CN109500023A - A kind of elemental analyser reaction tube cleaning plant and its application method - Google Patents

A kind of elemental analyser reaction tube cleaning plant and its application method Download PDF

Info

Publication number
CN109500023A
CN109500023A CN201811570590.6A CN201811570590A CN109500023A CN 109500023 A CN109500023 A CN 109500023A CN 201811570590 A CN201811570590 A CN 201811570590A CN 109500023 A CN109500023 A CN 109500023A
Authority
CN
China
Prior art keywords
reaction tube
elemental analyser
fixing sleeve
fixed plate
motor
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201811570590.6A
Other languages
Chinese (zh)
Inventor
郝翔翔
李禄军
邹文秀
李娜
尤孟阳
韩晓增
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Northeast Institute of Geography and Agroecology of CAS
Original Assignee
Northeast Institute of Geography and Agroecology of CAS
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Northeast Institute of Geography and Agroecology of CAS filed Critical Northeast Institute of Geography and Agroecology of CAS
Priority to CN201811570590.6A priority Critical patent/CN109500023A/en
Publication of CN109500023A publication Critical patent/CN109500023A/en
Pending legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B08CLEANING
    • B08BCLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
    • B08B9/00Cleaning hollow articles by methods or apparatus specially adapted thereto 
    • B08B9/08Cleaning containers, e.g. tanks
    • B08B9/0804Cleaning containers having tubular shape, e.g. casks, barrels, drums
    • B08B9/0808Cleaning containers having tubular shape, e.g. casks, barrels, drums by methods involving the use of tools, e.g. by brushes, scrapers

Landscapes

  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)

Abstract

A kind of elemental analyser reaction tube cleaning plant and its application method.The invention belongs to field of chemical detection, and in particular to a kind of elemental analyser reaction tube cleaning plant and its application method.The present invention is to solve catalyst efficiency in tradition cleaning elemental analyser crystal reaction tube is low, the problem of being easily destroyed reaction tube.It includes pedestal, side fixed plate, upper mounted plate, rear fixed plate, motor fixing plate, motor, drill bit, guide supporting seat, guide rail, sliding block, quartz ampoule fixing sleeve, fixing sleeve handle and activity waste material box.It drives drill bit to remove the catalyst copper oxide to agglomerate in crystal reaction tube using motor, removes thoroughly, and reaction tube will not be damaged.Catalyst in one crystal reaction tube is removed using the device in the present invention, the used time is no more than 2 minutes, compared with traditional artificial sweep-out method, saves physical strength, improve work efficiency, and is easy to operate.

