CN109432861A - A kind of novel germanium tetrachloride hydrolysate separator - Google Patents
A kind of novel germanium tetrachloride hydrolysate separator Download PDFInfo
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- CN109432861A CN109432861A CN201811424043.7A CN201811424043A CN109432861A CN 109432861 A CN109432861 A CN 109432861A CN 201811424043 A CN201811424043 A CN 201811424043A CN 109432861 A CN109432861 A CN 109432861A
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- sieve
- liquid
- branch pipe
- germanium tetrachloride
- mesh
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D33/00—Filters with filtering elements which move during the filtering operation
- B01D33/15—Filters with filtering elements which move during the filtering operation with rotary plane filtering surfaces
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D33/00—Filters with filtering elements which move during the filtering operation
- B01D33/70—Filters with filtering elements which move during the filtering operation having feed or discharge devices
- B01D33/72—Filters with filtering elements which move during the filtering operation having feed or discharge devices for feeding
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D33/00—Filters with filtering elements which move during the filtering operation
- B01D33/70—Filters with filtering elements which move during the filtering operation having feed or discharge devices
- B01D33/74—Filters with filtering elements which move during the filtering operation having feed or discharge devices for discharging filtrate
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D33/00—Filters with filtering elements which move during the filtering operation
- B01D33/80—Accessories
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G17/00—Compounds of germanium
- C01G17/02—Germanium dioxide
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
The invention belongs to germanium dioxide production equipment technologies, provide a kind of novel germanium tetrachloride hydrolysate separator, including support frame, liquid-holding bucket and separating mechanism, support frame as described above includes bottom plate, perpendicular branch pipe, oblique branch pipe and mounting sheet, the separating mechanism includes cylinder, motor, rotation axis, first sieve and the second sieve, the inside of the cylinder sets gradually the first groove and the second groove, first sieve and second sieve, which respectively correspond, to be set in first groove and second groove, and the diameter of first sieve is greater than the diameter of second sieve；First mesh is set in first sieve, the second mesh is set in second sieve, and the diameter of first mesh is greater than the diameter of second mesh.A kind of novel germanium tetrachloride hydrolysate separator provided by the invention facilitates following process convenient for separating the germanium dioxide solid of different-grain diameter.
Description
Technical field
The present invention relates to germanium dioxide production equipment technologies, and in particular to a kind of novel germanium tetrachloride hydrolysate point
From device.
Background technique
In the extractive process of germanium or germanium dioxide, it usually needs ultrapure water is added in germanium tetrachloride, reaction is hydrolyzed
And the solid matter of germanium dioxide is obtained, it needs to carry out separating-purifying to hydrolysate after hydrolysis；
It generallys use semi-open strainer in the prior art to separate hydrolysate, due to the generation in germanium dioxide
In the process since the influence of the factors such as stirring, temperature causes hydrolysate partial size different, the separation of the prior art can not will not
Germanium dioxide solid with partial size separates, and causes subsequent handling complicated.
Summary of the invention
For the defects in the prior art, the present invention provides a kind of novel germanium tetrachloride hydrolysate separator, is convenient for
The germanium dioxide solid of different-grain diameter is separated, following process is facilitated.
