CN109505146A - A kind of Thief zone dispersing type thermal transfer ink and preparation method thereof - Google Patents
A kind of Thief zone dispersing type thermal transfer ink and preparation method thereof Download PDFInfo
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- CN109505146A CN109505146A CN201811299124.9A CN201811299124A CN109505146A CN 109505146 A CN109505146 A CN 109505146A CN 201811299124 A CN201811299124 A CN 201811299124A CN 109505146 A CN109505146 A CN 109505146A
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- disperse dyes
- thermal transfer
- thief zone
- type thermal
- ink
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/16—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using dispersed, e.g. acetate, dyestuffs
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/003—Transfer printing
Abstract
The invention discloses a kind of Thief zone dispersing type thermal transfer inks and preparation method thereof, the Thief zone dispersing type thermal transfer ink is made of following mass percent component: infiltration disperse dyes 15~60%, common disperse dyes 15~60%, dispersing agent 0.3~20%, organic solvent 12~50%, deionized water 30~70%, surfactant 0.5~10%, preservative 0.05~0.2%.The preparation method is as follows: at room temperature, after disperse dyes, common disperse dyes and dispersant will be permeated by mass percentage, disperse dyes and dispersing agent being permeated in grinder and is being dispersed after mixing evenly, entering grinder is ground, and dispersion liquid is obtained；Dispersion liquid is put into reaction kettle again, after organic solvent, deionized water, surfactant, preservative stirring is added, with filter membrane or filter element filtering, obtains Thief zone dispersible ink.The present invention has good color fastness, fluency, stability, bright in luster, has good matching and adaptability to common digital-code printer in the market.
Description
Technical field
The present invention relates to thermal transfer technical field of ink more particularly to a kind of Thief zone dispersing type thermal transfer ink and its
Preparation method.
Background technique
China's traditional dyeing and finishing treatment process is essentially the process flows such as pre-treatment, dyeing, stamp, post-processing, washing, that
It is big to will appear blowdown flow rate, dye utilization rate is low in dyeing, and stamp engraving is at high cost, and the factors such as delivery cycle length lead to tradition
Printing and dyeing development is restricted.Because traditional dyeing and finishing has printing and dyeing fabrics good penetrability, color difference is consistent before and after cloth, leads to traditional print
Dye can not replace.Especially for chiffon class cloth, home textile lint class cloth, elastic woven material turns over yarn in positive and negative color difference, shows money or valuables one carries unintentionally
Etc. have very big advantage.
Ready-made ripe thermal transfer digital printing process, by the ink matched, desk-top publishing is changed the line map, and is beaten by number
Machine operation is printed, heat-transferring printing paper is printed to, using high temperature coining (generally roller coining or plate imprint) mode, 200
DEG C or more high temperature imprint 30s or more, be made into stamp semi-finished product.Such mode has the delivery cycle short, and it is excellent that typesetting expense is low etc.
Point can do means suitable and permeate not high product.But to chiffon class cloth, home textile lint class cloth, elastic woven material is positive and negative
Color difference turns over yarn, and show money or valuables one carries unintentionally etc. can not solve the problems, such as always it.
Also occurs a kind of digital direct ink-jet hydraulic art on the market, this technique is by handling starching before cloth, drying, beating
The process flows such as print, color development, washing solve the cost issues in terms of traditional stamp engraving, and require infiltration to ask cloth
Topic, but there are bigger drawbacks, such as: in longer period of time, machine cost is very high, especially spray head, before needing increase
The equipment of processing, color development and washing etc., early period, cost input was larger.In addition, direct-injection technique existing defects also reside in, ink
Water carries out color development by drying form, and color color fastness needs to improve, and direct-injection technique printing precision also can be poor；
In summary all kinds of production technology characteristics of market stamp using ready-made ripe digital printing process, and can reach solution
Certainly chiffon class cloth, home textile lint class cloth, elastic woven material in positive and negative color difference, the problems such as turning over yarn, showing money or valuables one carries unintentionally pain spot, while it is related
Digit printing industry need to only change newly developed infiltration ink without increasing equipment, change process flow.Without more
Change the digital printing process of comparative maturity, the requirement for solving client to infiltration can be reached.
Summary of the invention
In view of the above-mentioned problems, the present invention provides one kind to be able to solve ordinary hot transfer ink on certain type clothes
The Thief zone dispersing type thermal transfer ink and preparation method thereof for the problems such as what is occurred turns over yarn, shows money or valuables one carries unintentionally, and positive and negative color difference is bigger.
