CN109425562A - A kind of laser particle analyzer and its application for oil field reinjection water suspended matter partial size on-line monitoring - Google Patents
A kind of laser particle analyzer and its application for oil field reinjection water suspended matter partial size on-line monitoring Download PDFInfo
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- CN109425562A CN109425562A CN201710721543.6A CN201710721543A CN109425562A CN 109425562 A CN109425562 A CN 109425562A CN 201710721543 A CN201710721543 A CN 201710721543A CN 109425562 A CN109425562 A CN 109425562A
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- particle analyzer
- laser particle
- junction
- faying face
- pipeline
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N15/00—Investigating characteristics of particles; Investigating permeability, pore-volume, or surface-area of porous materials
- G01N15/02—Investigating particle size or size distribution
- G01N15/0205—Investigating particle size or size distribution by optical means, e.g. by light scattering, diffraction, holography or imaging
- G01N15/0211—Investigating a scatter or diffraction pattern
Abstract
A kind of laser particle analyzer for oil field reinjection water suspended matter partial size on-line monitoring provided by the invention, it include: laser, beam shaping system, sample cell system, fourier lense, photodetector and vacuum pump, the tool housing of the laser particle analyzer is tubular structure, the instrument outer diameter of the laser particle analyzer is less than the internal diameter of the pipeline of water injection pipeline, it is contactless between the laser particle analyzer and water injection pipeline, helicitic texture is used at the internal combustion of the laser particle analyzer, and sealing ring is used at faying face.The present invention also provides a kind of application of laser particle analyzer in oil field reinjection water suspended matter partial size on-line monitoring.The present invention devises outer dimension less than internal diameter of the pipeline, the laser particle analyzer with water-proof function, it is effectively applied in oil field reinjection water suspended matter partial size on-line monitoring, is immersed in water, easy, safety.
Description
Technical field
The present invention relates to oil field reinjection water water quality monitoring fields, more particularly to one kind to be used for oil field reinjection water suspended matter partial size
A kind of application of the laser particle analyzer of on-line monitoring and laser particle analyzer in oil field reinjection water suspended matter partial size on-line monitoring.
Background technique
After the investment exploitation of oil field, oil reservoir energy itself will be constantly consumed, and cause formation pressure constantly to decline, underground
Crude oil largely deaerates, and viscosity increases, and oil well output greatly reduces.In order to keep or improve formation pressure, higher harvesting is obtained
Rate, it is necessary to which oil field is filled the water.
It is largely oil field reinjection water used by oil-field flooding at present.If cannot find that suspended matter partial size does not reach in time
Target reinjected water is easy for blocking formation core, leads to the oil field underproduction.Therefore, it is necessary to carry out on-line checking to reinjected water.At present
Laser particle analyzer type is more, and most of is all use for laboratory instrument, offline inspection successively carries out field sampling, seals up for safekeeping, is real
Test room chemical examination, record data, feed back on-site.External particle size analyzer manufacturer starting is more early, and occupation rate of market is high.Comparative maturity has English
The Malvern (Malvern) of state, the Kurt (Coulter) in the U.S., French hila think (Cilas) company, German new bus too
Library (Sympatec), HORIBA company, Japan.Wherein the laser particle analyzer of Malvern company China's Mainland occupation rate most
It is more, it manufacture Mastersizer series particle size analyzers, single range, measurement particle size range be 0.02~2000 μm, can do wet process and
Drying measure.The development of domestic laser particle analyzer starts from the late nineteen eighties in last century, achieves certain progress in recent years, at present
Domestic many universities and research institution have all carried out the research of light scattering laser granularity Detection, such as University Of Chongqing, south China teacher successively
Model university, University Of Tianjin, Institutes Of Technology Of Nanjing, Shanghai ray machine institute, Harbin Institute of Technology etc..Occur Zhuhai " American-European gram ",
Jinan " micro-nano ", " essence new " in Chengdu, Dandong a series of manufacturers such as " hundred is special ".In measurement range, the repeatability of measurement, granularity
The Key Performance Indicators such as resolving power, reliability on still have certain gap with external product.
