CN109518481A - A kind of weaving ink-jet printing disperse dye ink and preparation method thereof - Google Patents
A kind of weaving ink-jet printing disperse dye ink and preparation method thereof Download PDFInfo
- Publication number
- CN109518481A CN109518481A CN201811304993.6A CN201811304993A CN109518481A CN 109518481 A CN109518481 A CN 109518481A CN 201811304993 A CN201811304993 A CN 201811304993A CN 109518481 A CN109518481 A CN 109518481A
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- Prior art keywords
- ink
- jet printing
- disperse dye
- weaving
- dye ink
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Classifications
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/16—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using dispersed, e.g. acetate, dyestuffs
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/52—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing synthetic macromolecular substances
- D06P1/5207—Macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- D06P1/525—Polymers of unsaturated carboxylic acids or functional derivatives thereof
- D06P1/5257—(Meth)acrylic acid
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/52—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing synthetic macromolecular substances
- D06P1/5264—Macromolecular compounds obtained otherwise than by reactions involving only unsaturated carbon-to-carbon bonds
- D06P1/5285—Polyurethanes; Polyurea; Polyguanides
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Dispersion Chemistry (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
- Coloring (AREA)
Abstract
The invention discloses a kind of weaving ink-jet printing disperse dye ink and preparation method thereof, the component material of the weaving ink-jet printing disperse dye ink includes: disperse dyes mill base, water-soluble cosolvent, polymer emulsion, fixation crosslinking agent, surfactant, pH controlling agent, fungicide and deionized water.The proportion regulation proportional region of the weaving ink-jet printing disperse dye ink and preparation method thereof is big, and operability is wide, with different application field or improvised means, there is different appearance effects；And inside is free of nitrito- compound, and small toxicity is more conducive to subsequent popularization and use.
Description
Technical field
The present invention relates to textile printing and dyeing technology and weaving ink-jet printing ink technical field, specially a kind of weaving ink-jet print
Flower disperse dye ink and preparation method thereof.
Background technique
Digital ink-jet printed is a kind of faster printing in textiles new technology of development in recent years, its main feature is that do not have to plate-making,
On demand piezoelectric, the ink-jet imaging directly on fabric or ready-made clothes, water consumption is few, and discharge amount is few, and occupied area is small, and recruitment is few, energy conservation
Environmental protection, and compared with traditional printing technology, digit printing is in color, clarity, in the performance of colour gamut, can achieve tradition
The unapproachable height of stamp has vast potential for future development.
Disperse dye ink is current mature production technology using a kind of extensive ink, is mainly used for chemical & blended fabric dyeing
Stamp.Existing commercial dispersants dye ink is broadly divided into sublimable ink and direct-injection ink, and sublimable ink is used for transfer printing, transfer print
Flower causes certain pollution to environment due to needing a large amount of transfer paper.And general disperse dyes direct-injection stamp post-processing
Cumbersome, washing causes biggish environmental pollution to also limit its application.
Summary of the invention
The purpose of the present invention is to provide a kind of weaving ink-jet printing disperse dye inks and preparation method thereof, on solving
State that the processing proposed in background technique is cumbersome and the larger problem of environmental pollution.
To achieve the above object, the invention provides the following technical scheme: a kind of weaving ink-jet printing disperse dye ink and
Preparation method, the component material of the weaving ink-jet printing disperse dye ink includes: disperse dyes mill base, water-soluble molten altogether
Agent, polymer emulsion, fixation crosslinking agent, surfactant, pH controlling agent, fungicide and deionized water.
Preferably, a kind of weaving ink-jet printing disperse dye ink and preparation method thereof, the percentage between each component are as follows:
Preferably, the water-soluble cosolvent is ethyl alcohol, isopropanol, ethylene glycol, diethylene glycol, triethylene glycol, tetrem two
Alcohol, 1,2-PD, 1,3-PD, methyl propanediol, a contracting propylene glycol, two contracting propylene glycol, glycerine, 1,2- butanediol,
1,4-butanediol, 1,5 pentanediols, pentaerythrite, 1,2- hexylene glycol, 2 methyl cyclohexanol, heptandiol, n-octyl alcohol, PEG200,
PEG400, PEG800,2-Pyrrolidone, two or more in n-methyl-2-pyrrolidone.
