CN109592657B - Yellow phosphorus cutting reaction device - Google Patents
Yellow phosphorus cutting reaction device Download PDFInfo
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- CN109592657B CN109592657B CN201910051500.0A CN201910051500A CN109592657B CN 109592657 B CN109592657 B CN 109592657B CN 201910051500 A CN201910051500 A CN 201910051500A CN 109592657 B CN109592657 B CN 109592657B
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- yellow phosphorus
- channel
- liquid level
- rotary cutting
- water inlet
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
- C01B25/12—Oxides of phosphorus
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- Inorganic Chemistry (AREA)
- Crushing And Pulverization Processes (AREA)
Abstract
The invention provides a yellow phosphorus cutting reaction device, which comprises a yellow phosphorus channel, a blocking port, a circulating channel, a reaction box, a discharge port, a controller, an upper liquid level sensor, a lower liquid level sensor, a water inlet switch, a sensor, a yellow phosphorus inlet, an emergency valve, an automatic valve, a manual valve, a blower, a fixed rod, a fan, a grid and a rotary cutting blade, wherein when the yellow phosphorus cutting device is used, the rotary cutting blade with an annular blade notch on the surface is arranged, after a yellow phosphorus block slides to the surface of the rotary cutting blade from the yellow phosphorus inlet, the yellow phosphorus block can rotate close to the inner wall of the yellow phosphorus channel under the action of the wind, the rotary cutting blade on the inner wall of the yellow phosphorus channel can cut and thin the yellow phosphorus, so that the contact area of the yellow phosphorus is increased, the subsequent reaction is more sufficient, the blocking port with small holes uniformly distributed on the surface is arranged, after the small yellow phosphorus block falls to a lane port, the small yellow phosphorus blocks cannot enter the circulating channel, so that the operation inside the circulating channel is influenced.
Description
Technical Field
The invention relates to the technical field of yellow phosphorus processing, in particular to a yellow phosphorus cutting reaction device.
Background
Yellow phosphorus, also known as white phosphorus, is a raw material for producing phosphate fertilizers, reacts with oxygen to produce phosphorus pentoxide, a well-known substance, and has an ignition point of 40 ℃ when exposed to air, so that yellow phosphorus is generally present in water and must be submerged under water without air. In the production process of phosphorus pentoxide, if the yellow phosphorus lumps are too large, the reaction is insufficient, which affects the production efficiency, and a general yellow phosphorus feeding device is lack of a control and condition device.
Disclosure of Invention
In order to solve the above-mentioned problems, the present invention provides a yellow phosphorus cutting reaction apparatus to solve the above-mentioned problem of the yellow phosphorus block being too large.
The invention relates to a yellow phosphorus cutting reaction device, which is realized by the following specific technical means:
a yellow phosphorus cutting reaction device comprises a yellow phosphorus channel, a blocking port, a circulating channel, a reaction box, a discharge port, a controller, an upper liquid level sensor, a lower liquid level sensor, a water inlet switch, a sensor, a yellow phosphorus inlet, an emergency valve, an automatic valve, a manual valve, a blower, a fixed rod, a fan, a grid and a rotary cutting blade; the yellow phosphorus inlet is distributed with an emergency valve, an automatic valve and a manual valve from top to bottom, the rotary cutting blade is rotationally distributed on the inner wall between the yellow phosphorus channel and the automatic valve channel on the yellow phosphorus channel, the left upper side of the rotary cutting blade is fixedly connected with a blower, the inside of the blower is distributed with a fixed rod, a fan and a grid from left to right, the lower part of the yellow phosphorus channel is provided with a branch port, the left side of the branch port is blocked by a blocking port, the circulating channel is a channel formed between the blocking port and the blower, the yellow phosphorus channel on the left side of the reaction box is distributed with the automatic valve and the manual valve from left to right, the discharge port is positioned on the right lower side of the reaction box, the upper part of the right side of the reaction box is distributed with an upper liquid level sensor, a lower liquid level sensor and a water inlet from top to bottom, the right upper side of the water inlet is distributed, the controller is connected with the upper liquid level sensor, the lower liquid level sensor and the sensor.