These existing instruments have problem jointly: whole process analytical cycle is long, not can be carried out on-line checking;Outer dimension
It is larger, do not have water-proof function, cannot be placed in filling pipe.
Summary of the invention
In view of this, the embodiment of the invention provides a kind of laser for oil field reinjection water suspended matter partial size on-line monitoring
A kind of application of particle size analyzer and laser particle analyzer in oil field reinjection water suspended matter partial size on-line monitoring.
In a first aspect, providing a kind of laser for oil field reinjection water suspended matter partial size on-line monitoring in the embodiment of the present invention
Particle size analyzer comprising: laser, beam shaping system, sample cell system, fourier lense, photodetector and vacuum pump, institute
The tool housing for stating laser particle analyzer is tubular structure, and the instrument outer diameter of the laser particle analyzer is less than the pipe of water injection pipeline
Road internal diameter, it is contactless between the laser particle analyzer and water injection pipeline, it is adopted at the internal combustion of the laser particle analyzer
With helicitic texture, and sealing ring is used at faying face.
Optionally, in some embodiments, the sealing ring is O-ring seal.
Optionally, in some embodiments, the outer path length at the instrument largest outside diameter of the laser particle analyzer and oil field note
The long ratio range of the internal diameter of the pipeline of waterpipe is 0.85~0.88.It is outer at the instrument largest outside diameter of the laser particle analyzer
The long ratio of the internal diameter of the pipeline of path length and water injection pipeline within the above range, can better ensure that laser particle analyzer is convenient
Increase the outer diameter of instrument as far as possible under the premise of reducing with inner wall of the pipe friction into water injection pipeline, increase the interior of instrument
Portion space.
Optionally, in some embodiments, the outer path length at the instrument largest outside diameter of the laser particle analyzer and oil field note
The long ratio of the internal diameter of the pipeline of waterpipe is 0.87.
Optionally, in some embodiments, the laser particle analyzer includes left end cap, left outside shell, right end cap and right casing,
The junction of the left end cap and left outside shell is denoted as the first junction, and the junction of the left outside shell and right casing is denoted as being
The junction of two junctions, the right casing and right end cap is denoted as third junction, includes the first knot at the internal combustion
At conjunction, the second junction and third junction;The docking smooth flat of the left end cap and left outside shell is denoted as the first faying face,
The docking smooth flat of the left outside shell and right casing is denoted as the second faying face, and the docking of the right casing and right end cap is smooth
Plane is denoted as third faying face, and the faying face includes the first faying face, the second faying face and third faying face.
Optionally, in some embodiments, a length of 46mm of the internal diameter of the pipeline of water injection pipeline, the laser particle analyzer
The a length of 40mm of outer diameter at instrument largest outside diameter.
Second aspect, the present invention also provides a kind of laser particle analyzers in oil field reinjection water suspended matter partial size on-line monitoring
Be less than the internal diameter of the pipeline of water injection pipeline using, wherein the instrument outer diameter of the laser particle analyzer, the laser particle analyzer with
It is contactless between water injection pipeline, helicitic texture is used at the internal combustion of the laser particle analyzer, and at faying face
Using sealing ring.
Optionally, in some embodiments, the laser particle analyzer is lifted by hawser, is put into water injection pipeline
Portion is submerged in oil field reinjection water, after instrument stabilizer, boots up detection.
Optionally, in some embodiments, laser particle analyzer is put into different depth, by the start and stop of vacuum pump, realized
Circulating sampling detection.Here " depth " refers to the depth of water inside oil-field flooding pipe.
Optionally, in some embodiments, the outer path length at the instrument largest outside diameter of the laser particle analyzer and oil field note
The long ratio range of the internal diameter of the pipeline of waterpipe is 0.85~0.88.