In order to achieve the above objectives, the present invention adopts the following technical scheme that:
A kind of novel germanium tetrachloride hydrolysate separator, including support frame, liquid-holding bucket and separating mechanism, the support
The top of frame sets gradually the liquid-holding bucket, the separating mechanism from top to bottom, and the liquid-holding bucket is correspondingly arranged in described point
It disembarks the top of structure；
Support frame as described above includes bottom plate, perpendicular branch pipe, oblique branch pipe and mounting sheet, and the perpendicular branch is arranged in the top of the bottom plate
Pipe, there are four the perpendicular branch pipe settings, and the corner of the perpendicular branch pipe and the bottom plate is arranged in a one-to-one correspondence；
The both ends of the oblique branch pipe are separately connected the opposite perpendicular branch pipe, and there are two the oblique branch pipe settings, and described
Oblique branch pipe intersection setting；Bearing is arranged in the top of the oblique branch pipe；The liquid-holding bucket is arranged in the top of the mounting sheet；
The separating mechanism includes cylinder, motor, rotation axis, the first sieve and the second sieve, and the motor is set to
The top of the bottom plate, one end of the rotation axis connect the motor, the other end of the rotation axis through the bearing with
The bottom of the cylinder connects；Fluid openings are arranged in the bottom of the cylinder；
The inside of the cylinder sets gradually the first groove and the second groove, first sieve and second sieve
It respectively corresponds and is set in first groove and second groove, and the diameter of first sieve is greater than second sieve
The diameter of net；
First mesh is set in first sieve, the second mesh, and first mesh are set in second sieve
Diameter be greater than second mesh diameter.
As an improvement technical solution, protective cover is arranged in the top of the liquid-holding bucket, and the protective cover is arcuation structure
Part, and the first in command is arranged in the top of the protective cover.
As an improvement technical solution, the bottom of the liquid-holding bucket is arranged sliding slot, adjusting block is arranged in the sliding slot,
Stretch rod is arranged in one end of the adjusting block, and second handle is arranged in the end of the stretch rod.
As an improvement technical solution, the adjusting block be silicone rubber material component.
As an improvement technical solution, window is checked in the outer wall setting of the liquid-holding bucket, described to check that window is rectangular structure
Part, and the length direction setting for checking liquid-holding bucket described in windowsill.
As an improvement technical solution, the top of first sieve is respectively provided with handle ring, the handle ring setting
There are two, and the handle ring is oppositely arranged.
As an improvement technical solution, the oblique branch pipe top setting receive liquid frame, it is described receive liquid frame intermediate ends
Outlet tube is arranged in setting opening, the lower part for receiving liquid frame, and valve is arranged in the outer wall of the outlet tube.
As an improvement technical solution, the bottom setting of the outlet tube is anti-to slip through the net, and the anti-interior setting of slipping through the net is anti-
Leak hole.
As an improvement technical solution, movable pulley is arranged in the bottom of the bottom plate, and there are four the movable pulley settings,
And the corner of the movable pulley and the bottom plate is arranged in a one-to-one correspondence.
Due to using the technology described above, the invention has the following advantages:
The present invention provides a kind of novel germanium tetrachloride hydrolysate separator, comprising: support frame, liquid-holding bucket and seperator
Structure, the top of support frame as described above sets gradually the liquid-holding bucket, the separating mechanism from top to bottom, and liquid-holding bucket correspondence is set
It is placed in the top of the separating mechanism；Support frame as described above includes bottom plate, erects branch pipe, oblique branch pipe and mounting sheet, the oblique branch pipe
Both ends are separately connected the opposite perpendicular branch pipe, and bearing is arranged in the top of the oblique branch pipe；Institute is arranged in the top of the mounting sheet
State liquid-holding bucket；The separating mechanism includes cylinder, motor, rotation axis, the first sieve and the second sieve, the cylinder it is interior
Portion sets gradually the first groove and the second groove, and first sieve and second sieve respectively correspond and be set to described first
In groove and second groove, and the diameter of first sieve is greater than the diameter of second sieve；First sieve
The first mesh of interior setting, second sieve is interior to be arranged the second mesh, and the diameter of first mesh is greater than second net
The diameter in hole；Based on the above mechanism, it is convenient for separating the germanium dioxide solid of different-grain diameter by the separating mechanism, side
Just following process.
In the present invention, the top of the liquid-holding bucket is arranged protective cover, and the protective cover is arcuation component, and the protective cover
Top be arranged the first in command；Based on the above mechanism, impurity is avoided to enter in the liquid-holding bucket.