Further, the surface of the rotary cutting blade is an annular blade notch.
Further, the fan pushes the yellow phosphorus to be cut on the rotary cutting piece in a rotating mode.
Furthermore, small holes are uniformly distributed on the surface of the blocking opening.
Further, after the upper liquid level sensor is triggered, the water inlet switch is turned off, and after the lower liquid level sensor is triggered, the water inlet switch is turned on.
Further, after the sensor is triggered, the emergency valve is closed.
Has the advantages that:
1. according to the invention, the rotary cutting blade with the annular blade notch on the surface is arranged, so that after the yellow phosphorus blocks slide to the surface of the rotary cutting blade from the yellow phosphorus inlet, the yellow phosphorus blocks can rotate close to the inner wall of the yellow phosphorus channel under the action of the forced air, and the rotary cutting blade on the inner wall of the yellow phosphorus channel can cut and thin the yellow phosphorus, so that the contact area of the yellow phosphorus is increased, and the subsequent reaction is more sufficient.
2. The fan for pushing the yellow phosphorus to slide on the rotary cutting blade is arranged, so that the yellow phosphorus can be clamped on the rotary cutting blade after falling on the rotary cutting blade to influence the falling of the subsequent yellow phosphorus, the thrust given by the fan can push the yellow phosphorus to slide on the rotary cutting blade to ensure that the yellow phosphorus blocks are cut more fully, the grid can prevent the flow guide of the cut yellow phosphorus blocks from influencing the operation of the fan, the fan can make the generated thrust in a vortex shape, and the yellow phosphorus is tightly attached to a yellow phosphorus channel under the action of the vortex thrust, so that the cutting is convenient.
3. The invention has the advantages that the small yellow phosphorus blocks cannot enter the circulating channel after falling to the branch openings due to the arrangement of the blocking openings with the small holes uniformly distributed on the surface, so that the operation in the circulating channel is influenced.
Drawings
Fig. 1 is a front structural sectional view of the present invention.
Fig. 2 is an enlarged sectional view of a portion a of the present invention.
Fig. 3 is a sectional view of the structure of the blower of the present invention.
Fig. 4 is a sectional view showing the structure of the blocking port in the present invention.
FIG. 5 is a sectional view of a rotary blade structure inside a partial yellow phosphorus channel according to the present invention.
FIG. 6 is a side cross-sectional view of the yellow phosphorus channel and the rotary cutting blade of the present invention.
In FIGS. 1-6: 1-yellow phosphorus channel, 2-blocking port, 3-circulation channel, 4-reaction box, 5-discharge port, 6-controller, 7-upper liquid level sensor, 8-lower liquid level sensor, 9-water inlet, 10-water inlet switch, 11-sensor, 12-yellow phosphorus inlet, 13-emergency valve, 14-automatic valve, 15-manual valve, 16-blower, 1601-fixed rod, 1602-fan, 1603-grid, 17-rotary cutting piece.
Detailed Description
As shown in figures 1 to 6:
the invention provides a yellow phosphorus cutting reaction device, which comprises a yellow phosphorus channel 1, a blocking port 2, a circulating channel 3, a reaction box 4, a discharge port 5, a controller 6, an upper liquid level sensor 7, a lower liquid level sensor 8, a water inlet 9, a water inlet switch 10, a sensor 11, a yellow phosphorus inlet 12, an emergency valve 13, an automatic valve 14, a manual valve 15, a blower fan 16, a fixed rod 1601, a fan 1602, a grid 1603 and a rotary cutting piece 17; an emergency valve 13, an automatic valve 14 and a manual valve 15 are distributed on a yellow phosphorus inlet 12 from top to bottom, a rotary cutting blade 17 is rotationally distributed on the inner wall between the yellow phosphorus channel 1 and the automatic valve 14 channel on the yellow phosphorus channel 1, a blower 16 is fixedly connected with the left upper side of the rotary cutting blade 17, a fixed rod 1601, a fan 1602 and a grid 1603 are distributed inside the blower 16 from left to right, a branch port is arranged at the lower part of the yellow phosphorus channel 1, a blocking port 2 is arranged at the left side of the branch port for blocking, a circulating channel 3 is a channel formed between the blocking port 2 and the blower 16, the automatic valve 14 and the manual valve 15 are distributed on the yellow phosphorus channel 1 at the left side of a reaction box 4 from left to right, a discharge port 5 is positioned at the right lower side of the reaction box 4, an upper liquid level sensor 7, a lower liquid level sensor 8 and a water inlet 9 are distributed on the upper right side of the reaction, the inductor 11 is positioned at the upper left corner of the reaction box 4, and the controller 6 is connected with the upper liquid level inductor 7, the lower liquid level inductor 8 and the inductor 11.
