CN109573998B - Graphite oxide device is peeled off to ultrasonic wave - Google Patents
Graphite oxide device is peeled off to ultrasonic wave Download PDFInfo
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- CN109573998B CN109573998B CN201811331684.8A CN201811331684A CN109573998B CN 109573998 B CN109573998 B CN 109573998B CN 201811331684 A CN201811331684 A CN 201811331684A CN 109573998 B CN109573998 B CN 109573998B
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- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/15—Nano-sized carbon materials
- C01B32/182—Graphene
- C01B32/198—Graphene oxide
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Abstract
The utility model provides an ultrasonic wave peels off graphite oxide device, including ultrasonic reaction cauldron, the through-hole is seted up to ultrasonic reaction cauldron's top surface, pass a dwang in the through-hole, the inside cavity that is of dwang, the upper end of dwang is located the outside of through-hole, the dwang passes through bearing fixed connection with the inner wall of through-hole, the curved stirring head of lower extreme fixed mounting of dwang, the inside one side fixed mounting ultrasonic vibration equipment of ultrasonic reaction cauldron, ultrasonic reaction cauldron's below is equipped with the casing, ultrasonic reaction cauldron places in the casing, ultrasonic reaction cauldron's outer wall passes through several branch fixed connection with the inner wall of casing, the lower extreme fixed mounting discharging pipe of casing, the upper end of discharging pipe pass the casing and with ultrasonic reaction cauldron's lower extreme fixed connection, the discharging pipe communicates with each. The stirring device is simple in structure, reasonable in design, convenient to use and simple to operate, and can be used for quickly stirring and mixing materials and improving the working efficiency.
Description
Technical Field
The invention belongs to the field of stripping of graphite oxide, and particularly relates to an ultrasonic graphite oxide stripping device.
Background
At present, the preparation method of the graphene material generally comprises the following steps: micro-computer lift-off, epitaxial growth, graphite oxide reduction and chemical vapor deposition. Among them, the microcomputer stripping method, the chemical vapor deposition method, and the epitaxial growth method all have the characteristics of high production cost, difficulty in large-scale industrial popularization, and the like, and are inconvenient to clean the inside of the reaction kettle after use and use next time.
Disclosure of Invention
The invention provides an ultrasonic graphite oxide stripping device, which is used for overcoming the defects in the prior art.
The invention is realized by the following technical scheme:
the utility model provides an ultrasonic wave peels off oxidation graphite equipment, including ultrasonic reaction cauldron, ultrasonic reaction cauldron's top surface sets up the through-hole, the dwang is inside to be cavity, the upper end of dwang is located the outside of through-hole, dwang and the inner wall of through-hole pass through bearing fixed connection, the curved stirring head of lower extreme fixed mounting of dwang, one side fixed mounting ultrasonic vibration equipment of ultrasonic reaction cauldron inside, ultrasonic reaction cauldron's below is equipped with the casing, ultrasonic reaction cauldron places in the casing, ultrasonic reaction cauldron's outer wall passes through several branch fixed connection with the inner wall of casing, the lower extreme fixed mounting discharging pipe of casing, the upper end of discharging pipe passes the casing and communicates with the lower extreme fixed connection of ultrasonic reaction cauldron, discharging pipe and ultrasonic reaction cauldron inside communicate with each other, fixed mounting valve on the discharging pipe, ultrasonic reaction cauldron's top is equipped with the motor, the output shaft of motor and the upper end fixed connection of dwang, the top surface fixed mounting air pump of dwang, the bottom surface of.
According to the ultrasonic graphite oxide stripping device, a plurality of movable wheels are fixedly arranged on the bottom surface of the base.
According to the ultrasonic graphite oxide stripping device, the damping spring is arranged on the outer ring of the elastic column, the upper end of the damping spring is fixedly connected with the bottom surface of the supporting seat, and the lower end of the damping spring is fixedly connected with the top surface of the base.
