CN109470632A - A kind of detection and evaluation method of cigarette tipping paper resistance to blocking energy - Google Patents

A kind of detection and evaluation method of cigarette tipping paper resistance to blocking energy Download PDF

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Publication number
CN109470632A
CN109470632A CN201811353758.8A CN201811353758A CN109470632A CN 109470632 A CN109470632 A CN 109470632A CN 201811353758 A CN201811353758 A CN 201811353758A CN 109470632 A CN109470632 A CN 109470632A
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China
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tipping paper
blocking
resistance
cigarette
blocking energy
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CN109470632B (en
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刘文婷
王建新
蔡冰
贾伟萍
程占刚
闫爱华
吴凯
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China Tobacco Hunan Industrial Co Ltd
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China Tobacco Hunan Industrial Co Ltd
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N19/00Investigating materials by mechanical methods
    • G01N19/04Measuring adhesive force between materials, e.g. of sealing tape, of coating

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  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Manufacturing Of Cigar And Cigarette Tobacco (AREA)
  • Cigarettes, Filters, And Manufacturing Of Filters (AREA)

Abstract

The present invention provides the detection and evaluation method of a kind of cigarette tipping paper resistance to blocking energy, its stretching using Texture instrument to speed and fixed height are fixed by pretreatment sample, pass through the peak value of power in record drawing process, to characterize the resistance to blocking energy of cigarette tipping paper, the present invention passes through to the measurement Jing Guo pretreated tipping paper peeling force, pass through the correlation of peeling force and tipping paper resistance to blocking energy, the difference of tipping paper resistance to blocking energy is measured, with the means of quantization to detect and determining that tipping paper resistance to blocking can provide data supporting.