Wherein, the surface of the rotary cutting piece 17 is an annular blade cut, after the yellow phosphorus blocks slide to the surface of the rotary cutting piece 17 from the yellow phosphorus inlet 12, the yellow phosphorus blocks can rotate close to the inner wall of the yellow phosphorus channel 1 under the action of the pushed air 12, and the rotary cutting piece 17 on the inner wall of the yellow phosphorus channel 1 can cut and thin the yellow phosphorus, so that the contact area of the yellow phosphorus is increased, and the subsequent reaction is more sufficient.
The pushing fan 16 pushes the yellow phosphorus to rotate and cut on the rotary cutting blade 17, and after the yellow phosphorus falls on the rotary cutting blade 17, the yellow phosphorus may be clamped on the rotary cutting blade 17 to affect the drop of the subsequent yellow phosphorus, and the pushing force given by the pushing fan 16 pushes the yellow phosphorus to slide on the rotary cutting blade 17 so as to enable the yellow phosphorus to be cut more sufficiently, the grid 1603 also prevents the flow of the cut yellow phosphorus from being guided to affect the operation of the pushing fan 16, the fan 1602 can generate a vortex-shaped pushing force, so that the yellow phosphorus is tightly attached to the yellow phosphorus channel 1 under the action of the vortex-shaped pushing force, and the cutting is facilitated.
Wherein, block 2 surface evenly distributed and have small-size hole, lie in when the little yellow phosphorus piece falls to the lane mouth after, little yellow phosphorus piece can not get into circulation channel 3 to influence the inside operation of circulation channel 3.
Wherein, go up liquid level inductor 7 and trigger the back, switch 10 that intakes closes, lower liquid level inductor 8 triggers the back, switch 10 that intakes opens, lies in can keeping the water level in reaction box 4 all the time and keep normal level, can not influence the efficiency of reaction, and in the time of intaking, inductor 11 closes automatic valve 14, can not influence reaction efficiency because of moisture is not enough.
Wherein, the back is triggered to inductor 11, and emergency valve 13 closes, lies in if go up liquid level sensor 7 after losing effect, thereby water can get into reaction box 4 always and influence reaction efficiency, causes certain accident even, and inductor 11 triggers the back, and corresponding alarm sounds, and emergency valve 13 closes the back then can interrupt the supply of yellow phosphorus.
When the invention is used, the yellow phosphorus slides from the yellow phosphorus channel 1 to the rotary cutting piece 17, under the action of the air pushing machine 16 and gravity, the yellow phosphorus is cut into small blocks, then enters the reaction box 4 through the yellow phosphorus channel 1 for reaction, finally the reactant is discharged from the discharge hole 5, if the water level in the reaction period induces the upper liquid level inductor 7 or the lower liquid level inductor 8, the water inlet switch 10 is closed or opened, so that the water level in the reaction box 4 is kept at a normal level, the reaction efficiency is not influenced, and in the water inlet time, the inductor 11 closes the automatic valve 14, the reaction efficiency is not influenced due to insufficient water, if the upper liquid level inductor 7 loses the action, the water can enter the reaction box 4 all the time, the reaction efficiency is influenced even to a certain degree, after the inductor 11 is triggered, the corresponding alarm is sounded, the supply of the yellow phosphorus is interrupted after the emergency valve 13 is closed, in case of emergency, the operator can also close the manual valve 15 to interrupt the reaction.