In order to solve the above technical problems, the technical scheme adopted by the invention is that: a kind of Thief zone dispersing type thermal transfer ink
Water, the Thief zone dispersing type thermal transfer ink are made of following mass percent component: infiltration disperse dyes 15~60%,
Common disperse dyes 15~60%, dispersing agent 0.3~20%, organic solvent 12~50%, deionized water 30~70%, surface
Activating agent 0.5~10%, preservative 0.05~0.2%.
Preferably, the infiltration disperse dyes use the solvent blue dye of composition cyan to number as 23,35,36,
45, one or more of 59,67,70,78,90,97,102,104,122,132.
Preferably, the common disperse dyes using composition cyan Disperse blue dye number 60,79,333,
359, one or more of 360,367 blendings form, or the solvent red dye number for forming magenta ink is 1,3,
41, one or more of 111,119,179,242；Common disperse dyes are using the dispersion orchil for forming magenta ink
One or more of number 4,22,55,59,60,146,152,191 blending forms, or the solvent yellow for forming yellow ink
Dyestuff number is one or more of 12,14,16,18,33,43,72,135；Common disperse dyes are using group yellowly color ink
One or more of the dispersion weld number 51,54,64,65,82,119,160 and 211 of water blending forms, or is used for group
It is 23,35,36,45,59,67,70,78,90,97,102,104,122,132 at the solvent blue dye number of black ink；It is general
Disperse blue dye number 60,79,333,359,360,367 of the logical disperse dyes using composition black ink, solvent red dye
Material number is 1,3,41,111,119,179,242；Common dispersion orchil number 4,22,55,59,60,146,152,
191, solvent yellow dye number is 12,14,16,18,33,43,72,135, it is common disperse weld number 51,54,64,
65, three kinds or more blendings in 82,119,160 and 211 form.
Preferably, the dispersing agent uses the lignin for having hydrophilic radical, condensation sodium salt substance, polyoxyethylene ether
One of substance.
Preferably, the organic solvent is ethylene glycol, polyethylene glycol 200, polyethylene glycol 400, Macrogol 600, poly- second
Glycol 800, cetomacrogol 1000, polyethylene glycol 1500, polyethylene glycol 2000, diethylene glycol (DEG), triethylene glycol, propylene glycol, glycerine,
1.5 pentanediols, polypropylene glycol, ethylene glycol monomethyl ether, diethylene glycol methyl ether and butyl glycol ether, polyvinylpyrrolidone, N- methyl pyrrole
One or more of pyrrolidone.
Preferably, the surfactant uses nonionic surfactant, anionic surfactant, amphoteric ion
One of surfactant.
A kind of preparation method of Thief zone dispersing type thermal transfer ink, described method includes following steps:
Step 1: at room temperature, by mass percentage, will infiltration disperse dyes 15~60%, common disperse dyes 15~
60% and dispersing agent 0.3~20% mix after, in grinder use diameter 0.25-0.35mm zirconium pearl, permeate disperse dyes
It is stirred evenly with dispersing agent in dispersion, 1500~2000r/min of revolving speed, after stirring 60min, enters grinder and ground, revolving speed
1270~1380r/min, grinding distribution 60-200h, obtains dispersion liquid；
Step 2: dispersion liquid is put into reaction kettle, organic solvent 12~50%, deionized water 30~70%, table is added
Face activating agent 0.5~10%, preservative 0.05~0.2%, 1500~2000r/min of revolving speed, after stirring 60min, with 0.22 μm
Filter membrane or filter element filtering obtain Thief zone dispersible ink.
By the above-mentioned description to structure of the invention it is found that compared to the prior art, the present invention has the advantage that
1, Thief zone dispersing type thermal transfer ink of the present invention compares traditional dyeing and finishing, pollution-free, digital typesetting, delivery cycle
The advantages such as short can reach osmotic effect of the traditional dyeing and finishing on cloth, ordinary hot transfer printing digital stamp be compared, using same
Technique just can solve the positive and negative color difference of cloth, and the problems such as turning over yarn, show money or valuables one carries unintentionally, osmotic effect increases 20-100% than ordinary ink,
It compares direct-injection number to handle without front and back, the modes such as washing just can solve infiltration problem, and precision and color and color fastness
It is better very much, is increased without equipment cost.
2, the present invention has good color fastness, fluency, stability, bright in luster, is not changing common thermal transfer number
Under the premise of code printing technology, it just can reach the required requirement to infiltration in market, have to common digital-code printer in the market
Good matching and adaptability.
Specific embodiment
In order to make the objectives, technical solutions, and advantages of the present invention clearer, with reference to embodiments, to this hair
It is bright to be further elaborated.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, not
For limiting the present invention.
