CN1094748A - A kind of pasty lubricant and method for making - Google Patents
A kind of pasty lubricant and method for making Download PDFInfo
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- CN1094748A CN1094748A CN 93111099 CN93111099A CN1094748A CN 1094748 A CN1094748 A CN 1094748A CN 93111099 CN93111099 CN 93111099 CN 93111099 A CN93111099 A CN 93111099A CN 1094748 A CN1094748 A CN 1094748A
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Abstract
A kind of pasty lubricant and method for making, lubricant of the present invention is a raw material with oil foot etc., behind chemical reaction, adding the multiple additives stirring again forms, have that good lubricity and tack, cost are low, save energy, nontoxic, pollution-free, easy to use, applied range, be applicable to the cold-drawn processing of plain carbon stool, low alloy steel, stainless steel and non-ferrous metal etc.
Description
The invention belongs to lubricating composition, relate to a kind of pasty lubricant and method for making that is suitable for cold group of processing of metal.
At present, in cold group of course of processing of metal, mostly adopt lubricants such as wire drawing powder, machine oil, but wire drawing powder, machine oil in use exist dust and grunge pollution, shortcomings such as poor lubricity.
The object of the present invention is to provide a kind of pollution-free, cost is low, lubricity good, the pasty lubricant of applied range and method for making.
The object of the present invention is achieved like this:
A kind of pasty lubricant is made up of following component:
Oil foot 90-120 part rosin 2-6 part
Caustic soda 5-20 part borax 3-7 part
Tripoly phosphate sodium STPP 1-5 part slaked lime 0-50 part
Tai-Ace S 150 0.1-1 part carboxymethyl cellulose 0-0.5 part
Talcum powder 0-50 part Graphite Powder 99 1-5 part
Molybdenumdisulphide 1-5 part calcium mahogany sulfonate 0-0.2 part
Pamorusa oil 0-0.01 part zinc dialkyl dithiophosphate 0-1 part
Trolamine 0-10 part
Tricresyl phosphate (2,3 two chloropropyl) ester 0-3 part
The preparation method of this pasty lubricant is achieved in that
1, the oil foot with said ratio joined in the reactor that has agitator, under agitation is warming up to 40-60 ℃, adds the Tai-Ace S 150 of said ratio then, in vacuum (0.05MPa) under the state deodorization and dehydration 2-3 hour;
2, the caustic soda of above-mentioned formula ratio is made into the alkaline solution that concentration is 20-50% after, add in the reactor earlier and carry out neutralization reaction, when the material pH value reaches 7-8 in the still, after being warming up to 60-100 ℃, add rosin and stirred 10-30 minute, continue to add alkaline solution then and carry out saponification reaction, keep pH value between 9-11, total saponification reaction time is 4-6 hour, adds borax again, tripoly phosphate sodium STPP is put into dispenser after stirring;
When 3, the material of dispenser being cooled to 30-50 ℃, after adding even stirrings such as slaked lime, talcum powder, Graphite Powder 99, molybdenumdisulphide, pamorusa oil, carboxymethyl cellulose, the horizontal sour calcium of oil, zinc dialkyl dithiophosphate, trolamine, tricresyl phosphate (2,3 two chloropropyl) ester again, the discharging packing is finished product.
Pasty lubricant of the present invention has following advantage:
(1) improve environment, thoroughly eliminate dust pollution or grunge pollution;
(2) lubricity is good, and surface smoothness can improve the 0.5-1 level;
(3) save energy is with the wire drawing powder comparison 15-20% that can economize on electricity;
(4) tack is good, leaves lubricant film for cold forging after cold group;
(5) applied range is applicable to cold group of processing of plain carbon stool, low alloy steel, stainless steel and non-ferrous metal.
Example 1: a kind of component that is used for plain carbon stool vertical pulling (without pickling) pasty lubricant is composed as follows:
9 parts in 100 parts of caustic soda of soya-bean oil sludge
4 parts of 5 parts of boraxs of rosin
0.1 part in 2 parts of Tai-Ace S 150 of tripoly phosphate sodium STPP
30 parts of 20 parts of talcum powder of slaked lime
0.1 part of 2 parts of calcium mahogany sulfonate of Graphite Powder 99
0.01 part of pamorusa oil
The preparation method of this pasty lubricant is achieved in that
(1), the soya-bean oil sludge of above-mentioned prescription added have in the reactor of agitator, under agitation be warming up to 40-60 ℃, add the Tai-Ace S 150 of said ratio then, at vacuum (0.05MP) deodorization and dehydration 2 hours under the state;
(2), the caustic soda of above-mentioned formula ratio being made into concentration is behind 50% the alkaline solution, carry out neutralization reaction a small amount of earlier the adding in the reactor, when the material pH value reaches 7 in the still, after being warming up to 60-100 ℃, adding rosin stirred 30 minutes, continue to add alkaline solution then and carry out saponification reaction, total saponification reaction time is 4 hours.Add borax again, tripoly phosphate sodium STPP is put into dispenser after stirring;
(3), when material in the dispenser is cooled to 50 ℃, add slaked lime, talcum powder, Graphite Powder 99, calcium mahogany sulfonate, pamorusa oil, stirring to be packaged as finished product.