Description

A kind of elemental analyser reaction tube cleaning plant and its application method
Technical field
The invention belongs to field of chemical detection, and in particular to a kind of elemental analyser reaction tube cleaning plant and its user Method.
Background technique
Elemental analyser is a kind of laboratory conventional instrument, is widely used in agricultural, environment and chemical field, work Principle is that sample is made to burn in the crystal reaction tube high temperature equipped with catalyst, and the gas for generation of burning is restored by reducing agent, Carbon therein, hydrogen, nitrogen, sulphur are completely converted into detectable gas, complete detection process finally by TCD thermal conductivity detector (TCD).Element The crystal reaction tube of analyzer is reusable, but need to remove the catalyst to fail in it and sample ash content, in reaction tube Loading most substances is reducing agent threadiness copper, it can be oxidized to copper oxide during sample test, and agglomerate.Therefore, Cleaning reaction tube is a cumbersome job, and conventional method is artificial the boring hard copper oxide slowly using hand drill, Time-consuming, laborious, inefficiency is also easy to cause reaction tube broken if firmly uneven.
Summary of the invention
The present invention is to solve tradition cleaning elemental analyser crystal reaction tube in catalyst efficiency it is low, be easily destroyed reaction The problem of pipe, and a kind of elemental analyser reaction tube cleaning plant and its application method are provided.
A kind of elemental analyser reaction tube cleaning plant of the present invention includes pedestal, side fixed plate, upper mounted plate, fixes afterwards Plate, motor fixing plate, motor, drill bit, guide supporting seat, guide rail, sliding block, quartz ampoule fixing sleeve, fixing sleeve handle and activity are useless Magazine;The pedestal, side fixed plate, upper mounted plate and rear fixed plate are encircled into a cuboid operating space, and the motor is solid Between pedestal and side fixed plate, motor is fixed on motor fixing plate fixed board oblique weld, and drill bit is connected on rotor; It is separately installed with guide supporting seat in the side fixed plate and upper mounted plate, is fixed with guide rail on the guide supporting seat, it is described Guide rail is perpendicular with motor fixing plate;Sliding is provided with sliding block on the guide rail, and quartz ampoule fixing sleeve is fixed by screw-clamped On sliding block, fixing sleeve handle is installed below quartz ampoule fixing sleeve, surface is provided with activity waste material box on the base, and living The underface of elemental analyser reaction tube lower end outlet is arranged in dynamic waste material box.
The application method of elemental analyser reaction tube cleaning plant of the present invention is to sequentially include the following steps:
Sliding block on guide rail is moved to highest point, then elemental analyser reaction tube is inserted into the quartz being connected with sliding block It is fixed in pipe fixing sleeve, unclamps sliding block, under the effect of gravity, sliding block drives elemental analyser reaction tube along guide rail nature It falls, until the drill bit being connected on motor withstands elemental analyser reaction tube, then connects motor power, grasp solid Surely it covering handle, opens motor switch, motor drives drill bit to start to rotate, situation is fallen according to catalyst in crystal reaction tube, Fixing sleeve handle is pushed down on, until the catalyst in elemental analyser reaction tube is all cleaned, clears up urging of getting off Agent residue can be fallen into activity waste material box under gravity.
The beneficial effects of the present invention are:
One, the present invention drives drill bit to remove the catalyst copper oxide to agglomerate in crystal reaction tube using motor, removes thorough Bottom, and reaction tube will not be damaged.Catalysis in one crystal reaction tube is removed using the device in the present invention Agent, used time are no more than 2 minutes, compared with traditional artificial sweep-out method, save physical strength, improve work efficiency, and operate Simply.
Two, the present invention drives drilling bit high-speed rotary, thus by elemental analyser crystal reaction tube using motor as power output The copper oxide of middle agglomeration slowly disperses, and realizes that stablizing for crystal reaction tube is moved using guide rail, to control drill bit to anti- The stress size of Ying Guanzhong catalyst, the configuration of the present invention is simple, cost of manufacture is cheap, and maintenance is simple.
Detailed description of the invention
Fig. 1 is a kind of structural schematic diagram of elemental analyser reaction tube cleaning plant.
Specific embodiment
The technical solution of the present invention is not limited to the following list, further includes between each specific embodiment Any combination.
Specific embodiment 1: embodiment is described with reference to Fig. 1, a kind of elemental analyser reaction tube of present embodiment is clear Managing device includes pedestal 1, side fixed plate 2, upper mounted plate 3, rear fixed plate 4, motor fixing plate 5, motor 6, drill bit 7, guide rail branch Support seat 8, guide rail 9, sliding block 10, quartz ampoule fixing sleeve 11, fixing sleeve handle 12 and activity waste material box 13;The pedestal 1, side are fixed Plate 2, upper mounted plate 3 and rear fixed plate 4 are encircled into a cuboid operating space, and 5 oblique weld of motor fixing plate is in base Between seat 1 and side fixed plate 2, motor 6 is fixed on motor fixing plate 5, and drill bit 7 is connected on rotor;The side is fixed It is separately installed with guide supporting seat 8 on plate 2 and upper mounted plate 3, guide rail 9, the guide rail 9 are fixed on the guide supporting seat 8 It is perpendicular with motor fixing plate 5;Sliding is provided with sliding block 10 on the guide rail 8, and quartz ampoule fixing sleeve 11 is fastened by screw clamp It is scheduled on sliding block 10, the lower section of quartz ampoule fixing sleeve 11 is equipped with fixing sleeve handle 12, and it is useless that 1 upper surface of pedestal is provided with activity Magazine 13, and the underface of elemental analyser reaction tube lower end outlet is arranged in activity waste material box 13.