Description

A kind of detection and evaluation method of cigarette tipping paper resistance to blocking energy
Technical field
The present invention relates to cigarette tipping paper detection technique field, the detection of specifically a kind of cigarette tipping paper resistance to blocking energy And evaluation method.
Background technique
Tipping paper refers to the dedicated paper that filter tip and Cigarette tipping get up, and is commonly called as cork paper.In recent years, China tobacco The fast development of industry promotes the promotion of associated joint product and technology, and cigarette tipping paper is as a member important in cigarette Element, there is very big innovation in function and purposes, and cigarette enterprise is no longer limited to simply wrap to the purposes of cigarette tipping paper Dress, the more dicoration of attention cigarette tipping paper, printing aesthetics.As cigarette enterprise pays close attention to cigarette tipping paper decorative performance The raising of degree has more and more cigarette enterprises and selects new mode of printing, printing material, printing technology on new product New feature, bright spot and attraction are provided for Cigarette design.
With the application of new process, while meeting beautiful, other problems are gradually highlighted, since paper surface handles work The diversification of skill complicates, and will appear paper printing face once in a while in cigarette making process link or under improper storage condition There is adhesion phenomenon.The experience of consumer of this phenomena impair increases enterprise's loss, affects brand value.Therefore exist Before manufacture and intermediate links, it can establish for the resistance to blocking of cigarette tipping paper and a set of operate quantifiable detection method pair The loss of manufacturing process is reduced, improves product quality, it is very necessary for meeting consumer demand.And existing national standard, rower Still locate blank in evaluation cigarette tipping paper resistance to blocking energy this respect, lacks detection means and corresponding evaluation method.Texture instrument can The position changed over time with accurate test sample and weight to provide the physical property characteristic of sample, provide digitization as a result, but It yet there are no relevant report using the method for instrumental test cigarette tipping paper resistance to blocking energy.
Summary of the invention
It is an object of the present invention to provide a kind of cigarette in the blank of resistance to blocking energy context of detection for cigarette tipping paper With the detection and evaluation method of tipping paper resistance to blocking energy.
In order to realize the goal of the invention, a kind of the taken following technical scheme of the present invention: cigarette tipping paper resistance to blocking energy Detection and evaluation method, the stretching of speed and fixed height is fixed to by pretreatment sample using Texture instrument, leads to The peak value of power in overwriting drawing process, to characterize the resistance to blocking energy of cigarette tipping paper, the specific steps of the method are as follows:
(1) tipping paper to be measured is carried out to no less than 24 hours flat under the conditions of 20~30 DEG C of temperature, humidity 55~65% Weighing apparatus, guarantees that all sample preparation original states are consistent;
(2) tipping paper for cutting 24 centimeter lengths is pre-processed, and sampling should not take outermost layer 3 to enclose pattern, and pattern is carried out Fold folds back and forth, and folding times 11~21 times, it is ensured that folding times are odd number, fold the pattern of completion, and two sides is all non-print Brush finish outwardly, facilitates the fixation of sample preparation;Folding times are very few, and the peeling force between paper is too small, and instrument can not be read or data deviation It is excessive;Folding times are excessive, are unfavorable for the processing of pattern, can also exceed the altitude range of instrument;
(3) above-mentioned pattern is placed on to the metal plate of glass plate of two pieces of areas greater than 100mm*100mm or smooth surface Between material, 1000g counterweight is placed on top, is integrally put into warmed-up 30 minutes, in the baking oven that 100 DEG C~110 DEG C of temperature, 15~25 Sample is taken out after minute, at room temperature natural cooling;Pattern is placed between smooth plate between ensure that different patterns by Power is uniform, reduces error caused by operating;It gives the certain pressure of sample, temperature and baking time and simulates tipping paper in life The state that may be undergone in production and storage process;
(4) it is separately fixed at what is pre-processed on Texture instrument pedestal and probe to both sides above and below test sample with adhesive tape, probe 10s is gently pressed in test, and pressure is set as 150N, then starts upward uniform motion, and climb is 20cm~40cm, record removing Power;
(5) resist blocking and that results of property is stated: peeling force can be negatively correlated with tipping paper resistance to blocking, and the peeling force measured is got over Big tipping paper resistance to blocking can be lower, and the resistance to blocking energy of tipping paper is characterized with the size mean value of peeling force;
(6) according to the adhesion packet number and number situation in tobacco product heatproof test result early period, to tipping paper resistance to blocking It can be carried out classification, tipping paper resistance to blocking can be carried out classification, be divided into strong, medium, the weak three grades of resistance to blocking energy, by Texture instrument The tipping paper removing force value of measurement is ranked up from low to high, and pair of force value and tipping paper resistance to blocking energy is removed by tipping paper It should be related to, a kind of detection method of quantifiable cigarette tipping paper resistance to blocking energy can be established.
Further, it pops one's head in step (4) and upward uniform motion is started with the rate of 15mm/s.
The present invention is by passing through peeling force and tipping paper resistance to blocking to the measurement Jing Guo pretreated tipping paper peeling force The correlation of energy has measured the difference of tipping paper resistance to blocking energy, with the means of quantization to detect and determining tipping paper resist blocking and that Performance provides data supporting.
Detailed description of the invention
Folding when Fig. 1 is tipping paper pretreatment in the detection and evaluation method of cigarette tipping paper resistance to blocking energy of the present invention Effect diagram.
Specific embodiment
The temperature environment that the present invention is likely encountered during production or storage by simulating cigarette carries out tipping paper pre- Processing gives the stretching time and height of test sample setting using Texture instrument, by stretching, when measurement stretches fixed height Maximum pull value, pulling force is bigger, and resistance to blocking can be poorer, with this come to cigarette tipping paper resistance to blocking can be carried out detection and comment Valence.
Below in conjunction with specific embodiment, the technical solution in the present invention is clearly and completely described.
Embodiment 1
A kind of detection and evaluation method of cigarette tipping paper resistance to blocking energy, include the following steps:
(1) tipping paper to be measured is carried out to 24 hours balances under the conditions of 25 DEG C of temperature, humidity 65%;
(2) tipping paper for cutting 24 centimeter lengths is pre-processed, sampling should not take outermost layer 3 enclose pattern, by pattern according to The mode of Fig. 1 is turned down folding back and forth, and folding times are 11 times, takes 5 groups of samples altogether;
(3) by above-mentioned single pattern be placed on two pieces of 100mm*100mm glass plate or smooth surface sheet metal it Between, 1000g counterweight is placed on top, is integrally put into warmed-up 30 minutes, in the baking oven that 100 DEG C of temperature, is taken out sample after twenty minutes, Natural cooling at room temperature;
(4) it is separately fixed at what is pre-processed on Texture instrument pedestal and probe to both sides above and below test sample with adhesive tape, probe 10s is gently pressed in test;
The location parameter of Texture instrument is set are as follows:
Pressure setting: 150N;
Extrusion time: 10s;
Push the probe rate of climb: 15mm/s;
Push probe lifting height: 20cm.
The calculating of peeling force: 5 groups are waited for test sample, remove a maximum value and a minimum value, and remaining 3 peeling forces are averaged It is worth the peeling force as the sample.
Embodiment 2
A kind of detection and evaluation method of cigarette tipping paper resistance to blocking energy, include the following steps:
(1) tipping paper to be measured is carried out to 48 hours balances under the conditions of 30 DEG C of temperature, humidity 60%;
(2) tipping paper for cutting 24 centimeter lengths is pre-processed, sampling should not take outermost layer 3 enclose pattern, by pattern according to The mode of Fig. 1 is turned down folding back and forth, and folding times are 9 times, takes 5 groups of samples altogether;
(3) by above-mentioned single pattern be placed on two pieces of 100mm*100mm glass plate or smooth surface sheet metal it Between, 1000g counterweight is placed on top, is integrally put into warmed-up 30 minutes, in the baking oven that 105 DEG C of temperature, is taken out sample after 25 minutes, Natural cooling at room temperature;
(4) it is separately fixed at what is pre-processed on Texture instrument pedestal and probe to both sides above and below test sample with adhesive tape, probe 10s is gently pressed in test;
The location parameter of Texture instrument is set are as follows:
Pressure setting: 150N;
Extrusion time: 10s;
Push the probe rate of climb: 15mm/s;
Push probe lifting height: 20cm.
The calculating of peeling force: 5 groups are waited for test sample, remove a maximum value and a minimum value, and remaining 3 peeling forces are averaged It is worth the peeling force as the sample.
According to the Texture instrument parameter of setting, the peeling force of ten kinds of cigarette tipping papers, and and finished product are measured according to above-mentioned steps Cigarette heatproof test adhesion situation compares, and the results are shown in Table 1:
Table 1
It can be seen that finished product cigarette adhesion situation is similar, and cigarette tipping paper peeling force difference is smaller by upper table;Finished product Cigarette adhesion situation difference is big, and cigarette tipping paper peeling force difference is obvious, therefore method described in the present invention can be used as cigarette use The detection method of tipping paper resistance to blocking energy.
The above description is merely a specific embodiment, but scope of protection of the present invention is not limited thereto, any Belong to those skilled in the art in the technical scope disclosed by the present invention, any changes or substitutions that can be easily thought of, all answers It is included within the scope of the present invention.