Preferably, the polymer emulsion is aqueous polyurethane emulsion or water-and acrylate lotion.
Preferably, the crosslinking agent is closure isocyanates.
Preferably, the surfactant be nonionic surface active agent triton x-100, this Pan 20, this Pan 60, this
It is Pan 80, polysorbate40, polysorbate60, polysorbate65, Tween 80, OP-7, OP-10, OP-15, paregal O -10, paregal O -20, average
Add that O-25, SG-10, SE-10, OE-1, the worry 420 that disappears, the worry 440 that disappears, the worry 465 that disappears, disappear worry one of 485 or more
Kind.
Preferably, the pH controlling agent is sodium hydroxide, ammonium hydroxide, diethanol amine, one of triethanolamine or a variety of, institute
Stating fungicide is vanillic aldehyde or ethyl vanillin aldehydes compound, anilid class, thiazoles, isothiazole ketone, in imidazoles
Any one.
Preferably, a kind of weaving ink-jet printing disperse dye ink and preparation method thereof, preparation method are as follows:
Surfactant, water-soluble cosolvent, fungicide, 300-500 revs/min of stirring is added in deionized water according to the ratio
10-40 minutes, after mixing evenly, polymer emulsion and fixation crosslinking agent, 300-500 revs/min of stirring are added in the above solution
10-40 minutes, it is eventually adding disperse dyes mill base, adjusting ink pH value is 7-9, and 500nm filter membrane mistake is used after stirring
Weaving ink-jet printing disperse dye ink is made in filter.
Compared with prior art, the beneficial effects of the present invention are:
1, by the way that specific lotion and curing agent is added, not only increase the affinity of disperse dyes and fabric fibre and
The storage stability of disperse dye ink is increased, gained ink printed is smooth, and bright in colour, post-processing is simple, it is not necessarily to washing,
Working strength is reduced, pollution is reduced.
2, pH controlling agent is added, the pH value of mixture can be adjusted to 7-9, reduce soda acid in stirring and processing
Influence of the property to mixture quality.
Specific embodiment
The embodiment of the present application solves existing by providing a kind of weaving ink-jet printing disperse dye ink and preparation method thereof
There is in technology the post-processing of disperse dyes direct-injection stamp cumbersome, washing causes biggish environmental pollution to also limit asking for its application
Topic.
It is clearly and completely described below in conjunction with the technical solution in the embodiment of the present invention, it is clear that described reality
Applying example is only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, this field is general
Logical technical staff every other embodiment obtained without making creative work belongs to what the present invention protected
Range.
Embodiment 1
A kind of weaving ink-jet printing disperse dye ink and preparation method thereof, the weaving ink-jet printing disperse dye ink
Component material include: disperse dyes mill base, water-soluble cosolvent, polymer emulsion, fixation crosslinking agent, surfactant, pH
Specific lotion and curing agent is added in controlling agent, fungicide and deionized water, not only increases disperse dyes and fabric fibre
Affinity and the storage stability for increasing disperse dye ink, gained ink printed is smooth, bright in colour, post-processing letter
It is single, without washing, working strength is reduced, pollution is reduced.
Preferably, a kind of weaving ink-jet printing disperse dye ink and preparation method thereof, the percentage between each component
Are as follows:
Preferably, the water-soluble cosolvent is ethyl alcohol, isopropanol, ethylene glycol, diethylene glycol, triethylene glycol, tetrem two
Alcohol, 1,2-PD, 1,3-PD, methyl propanediol, a contracting propylene glycol, two contracting propylene glycol, glycerine, 1,2- butanediol,
1,4-butanediol, 1,5 pentanediols, pentaerythrite, 1,2- hexylene glycol, 2 methyl cyclohexanol, heptandiol, n-octyl alcohol, PEG200,
PEG400, PEG800, (PEG200, PEG400, PEG800 are polyethylene glycol), in 2-Pyrrolidone, n-methyl-2-pyrrolidone
Two or more mill base can quickly be incorporated in water by a variety of water-soluble cosolvents.