Specific embodiment 2: the present embodiment is different from the first embodiment in that: the pedestal 1 be long 80cm, The rectangle iron plate of wide 60cm, side fixed plate 2 are the rectangle iron plate of long 80cm, width 60cm, and upper mounted plate 3 is long 80cm, width The rectangle iron plate of 60cm, rear fixed plate 4 be the rectangle iron plate of long 80cm, width 60cm, the pedestal 1 and side fixed plate 2 and The bottom surface of rear fixed plate 4 is welded to connect, and fixed plate 3 is welded to connect with the upper surface of side fixed plate 2 and rear fixed plate 4, The side fixed plate 2 and rear fixed plate 4 are welded to connect.Other are same as the specific embodiment one.
Specific embodiment 3: the present embodiment is different from the first and the second embodiment in that: the drill bit 7 is circle Fluted drill, material are M35 high-speed steel, and drill bit 7 is parallel with quartz ampoule fixing sleeve 11, and drill bit 7 is located at quartz ampoule fixing sleeve 11 Middle round position, total length >=crystal reaction tube length of drill bit 7 and rotor, the diameter of the drill bit 7 is 10mm, sword is long 87mm, total length 168mm.Other are the same as one or two specific embodiments.
Specific embodiment 4: unlike one of present embodiment and specific embodiment one to three: 9 material of guide rail Matter is aluminium alloy, and slideway is cylindrical, and the length of guide rail 9 is 50cm.Other are identical as one of specific embodiment one to three.
Specific embodiment 5: unlike one of present embodiment and specific embodiment one to four: the quartz ampoule 11 material of fixing sleeve is soft rubber, cylindrical in shape, lower ending opening, upper end closure, and internal diameter is equal to the outer of elemental analyser reaction tube Diameter, the length of quartz ampoule fixing sleeve 11 are 25cm.Other are identical as one of specific embodiment one to four.
Specific embodiment 6: unlike one of present embodiment and specific embodiment one to five: the motor is solid The angle of plate 4 and pedestal 1 is 45 °.Other are identical as one of specific embodiment one to five.
Specific embodiment 7: unlike one of present embodiment and specific embodiment one to five: the fixing sleeve Handle 12 is vertically set on the middle position of quartz ampoule fixing sleeve 11, and shape is cylinder, diameter 3cm, length 8cm. Other are identical as one of specific embodiment one to five.
Specific embodiment 8: a kind of application method of elemental analyser reaction tube cleaning plant of present embodiment be by with Lower step carries out:
Sliding block 10 on guide rail 9 is moved to highest point, then elemental analyser reaction tube is inserted into and is connected with sliding block 10 Quartz ampoule fixing sleeve 11 in be fixed, unclamp sliding block 10, under the effect of gravity, sliding block 10 drive elemental analyser reaction tube It falls naturally along guide rail 9, until the drill bit 7 being connected on motor 6 withstands elemental analyser reaction tube, then connects motor 6 power supplys grasp fixing sleeve handle 12, open motor 6 and switch, motor 6 drives drill bit 7 to start to rotate, according to quartz reaction Catalyst falls situation in pipe, and fixing sleeve handle is pushed down on, until the catalyst in elemental analyser reaction tube all by It cleans out, clearing up the catalyst residue to get off can fall into activity waste material box 13 under gravity.
Beneficial effects of the present invention are verified by following embodiment:
Embodiment: the application method of elemental analyser reaction tube cleaning plant is to sequentially include the following steps:
Sliding block 10 on guide rail 9 is moved to highest point, then elemental analyser reaction tube is inserted into and is connected with sliding block 10 Quartz ampoule fixing sleeve 11 in be fixed, unclamp sliding block 10, under the effect of gravity, sliding block 10 drive elemental analyser reaction tube It falls naturally along guide rail 9, until the drill bit 7 being connected on motor 6 withstands elemental analyser reaction tube, then connects motor 6 power supplys grasp fixing sleeve handle 12, open motor 6 and switch, motor 6 drives drill bit 7 to start to rotate, according to quartz reaction Catalyst falls situation in pipe, and fixing sleeve handle is pushed down on, until the catalyst in elemental analyser reaction tube all by It cleans out, clearing up the catalyst residue to get off can fall into activity waste material box 13 under gravity.
The present embodiment drives drill bit to remove the catalyst copper oxide to agglomerate in crystal reaction tube using motor, removes thorough Bottom, and reaction tube will not be damaged.Catalysis in one crystal reaction tube is removed using the device in the present invention Agent, used time are no more than 2 minutes, compared with traditional artificial sweep-out method, save physical strength, improve work efficiency, and operate Simply.
The present embodiment drives drilling bit high-speed rotary, thus by elemental analyser crystal reaction tube using motor as power output The copper oxide of middle agglomeration slowly disperses, and realizes that stablizing for crystal reaction tube is moved using guide rail, to control drill bit to anti- The stress size of Ying Guanzhong catalyst, the configuration of the present invention is simple, cost of manufacture is cheap, and maintenance is simple.