In the present invention, sliding slot is arranged in the bottom of the liquid-holding bucket, setting adjusting block in the sliding slot, and the one of the adjusting block
Second handle is arranged in end setting stretch rod, the end of the stretch rod；Based on the above mechanism, the stream of liquid is adjusted according to demand
Amount.
In the present invention, the adjusting block is silicone rubber material component；Based on the above mechanism, sealing effect is good, avoids liquid
It leaks.
In the present invention, window is checked in the setting of the outer wall of the liquid-holding bucket, described to check that window is square member, and described checks window
Length direction along the liquid-holding bucket is arranged；Based on the above mechanism, the liquid-holding bucket internal state is conveniently checked.
In the present invention, the top of first sieve is respectively provided with handle ring, and there are two the handle ring settings, and described mentions
Bracelet is oppositely arranged；It is convenient timely to collect germanium dioxide based on the above mechanism.
In the present invention, liquid frame is received in the top setting of the oblique branch pipe, and opening, the receipts are arranged in the intermediate ends for receiving liquid frame
Outlet tube is arranged in the lower part of liquid frame；Based on the above mechanism, treatment liquid is timely collected.
In the present invention, the bottom setting of the outlet tube is anti-to slip through the net, the anti-interior anti-leak hole of setting of slipping through the net；Based on the above machine
Structure is avoided omitting germanium dioxide, be caused damages.
In the present invention, movable pulley is arranged in the bottom of the bottom plate, and the corner one of the movable pulley and the bottom plate is a pair of
It should be arranged；Based on the above mechanism, position easy to remove to arbitrary is used.
In conclusion a kind of novel germanium tetrachloride hydrolysate separator provided by the invention, by the two of different-grain diameter
Germanium oxide solid is separated, and facilitates following process, while structure is simple and easy to operate, is conducive to promote the use of.
Detailed description of the invention
It, below will be to specific in order to illustrate more clearly of the specific embodiment of the invention or technical solution in the prior art
Embodiment or attached drawing needed to be used in the description of the prior art are briefly described.In all the appended drawings, similar element
Or part is generally identified by similar appended drawing reference.In attached drawing, each element or part might not be drawn according to actual ratio.
Fig. 1 is a kind of novel germanium tetrachloride hydrolysate separator structural schematic diagram；
Fig. 2 is support frame structure diagram；
Fig. 3 is liquid-holding bucket partial structural diagram；
Fig. 4 is to receive liquid mount structure schematic diagram.
In attached drawing, 1, support frame, 11, bottom plate, 12, perpendicular branch pipe, 13, oblique branch pipe, 131, bearing, 14, mounting sheet, 2, Sheng liquid
Bucket, 21, sliding slot, 22, adjusting block, 23, stretch rod, 24, second handle, 25, check window, 3, separating mechanism, 31, cylinder,
311, the first groove, the 312, second groove, 313, fluid openings, 32, motor, 33, rotation axis, the 34, first sieve, 341, first
Mesh, 342, handle ring, the 35, second sieve, the 352, second mesh, 4, protective cover, 41, the first in command, 5, receive liquid frame, 51, open
Mouthful, 52, outlet tube, 53, valve, 54, it is anti-slip through the net, 541, anti-leak hole, 6, movable pulley.
Specific embodiment
Technical solution of the present invention is described in detail below in conjunction with specific embodiment.Following embodiment is only used for more
Add and clearly demonstrate technical solution of the present invention, therefore be only used as example, and not intended to limit the protection scope of the present invention.
