CN109433403A - A kind of v-ti magnetite tailing recycling titanium separation method - Google Patents
A kind of v-ti magnetite tailing recycling titanium separation method Download PDFInfo
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- CN109433403A CN109433403A CN201811287839.2A CN201811287839A CN109433403A CN 109433403 A CN109433403 A CN 109433403A CN 201811287839 A CN201811287839 A CN 201811287839A CN 109433403 A CN109433403 A CN 109433403A
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- tailing
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B03—SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
- B03B—SEPARATING SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS
- B03B7/00—Combinations of wet processes or apparatus with other processes or apparatus, e.g. for dressing ores or garbage
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B03—SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
- B03B—SEPARATING SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS
- B03B9/00—General arrangement of separating plant, e.g. flow sheets
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Abstract
The invention discloses a kind of v-ti magnetite tailing recycling titanium separation methods, process is few, it is easy to operate, it is not necessary that slurry concentrating can be directly entered production, hardly change the mechanics index of physics such as tailings granularity, bulk density, internal friction angle, cohesive strength, and tailing pulp density remains unchanged after selecting again, and Tailings Dam operational safety is protected.V-ti magnetite tailing can be recycled by titanium separation method of the present invention, then the titanium chats taste obtained after selecting is significantly improved compared with original debris, is taken full advantage of natural resources, while reducing pollution of the tailing to environment, is turned waste into wealth.
Description
Technical field
The present invention relates to titanium separation method fields, more particularly to v-ti magnetite tailing recycling titanium separation method.
Background technique
China v-ti magnetite mineral deposit is widely distributed, rich reserves, and the third position of the national iron ore of reserves and yield residence has been visited
98.3 hundred million tons of bright reserves, prospective reserves are mainly distributed on Panxi, Sichuan (Panzhihua-Xichang) area, Hebei up to 30,000,000,000 tons or more
Chengde area, Hanzhong Area of Shaanxi, Hubei Yun county sun, Xiangyang area, Shandong Linyi, Xingning of Guangdong Province and Shanxi Dai County, Chaoyang
Equal areas.Wherein, Pan Xi (Panzhihua-Xichang) area is the Main Metallogenic band of China's vanadium titano-magnetite, and similar in the world
One of the important producing region in mineral deposit, north and south are about 300km, have verified at large-scale, oversized mineral deposit 7, at medium-sized mineral deposit 6.Navajoite money
Source is more, total reserves V2O525960000 tons, occupy the 3rd, the world.Navajoite mainly originate in magma lithotype vanadium titano-magnetite bed it
In, as associated minerals output.Navajoite is mainly Cambrian Black Shale-type navajoite as independent deposit.Navajoite is distributed more widely,
There are proved reserves in 19 provinces (area), Sichuan vanadium reserves rank first in the whole country, and account for the 49% of gross reserves；Hunan, Anhui, Guangxi, lake
North, Shandong, Gansu etc. save (area) and take second place.Vanadium titano-magnetite is with being distributed mainly on Sichuan-Xichang Region and Chengde
Area, Black Shale-type navajoite are distributed mainly on Hunan, Hubei Province, Anhui, one band of Jiangxi.
Vanadium titano-magnetite rock mass is divided into basic rock (gabbro) type and basic-ultrabasic rock (gabbro-pyroxenite-brightness
Rock) type two major classes, the important sources of iron, and the Multicomponents such as the vanadium of association, titanium, chromium, cobalt, nickel, platinum family and scandium are not only, are had
There is very high comprehensive utilization value.
Titanium is a kind of rare metal, it, which exists, in nature disperses and be difficult to extract, it has many excellent performances.Liquid
State titanium can almost dissolve all metals, therefore can form alloy with various metals.It is tough and tensile that titanium steel obtained in steel is added in titanium
And aircraft people more than 100 than the aircraft overloading passenger that same weight is made in other metals are made in high resilience, titanium alloy.It is manufactured latent
Ship, can anti-seawater corrosion and deep layer pressure, submerged depth than stainless steel submarine increase by 80%.Meanwhile titanium is nonmagnetic,
It will not be found that there is good anti-monitoring effect by submarine mine.Titanium also has " one's own object " property.In human body, secretion can be resisted
Corrosion and nontoxic, any method for disinfection is all adapted to.Therefore it is widely used in medical instrument processed, artificial femoral articulation processed, knee close
Section, shoulder joint, the side of body joint, cranium, active heart valve, skeletal fixation folder.When new meat fiber ring packet is on these " titanium bones "
When, these titanium bones begin to maintain the normal activity of human body.