Embodiment
A kind of Thief zone dispersing type thermal transfer ink, the Thief zone dispersing type thermal transfer ink is by following quality percentage
It is formed than component: infiltration disperse dyes 15~60%, common disperse dyes 15~60%, dispersing agent 0.3~20%, You Jirong
Agent 12~50%, deionized water 30~70%, surfactant 0.5~10%, preservative 0.05~0.2%.
It is preferred that are as follows: infiltration disperse dyes 15~40%, common disperse dyes 15~40%, dispersing agent 0.3~15% have
Solvent 30~50%, water 35~60%, surfactant 0.5~8%, preservative 0.05~0.2%；
Further preferably are as follows: deionized water 40~50%.
The infiltration disperse dyes use the solvent blue dye of composition cyan to number as 23,35,36,45,59,67,
70, one or more of 78,90,97,102,104,122,132.The common disperse dyes are divided using composition cyan
It dissipates one or more of blue dyes number 60,79,333,359,360,367 blending to form, or for forming magenta ink
Solvent red dye number be one or more of 1,3,41,111,119,179,242；Common disperse dyes are using composition ocean
One or more of the dispersion orchil number 4,22,55,59,60,146,152,191 of red ink blending forms, or uses
Numbering in the solvent yellow dye of composition yellow ink is one or more of 12,14,16,18,33,43,72,135；Common point
Dyestuff is dissipated using one in the dispersion weld number 51,54,64,65,82,119,160 and 211 of group yellowly chromatic ink
Kind or more blending form, or the solvent blue dye number for forming black ink is 23,35,36,45,59,67,70,78,
90,97,102,104,122,132；Common disperse dyes using composition black ink Disperse blue dye number 60,79,
333,359,360,367, solvent red dye number is 1,3,41,111,119,179,242；Common dispersion orchil number
4,22,55,59,60,146,152,191, solvent yellow dye number is 12,14,16,18,33,43,72,135, common to disperse
Three kinds or more blendings in weld number 51,54,64,65,82,119,160 and 211 form.
The dispersing agent use with hydrophilic radical lignin, as lignin sulfonic acid sodium salt (REAX85A or
) or lignosulfonates, dispersing agent MF (Dispersant MF) REAX907；Dispersing agent is using condensation sodium salt object
Matter, such as methanonaphthalene sodium sulfonate salt (dispersing agent NNO), phenolsulfonic acid condensation sodium salt (dispersing agent DN), dimethylsuccinic sodium sulfonate
Salt (dispersing agent OT-75), dodecyl benzene sulfonic acid and its sodium salt ABS；Dispersing agent uses polyoxyethylene ether substance, such as fat
Alcohols polyoxyethylene ether (such as 0 series of peregal).
The organic solvent is ethylene glycol, polyethylene glycol 200, polyethylene glycol 400, Macrogol 600, polyethylene glycol
800, cetomacrogol 1000, polyethylene glycol 1500, polyethylene glycol 2000, diethylene glycol (DEG), triethylene glycol, propylene glycol, glycerine, 1.5 penta
Glycol, polypropylene glycol, ethylene glycol monomethyl ether, diethylene glycol methyl ether and butyl glycol ether, polyvinylpyrrolidone, N- crassitude
One or more of ketone.
The surfactant uses nonionic surfactant, anionic surfactant, amphoteric ion surface-active
One of agent.Such as: acetylenic diols surfactant (U.S. gas surfynol 104E, 465), modified polyorganosiloxane class table
Face activating agent (U.S. gas surfynol 960), fluorinated surfactant (Du Pont FS-3100).
The preservative uses BIT-20.
Thief zone dispersing type thermal transfer ink of the invention, viscosity 2.5-5mPa.s, preferable viscosity are 3.5-
4.3mPa.s, surface tension 18-50mN/m, preferable surface tension 22-35mN/m.
A kind of preparation method of Thief zone dispersing type thermal transfer ink, described method includes following steps:
Step 1: under room temperature (20 DEG C) by mass percentage, disperse dyes 15~60%, common disperse dyes will be permeated
15~60% and dispersing agent 0.3~20% mix after, in grinder use diameter 0.25-0.35mm zirconium pearl, infiltration dispersion
Dyestuff and dispersing agent are stirred evenly in dispersion, 1500~2000r/min of revolving speed, after stirring 60min, are entered grinder and are ground,
1270~1380r/min of revolving speed, grinding distribution 60-200h, obtains dispersion liquid；
Step 2: dispersion liquid is put into reaction kettle, organic solvent 12~50%, deionized water 30~70%, table is added
Face activating agent 0.5~10%, preservative 0.05~0.2%, 1500~2000r/min of revolving speed, after stirring 60min, with 0.22 μm
Filter membrane or filter element filtering obtain Thief zone dispersible ink.