As shown in Figs 1-4, the present invention provides a kind of novel germanium tetrachloride hydrolysate separator, including support frame 1, Sheng
Liquid bucket 2 and separating mechanism 3, the top of support frame 1 sets gradually liquid-holding bucket 2, separating mechanism 3 from top to bottom, and liquid-holding bucket 2 is corresponding
It is set to the top of separating mechanism 3；
Support frame 1 includes bottom plate 11, perpendicular branch pipe 12, oblique branch pipe 13 and mounting sheet 14, and perpendicular branch pipe is arranged in the top of bottom plate 11
12, it erects there are four the settings of branch pipe 12, and the corner of perpendicular branch pipe 12 and bottom plate 11 is arranged in a one-to-one correspondence；Perpendicular branch pipe 12 is supported；
Movable pulley 6 is arranged in the bottom of bottom plate 11, and there are four the settings of movable pulley 6, and the corner of movable pulley 6 and bottom plate 11 is one by one
It is correspondingly arranged；It is used by the position easy to remove to arbitrary of movable pulley 6；
The both ends of oblique branch pipe 13 are separately connected opposite perpendicular branch pipe 12, and there are two the oblique settings of branch pipe 13, and tiltedly 13 phase of branch pipe
Hand over setting；Bearing 131 is arranged in the top of oblique branch pipe 13；Liquid-holding bucket 2 is arranged in the top of mounting sheet 14；
Protective cover 4 is arranged in the top of liquid-holding bucket 2, and protective cover 4 is arcuation component, and the first is arranged in the top of protective cover 4
Hand 41；Impurity is avoided to enter in liquid-holding bucket 2, when use directly takes the first in command 41；
Sliding slot 21 is arranged in the bottom of liquid-holding bucket 2, and adjusting block 22 is arranged in sliding slot 21, and stretch rod is arranged in one end of adjusting block 22
23, second handle 24 is arranged in the end of stretch rod 23；The flow for adjusting liquid according to demand, along the outlet of liquid-holding bucket 2 when adjusting
It is stretched, stretch rod 23 moves in 21 along the chute, easy to adjust；
Adjusting block 22 is silicone rubber material component；Sealing effect is good, avoids leaked liquid；The outer wall setting of liquid-holding bucket 2 is looked into
Looking glass 25 checks that window 25 is square member, and checks that window 25 is arranged along the length direction of liquid-holding bucket 2；It conveniently checks in liquid-holding bucket 2
Portion's situation；
Separating mechanism 3 includes that cylinder 31, motor 32, rotation axis 33, the first sieve 34 and the second sieve 35, motor 32 are set
It is placed in the top of bottom plate 11, one end of rotation axis 33 connects motor 32, and the other end of rotation axis 33 runs through bearing 131 and cylinder
31 bottom connection；Fluid openings 313 are arranged in the bottom of cylinder 31；
The inside of cylinder 31 sets gradually the first groove 311 and the second groove 312, the first sieve 34 and the second sieve 35
It respectively corresponds and is set in the first groove 311 and the second groove 312, and the diameter of the first sieve 34 is greater than the straight of the second sieve 35
Diameter；Different diameters is set convenient for successively take the first sieve 34 and the second sieve 35；
First mesh 341 is set in first sieve 34, the second mesh 352, and the first mesh 341 are set in second sieve 35
Diameter be greater than the second mesh 352 diameter；
Isolated process is: the liquid in liquid-holding bucket 2 constantly falls, and motor 32 drives the rotation of rotation axis 33,
The rotation of the drive cylinder 31 of rotation axis 33；The rotation of drive the first sieve 34 and the second sieve 35 of cylinder 31；It rotated
Cheng Zhong, for the germanium dioxide solids retention of major diameter in the first sieve 34, the germanium dioxide solid of minor diameter falls to the second sieve
In net 35；Remaining liquid, which enters, receives collection processing in liquid frame 5；
Liquid frame 5 is received in the top setting of oblique branch pipe 13, is received the intermediate ends setting opening 51 of liquid frame 5, is turned by opening 51
Moving axis 33 passes through；Valve 53 is arranged in the outer wall of outlet tube 52, and outlet tube 52 is arranged in the lower part for receiving liquid frame 5；It is timely to open valve 53
Collection treatment liquid；
The bottom setting of outlet tube 52 is anti-to slip through the net 54, the anti-anti- leak holes 541 of setting in 54 of slipping through the net；It avoids omitting germanium dioxide,
It causes damages；
The top of first sieve 34 is respectively provided with handle ring 342, and there are two the settings of handle ring 342, and handle ring 342 is set relatively
It sets；For the ease of extracting germanium dioxide, it is respectively provided with handle ring 342 on the top of the first sieve 34, structure is simple and easy to operate.