According to the ultrasonic graphite oxide stripping device, the stirring rake is fixedly arranged on the bottom surface of the stirring head and can contact the bottom surface inside the ultrasonic reaction kettle.
According to the ultrasonic graphite oxide stripping device, the top surface of the ultrasonic reaction kettle is provided with the annular guide groove, the bottom surface of the transverse plate is fixedly provided with the support rod, and the lower end of the support rod is positioned in the guide groove and can move along the guide groove.
According to the ultrasonic graphite oxide stripping device, the guide plates are fixedly arranged on two sides of the top surface inside the ultrasonic reaction kettle and correspond to the feeding pipes.
The invention has the advantages that: the ultrasonic vibration device has the advantages of simple structure, reasonable design, convenience in use and simplicity in operation, can quickly stir and mix materials, improves the working efficiency, can scrape the inner wall of the ultrasonic reaction kettle completely when discharging and cleaning the inside of the ultrasonic reaction kettle, prevents residual materials, can save materials, can prevent the inner wall of the ultrasonic reaction kettle from being cleaned incompletely, can effectively strip graphite oxide, and can keep the temperature of a solution in the reaction kettle stable, thereby ensuring the output efficiency of the ultrasonic vibration device. When the device is used, materials can be added into the ultrasonic reaction kettle through the feeding pipe, the motor works, the output shaft of the motor drives the rotating rod to rotate, the rotating rod drives the sleeve to rotate, the sleeve drives the scraper blade to rotate through the piston rod, meanwhile, the rotating rod drives the stirring head to rotate, the materials in the ultrasonic reaction kettle can be quickly stirred and mixed, after the materials are mixed, the graphite oxide solution is placed in the ultrasonic reaction kettle, the circulating pump works, the cooling liquid in the cooling box flows into the shell through the circulating pipe, the cooling liquid in the shell can cool the materials in the ultrasonic reaction kettle, meanwhile, the control valve on the exhaust pipe is opened, the waste gas in the ultrasonic reaction kettle enters the waste gas collection device through the exhaust pipe, the liquid storage tank can be used for recycling the graphite oxide solution overflowing from the exhaust pipe, the ultrasonic vibration device can be controlled to work in the ultrasonic reaction kettle by opening the ultrasonic controller, the ultrasonic vibration equipment can generate ultrasonic waves, so that all graphite oxide solution flowing through the reaction kettle can be stripped, a valve is opened, and the graphite oxide can flow out of the ultrasonic reaction kettle through the discharge pipe to perform the next link; when discharging and cleaning the inside of the ultrasonic reaction kettle, the motor and the air pump work simultaneously, the motor can drive the scraper blade to rotate, the air pump can enable air to enter the rotating rod through the connecting pipe, the air in the rotating rod enters the sleeve through the air pipe, the air in the sleeve pushes the piston rod to drive the scraper blade to move outwards along the sleeve, the scraper blade is made to contact with the inner wall of the ultrasonic reaction kettle, materials on the inner wall of the ultrasonic reaction kettle can be completely scraped, residual materials are prevented, materials can be saved, and the inner wall of the ultrasonic reaction kettle can be prevented from being cleaned incompletely; after the scraper is used, the motor and the air pump stop working, the piston rod is pulled under the action of the first spring to drive the scraper to reset, and the scraper is simple to operate and convenient to use.
Drawings
In order to more clearly illustrate the embodiments of the present invention or the technical solutions in the prior art, the drawings needed to be used in the description of the embodiments or the prior art will be briefly introduced below, and it is obvious that the drawings in the following description are some embodiments of the present invention, and for those skilled in the art, other drawings can be obtained according to these drawings without creative efforts.
FIG. 1 is a schematic structural view of the present invention; fig. 2 is a view in the direction a of fig. 1.