Embodiment 1 (blue) that the method for the present invention is prepared, 3 (yellow), 5 (red), 7 (black) Thief zone types point
Heat dissipation transfer ink (self-control) comparative example 2 (blue), 4 (yellow), 6 (red), 8 (black) ordinary hots transfer ink (use ten thousand
Exquisite black, red, yellow, blue (source area: Italian retailer: the heat of the exquisite chemical industry (Shanghai) Co., Ltd. of Kai Angwan
Sublimable ink)) osmotic effect is shown in Table 1.
Embodiment 1,3,5,7, viscosity test DV-II+Pro type Digital Viscometer, is set as 25 DEG C &60rpm, table
The face tension full-automatic surface tension instrument of BZY-1, the test of adopting platinum plate method；Respectively in MIMAKI JV33, imperial 5113 double ends of precious bodyguard,
Bao Shilong 5,113 3 and the imperial 4,720 3 fluency test results of precious bodyguard are shown in Table 2.
As it can be seen from table 1 the comparison coining comparison of embodiment 1,3,5,7, osmotic effect are common significantly better than 2,4,6,8
Thermal transfer ink.
From table 2 it can be seen that the range of viscosities of embodiment 1,3,5,7 is in 3.5~4.5mPa.s, surface tension 22-
28mN/m；MIMAKI JV33,5113 double ends of precious bodyguard dragon, imperial 5,113 3 and imperial 4,720 3, precious bodyguard, precious bodyguard upper with good
Adaptability and matching.
Embodiment 1 that the method for the present invention is prepared, 3,5,7, MIMAKI JV33, imperial 5113 double ends of precious bodyguard, Bao Shilong
On 5113 3 and dragon 4,720 3, treasured bodyguard, the printing fluency of ink is detected.Print media is " beautiful shadow " heat-transferring printing paper J10
Series, ink printed fluency test result are shown in Table 3.
The assessment method of ink fluency test are as follows:
A grades: continuously printing 10000ml, printing smoothness is without broken string；
B grades: continuously printing 10000ml, 3 lattice of print procedure interrupt line <；
C grades: continuously printing 10000ml, print procedure interrupt line >=3 lattice test printing fluencies.
According to test result, illustrate Thief zone dispersing type thermal transfer ink viscosity that the method for the present invention is prepared 3.5
In MIMAKI JV33, imperial 5113 double ends of precious bodyguard, precious bodyguard dragon 5,113 3 within the scope of~4.5mPa.s, surface tension 22-28mN/m
Head and precious bodyguard dragon 4,720 3 are precious in MIMAKI JV33, imperial 5113 double ends of precious bodyguard above with good adaptability and matching
Bodyguard dragon 5,113 3 and precious bodyguard dragon 4,720 3 upper printings have good fluency.
The component and technological parameter of 1 embodiment of table
The Thief zone dispersing type thermal transfer ink tested viscosity and surface tension result of 2 embodiment of table
| Embodiment and comparative example | Embodiment 1 | Embodiment 3 | Embodiment 5 | Embodiment 7 |
| Viscosity (mPa.s) | 3.8 | 3.9 | 3.5 | 4.1 |
| Surface tension mN/m | 28.2 | 27.8 | 28 | 28.5 |
The Thief zone dispersing type thermal transfer ink printed fluency test result of 3 embodiment of table
| Embodiment and comparative example | Embodiment 1 | Embodiment 3 | Embodiment 5 | Embodiment 7 |
| Fluency test | A | A | B | B |
In conclusion Thief zone dispersing type thermal transfer ink of the present invention compares traditional dyeing and finishing, pollution-free, digital typesetting is handed over
The advantages such as the goods period is short can reach osmotic effect of the traditional dyeing and finishing on cloth, compare ordinary hot transfer printing digital stamp, use
Same technique just can solve the positive and negative color difference of cloth, and the problems such as turning over yarn, show money or valuables one carries unintentionally, osmotic effect increases 20- than ordinary ink
100%, comparison direct-injection number is handled without front and back, the modes such as is washed, just be can solve infiltration problem, and precision and color and
Color fastness is well very much, is increased without equipment cost.