Finally, it should be noted that the above embodiments are only used to illustrate the technical solution of the present invention., rather than its limitations；To the greatest extent
Pipe present invention has been described in detail with reference to the aforementioned embodiments, those skilled in the art should understand that: its according to
So be possible to modify the technical solutions described in the foregoing embodiments, or to some or all of the technical features into
Row equivalent replacement；And these are modified or replaceed, various embodiments of the present invention technology that it does not separate the essence of the corresponding technical solution
The range of scheme should all cover within the scope of the claims and the description of the invention.
Claims (9)
1. a kind of novel germanium tetrachloride hydrolysate separator, it is characterised in that: including support frame, liquid-holding bucket and seperator
Structure, the top of support frame as described above sets gradually the liquid-holding bucket, the separating mechanism from top to bottom, and liquid-holding bucket correspondence is set
It is placed in the top of the separating mechanism；
Support frame as described above includes bottom plate, perpendicular branch pipe, oblique branch pipe and mounting sheet, and the perpendicular branch pipe, institute is arranged in the top of the bottom plate
It states there are four perpendicular branch pipe settings, and the corner of the perpendicular branch pipe and the bottom plate is arranged in a one-to-one correspondence；
The both ends of the oblique branch pipe are separately connected the opposite perpendicular branch pipe, and there are two the oblique branch pipe settings, and the oblique branch
Pipe intersection setting；Bearing is arranged in the top of the oblique branch pipe；The liquid-holding bucket is arranged in the top of the mounting sheet；
The separating mechanism includes cylinder, motor, rotation axis, the first sieve and the second sieve, and the motor is set to described
The top of bottom plate, one end of the rotation axis connect the motor, the other end of the rotation axis through the bearing with it is described
The bottom of cylinder connects；Fluid openings are arranged in the bottom of the cylinder；
The inside of the cylinder sets gradually the first groove and the second groove, first sieve and second sieve difference
It is correspondingly arranged in first groove and second groove, and the diameter of first sieve is greater than second sieve
Diameter；
First mesh is set in first sieve, the second mesh is set in second sieve, and first mesh is straight
Diameter is greater than the diameter of second mesh.
2. a kind of novel germanium tetrachloride hydrolysate separator according to claim 1, it is characterised in that: the Sheng liquid
Protective cover is arranged in the top of bucket, and the protective cover is arcuation component, and the first in command is arranged in the top of the protective cover.
3. a kind of novel germanium tetrachloride hydrolysate separator according to claim 1, it is characterised in that: the Sheng liquid
Sliding slot is arranged in the bottom of bucket, and adjusting block is arranged in the sliding slot, and stretch rod is arranged in one end of the adjusting block, the stretch rod
Second handle is arranged in end.
4. a kind of novel germanium tetrachloride hydrolysate separator according to claim 3, it is characterised in that: the adjusting
Block is silicone rubber material component.
5. a kind of novel germanium tetrachloride hydrolysate separator according to claim 1, it is characterised in that: the Sheng liquid
Window is checked in the outer wall setting of bucket, described to check that window is square member, and the length direction for checking liquid-holding bucket described in windowsill is set
It sets.
6. a kind of novel germanium tetrachloride hydrolysate separator according to claim 1, it is characterised in that: described first
The top of sieve is respectively provided with handle ring, and there are two the handle ring settings, and the handle ring is oppositely arranged.