Example 2, it is a kind of that to be used for low alloy steel component of pasty lubricant of cold group after pickling composed as follows:
10 parts in 100 parts of caustic soda of soya-bean oil sludge
2 parts of 0.3 part of rosin of Tai-Ace S 150
1 part of 5 parts of tripoly phosphate sodium STPP of borax
0.5 part of 10 parts of carboxymethyl cellulose of slaked lime
5 parts of 0.5 part of trolamines of Graphite Powder 99
20 parts of 0.01 part of talcum powder of pamorusa oil
Example 3: a kind of component of the pasty lubricant that is used for cold group of carbon steel seamless tube (behind phosphate coat) is composed as follows:
3 parts in 100 parts of caustic soda of soya-bean oil sludge
5 parts of 5 parts of boraxs of rosin
0.3 part of 3 parts of carboxymethyl cellulose of tripoly phosphate sodium STPP
0.1 part in 0.01 part of Tai-Ace S 150 of pamorusa oil
Claims (1)
1, a kind of pasty lubricant that is used for cold group of processing of metal is characterized in that it is made up of following component:
Oil foot 90-120 part caustic soda 5-20 part
Rosin 2-6 part borax 3-7 part
Tripoly phosphate sodium STPP 1-5 part slaked lime 0-50 part
Tai-Ace S 150 0.1-1 part carboxymethyl cellulose 0-0.5 part
Talcum powder 0-50 part Graphite Powder 99 1-5 part
Calcium mahogany sulfonate 0-0.2 part molybdenumdisulphide 1-5 part
Zinc dialkyl dithiophosphate 0-1 part trolamine 0-10 part
Tricresyl phosphate (2,3 two chloropropyl) 0-3 part
Its preparation method is characterized in that:
(1), by said ratio oil foot is added and to have in the reactor of agitator, under agitation be warming up to 40-60 ℃, add the Tai-Ace S 150 of said ratio then, reactor was in vacuum (0.05MPa) under the state deodorization and dehydration 2-3 hour;
(2), the caustic soda of above-mentioned formula ratio is made into the alkaline solution that concentration is 20-50% after, add in the reactor earlier and carry out neutralization reaction, when the material pH value reaches 7-8 in the still, after being warming up to 60-100 ℃, adding rosin and stirred 10-30 minute, continue to add alkaline solution then and carry out saponification reaction, keep pH value between 9-11, total saponification reaction time is 4-6 hour, adds borax again, puts into dispenser after tripoly phosphate sodium STPP stirs;
When (3), the material of dispenser being cooled to 30-50 ℃, after adding even stirring such as slaked lime, talcum powder, Graphite Powder 99, molybdenumdisulphide, pamorusa oil, carboxymethyl cellulose, calcium mahogany sulfonate, zinc dialkyl dithiophosphate, trolamine, tricresyl phosphate (2,3 two chloropropyl) fat again, the discharging packing is finished product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 93111099 CN1094748A (en) | 1993-05-06 | 1993-05-06 | A kind of pasty lubricant and method for making |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 93111099 CN1094748A (en) | 1993-05-06 | 1993-05-06 | A kind of pasty lubricant and method for making |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN1094748A true CN1094748A (en) | 1994-11-09 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 93111099 Pending CN1094748A (en) | 1993-05-06 | 1993-05-06 | A kind of pasty lubricant and method for making |
Country Status (1)
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| CN (1) | CN1094748A (en) |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1072563C (en) * | 1997-03-28 | 2001-10-10 | 郄世杰 | Protecting agent for leather belt |
| CN1087025C (en) * | 1999-04-29 | 2002-07-03 | 中国石油化工集团公司 | Preparation method of high dropping point diurea grease lubricant |
| CN100425683C (en) * | 2006-07-27 | 2008-10-15 | 周永宽 | Hot rolling steel pipe expanding top lubricant |
| CN102085562A (en) * | 2009-12-02 | 2011-06-08 | 上海康巴赛特科技发展有限公司 | Mould release agent for spinning and necking and preparation method thereof |
| CN101619256B (en) * | 2009-08-07 | 2012-05-23 | 安庆市中天石油化工有限公司 | Special lubricating grease for main shaft coupling in rolling mill and preparation method thereof |
| CN104449966A (en) * | 2014-11-05 | 2015-03-25 | 吴江华威特种油有限公司 | Wear-resistant lubricating oil and preparation method thereof |
| CN104498154A (en) * | 2015-01-04 | 2015-04-08 | 吴江华威特种油有限公司 | Anti-wear lubricating oil |
-
1993
- 1993-05-06 CN CN 93111099 patent/CN1094748A/en active Pending
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1072563C (en) * | 1997-03-28 | 2001-10-10 | 郄世杰 | Protecting agent for leather belt |
| CN1087025C (en) * | 1999-04-29 | 2002-07-03 | 中国石油化工集团公司 | Preparation method of high dropping point diurea grease lubricant |
| CN100425683C (en) * | 2006-07-27 | 2008-10-15 | 周永宽 | Hot rolling steel pipe expanding top lubricant |
| CN101619256B (en) * | 2009-08-07 | 2012-05-23 | 安庆市中天石油化工有限公司 | Special lubricating grease for main shaft coupling in rolling mill and preparation method thereof |
| CN102085562A (en) * | 2009-12-02 | 2011-06-08 | 上海康巴赛特科技发展有限公司 | Mould release agent for spinning and necking and preparation method thereof |
| CN104449966A (en) * | 2014-11-05 | 2015-03-25 | 吴江华威特种油有限公司 | Wear-resistant lubricating oil and preparation method thereof |
| CN104498154A (en) * | 2015-01-04 | 2015-04-08 | 吴江华威特种油有限公司 | Anti-wear lubricating oil |
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