Optionally, in some embodiments, the outer path length at the instrument largest outside diameter of the laser particle analyzer and oil field note
The long ratio of the internal diameter of the pipeline of waterpipe is 0.87.
As can be seen from the above technical solutions, the embodiment of the present invention has the advantage that
The present invention devises outer dimension less than internal diameter of the pipeline, the laser particle analyzer with water-proof function, is there is effect
It uses in oil field reinjection water suspended matter partial size on-line monitoring, is immersed in water, easy, safety.In the present invention, laser particle size
It is not contacted between instrument and water injection pipeline, helicitic texture is used at the internal combustion of laser particle analyzer, and combining
Sealed horizontal is improved using sealing ring at face.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of the laser particle analyzer of the embodiment of the present invention;
Fig. 2 is the structural schematic diagram when laser particle analyzer of the embodiment of the present invention is applied in oil-field flooding pipe.
Appended drawing reference: 1, laser;2, beam shaping system;3, sample cell system;4, fourier lense;5, photodetection
Device;6, vacuum pump;7, water inlet pipe;8, outlet pipe;10, laser particle analyzer;11, sealing ring;12, screw thread;13, left end cap;14, left
Shell;15, right casing;16, right end cap;20, water injection pipeline;30, oil field reinjection water;40;Hawser.
Specific embodiment
In order to enable those skilled in the art to better understand the solution of the present invention, below in conjunction in the embodiment of the present invention
Attached drawing, technical scheme in the embodiment of the invention is clearly and completely described, it is clear that described embodiment is only
The embodiment of a part of the invention, instead of all the embodiments.Based on the embodiments of the present invention, ordinary skill people
The model that the present invention protects all should belong in member's every other embodiment obtained without making creative work
It encloses.
Description and claims of this specification and term " first ", " second ", " third ", " in above-mentioned attached drawing
The (if present)s such as four " are to be used to distinguish similar objects, without being used to describe a particular order or precedence order.It should manage
The data that solution uses in this way are interchangeable under appropriate circumstances, so that the embodiments described herein can be in addition to illustrating herein
Or the sequence other than the content of description is implemented.In addition, term " includes " and " having " and their any deformation, it is intended that
Cover it is non-exclusive include, for example, containing the process, method, system, product or equipment of a series of steps or units need not limit
In step or unit those of is clearly listed, but may include be not clearly listed or for these process, methods, produce
The other step or units of product or equipment inherently.
The laser particle analyzer 10 for oil field reinjection water suspended matter partial size on-line monitoring provided in the embodiment of the present invention, knot
It closes and gives the structural schematic diagram of the laser particle analyzer for oil field reinjection water suspended matter partial size on-line monitoring, packet shown in Fig. 1
It includes: laser 1, beam shaping system 2, sample cell system 3, fourier lense 4, photodetector 5 and vacuum pump 6, it is described to swash
The tool housing of light particle size analyzer 10 is tubular structure, and the instrument outer diameter of the laser particle analyzer 10 is less than the pipe of water injection pipeline
Road internal diameter, it is contactless between the laser particle analyzer 10 and water injection pipeline, in the internal combustion of the laser particle analyzer 10
Place uses helicitic texture, and sealing ring 11 is used at faying face.
In the particular embodiment, the sealing ring 11 is O-ring seal.
In the particular embodiment, the outer path length and oil-field flooding pipe at the instrument largest outside diameter of the laser particle analyzer 10
The long ratio range of the internal diameter of the pipeline in road 20 is 0.85~0.88.
In the particular embodiment, the outer path length and oil-field flooding pipe at the instrument largest outside diameter of the laser particle analyzer 10
The long ratio of the internal diameter of the pipeline in road 20 is 0.87.