Detailed Description
In order to make the objects, technical solutions and advantages of the embodiments of the present invention clearer, the technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are some, but not all, embodiments of the present invention. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
A graphite oxide stripping device comprises an ultrasonic reaction kettle 1, a through hole 2 is formed in the top surface of the ultrasonic reaction kettle 1, a rotating rod 3 passes through the inside of the through hole 2, the inside of the rotating rod 3 is hollow, the upper end of the rotating rod 3 is positioned outside the through hole 2, the rotating rod 3 is fixedly connected with the inner wall of the through hole 2 through a bearing, an arc-shaped stirring head 4 is fixedly installed at the lower end of the rotating rod 3, an ultrasonic vibration device 5 is fixedly installed at one side inside the ultrasonic reaction kettle 1, a shell 6 is arranged below the ultrasonic reaction kettle 1, the ultrasonic reaction kettle 1 is arranged in the shell 6, the outer wall of the ultrasonic reaction kettle 1 is fixedly connected with the inner wall of the shell 6 through a plurality of supporting rods 7, a discharge pipe 8 is fixedly installed at the lower end of the shell 6, the upper end of the discharge pipe 8 passes through the shell 6 and is fixedly connected with the lower end of the ultrasonic reaction kettle 1, a discharge pipe 8 is fixedly connected with a circulation pipe 1, a valve 9 is fixedly installed on the rotating rod 1, a motor 10 is arranged above the rotating rod 1, the output shaft of the motor 10, the motor 10 is fixedly connected with the discharge pipe 3, the discharge pipe 10, the motor 10 is fixedly connected with the ultrasonic reaction kettle 1 through a support 11, the ultrasonic reaction kettle 1, the ultrasonic pump 15, the ultrasonic circulation pipe 6, the ultrasonic circulation pipe 13 is fixedly connected with the ultrasonic reaction kettle 1, the ultrasonic circulation pipe 13, the ultrasonic reaction kettle 1, the ultrasonic circulation pipe 13 is fixedly connected with the ultrasonic pump 15, the ultrasonic circulation pipe 13, the ultrasonic circulation pipe 6, the ultrasonic circulation pipe 13 is arranged in the ultrasonic circulation pipe 13, the ultrasonic circulation pipe 6, the ultrasonic circulation pipe 13 is arranged, the ultrasonic circulation pipe 13, the ultrasonic circulation pipe 6, the ultrasonic circulation pipe 13 is arranged, the ultrasonic circulation pipe 6, the ultrasonic circulation pipe 2, the ultrasonic reaction kettle 1, the ultrasonic circulation pipe 2 is arranged, the ultrasonic circulation pipe 2, the ultrasonic reaction kettle 1, the ultrasonic circulation pipe 2 is arranged, the ultrasonic circulation pipe 2 is arranged, the ultrasonic circulation pipe 13 is arranged in the ultrasonic circulation pipe 13, the ultrasonic circulation pipe 2 is arranged in the ultrasonic circulation pipe 2, the ultrasonic circulation pipe 2 is arranged in the ultrasonic circulation pipe 2, the ultrasonic circulation pipe 13, the ultrasonic circulation pipe 2, the ultrasonic circulation pipe 13 is arranged, the ultrasonic circulation pipe 2 is arranged, the ultrasonic circulation pipe 1, the ultrasonic circulation pipe 2, the ultrasonic circulation pipe 6, the ultrasonic circulation pipe 13 is arranged, the ultrasonic circulation pipe 2, the ultrasonic circulation pipe 1, the ultrasonic circulation pipe 13 is arranged, the ultrasonic circulation pipe 1, the ultrasonic circulation pipe 2, the ultrasonic circulation pipe 1 is arranged, the ultrasonic circulation pipe 1 is arranged, the ultrasonic circulation pipe 1, the ultrasonic circulation pipe 13 is arranged, the ultrasonic circulation pipe 2 is arranged, the ultrasonic circulation pipe 1, the ultrasonic circulation pipe 2 is arranged in the ultrasonic circulation pipe 2, the ultrasonic circulation pipe 1, the ultrasonic circulation pipe 2, the ultrasonic circulation pipe 13 is arranged, the ultrasonic circulation pipe 2, the ultrasonic circulation pipe 1, the ultrasonic circulation pipe 2 is arranged in the ultrasonic circulation pipe 13 is arranged, the ultrasonic circulation pipe 2 is arranged in the ultrasonic circulation.