And in actual industrial production, when dressing plant's concentrate selection, is poor to the rate of recovery of ilmenite concentrate, and there are still have titanium in tailing
Concentrate is not selected, as Tailings Slurry is discharged into Tailings Dam.And ore belongs to non-renewable resources, can increasingly reduce with exploitation, such as
Fruit more fully becomes the unique channel solved the problems, such as using existing resource.
Summary of the invention
The object of the present invention is to provide a kind of v-ti magnetite tailing recycling titanium separation methods, can be by v-ti magnetite tailing again
Titanium is selected in recycling, makes full use of the natural resources.
In order to solve the above technical problems, one technical scheme adopted by the invention is that:
A kind of v-ti magnetite tailing recycling titanium separation method is provided, including the following steps:
(1) v-ti magnetite tailing is subjected to progress high intensity magnetic separation after weak magnetic removes iron and obtains high intensity magnetic mineral；
(2) high intensity magnetic mineral be dehydrated after gravity treatment roughing, gravity treatment are selected up to titanium chats.
The iron tailings of low-grade vanadium titano is the vanadium titano-magnetite tailing by being conventionally treated in this field.
Further, it is 2300~3000Gs that the weak magnetic, which removes the field strength of iron,.
Further, the background lectromagnetism field of the high intensity magnetic separation is 4000~10000Gs.
Further, it is 2500~2800Gs that the weak magnetic, which removes the field strength of iron,.
Further, the field strength of the high intensity magnetic separation is 5500~6500Gs.
Further, the v-ti magnetite tailing includes coarse fraction mineral and fine-grained minerals.
It can be ability that the v-ti magnetite tailing, which is classified as raw material coarse fraction mineral aggregate and the method for raw ore fine fraction mineral aggregate,
Common method in domain requires as long as raw ore coarse fraction mineral aggregate and raw ore fine fraction mineral aggregate is made to meet recycling.Such as it is logical
It crosses inclined plate concentration classification case classification and obtains raw ore coarse fraction mineral aggregate and raw ore fine fraction mineral aggregate.
Further, it when the v-ti magnetite tailing is coarse fraction mineral, is first carried out every Slag treatment before weak magnetic is except iron.
Further, the gravity treatment is using one or more progress in spiral chute, spiral concentrator and shaking table.
In one embodiment of the invention, the gravity treatment is carried out using spiral chute.
Further, the iron tailings of low-grade vanadium titano contains TiO2Grade is 3.0~12.0%.
The beneficial effects of the present invention are:
(1) titanium separation method process of the present invention is few, easy to operate, then is not necessarily to slurry concentrating can be directly entered production before selecting, then
Selecting technique is that magnetic separation aggravates choosing, hardly changes the mechanics index of physics such as tailings granularity, bulk density, internal friction angle, cohesive strength, and
Tailing pulp density remains unchanged after selecting again, consistent with the tailing pulp density of former v-ti magnetite Tailings Dam, therefore tailings is not present
Inconsistent situation is designed with former, Tailings Dam operational safety can be protected.
(2) v-ti magnetite tailing can be recycled by titanium separation method of the present invention, then the titanium chats TiO obtained after selecting2Product
Position is significantly improved compared with original debris, is taken full advantage of natural resources, while reducing pollution of the tailing to environment, is turned waste into wealth.
Specific embodiment
Technical solution of the present invention is clearly and completely described below, it is clear that described embodiment is the present invention one
Section Example, instead of all the embodiments.Based on the embodiments of the present invention, those of ordinary skill in the art are not doing
Every other embodiment obtained under the premise of creative work out, shall fall within the protection scope of the present invention.
Embodiment 1
(1) mineral for the v-ti magnetite tailing for being 40% by pulp density carry out one by half adverse current type cylinder magnetic separator of wet type
Secondary to remove iron, the field strength of iron removal by magnetic separation is 2300Gs, then will obtain strong magnetic essence except the tailing after iron carries out High gradient high intensity magnetic separation again
Mine, the background lectromagnetism field of High gradient high intensity magnetic separation are 7000Gs.