In the particular embodiment, the laser particle analyzer 10 includes outside left end cap 13, left outside shell 14, right end cap 16 and the right side
The junction of shell 15, the left end cap 13 and left outside shell 14 is denoted as the first junction, the left outside shell 14 and right casing 15
Junction is denoted as the second junction, and the junction of the right casing 15 and right end cap 16 is denoted as third junction, it is described in
Portion junction includes the first junction, the second junction and third junction;The docking light of the left end cap 13 and left outside shell 14
Sliding plane is denoted as the first faying face, and the docking smooth flat of the left outside shell 14 and right casing 15 is denoted as the second faying face,
The docking smooth flat of the right casing 15 and right end cap 16 is denoted as third faying face, and the faying face includes first combining
Face, the second faying face and third faying face.
In the particular embodiment, a length of 46mm of the internal diameter of the pipeline of water injection pipeline 20, the laser particle analyzer 10
The a length of 40mm of outer diameter at instrument largest outside diameter.
The embodiment of the present invention also provides a kind of laser particle analyzer 10 in oil field reinjection water suspended matter partial size on-line monitoring
Application, as shown in Fig. 2, the instrument outer diameter of the laser particle analyzer 10 be less than water injection pipeline 20 internal diameter of the pipeline, it is described
It is contactless between laser particle analyzer 10 and water injection pipeline 20, screw thread is used at the internal combustion of the laser particle analyzer 10
Structure, and sealing ring 11 is used at faying face.Preferably, in order to meet the requirement being placed in instrument inside oil-field flooding pipe
(in the present embodiment, oil-field flooding bore is 46mm), 10 outer diameter of laser particle analyzer of the present invention is 40mm, overall length
335mm.Instrument configurations size is small, facilitates access for water injection pipeline 20.Tool housing use tubular structure, laser particle analyzer with
It is contactless between water injection pipeline, at the internal combustion of the laser particle analyzer use helicitic texture, and faying face it
Between plus O-ring sealing, have stronger waterproof ability.
In the particular embodiment, the laser particle analyzer 10 is lifted by hawser 40, is put into water injection pipeline 20
Portion is submerged in oil field reinjection water 30, after instrument stabilizer, boots up detection.Laser particle analyzer 10 of the present invention is led to
The lifting of hawser 40 is crossed, is put into inside oil-field flooding pipe 20, submerges in oil field reinjection water 30, after instrument stabilizer, boot up inspection
It surveys.After laser particle analyzer 10 is switched on, vacuum pump 6 starts, and the oil field reinjection water 30 in oil-field flooding pipe 20 is sucked sample cell system
System 3, to sample cell system 3 full of after water, vacuum pump 6 stops.Laser particle analyzer is put into different depth, passes through vacuum pump 6
Start and stop, may be implemented circulating sampling detection.After liquid stabilising in sample cell system 3, the laser that laser 1 is launched,
The collimator and extender of light beam is carried out by beam shaping system 2, injects sample cell system 3, and scattering light is converged by fourier lense 4
Gather photodetector 5, carries out the acquisition of photosignal.Collected photosignal is handled by inversion algorithm, is hanged
The distribution results of floating object partial size, to judge whether water filling is up to standard.
In the particular embodiment, the outer path length and oil-field flooding pipe at the instrument largest outside diameter of the laser particle analyzer 10
The long ratio range of the internal diameter of the pipeline in road 20 is 0.85~0.88.
In the particular embodiment, the outer path length and oil-field flooding pipe at the instrument largest outside diameter of the laser particle analyzer 10
The long ratio of the internal diameter of the pipeline in road 20 is 0.87.
The present invention devises outer dimension less than internal diameter of the pipeline, the laser particle analyzer with water-proof function, is there is effect
It uses in oil field reinjection water suspended matter partial size on-line monitoring, is immersed in water, easy, safety.
It is apparent to those skilled in the art that for convenience and simplicity of description, the system of foregoing description,
The specific work process of device and unit, can refer to corresponding processes in the foregoing method embodiment, and details are not described herein.
