.Preparation method including the following steps:
Step 1): the full fresh black fruit Sorbus alnifloria of juice is selected, cleans spare, black fruit Sorbus alnifloria will be cleaned with enzyme according to 1:0.05's Ratio digests 4h at room temperature;
Step 2): first the components such as water-soluble fibre, corrigent, vegetable fat powder, citric acid, plant polyose are dissolved or added with water Water stirring becomes uniform suspension, then is put into colloid mill according to the ratio of 1:2 together with the fresh black fruit Sorbus alnifloria after enzymatic hydrolysis, beats Slurry, obtains slurries;
Step 3): the fresh black fruit Sorbus alnifloria slurries in step 2 are crossed into homogenizer, homogenization cycles are 2-3 times, homogenization pressure 0MP, Fresh black fruit Sorbus alnifloria slurries after obtaining homogeneous;
Step 4): black fruit Sorbus alnifloria slurries fresh in step 3 are crossed into high pressure homogenizer, homogenization pressure be 50MP obtain it is high-pressure homogeneous after Fresh black fruit Sorbus alnifloria slurries, fresh black fruit Sorbus alnifloria slurries obtain fresh black fruit Sorbus alnifloria powder through low temperature spray drying, fresh black fruit Sorbus alnifloria powder Diameter is 300nm.
Phloridzin assay in the black fruit Sorbus alnifloria powder of embodiment 4
1 instrument and reagent
LC-20A type high performance liquid chromatograph (Japanese Shimadzu, SPD-20A UV detector) ultrasonic cleaner (KQ-250DB, Kunshan ultrasonic instrument Co., Ltd), BP211D electronic balance (German Sartorious company), automatic dual pure water distiller SZ-93(Shanghai Yarong Biochemical Instrument Plant) etc..
Fresh black fruit Sorbus alnifloria powder, self-control.Reference substance phloridzin is purchased from Products in China research institute, acetonitrile (chromatographically pure, beauty Fisher company, state), pure water (Hangzhou Wahaha Co., Ltd), remaining reagent is that analysis is pure.
2 methods and result
The preparation of 2.1 solution
2.1.1 reference substance solution precision weighs phloridzin reference substance 10.00mg, is placed in 100ml volumetric flask and is dissolved with methanol Fixed molten, 0.45 μm of filtering with microporous membrane afterwards can be prepared by the phloridzin reference substance stock solution that concentration is 0.1mg/ml.
2.1.2 test solution takes sample 3.0060g to be put into the conical flask of the identical 250ml of specification, is separately added into 50ml methanol extracts 30min at 40 DEG C under the conditions of 100HZ, extract 2 times, is settled to 100ml after merging extracting solution filtering twice Volumetric flask in, 0.45 μm of filtering with microporous membrane to get arrive test sample stock solution.
2.2 chromatographic conditions and system suitability test chromatographic column: Dalian Yi Lite HypersilODS2(250mm × 4.6mm, 5 μm);Column temperature: 30;Mobile phase: acetonitrile-water (25:75);Flow velocity: 1.0mlmin-1;Detection wavelength: 285nm;Sample introduction Amount: 20 μ l.Under above-mentioned chromatographic condition, sample and the phloridzin retention time in reference substance are almost the same, and theoretical cam curve is equal Greater than 3000, the retention time of phloridzin is 7.123min.
The measurement of 2.3 sample sizes takes 3 batches of samples, prepares test solution by " 2.1.2 " item method, and 20 μ l of sample introduction is measured, It is calculated with peak area by external standard method, the content of phloridzin is 0.6%, 0.9%, 1.6% in fresh black fruit Sorbus alnifloria powder after measured.
The anti-fatigue active of the fresh black fruit Sorbus alnifloria powder of embodiment 5 is tested
By table it can be seen that phloridzin and fresh black fruit Sorbus alnifloria powder high and low dose group have antifatigue activity.
Embodiment 6 is using the black fresh powder of fruit Sorbus alnifloria in embodiment 2 or 3, and through human trial, test number is 20 people, feedback It is found that fresh powder is good in taste, no bitterness.

Claims (9)