7. a kind of novel germanium tetrachloride hydrolysate separator according to claim 1, it is characterised in that: the oblique branch
Liquid frame is received in the top setting of pipe, and opening is arranged in the intermediate ends for receiving liquid frame, and outlet tube is arranged in the lower part for receiving liquid frame, described
Valve is arranged in the outer wall of outlet tube.
8. a kind of novel germanium tetrachloride hydrolysate separator according to claim 1, it is characterised in that: the liquid out
The bottom setting of pipe is anti-to slip through the net, the anti-interior anti-leak hole of setting of slipping through the net.
9. a kind of novel germanium tetrachloride hydrolysate separator according to claim 1, it is characterised in that: the bottom plate
Bottom movable pulley is set, there are four movable pulley settings, and the corner of the movable pulley and the bottom plate corresponds and sets
It sets.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811424043.7A CN109432861A (en) | 2018-11-27 | 2018-11-27 | A kind of novel germanium tetrachloride hydrolysate separator |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811424043.7A CN109432861A (en) | 2018-11-27 | 2018-11-27 | A kind of novel germanium tetrachloride hydrolysate separator |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109432861A true CN109432861A (en) | 2019-03-08 |
Family
ID=65555560
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811424043.7A Pending CN109432861A (en) | 2018-11-27 | 2018-11-27 | A kind of novel germanium tetrachloride hydrolysate separator |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109432861A (en) |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN205235520U (en) * | 2015-11-20 | 2016-05-18 | 天津美士邦涂料化工有限公司 | Coating filtering device |
| CN106731076A (en) * | 2015-11-25 | 2017-05-31 | 衡阳恒荣高纯半导体材料有限公司 | A kind of germanium tetrachloride hydrolysate solid-liquid separating machine |
| CN107789881A (en) * | 2017-11-17 | 2018-03-13 | 盱眙县生产力促进中心 | A kind of smart home sewage-treatment plant of replaceable filter screen |
| CN107792684A (en) * | 2017-11-22 | 2018-03-13 | 佛山市因诺维生物科技有限公司 | A kind of feeding mechanism for biomass extraction equipment |
| CN207286856U (en) * | 2017-08-26 | 2018-05-01 | 钟元召 | A kind of pig farm sewage-treatment plant for reducing filtration resistance |
| CN108579178A (en) * | 2018-03-08 | 2018-09-28 | 浙江康豪诺特装饰材料有限公司 | A kind of filter with layered shaping function |
| CN208098212U (en) * | 2017-12-29 | 2018-11-16 | 郑州网知汇信息科技有限公司 | It is a kind of for producing the grinding apparatus of brown fused alumina micropowder |
-
2018
- 2018-11-27 CN CN201811424043.7A patent/CN109432861A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN205235520U (en) * | 2015-11-20 | 2016-05-18 | 天津美士邦涂料化工有限公司 | Coating filtering device |
| CN106731076A (en) * | 2015-11-25 | 2017-05-31 | 衡阳恒荣高纯半导体材料有限公司 | A kind of germanium tetrachloride hydrolysate solid-liquid separating machine |
| CN207286856U (en) * | 2017-08-26 | 2018-05-01 | 钟元召 | A kind of pig farm sewage-treatment plant for reducing filtration resistance |
| CN107789881A (en) * | 2017-11-17 | 2018-03-13 | 盱眙县生产力促进中心 | A kind of smart home sewage-treatment plant of replaceable filter screen |
| CN107792684A (en) * | 2017-11-22 | 2018-03-13 | 佛山市因诺维生物科技有限公司 | A kind of feeding mechanism for biomass extraction equipment |
| CN208098212U (en) * | 2017-12-29 | 2018-11-16 | 郑州网知汇信息科技有限公司 | It is a kind of for producing the grinding apparatus of brown fused alumina micropowder |
| CN108579178A (en) * | 2018-03-08 | 2018-09-28 | 浙江康豪诺特装饰材料有限公司 | A kind of filter with layered shaping function |
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Application publication date: 20190308 |
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| RJ01 | Rejection of invention patent application after publication |