In embodiment provided herein, it should be understood that disclosed system, device and method can pass through
Other modes are realized.For example, the apparatus embodiments described above are merely exemplary, for example, the division of the unit,
Only a kind of logical function partition, there may be another division manner in actual implementation, such as multiple units or components can be with
In conjunction with or be desirably integrated into another system, or some features can be ignored or not executed.For the general technology of this field
Personnel, thought according to an embodiment of the present invention, there will be changes in the specific implementation manner and application range, to sum up institute
It states, the contents of this specification are not to be construed as limiting the invention.
Claims (10)
1. a kind of laser particle analyzer for oil field reinjection water suspended matter partial size on-line monitoring characterized by comprising laser
Device, beam shaping system, sample cell system, fourier lense, photodetector and vacuum pump, the instrument of the laser particle analyzer
Shell is tubular structure, and the instrument outer diameter of the laser particle analyzer is less than the internal diameter of the pipeline of water injection pipeline, the laser grain
It is contactless between degree instrument and water injection pipeline, helicitic texture is used at the internal combustion of the laser particle analyzer, and tying
Conjunction face place uses sealing ring.
2. laser particle analyzer according to claim 1, which is characterized in that the sealing ring is O-ring seal.
3. laser particle analyzer according to claim 1, which is characterized in that at the instrument largest outside diameter of the laser particle analyzer
Outer path length and the long ratio range of internal diameter of the pipeline of water injection pipeline be 0.85~0.88.
4. laser particle analyzer according to claim 1, which is characterized in that the laser particle analyzer includes left end cap, left outside
The junction of shell, right end cap and right casing, the left end cap and left outside shell is denoted as the first junction, outside the left outside shell and the right side
The junction of shell is denoted as the second junction, and the junction of the right casing and right end cap is denoted as third junction, it is described in
Portion junction includes the first junction, the second junction and third junction;The docking of the left end cap and left outside shell is smooth flat
Face is denoted as the first faying face, and the docking smooth flat of the left outside shell and right casing is denoted as the second faying face, described right outer
The docking smooth flat of shell and right end cap is denoted as third faying face, and the faying face includes the first faying face, the second faying face
With third faying face.
5. laser particle analyzer according to claim 1, which is characterized in that at the instrument largest outside diameter of the laser particle analyzer
Outer path length and the long ratio of internal diameter of the pipeline of water injection pipeline be 0.87.
6. laser particle analyzer according to claim 1, which is characterized in that the internal diameter of the pipeline of water injection pipeline is a length of
46mm, a length of 40mm of outer diameter at the instrument largest outside diameter of the laser particle analyzer.
7. a kind of application of laser particle analyzer in oil field reinjection water suspended matter partial size on-line monitoring, which is characterized in that described to swash
Light particle size analyzer is lifted by hawser, is put into inside water injection pipeline, is submerged in oil field reinjection water, after instrument stabilizer, is carried out
Booting detection;The instrument outer diameter of the laser particle analyzer be less than water injection pipeline internal diameter of the pipeline, the laser particle analyzer with
It is contactless between water injection pipeline, helicitic texture is used at the internal combustion of the laser particle analyzer, and at faying face
Using sealing ring.
8. application according to claim 7, which is characterized in that laser particle analyzer is put into different depth, passes through vacuum pump
Start and stop, realize circulating sampling detection.
9. application according to claim 7, which is characterized in that the outer diameter at the instrument largest outside diameter of the laser particle analyzer
The long ratio range of long and water injection pipeline internal diameter of the pipeline is 0.85~0.88.
10. application according to claim 7, which is characterized in that the laser particle analyzer includes left end cap, left outside shell, the right side
The junction of end cap and right casing, the left end cap and left outside shell is denoted as the first junction, the left outside shell and right casing
Junction is denoted as the second junction, and the junction of the right casing and right end cap is denoted as third junction, the internal junction
It include the first junction, the second junction and third junction at conjunction;The docking smooth flat of the left end cap and left outside shell note
As the first faying face, the docking smooth flat of the left outside shell and right casing is denoted as the second faying face, the right casing and
The docking smooth flat of right end cap is denoted as third faying face, and the faying face includes the first faying face, the second faying face and the
Three faying faces.
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