Claims (6)
1. A yellow phosphorus cutting reaction device comprises a yellow phosphorus channel (1), a blocking opening (2), a circulating channel (3), a reaction box (4), a discharge opening (5), a controller (6), an upper liquid level sensor (7), a lower liquid level sensor (8), a water inlet (9), a water inlet switch (10), a sensor (11), a yellow phosphorus inlet (12), an emergency valve (13), an automatic valve (14), a manual valve (15), a blower (16), a fixing rod (1601), a fan (1602), a grid (1603) and a rotary cutting blade (17), and is characterized in that the emergency valve (13), the automatic valve (14) and the manual valve (15) are distributed at the yellow phosphorus inlet (12) from top to bottom, and the rotary cutting blade (17) is rotationally distributed at the inner wall between the yellow phosphorus channel (1) and the automatic valve (14) on the yellow phosphorus channel (1), the rotary cutting blade (17) is fixedly connected with a blower (16) at the upper left side, a fixed rod (1601), a fan (1602) and a grid (1603) are distributed inside the blower (16) from left to right, a branch port is arranged at the lower part of a yellow phosphorus channel (1), a blocking port (2) is arranged at the left side of the branch port to block, a circulating channel (3) is a channel formed between the blocking port (2) and the blower (16), an automatic valve (14) and a manual valve (15) are distributed on the left yellow phosphorus channel (1) at the left side of the reaction box (4) from left to right, a discharge port (5) is positioned at the lower right side of the reaction box (4), an upper liquid level inductor (7), a lower liquid level inductor (8) and a water inlet (9) are distributed on the upper right side of the water inlet (9), a water inlet switch (10) is distributed on the upper right side of the water inlet (9), and the inductor (11) is positioned at the upper left corner of the reaction box (4, the controller (6) is connected with the upper liquid level sensor (7), the lower liquid level sensor (8) and the sensor (11).
2. The yellow phosphorus cutting reaction device according to claim 1, wherein: the surface of the rotary cutting blade (17) is an annular blade notch.
3. The yellow phosphorus cutting reaction device according to claim 1, wherein: the air pushing machine (16) pushes the yellow phosphorus to rotate and cut on the rotary cutting piece (17).
4. The yellow phosphorus cutting reaction device according to claim 1, wherein: small holes are uniformly distributed on the surface of the blocking opening (2).
5. The yellow phosphorus cutting reaction device according to claim 1, wherein: after the upper liquid level sensor (7) is triggered, the water inlet switch (10) is closed, and after the lower liquid level sensor (8) is triggered, the water inlet switch (10) is opened.
6. The yellow phosphorus cutting reaction device according to claim 1, wherein: after the sensor (11) is triggered, the emergency valve (13) is closed.
Priority Applications (1)
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CN201910051500.0A CN109592657B (en) | 2019-01-21 | 2019-01-21 | Yellow phosphorus cutting reaction device |
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CN201910051500.0A CN109592657B (en) | 2019-01-21 | 2019-01-21 | Yellow phosphorus cutting reaction device |
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CN109592657A CN109592657A (en) | 2019-04-09 |
CN109592657B true CN109592657B (en) | 2020-04-03 |
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CN100581997C (en) * | 2008-01-04 | 2010-01-20 | 四川大学 | Method for producing ultra-pure yellow phosphorus |
CN203528770U (en) * | 2013-09-04 | 2014-04-09 | 中国船舶重工集团公司第七○二研究所 | Mechanization aquatic plant fishing boat |
CN203498090U (en) * | 2013-09-09 | 2014-03-26 | 江山市艺康化学有限公司 | Yellow phosphorus supply adjustment device |
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Denomination of invention: A yellow phosphorus cutting reaction device Effective date of registration: 20230928 Granted publication date: 20200403 Pledgee: Zhejiang Jiangshan rural commercial bank Limited by Share Ltd. Pledgor: JIANGSHAN YIKANG CHEMICAL Co.,Ltd. Registration number: Y2023980059446 |