(2) step (1) resulting high intensity magnetic mineral is entered into spiral chute roughing, then the concentrate of spiral chute roughing is given to
Spiral chute is selected.
(3) titanium chats, the titanium chats is made in the wet feed by step (2) spiral chute after selected after high-frequency dewatering screen is dehydrated
TiO2Grade is 18%, then the tailing pulp density after selecting still is 40%.
Embodiment 2
(1) fine-grained minerals for the v-ti magnetite tailing for being 40% by pulp density pass through half adverse current type cylinder magnetic separator of wet type
It carries out once removing iron, the field strength of iron removal by magnetic separation is 3000Gs, then will be obtained except the tailing after iron carries out High gradient high intensity magnetic separation again
High intensity magnetic mineral, the background lectromagnetism field of High gradient high intensity magnetic separation are 10000Gs.
(2) step (1) resulting high intensity magnetic mineral is entered into spiral chute roughing, then the concentrate of spiral chute roughing is given to
Spiral chute is selected.
(3) particulate titanium chats is made in the wet feed by step (2) spiral chute after selected after high-frequency dewatering screen is dehydrated, this is thin
Grain titanium chats grade is 17%, then the tailing pulp density after selecting still is 40%.
Embodiment 3
(1) the coarse fraction mineral for the v-ti magnetite tailing for being 40% by pulp density are carried out every Slag treatment, then pass through half adverse current of wet type
The progress of type cylinder magnetic separator once removes iron, and the field strength of iron removal by magnetic separation is 2300Gs, then again will be strong except the tailing progress after iron
Magnetic separation obtains high intensity magnetic mineral, and the field strength of high intensity magnetic separation is 4000Gs.
(2) step (1) resulting high intensity magnetic mineral is entered into spiral chute roughing, then the concentrate of spiral chute roughing is given to
Spiral chute is selected.
(3) particulate titanium chats is made in the wet feed by step (2) spiral chute after selected after high-frequency dewatering screen is dehydrated, this is thin
Grain titanium chats grade is 18%, then the tailing pulp density after selecting still is 40%.
Embodiment 4
(1) the coarse fraction mineral for the v-ti magnetite tailing for being 40% by pulp density are carried out every Slag treatment, then pass through half adverse current of wet type
The progress of type cylinder magnetic separator once removes iron, and the field strength of iron removal by magnetic separation is 3000Gs, then again will be high except the tailing progress after iron
Gradient strong magnetic is selected to obtain high intensity magnetic mineral, and the background lectromagnetism field of High gradient high intensity magnetic separation is 10000Gs.
(2) step (1) resulting high intensity magnetic mineral is entered into spiral chute roughing, then the concentrate of spiral chute roughing is given to
Spiral chute is selected.
(3) particulate titanium chats is made in the wet feed by step (2) spiral chute after selected after high-frequency dewatering screen is dehydrated, this is thin
Grain titanium chats grade is 18%, then the tailing pulp density after selecting still is 40%.
Embodiment 5
(1) the coarse fraction mineral for the v-ti magnetite tailing for being 40% by pulp density are carried out every Slag treatment, then pass through half adverse current of wet type
The progress of type cylinder magnetic separator once removes iron, and the field strength of iron removal by magnetic separation is 2500Gs, then again will be strong except the tailing progress after iron
Magnetic separation obtains high intensity magnetic mineral, and the field strength of high intensity magnetic separation is 5500Gs.
(2) step (1) resulting high intensity magnetic mineral is entered into spiral chute roughing, then the concentrate of spiral chute roughing is given to
Spiral chute is selected.
(3) particulate titanium chats is made in the wet feed by step (2) spiral chute after selected after high-frequency dewatering screen is dehydrated, this is thin
Grain titanium chats grade is 19%, then the tailing pulp density after selecting still is 40%.
Embodiment 6
(1) the coarse fraction mineral for the v-ti magnetite tailing for being 40% by pulp density are carried out every Slag treatment, then pass through half adverse current of wet type
The progress of type cylinder magnetic separator once removes iron, and the field strength of iron removal by magnetic separation is 2800Gs, then again will be strong except the tailing progress after iron
Magnetic separation obtains high intensity magnetic mineral, and the field strength of high intensity magnetic separation is 6500Gs.
(2) step (1) resulting high intensity magnetic mineral is entered into spiral chute roughing, then the concentrate of spiral chute roughing is given to
Spiral chute is selected.