Preferably, the polymer emulsion is aqueous polyurethane emulsion or water-and acrylate lotion, including PU625 (gathers
Urethane), PD-1 (chemical method adhesive), PD-2 (urethane acrylate adhesive), HF-1 (irradiation method adhesive), HF-
1901R (polymerization spokeization imitates reactive adhesive), HF-333R (superelevation fastness imitates reactive coating printing adhesive) etc., using polymerization
Object lotion accelerates mill base dissolution as lytic agent.
Preferably, the crosslinking agent is closure isocyanates, and there is ambient-temp-stable to be heated to 100 degree of temperatures above and start
React (temperature is higher, and the time is shorter) prevents dye ink from taking off after use so as to be configured to stable one-component system
Color.
Preferably, the surfactant be nonionic surface active agent triton x-100, this Pan 20, this Pan 60, this
Pan 80 (Si Panwei sorbitol anhydride laurate), polysorbate40 (polyoxyethylene sorbitan monopalmitate), polysorbate60 (polyoxy
Ethylene sorbitan monostearate), polysorbate65 (polyoxyethylene sorbitol acid anhydride tristearate), (polyoxyethylene is de- for Tween 80
Water sorbitol monooleate), (OP-7, OP-10, OP-15 are emulsifier, specially alkyl phenol polyoxy by OP-7, OP-10, OP-15
Vinethene), paregal O -10, paregal O -20, peregal O-25 (average to add as natural fatty alcohol and ethylene oxide adduct),
SG-10 (stearic acid polyoxyethylene ether emulsifier), SE-10 (polyoxyethylene stearic acid ester), OE-1 (PVA glue), disappear worry 420,
Disappear one of worry 440, the worry 465 that disappears, the worry 485 that disappears (disappearing worried is surfactant) or a variety of, surfactant tool
Having can align on the surface of solution, and the substance that surface tension can be made to be remarkably decreased, convenient for the use of ink, (PD-1 with
PD-2 is provided by Hefei Juhe Fuhua Technology Co., Ltd.).
Preferably, the pH controlling agent is sodium hydroxide, ammonium hydroxide, diethanol amine, one of triethanolamine or a variety of, institute
Stating fungicide is vanillic aldehyde or ethyl vanillin aldehydes compound, anilid class, thiazoles, isothiazole ketone, in imidazoles
The pH value of mixture can be adjusted in 7-9 by pH controlling agent, reduce the destruction of the material of acid-base property by any one.
Preferably, a kind of weaving ink-jet printing disperse dye ink and preparation method thereof, the specific steps are that:
Surfactant, water-soluble cosolvent, fungicide, 300-500 revs/min of stirring is added in deionized water according to the ratio
10-40 minutes, after mixing evenly, polymer emulsion and fixation crosslinking agent, 300-500 revs/min of stirring are added in the above solution
10-40 minutes, it is eventually adding disperse dyes mill base, adjusting ink pH value is 7-9, and 500nm filter membrane mistake is used after stirring
Weaving ink-jet printing disperse dye ink is made in filter
Embodiment 2
A kind of weaving ink-jet printing disperse dye ink and preparation method thereof, the mixing ratio by weight between each component are as follows:
In the present embodiment, 1.0g is disappeared worry 465,0.2g isothiazolone, 15g diethylene glycol, 10g ethylene glycol is added
In 21.8g water, after stirring under 500 revs/min of revolving speed, the crosslinking of 10gHF-1 and 2g blocked isocyanate is added
Agent stirs evenly under 500 revs/min of revolving speed, and 40g black disperse dye mill base is added, and adjusts pH to 7- with appropriate triethanolamine
9, black disperse dye ink is obtained with 500nm membrane filtration after stirring, physical index is as follows: surface tension:
33.8mN/m, rotary viscosity: 3.8mpa.s, average grain diameter: 125nm, 2103 μ S/cm of conductivity.Through high temperature (60 DEG C) low temperature (0
DEG C) weather resistance tests: the black ink storage stability is good.Ink-jet printed test obtains on chemical & blended fabric: the black
Ink printed fluency is good, bright in colour, good hand touch, without washing after printing, only need in 170-180 DEG C of high temperature steaming 8min or
1-2min is baked and banked up with earth at 180-200 DEG C, dry and wet crock fastness and washing fastness can reach 4 grades or more.