Specifically, in order to facilitate the movement of the device, a plurality of moving wheels are fixedly mounted on the bottom surface of the base 26. When the device is used, the movable wheel can be used for facilitating the movement of the device, and the use is convenient.
Specifically, in order to absorb shock, the outer ring of the elastic column 27 in this embodiment is provided with a damping spring, the upper end of the damping spring is fixedly connected with the bottom surface of the supporting seat 24, and the lower end of the damping spring is fixedly connected with the top surface of the base 26. When the damping device is used, the damping spring can be used for buffering and damping the damping device, so that the damping device is more stable in the working process.
Further, in order to facilitate the mixing of the materials, a stirring rake is fixedly installed on the bottom surface of the stirring head 4 in the embodiment, and the stirring rake can contact the bottom surface inside the ultrasonic reaction kettle 1. When the ultrasonic reaction kettle 1 is used, sediment can be stirred under the action of the stirring rake, so that the sediment can be quickly mixed.
Furthermore, in order to support and guide the transverse plate 12, the top surface of the ultrasonic reactor 1 according to this embodiment is provided with an annular guide groove 20, the bottom surface of the transverse plate 12 is fixedly provided with a support rod 21, and the lower end of the support rod 21 is located in the guide groove 20 and can move along the guide groove 20. When the device is used, the support rod 21 moves in the guide groove 20, thereby supporting and guiding the transverse plate 12.
Furthermore, in order to guide the flow of the material, guide plates are fixedly mounted on two sides of the top surface inside the ultrasonic reaction kettle 1, and the guide plates correspond to the feeding pipes 22. When using this device, can carry out the water conservancy diversion to the material through the guide plate to can be convenient for the material enter into in ultrasonic reaction cauldron 1.
Finally, it should be noted that: the above examples are only intended to illustrate the technical solution of the present invention, but not to limit it; although the present invention has been described in detail with reference to the foregoing embodiments, it will be understood by those of ordinary skill in the art that: the technical solutions described in the foregoing embodiments may still be modified, or some technical features may be equivalently replaced; and such modifications or substitutions do not depart from the spirit and scope of the corresponding technical solutions of the embodiments of the present invention.
Claims (6)
1. The utility model provides an ultrasonic wave peels off oxidation graphite device, which is characterized in that includes ultrasonic reaction cauldron (1), through-hole (2) are seted up to the top surface of ultrasonic reaction cauldron (1), pass a dwang (3) in through-hole (2), dwang (3) inside is cavity, the upper end of dwang (3) is located the outside of through-hole (2), dwang (3) and the inner wall of through-hole (2) pass through bearing fixed connection, curved stirring head (4) is fixed to the lower extreme fixed mounting of dwang (3), one side fixed mounting ultrasonic vibration equipment (5) of ultrasonic reaction cauldron (1) inside, the below of ultrasonic reaction cauldron (1) is equipped with casing (6), ultrasonic reaction cauldron (1) is placed in casing (6), the outer wall of ultrasonic reaction cauldron (1) and the inner wall of casing (6) pass through several branch rod (7) fixed connection, the lower extreme fixed mounting of discharging pipe (8) of dwang (8) passes through casing (6) and is connected with the lower extreme fixed connection of ultrasonic reaction cauldron (1), discharging pipe (8) and the lower extreme fixed connection of ultrasonic reaction cauldron (1), discharging pipe (1) and the lower extreme of ultrasonic reaction cauldron (1), discharging pipe (16) are equipped with the bottom surface of ultrasonic reaction cauldron (16) fixed connection of ultrasonic reaction cauldron (16), the fixed connection pipe (24) of