1. a kind of preparation method of fresh black fruit Sorbus alnifloria powder, which is characterized in that the weight percent of the component of the fresh black fruit Sorbus alnifloria powder Number are as follows: fresh black fruit Sorbus alnifloria 60-100%, water-soluble cellulose 0-10%, corrigent 0-1% or more, vegetable fat powder 0-40%, citric acid 0- 2%, white granulated sugar 0-20%, plant polyose 0-10%.
2. the preparation method of the fresh black fruit Sorbus alnifloria powder according to claim 1, which is characterized in that including the following steps:
Step 1): the full fresh black fruit Sorbus alnifloria of juice is selected, cleans spare, black fruit Sorbus alnifloria will be cleaned with enzyme according to 1:0.01- 0.05 ratio digests 1-4h at room temperature;
Step 2): the ratio of fresh black fruit Sorbus alnifloria and water after enzymatic hydrolysis is put into colloid mill according to the ratio of 1:2-8, is beaten, obtains Fresh black fruit Sorbus alnifloria slurries, such as must addition water-soluble fibre, corrigent, vegetable fat powder, citric acid, plant polyose component, can first by These component water are dissolved or are added water and stirred as uniform suspension, then are beaten together with the fresh black fruit Sorbus alnifloria after enzymatic hydrolysis;
Step 3): the fresh black fruit Sorbus alnifloria slurries in step 2 are crossed into homogenizer, homogenization cycles are 2-3 times, fresh after obtaining homogeneous Black fruit Sorbus alnifloria slurries;
Step 4): black fruit Sorbus alnifloria slurries fresh in step 3 are crossed into high pressure homogenizer, obtain it is high-pressure homogeneous after fresh black fruit Sorbus alnifloria slurry Liquid, fresh black fruit Sorbus alnifloria slurries obtain fresh black fruit Sorbus alnifloria powder through low temperature spray drying.
3. the preparation method of fresh black fruit Sorbus alnifloria powder according to claim 1, which is characterized in that water-soluble fibre can be Ah Draw one of primary galactan, inulin, chitosan or two or more mixtures.
4. the preparation method of fresh black fruit Sorbus alnifloria powder according to claim 2, which is characterized in that the pressure of homogeneous in step 3 Power is 0-10 megapascal, and the high-pressure homogeneous pressure in step 4 is 50-500 megapascal.
5. the fresh black fruit Sorbus alnifloria powder obtained according to the preparation method of the fresh black fruit Sorbus alnifloria powder described in claim 2, which is characterized in that The diameter of fresh black fruit Sorbus alnifloria powder is 10-300nm.
6. the fresh black fruit Sorbus alnifloria powder obtained according to the preparation method of the fresh black fruit Sorbus alnifloria powder described in claim 2, which is characterized in that Fresh black fruit Sorbus alnifloria powder effective component remains larger than 95%.
7. according to the preparation method of the fresh black fruit Sorbus alnifloria powder described in claim 2, which is characterized in that enzyme required for digesting is single One or two kinds of above mixed enzyme of the enzymes such as peaceful enzyme, pectase, naringinase.
8. the fresh black fruit Sorbus alnifloria powder obtained according to the preparation method of the fresh black fruit Sorbus alnifloria powder described in claim 2, which is characterized in that Fresh black fruit Sorbus alnifloria powder can be prepared into the products such as lozenge, microcapsules.
9. the fresh black fruit Sorbus alnifloria powder obtained according to the preparation method of the fresh black fruit Sorbus alnifloria powder described in claim 2, which is characterized in that The content of phloridzin is 0.5-2.6% in fresh black fruit Sorbus alnifloria powder.
CN201811560414.4A 2018-12-20 2018-12-20 A kind of preparation method of fresh black fruit Sorbus alnifloria powder Pending CN109619475A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110236104A (en) * 2019-07-18 2019-09-17 潘春田 A kind of formula and preparation method thereof of anthocyanidin huyashi-chuuka (cold chinese-style noodles)
CN114431374A (en) * 2022-02-15 2022-05-06 晨日不老莓(辽宁)大健康有限责任公司 Aronia melanocarpa fruit juice freeze-dried powder and preparation process thereof

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104351869A (en) * 2014-10-18 2015-02-18 辽宁省干旱地区造林研究所 Aronia melenocarpa composite juice beverage and preparation method thereof
CN107897920A (en) * 2017-11-28 2018-04-13 中国科学院天津工业生物技术研究所 A kind of black fruit Sorbus alnifloria powder capsule and its preparation process
CN108077522A (en) * 2017-12-28 2018-05-29 天津科技大学 A kind of compound pressed candy of Black Box Tracing and preparation method thereof
CN108094811A (en) * 2017-12-15 2018-06-01 柳州市柳科科技有限公司 A kind of mulberries instant powder and preparation method thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104351869A (en) * 2014-10-18 2015-02-18 辽宁省干旱地区造林研究所 Aronia melenocarpa composite juice beverage and preparation method thereof
CN107897920A (en) * 2017-11-28 2018-04-13 中国科学院天津工业生物技术研究所 A kind of black fruit Sorbus alnifloria powder capsule and its preparation process
CN108094811A (en) * 2017-12-15 2018-06-01 柳州市柳科科技有限公司 A kind of mulberries instant powder and preparation method thereof
CN108077522A (en) * 2017-12-28 2018-05-29 天津科技大学 A kind of compound pressed candy of Black Box Tracing and preparation method thereof

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110236104A (en) * 2019-07-18 2019-09-17 潘春田 A kind of formula and preparation method thereof of anthocyanidin huyashi-chuuka (cold chinese-style noodles)
CN114431374A (en) * 2022-02-15 2022-05-06 晨日不老莓(辽宁)大健康有限责任公司 Aronia melanocarpa fruit juice freeze-dried powder and preparation process thereof

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Application publication date: 20190416