Embodiment 3
A kind of weaving ink-jet printing disperse dye ink and preparation method thereof, the mixing ratio by weight between each component are as follows:
In the present embodiment, by 0.5g triton x-100,0.3g isothiazolone, 25g glycerine, 10g PEG400,5g isopropyl
Alcohol is added in 19.2g water, 8gPD-1 and 2g blocked isocyanate is added after stirring under 500 revs/min of revolving speed
Crosslinking agent stirs evenly under 500 revs/min of revolving speed, and 30g cyan disperse dyes mill base is added, and adjusts pH with appropriate diethanol amine
To 7-9, cyan disperse dye ink is obtained with 500nm membrane filtration after stirring, physical index is as follows: surface
Power: 34.5mN/m, rotary viscosity: 9.2mpa.s, average grain diameter: 107nm, 2520 μ S/cm of conductivity.Through high temperature (60 DEG C) low temperature
(0 DEG C) weather resistance is tested: the cyan storage stability is good.Ink-jet printed test obtains on chemical & blended fabric: the blueness
Chromatic ink printing fluency is good, bright in colour, good hand touch, only need to be in 170-180 DEG C of high temperature steaming 8min without washing after printing
Or 1-2min is baked and banked up with earth at 180-200 DEG C, dry and wet crock fastness and washing fastness can reach 4 grades or more.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
A variety of variations, modification, replacement can be carried out to these embodiments without departing from the principles and spirit of the present invention by understanding
And modification, the scope of the present invention is defined by the appended.
Claims (8)
1. a kind of weaving ink-jet printing disperse dye ink, it is characterised in that: the weaving ink-jet printing disperse dye ink
Component material includes: disperse dyes mill base, water-soluble cosolvent, polymer emulsion, fixation crosslinking agent, surfactant, pH control
Preparation, fungicide and deionized water.
2. a kind of weaving ink-jet printing disperse dye ink according to claim 1, it is characterised in that: between each component
Percentage are as follows:
。
3. a kind of weaving ink-jet printing disperse dye ink according to claim 2, it is characterised in that: described water-soluble total
Solvent is ethyl alcohol, isopropanol, ethylene glycol, diethylene glycol, triethylene glycol, tetraethylene glycol, 1,2-PD, 1,3-PD, first
Base propylene glycol, a contracting propylene glycol, two contracting propylene glycol, glycerine, 1,2- butanediol, 1,4-butanediol, 1,5 pentanediols, Ji Wusi
Alcohol, 1,2- hexylene glycol, 2 methyl cyclohexanol, heptandiol, n-octyl alcohol, PEG200, PEG400, PEG800,2-Pyrrolidone, N- first
Two or more in base -2-Pyrrolidone.
4. a kind of weaving ink-jet printing disperse dye ink according to claim 1, it is characterised in that: the polymer cream
Liquid is aqueous polyurethane emulsion or water-and acrylate lotion.
5. a kind of weaving ink-jet printing disperse dye ink according to claim 1, it is characterised in that: the crosslinking agent is
Closure isocyanates.