Claims (8)

1. a kind of elemental analyser reaction tube cleaning plant, it is characterised in that a kind of elemental analyser reaction tube cleaning plant includes Pedestal (1), upper mounted plate (3), rear fixed plate (4), motor fixing plate (5), motor (6), drill bit (7), is led side fixed plate (2) Rail support base (8), guide rail (9), sliding block (10), quartz ampoule fixing sleeve (11), fixing sleeve handle (12) and activity waste material box (13); The pedestal (1), side fixed plate (2), upper mounted plate (3) and rear fixed plate (4) are encircled into a cuboid operating space, described Between pedestal (1) and side fixed plate (2), motor (6) is fixed on motor fixing plate (5) motor fixing plate (5) oblique weld, Drill bit (7) are connected on rotor;Guide supporting seat is separately installed on the side fixed plate (2) and upper mounted plate (3) (8), it is fixed with guide rail (9) on the guide supporting seat (8), the guide rail (9) and motor fixing plate (5) are perpendicular;It is described to lead Sliding is provided with sliding block (10) on rail (8), and quartz ampoule fixing sleeve (11) is fixed on sliding block (10) by screw-clamped, quartz ampoule Fixing sleeve handle (12) are installed below fixing sleeve (11), are provided with activity waste material box (13) in pedestal (1) upper surface, and is living The underface of elemental analyser reaction tube lower end outlet is arranged in dynamic waste material box (13).
2. a kind of elemental analyser reaction tube cleaning plant according to claim 1, it is characterised in that the pedestal (1) is The rectangle iron plate of long 80cm, width 60cm, side fixed plate (2) are the rectangle iron plate of long 80cm, width 60cm, upper mounted plate (3) For the rectangle iron plate of long 80cm, width 60cm, rear fixed plate (4) is the rectangle iron plate of long 80cm, width 60cm, the pedestal (1) be welded to connect with the bottom surface of side fixed plate (2) and rear fixed plate (4), fixed plate (3) and side fixed plate (2) and after The upper surface of fixed plate (4) is welded to connect, and the side fixed plate (2) and rear fixed plate (4) are welded to connect.
3. a kind of elemental analyser reaction tube cleaning plant according to claim 1, it is characterised in that the drill bit (7) is Round fluted drill, material are M35 high-speed steel, and drill bit (7) is parallel with quartz ampoule fixing sleeve (11), and drill bit (7) is located at quartz ampoule The middle round position of fixing sleeve (11), total length >=crystal reaction tube length of drill bit (7) and rotor, the drill bit (7) Diameter be 10mm, the long 87mm of sword, total length 168mm.
4. a kind of elemental analyser reaction tube cleaning plant according to claim 1, it is characterised in that guide rail (9) material Matter is aluminium alloy, and slideway is cylindrical, and the length of guide rail (9) is 50cm.
5. a kind of elemental analyser reaction tube cleaning plant according to claim 1, it is characterised in that the quartz ampoule is solid Fixed (11) material that covers is soft rubber, cylindrical in shape, lower ending opening, upper end closure, and internal diameter is equal to the outer of elemental analyser reaction tube Diameter, the length of quartz ampoule fixing sleeve (11) are 25cm.
6. a kind of elemental analyser reaction tube cleaning plant according to claim 1, it is characterised in that the motor solid plate It (4) is 45 ° with the angle of pedestal (1).
7. a kind of elemental analyser reaction tube cleaning plant according to claim 1, it is characterised in that the fixing sleeve handle Hand (12) is vertically set on the middle position of quartz ampoule fixing sleeve (11), and shape is cylindrical, diameter 3cm, and length is 8cm。
8. a kind of application method of elemental analyser reaction tube cleaning plant as described in claim 1, it is characterised in that element The application method of analyzer reaction tube cleaning plant is to sequentially include the following steps:
Sliding block (10) on guide rail (9) is moved to highest point, then elemental analyser reaction tube is inserted into and sliding block (10) phase It is fixed, unclamps sliding block (10) in quartz ampoule fixing sleeve (11) even, under the effect of gravity, sliding block (10) drives elemental analysis Instrument reaction tube falls naturally along guide rail (9), until elemental analyser is reacted tube top by the drill bit (7) being connected on motor (6) Firmly, motor (6) power supply is then connected, is grasped fixing sleeve handle (12), motor (6) switch is opened, motor (6) drives drill bit (7) start to rotate, situation is fallen according to catalyst in crystal reaction tube, fixing sleeve handle pushed down on, until element point Catalyst in analyzer reaction tube is all cleaned, and work can be fallen under gravity by clearing up the catalyst residue to get off In dynamic waste material box (13).
CN201811570590.6A 2018-12-21 2018-12-21 A kind of elemental analyser reaction tube cleaning plant and its application method Pending CN109500023A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201811570590.6A CN109500023A (en) 2018-12-21 2018-12-21 A kind of elemental analyser reaction tube cleaning plant and its application method

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201811570590.6A CN109500023A (en) 2018-12-21 2018-12-21 A kind of elemental analyser reaction tube cleaning plant and its application method

Publications (1)

Publication Number Publication Date
CN109500023A true CN109500023A (en) 2019-03-22