Claims (2)

1. a kind of detection and evaluation method of cigarette tipping paper resistance to blocking energy, it is characterised in that: it is using Texture instrument to process The stretching of speed and fixed height is fixed in pretreatment sample, by the peak value of power in record drawing process, uses to characterize cigarette The resistance to blocking energy of tipping paper, the specific steps of the method are as follows:
(1) tipping paper to be measured is carried out to no less than 24 hours balances under the conditions of 20~30 DEG C of temperature, humidity 55~65%, is protected It is consistent to demonstrate,prove all sample preparation original states;
(2) tipping paper for cutting 24 centimeter lengths is pre-processed, and sampling should not take outermost layer 3 to enclose pattern, and pattern is carried out back and forth Fold folds, and folding times 11~21 times, it is ensured that folding times are odd number, fold the pattern of completion, and two sides is all non-printed side Outwardly;
(3) by above-mentioned pattern be placed on two pieces of areas greater than 100mm*100mm glass plate or smooth surface sheet metal it Between, 1000g counterweight is placed on top, is integrally put into warmed-up 30 minutes, in the baking oven that 100 DEG C~110 DEG C of temperature, 15~25 minutes After take out sample, natural cooling at room temperature;
(4) it is separately fixed at what is pre-processed on Texture instrument pedestal and probe to both sides above and below test sample with adhesive tape, probe test, Light pressure 10s, pressure are set as 150N, then upward uniform motion, and climb is 20cm~40cm, record peeling force;
(5) resist blocking and that results of property is stated: peeling force can be negatively correlated with tipping paper resistance to blocking, and the peeling force measured connects more greatly Filling paper resistance to blocking can be lower, and the resistance to blocking energy of tipping paper is characterized with the size mean value of peeling force;
It (6), can be into tipping paper resistance to blocking according to the adhesion packet number and number situation in tobacco product heatproof test result early period Row classification, tipping paper resistance to blocking can be carried out classification, be divided into strong, medium, the weak three grades of resistance to blocking energy, by instrumental test Tipping paper removing force value be ranked up from low to high, pass through tipping paper remove force value and tipping paper resistance to blocking can corresponding closing System can establish a kind of detection method of quantifiable cigarette tipping paper resistance to blocking energy.
2. the detection and evaluation method of cigarette tipping paper resistance to blocking energy as described in claim 1, it is characterised in that: step (4) probe starts upward uniform motion with the rate of 15mm/s in.
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CN110567872A (en) * 2019-10-10 2019-12-13 湖北淡雅香生物科技股份有限公司 Tension detection device for anti-adhesion degree of tipping paper printing ink
CN111024764A (en) * 2019-12-26 2020-04-17 湛江卷烟包装材料印刷有限公司 Cigarette packet adhesion tester and test method
CN111721702A (en) * 2020-06-22 2020-09-29 云南中烟工业有限责任公司 Method for measuring lip adhesion force of cigarette tipping paper
CN111721700A (en) * 2020-06-22 2020-09-29 云南中烟工业有限责任公司 Method for rapidly detecting whether cigarette tipping paper is adhered to lips
CN111721701A (en) * 2020-06-22 2020-09-29 云南中烟工业有限责任公司 Method for measuring lip adhesion force of cigarette tipping paper
CN112033900A (en) * 2020-10-12 2020-12-04 常德市芙蓉实业发展有限责任公司 Paper adhesion testing method
CN113607639A (en) * 2021-06-30 2021-11-05 安徽集友纸业包装有限公司 Method for testing anti-adhesion performance of tipping paper for taste cigarettes
WO2023065379A1 (en) * 2021-10-19 2023-04-27 云南中烟工业有限责任公司 Device for testing adhesion resistance of tipping paper for cigarettes and use method therefor