the fixed connection between the bottom surface of the fixed connection pipe (24) of the fixed connection pipe (13), the fixed connection pipe (13) of the fixed connection pipe (6), the fixed connection pipe (13) of the fixed connection pipe (13), the fixed connection pipe (13) of the fixed connection pipe (6), the fixed connection pipe (6) of the fixed connection pipe (13) of the fixed connection pipe (6), the fixed connection pipe (6) of the fixed connection pipe (13) of the fixed connection pipe (6) of the fixed connection pipe (3) of the fixed connection pipe (6) and the fixed connection pipe (6), the fixed connection pipe (13) of the fixed connection pipe (3) of the fixed connection pipe (13) of the fixed connection pipe (6), the fixed connection pipe (3) and the fixed connection pipe (3) of the fixed connection pipe (3), the fixed connection pipe (2) of the fixed connection pipe (3), the fixed connection pipe (3) and the fixed connection pipe (3) of the fixed connection pipe (13) of the fixed connection pipe (3), the fixed connection pipe (3) of the fixed connection pipe (3) and the fixed connection pipe (3) of the fixed connection pipe (3), the fixed connection pipe (3) of the fixed connection pipe (2) and the fixed connection pipe (3), the fixed connection pipe (2) and the fixed connection pipe (2) fixed connection pipe (6), the fixed connection pipe (2) and the fixed connection pipe (6), the fixed connection pipe (3) and the fixed.
2. The ultrasonic graphite oxide stripping device according to claim 1, wherein: a plurality of movable wheels are fixedly arranged on the bottom surface of the base (26).
3. The ultrasonic graphite oxide stripping device according to claim 1, wherein: the outer ring of the elastic column (27) is provided with a damping spring, the upper end of the damping spring is fixedly connected with the bottom surface of the supporting seat (24), and the lower end of the damping spring is fixedly connected with the top surface of the base (26).
4. The ultrasonic graphite oxide stripping device according to claim 1, wherein: the bottom surface of the stirring head (4) is fixedly provided with a stirring rake which can contact the bottom surface inside the ultrasonic reaction kettle (1).
5. The ultrasonic graphite oxide stripping device according to claim 1, wherein: the top surface of the ultrasonic reaction kettle (1) is provided with an annular guide groove (20), the bottom surface of the transverse plate (12) is fixedly provided with a support rod (21), and the lower end of the support rod (21) is positioned in the guide groove (20) and can move along the guide groove (20).
6. The ultrasonic graphite oxide stripping device according to claim 1, wherein: the guide plates are fixedly arranged on two sides of the inner top surface of the ultrasonic reaction kettle (1) and correspond to the feeding pipe (22).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811331684.8A CN109573998B (en) | 2018-11-09 | 2018-11-09 | Graphite oxide device is peeled off to ultrasonic wave |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811331684.8A CN109573998B (en) | 2018-11-09 | 2018-11-09 | Graphite oxide device is peeled off to ultrasonic wave |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN109573998A CN109573998A (en) | 2019-04-05 |
| CN109573998B true CN109573998B (en) | 2020-07-14 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811331684.8A Expired - Fee Related CN109573998B (en) | 2018-11-09 | 2018-11-09 | Graphite oxide device is peeled off to ultrasonic wave |
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Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110282618B (en) * | 2019-07-23 | 2022-09-23 | 无锡乘臻科技有限公司 | Large-scale graphite alkene ultrasonic stripping off device |
| CN112892305B (en) * | 2021-01-28 | 2022-11-08 | 淄博高新区成大机械设计研究所 | Sol tank with vacuum hole filtering device and using method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106365160B (en) * | 2016-10-21 | 2018-06-08 | 杭州国彪超声设备有限公司 | A kind of ultrasonic wave removes graphite oxide device |
| CN206188395U (en) * | 2016-10-21 | 2017-05-24 | 杭州国彪超声设备有限公司 | Oxidation graphite device is peeled off to ultrasonic wave |
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