6. a kind of weaving ink-jet printing disperse dye ink according to claim 1, it is characterised in that: the surface-active
Agent be nonionic surface active agent triton x-100, this Pan 20, this Pan 60, this Pan 80, polysorbate40, polysorbate60, polysorbate65,
Tween 80, OP-15, paregal O -10, paregal O -20, peregal O-25, SG-10, SE-10, OE-1, disappears at OP-7, OP-10
Worry 420, the worry 440 that disappears, the worry 465 that disappears, disappear one of worry 485 or a variety of.
7. a kind of weaving ink-jet printing disperse dye ink according to claim 1, it is characterised in that: the pH controlling agent
For sodium hydroxide, ammonium hydroxide, diethanol amine, one of triethanolamine or a variety of, the fungicide is vanillic aldehyde or ethyl vanillin
Aldehyde compound, anilid class, thiazoles, isothiazole ketone, any one in imidazoles.
8. a kind of weaving ink-jet printing disperse dye ink according to claim 1, preparation method are as follows:
Surfactant, water-soluble cosolvent, fungicide, 300-500 revs/min of stirring 10- is added in deionized water according to the ratio
40 minutes, after mixing evenly, polymer emulsion and fixation crosslinking agent, 300-500 revs/min of stirring 10- are added in the above solution
40 minutes, it is eventually adding disperse dyes mill base, adjusting ink pH value is 7-9, and 500nm membrane filtration system is used after stirring
Must weave ink-jet printing disperse dye ink.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811304993.6A CN109518481A (en) | 2018-11-05 | 2018-11-05 | A kind of weaving ink-jet printing disperse dye ink and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811304993.6A CN109518481A (en) | 2018-11-05 | 2018-11-05 | A kind of weaving ink-jet printing disperse dye ink and preparation method thereof |
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| CN109518481A true CN109518481A (en) | 2019-03-26 |
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| CN201811304993.6A Pending CN109518481A (en) | 2018-11-05 | 2018-11-05 | A kind of weaving ink-jet printing disperse dye ink and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109988456A (en) * | 2019-04-28 | 2019-07-09 | 新昌县高纤纺织有限公司 | Environment-friendly type textile printing ink and preparation method thereof |
| CN112301761A (en) * | 2020-11-06 | 2021-02-02 | 安徽聚合辐化化工有限公司 | Printing method free of washing or less washing |
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| CN105968955A (en) * | 2016-05-24 | 2016-09-28 | 鲁继烈 | Direct spraying ink for dispersed dye spinning |
| CN107603342A (en) * | 2017-06-10 | 2018-01-19 | 合肥聚合辐化技术有限公司 | A kind of ink-jet printed white coating ink of fabric |
| CN107904984A (en) * | 2017-12-28 | 2018-04-13 | 郑州鸿盛数码科技股份有限公司 | A kind of water nano digit printing direct-injection ink, production technology and Method of printing |
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| CN104153222A (en) * | 2014-09-02 | 2014-11-19 | 江苏格美高科技发展有限公司 | Direct injection ink-jet printing dispersion ink and preparation method thereof |
| CN104194494A (en) * | 2014-09-02 | 2014-12-10 | 江苏格美高科技发展有限公司 | High-color-fastness inkjet printing pigment ink and preparation method thereof |
| CN105968955A (en) * | 2016-05-24 | 2016-09-28 | 鲁继烈 | Direct spraying ink for dispersed dye spinning |
| CN107603342A (en) * | 2017-06-10 | 2018-01-19 | 合肥聚合辐化技术有限公司 | A kind of ink-jet printed white coating ink of fabric |
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| CN109988456A (en) * | 2019-04-28 | 2019-07-09 | 新昌县高纤纺织有限公司 | Environment-friendly type textile printing ink and preparation method thereof |
| CN112301761A (en) * | 2020-11-06 | 2021-02-02 | 安徽聚合辐化化工有限公司 | Printing method free of washing or less washing |
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Application publication date: 20190326 |