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JP2006153533A (en) * 2004-11-26 2006-06-15 Katayama Chem Works Co Ltd Analysis method of adhesive adhering to paper or pulp product, and adhesion prevention method of adhesive
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Publication number Priority date Publication date Assignee Title
CN110567872A (en) * 2019-10-10 2019-12-13 湖北淡雅香生物科技股份有限公司 Tension detection device for anti-adhesion degree of tipping paper printing ink
CN111024764A (en) * 2019-12-26 2020-04-17 湛江卷烟包装材料印刷有限公司 Cigarette packet adhesion tester and test method
CN111721702B (en) * 2020-06-22 2022-04-01 云南中烟工业有限责任公司 Method for measuring lip adhesion force of cigarette tipping paper
CN111721700A (en) * 2020-06-22 2020-09-29 云南中烟工业有限责任公司 Method for rapidly detecting whether cigarette tipping paper is adhered to lips
CN111721701A (en) * 2020-06-22 2020-09-29 云南中烟工业有限责任公司 Method for measuring lip adhesion force of cigarette tipping paper
CN111721701B (en) * 2020-06-22 2022-04-01 云南中烟工业有限责任公司 Method for measuring lip adhesion force of cigarette tipping paper
CN111721700B (en) * 2020-06-22 2022-04-01 云南中烟工业有限责任公司 Method for rapidly detecting whether cigarette tipping paper is adhered to lips
CN111721702A (en) * 2020-06-22 2020-09-29 云南中烟工业有限责任公司 Method for measuring lip adhesion force of cigarette tipping paper
CN112033900A (en) * 2020-10-12 2020-12-04 常德市芙蓉实业发展有限责任公司 Paper adhesion testing method
CN113607639A (en) * 2021-06-30 2021-11-05 安徽集友纸业包装有限公司 Method for testing anti-adhesion performance of tipping paper for taste cigarettes
WO2023065379A1 (en) * 2021-10-19 2023-04-27 云南中烟工业有限责任公司 Device for testing adhesion resistance of tipping paper for cigarettes and use method therefor
KR20230058005A (en) * 2021-10-19 2023-05-02 차이나 타바코 윈난 인더스트리얼 컴퍼니 리미티드 Tobacco tipping paper anti-adhesion test device and method of use
KR102573418B1 (en) 2021-10-19 2023-09-01 차이나 타바코 윈난 인더스트리얼 컴퍼니 리미티드 Tobacco tipping paper anti-adhesion test device and method of use
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