The present invention has good color fastness, fluency, stability, bright in luster, is not changing ordinary hot transfer printing digital
It under the premise of printing technology, just can reach the required requirement to infiltration in market, have to common digital-code printer in the market good
Good matching and adaptability.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all in essence of the invention
Made any modifications, equivalent replacements, and improvements etc., should all be included in the protection scope of the present invention within mind and principle.
Claims (7)
1. a kind of Thief zone dispersing type thermal transfer ink, it is characterised in that: the Thief zone dispersing type thermal transfer ink is by following
Mass percent component composition: infiltration disperse dyes 15~60%, common disperse dyes 15~60%, dispersing agent 0.3~20%,
Organic solvent 12~50%, deionized water 30~70%, surfactant 0.5~10%, preservative 0.05~0.2%.
2. a kind of Thief zone dispersing type thermal transfer ink according to claim 1, it is characterised in that: the infiltration disperse dyes
Use the solvent blue dye number of composition cyan for 23,35,36,45,59,67,70,78,90,97,102,104,122,
One or more of 132.
3. a kind of Thief zone dispersing type thermal transfer ink according to claim 1, it is characterised in that: the common disperse dyes
One or more of Disperse blue dye number 60,79,333,359,360,367 using composition cyan blending forms,
Or the solvent red dye number for forming magenta ink is one or more of 1,3,41,111,119,179,242；Commonly
Disperse dyes are using one of the dispersion orchil number 4,22,55,59,60,146,152,191 for forming magenta ink
The above blending forms, or the solvent yellow dye number for forming yellow ink is in 12,14,16,18,33,43,72,135
More than one；Common disperse dyes using group yellowly chromatic ink dispersion weld number 51,54,64,65,82,119,
One or more of 160 and 211 blendings form, or the solvent blue dye number for forming black ink is 23,35,36,45,
59,67,70,78,90,97,102,104,122,132；Common disperse dyes are using the Disperse blue dye for forming black ink
Number 60,79,333,359,360,367, solvent red dye number is 1,3,41,111,119,179,242；Common dispersion is red
Dyestuff number 4,22,55,59,60,146,152,191, solvent yellow dye number is 12,14,16,18,33,43,72,135, general
Three kinds or more the blendings that the reduction of fractions to a common denominator dissipates in weld number 51,54,64,65,82,119,160 and 211 form.
4. a kind of Thief zone dispersing type thermal transfer ink according to claim 1, it is characterised in that: the dispersing agent uses band
One of have the lignin of hydrophilic radical, be condensed sodium salt substance, polyoxyethylene ether substance.
5. a kind of Thief zone dispersing type thermal transfer ink according to claim 1, it is characterised in that: the organic solvent is second
Glycol, polyethylene glycol 200, polyethylene glycol 400, Macrogol 600, polyethylene glycol-800, cetomacrogol 1000, polyethylene glycol
1500, polyethylene glycol 2000, diethylene glycol (DEG), triethylene glycol, propylene glycol, glycerine, 1.5 pentanediols, polypropylene glycol, ethylene glycol monomethyl ether,
One or more of diethylene glycol methyl ether and butyl glycol ether, polyvinylpyrrolidone, N-Methyl pyrrolidone.
6. a kind of Thief zone dispersing type thermal transfer ink according to claim 1, it is characterised in that: the surfactant is adopted
With one of nonionic surfactant, anionic surfactant, zwitterionic surfactant.
7. the preparation method of Thief zone dispersing type thermal transfer ink described in a kind of claim 1, it is characterised in that: the method packet
Include following steps:
Step 1: at room temperature, by mass percentage, disperse dyes 15~60%, 15~60% and of common disperse dyes will be permeated
After dispersing agent 0.3~20% mixes, the zirconium pearl of diameter 0.25-0.35mm is used in grinder, permeates disperse dyes and dispersion
Agent is stirred evenly in dispersion, 1500~2000r/min of revolving speed, after stirring 60min, is entered grinder and is ground, and revolving speed 1270~
1380r/min, grinding distribution 60-200h, obtains dispersion liquid；
Step 2: dispersion liquid is put into reaction kettle, organic solvent 12~50%, deionized water 30~70% is added, surface is lived
Property agent 0.5~10%, preservative 0.05~0.2%, 1500~2000r/min of revolving speed, stir 60min after, with 0.22 μm of filter membrane
Or filter element filtering, obtain Thief zone dispersible ink.
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| CN114892423A (en) * | 2022-06-15 | 2022-08-12 | 江苏泰慕士针纺科技股份有限公司 | Thermal transfer digital printing process of natural fiber composite fabric |
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| CN109505146B (en) | 2021-11-16 |
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