Family

ID=65754118

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201811570590.6A Pending CN109500023A (en) 2018-12-21 2018-12-21 A kind of elemental analyser reaction tube cleaning plant and its application method

Country Status (1)

Country Link
CN (1) CN109500023A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111088501A (en) * 2019-12-16 2020-05-01 浙江大学 Recovery and reuse method of element analyzer reduction tube

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH078931A (en) * 1993-06-29 1995-01-13 Daido Steel Co Ltd Inner surface grinding device for long tubular member and brush therefor
CN202398585U (en) * 2011-12-30 2012-08-29 中国原子能科学研究院 Descaling tool for swimming pool reactor heat exchangers
CN107252802A (en) * 2017-06-30 2017-10-17 安徽工程大学 A kind of cleaning device for genetic engineering test tube
CN206763547U (en) * 2017-05-23 2017-12-19 丰航 A kind of test tube cleaning sterilizer
CN207042965U (en) * 2017-01-18 2018-02-27 南通沃兰化工有限公司 A kind of test tube Quick cleaning device
CN207119612U (en) * 2017-07-08 2018-03-20 张艺宝 A kind of cleaning device for chemical experiment test tube
CN108421794A (en) * 2018-02-27 2018-08-21 陈鑫利 A kind of clinical laboratory's test tube cleaning device
CN209334393U (en) * 2018-12-21 2019-09-03 中国科学院东北地理与农业生态研究所 A kind of elemental analyser reaction tube cleaning plant

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH078931A (en) * 1993-06-29 1995-01-13 Daido Steel Co Ltd Inner surface grinding device for long tubular member and brush therefor
CN202398585U (en) * 2011-12-30 2012-08-29 中国原子能科学研究院 Descaling tool for swimming pool reactor heat exchangers
CN207042965U (en) * 2017-01-18 2018-02-27 南通沃兰化工有限公司 A kind of test tube Quick cleaning device
CN206763547U (en) * 2017-05-23 2017-12-19 丰航 A kind of test tube cleaning sterilizer
CN107252802A (en) * 2017-06-30 2017-10-17 安徽工程大学 A kind of cleaning device for genetic engineering test tube
CN207119612U (en) * 2017-07-08 2018-03-20 张艺宝 A kind of cleaning device for chemical experiment test tube
CN108421794A (en) * 2018-02-27 2018-08-21 陈鑫利 A kind of clinical laboratory's test tube cleaning device
CN209334393U (en) * 2018-12-21 2019-09-03 中国科学院东北地理与农业生态研究所 A kind of elemental analyser reaction tube cleaning plant

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111088501A (en) * 2019-12-16 2020-05-01 浙江大学 Recovery and reuse method of element analyzer reduction tube

Similar Documents

Publication Publication Date Title
CN209334393U (en) A kind of elemental analyser reaction tube cleaning plant
CN107290454B (en) Portable soil remediation polycyclic aromatic hydrocarbon's quick detection device
CN110044915B (en) Detection device for steel pipe cracks
CN109500023A (en) A kind of elemental analyser reaction tube cleaning plant and its application method
CN203405469U (en) Full automatic immunization analyzer
CN209349208U (en) A kind of elemental analyser crystal reaction tube cleaner
CN209043727U (en) The cleaning plant of concrete test block electric bending testing machine
CN109482585A (en) A kind of elemental analyser crystal reaction tube cleaner and its application method
CN209085999U (en) Sediment sampling drilling tool
CN201413257Y (en) Device integrating substrate sludge sampling with testing
CN101196501A (en) Gas analyzer with automatic sample feeding mechanism
CN209446361U (en) Device shakes with efficient blood is mixed in a kind of clinical laboratory
CN211802893U (en) Crucible cleaning device
CN209400517U (en) Portable flocculating setting degree analyzer
CN203881562U (en) Pathology material-taking device
CN219455501U (en) Automatic tobacco sampling device
CN216433747U (en) Damaged house floor compressive property detecting instrument
CN201470405U (en) Crucible for an industrial analyzer
CN221078560U (en) Steel structure ultrasonic probe operating device
CN203582434U (en) decapping device for vacuum blood collection tubes
CN217605861U (en) Low-temperature test device
CN215458234U (en) Sampling and censorship device for oncology department
CN215179912U (en) Power plant pressure vessel head nondestructive test device
CN216207785U (en) Oil sampling device of large power transformer
CN220418871U (en) Sampling clamping device of coal chemical examination equipment

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
WD01 Invention patent application deemed withdrawn after publication

Application publication date: 20190322

WD01 Invention patent application deemed withdrawn after publication