(3) particulate titanium chats is made in the wet feed by step (2) spiral chute after selected after high-frequency dewatering screen is dehydrated, this is thin
Grain titanium chats grade is 20%, then the tailing pulp density after selecting still is 40%.
Embodiment 7
(1) the coarse fraction mineral for the v-ti magnetite tailing for being 40% by pulp density are carried out every Slag treatment, then pass through half adverse current of wet type
The progress of type cylinder magnetic separator once removes iron, and the field strength of iron removal by magnetic separation is 2700Gs, then again will be strong except the tailing progress after iron
Magnetic separation obtains high intensity magnetic mineral, and the field strength of high intensity magnetic separation is 6000Gs.
(2) step (1) resulting high intensity magnetic mineral is entered into spiral chute roughing, then the concentrate of spiral chute roughing is given to
Spiral chute is selected.
(3) particulate titanium chats is made in the wet feed by step (2) spiral chute after selected after high-frequency dewatering screen is dehydrated, this is thin
Grain titanium chats grade is 18%, then the tailing pulp density after selecting still is 40%.
Embodiment 8
(1) fine-grained minerals for the v-ti magnetite tailing for being 40% by pulp density pass through half adverse current type cylinder magnetic separator of wet type
It carries out once removing iron, the field strength of iron removal by magnetic separation is 2600Gs, then will obtain strong magnetic essence except the tailing after iron carries out high intensity magnetic separation again
Mine, the field strength of high intensity magnetic separation are 6500Gs.
(2) step (1) resulting high intensity magnetic mineral is entered into spiral chute roughing, then the concentrate of spiral chute roughing is given to
Table concentration.
(3) wet feed after step (2) table concentration is made to particulate titanium chats, the particulate titanium after high-frequency dewatering screen is dehydrated
Chats grade is 15%, then the tailing pulp density after selecting still is 40%.
Embodiment 9
(1) fine-grained minerals for the v-ti magnetite tailing for being 40% by pulp density pass through half adverse current type cylinder magnetic separator of wet type
It carries out once removing iron, the field strength of iron removal by magnetic separation is 2600Gs, then will obtain strong magnetic essence except the tailing after iron carries out high intensity magnetic separation again
Mine, the field strength of high intensity magnetic separation are 6000Gs.
(2) step (1) resulting high intensity magnetic mineral is entered into spiral chute roughing, then the concentrate of spiral chute roughing is given to
Spiral concentrator is selected.
(3) particulate titanium chats is made in the wet feed by step (2) spiral concentrator after selected after high-frequency dewatering screen is dehydrated, should
Particulate titanium chats grade is 17%, then the tailing pulp density after selecting still is 40%.
Embodiment 10
(1) the coarse fraction mineral for the v-ti magnetite tailing for being 40% by pulp density are carried out every Slag treatment, then pass through half adverse current of wet type
The progress of type cylinder magnetic separator once removes iron, and the field strength of iron removal by magnetic separation is 2800Gs, then again will be strong except the tailing progress after iron
Magnetic separation obtains high intensity magnetic mineral, and the field strength of high intensity magnetic separation is 6500Gs.
(2) step (1) resulting high intensity magnetic mineral is entered into spiral chute roughing, then the concentrate of spiral chute roughing is given to
Table concentration.
(3) wet feed after step (2) table concentration is made to particulate titanium chats, the particulate titanium after high-frequency dewatering screen is dehydrated
Chats grade is 15%, then the tailing pulp density after selecting still is 40%.
Embodiment 11
(1) the coarse fraction mineral for the v-ti magnetite tailing for being 40% by pulp density are carried out every Slag treatment, then pass through half adverse current of wet type
The progress of type cylinder magnetic separator once removes iron, and the field strength of iron removal by magnetic separation is 2800Gs, then again will be strong except the tailing progress after iron
Magnetic separation obtains high intensity magnetic mineral, and the field strength of high intensity magnetic separation is 6500Gs.
(2) step (1) resulting high intensity magnetic mineral is entered into spiral chute roughing, then the concentrate of spiral chute roughing is given to
Spiral concentrator is selected.
(3) particulate titanium chats is made in the wet feed by step (2) spiral concentrator after selected after high-frequency dewatering screen is dehydrated, should
Particulate titanium chats grade is 15%, then the tailing pulp density after selecting still is 40%.
Embodiment 12
(1) the coarse fraction mineral for the v-ti magnetite tailing for being 40% by pulp density are carried out every Slag treatment, then pass through half adverse current of wet type
The progress of type cylinder magnetic separator once removes iron, and the field strength of iron removal by magnetic separation is 2800Gs, then again will be strong except the tailing progress after iron
Magnetic separation obtains high intensity magnetic mineral, and the field strength of high intensity magnetic separation is 6500Gs.
(2) step (1) resulting high intensity magnetic mineral is entered into spiral concentrator roughing, then by the concentrate of spiral concentrator roughing
It is selected to be given to spiral chute.
(3) particulate titanium chats is made in the wet feed by step (2) spiral chute after selected after high-frequency dewatering screen is dehydrated, this is thin
Grain titanium chats grade is 14%, then the tailing pulp density after selecting still is 40%.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
A variety of variations, modification, replacement can be carried out to these embodiments without departing from the principles and spirit of the present invention by understanding
And modification, the scope of the present invention is defined by the appended.
Claims (10)
1. a kind of v-ti magnetite tailing recycling titanium separation method, characterized in that it comprises the following steps:
(1) v-ti magnetite tailing is subjected to progress high intensity magnetic separation after weak magnetic removes iron and obtains high intensity magnetic mineral；
(2) high intensity magnetic mineral be dehydrated after gravity treatment roughing, gravity treatment are selected up to titanium chats.
2. the method according to claim 1, wherein the weak magnetic is 2300~3000Gs except the field strength of iron.
3. the method according to claim 1, wherein the background lectromagnetism field of the high intensity magnetic separation is 4000~10000Gs.
4. according to the method described in claim 2, it is characterized in that, the field strength that the weak magnetic removes iron is 2500~2800Gs.
5. according to the method described in claim 3, it is characterized in that, the field strength of the high intensity magnetic separation is 5500~6500Gs.
6. the method according to claim 1, wherein the v-ti magnetite tailing includes coarse fraction mineral and particulate
Grade mineral.
7. according to the method described in claim 6, it is characterized in that, the v-ti magnetite tailing be coarse fraction mineral when, weak
Magnetic is first carried out every Slag treatment before removing iron.
8. the method according to claim 1, wherein the gravity treatment is using spiral chute, spiral concentrator and shakes
One or more progress in bed.
9. according to the method described in claim 8, it is characterized in that, the gravity treatment is carried out using spiral chute.
10. the method according to claim 1, wherein the iron tailings of low-grade vanadium titano contains TiO2Grade is
3.0~12.0%.
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110665634A (en) * | 2019-11-13 | 2020-01-10 | 攀枝花钢城集团米易瑞地矿业有限公司 | Method for selecting titanium from iron ore tailings of extremely poor exterior vanadium titano-magnetite |
| CN111040730A (en) * | 2019-11-15 | 2020-04-21 | 鞍钢集团矿业有限公司 | Brake pad composite friction material and preparation method thereof |
| CN114054199A (en) * | 2021-11-15 | 2022-02-18 | 攀钢集团攀枝花钢铁研究院有限公司 | Method for producing titanium middling by utilizing titanium-selecting tailings |
| GB2616642A (en) * | 2022-03-16 | 2023-09-20 | Butterworth Colin | Oil Sands Tailings Liability, Existance Reduction (OSTLER) |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN110665634A (en) * | 2019-11-13 | 2020-01-10 | 攀枝花钢城集团米易瑞地矿业有限公司 | Method for selecting titanium from iron ore tailings of extremely poor exterior vanadium titano-magnetite |
| CN111040730A (en) * | 2019-11-15 | 2020-04-21 | 鞍钢集团矿业有限公司 | Brake pad composite friction material and preparation method thereof |
| CN111040730B (en) * | 2019-11-15 | 2021-02-26 | 鞍钢集团矿业有限公司 | Brake pad composite friction material and preparation method thereof |
| CN114054199A (en) * | 2021-11-15 | 2022-02-18 | 攀钢集团攀枝花钢铁研究院有限公司 | Method for producing titanium middling by utilizing titanium-selecting tailings |
| GB2616642A (en) * | 2022-03-16 | 2023-09-20 | Butterworth Colin | Oil Sands Tailings Liability, Existance Reduction (OSTLER) |
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