CN109402355A - A kind of 600MPa grades of hot rolling TRIP type dual phase steel and preparation method thereof - Google Patents

A kind of 600MPa grades of hot rolling TRIP type dual phase steel and preparation method thereof Download PDF

Info

Publication number
CN109402355A
CN109402355A CN201811639349.4A CN201811639349A CN109402355A CN 109402355 A CN109402355 A CN 109402355A CN 201811639349 A CN201811639349 A CN 201811639349A CN 109402355 A CN109402355 A CN 109402355A
Authority
CN
China
Prior art keywords
steel
hot rolling
dual phase
type dual
trip type
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201811639349.4A
Other languages
Chinese (zh)
Other versions
CN109402355B (en
Inventor
刘杰
郭佳
代晓莉
郭子峰
刘锟
李文远
陈斌
张旭
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shougang Group Co Ltd
Original Assignee
Shougang Group Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shougang Group Co Ltd filed Critical Shougang Group Co Ltd
Priority to CN201811639349.4A priority Critical patent/CN109402355B/en
Publication of CN109402355A publication Critical patent/CN109402355A/en
Application granted granted Critical
Publication of CN109402355B publication Critical patent/CN109402355B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/04Ferrous alloys, e.g. steel alloys containing manganese
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D1/00General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering
    • C21D1/18Hardening; Quenching with or without subsequent tempering
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D8/00Modifying the physical properties by deformation combined with, or followed by, heat treatment
    • C21D8/02Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of plates or strips
    • C21D8/0221Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of plates or strips characterised by the working steps
    • C21D8/0226Hot rolling
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/002Ferrous alloys, e.g. steel alloys containing In, Mg, or other elements not provided for in one single group C22C38/001 - C22C38/60
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/02Ferrous alloys, e.g. steel alloys containing silicon
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/06Ferrous alloys, e.g. steel alloys containing aluminium
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D2211/00Microstructure comprising significant phases
    • C21D2211/001Austenite
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D2211/00Microstructure comprising significant phases
    • C21D2211/005Ferrite
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D2211/00Microstructure comprising significant phases
    • C21D2211/008Martensite

Abstract

The present invention provides a kind of 600MPa grades of hot rolling TRIP type dual phase steels and preparation method thereof, it organizes to be retained austenite, martensite and ferrite, textura epidermoidea are as follows: the retained austenite of 4-6%, the martensite of 5-15%, remaining is ferrite, and has rodlike carbide in the ferrite;The steel subject organization are as follows: the retained austenite of 2-5%, the martensite of 25-40%, remaining is ferrite, and carbides-free is precipitated in the ferrite.The regulation plastic elongation intensity of steel of the present invention is 333-351MPa, and tensile strength 602-614MPa, elongation after fracture (80mm gauge length) is 23-25%.Steel of the invention can be applied to complicated automobile structure, chassis member, have preferable economy and application prospect.

Description

A kind of 600MPa grades of hot rolling TRIP type dual phase steel and preparation method thereof
Technical field
The invention belongs to the advanced high-strength steel technical fields of Hot Rolling Automobile, and in particular to a kind of 600MPa grades of hot rolling TRIP type Dual phase steel and preparation method thereof.
Background technique
Currently, the advanced high-strength steel of automobile hot rolling such as two-phase (DP) steel, phase-change induced plastic (TRIP) steel has been applied to vapour The preparation of bassinet structure part.In the actual production process, it has been found that traditional dual phase steel on many high drawability parts at Shape is difficult, it is difficult to meet the requirement of Automobile Design complexity punching structure part.And transformation induced plasticity steel is used, elongation percentage exists again Certain surplus capacity causes to waste, and strength grade is higher, and weldability is poorer, but the retained austenite in TRIP steel is outside The masterpiece used time, energy can be absorbed, undergoes phase transition induced plastic transformation, i.e. generation TRIP effect, improve safety coefficient.
Therefore the dual phase steel that a kind of high-intensitive, high ductibility has TRIP effect again is developed, not only can satisfy complicated punching press The requirement of structural member, and there is preferable economic serviceability, safety.
Summary of the invention
In view of this, passing through group the present invention provides a kind of 600MPa grades of hot rolling TRIP type dual phase steel and preparation method thereof The control of each phase component in knitting, the characteristics of making it have high intensity, high-elongation, TRIP effect.
First aspect present invention provides a kind of 600MPa grades of hot rolling TRIP type dual phase steel, including steel main body and covering steel master The surface layer of body, the microstructure of the 600MPa grades of hot rolling TRIP type dual phase steel is by ferrite, martensite, three kinds of retained austenite Phase composition;With volume percentage, the textura epidermoidea are as follows: the retained austenite of 4-6%, the martensite of 5-15%, remaining is There is the ferrite of rodlike Carbide Precipitation;The steel subject organization are as follows: the retained austenite of 2-5%, the martensite of 25-40%, Remaining is the ferrite that carbides-free is precipitated.
Preferably, average every within the scope of away from the 600MPa grades of hot rolling TRIP type two-phase steel surface 0-22 μ m thick The quantity of rodlike carbide in 1000 square microns is 23-27;It is average every within the scope of away from surface 22-43 μ m thick The quantity of rodlike carbide in 1000 square microns is 8-10;At 43 μm away from surface to thickness of strips half, nothing Carbide Precipitation.Carbide Precipitation is in the trend gradually successively decreased, the direct shadow of carbide precipitate distribution trend within the scope of skin depth Ring the formation of Steel Properties and retained austenite.
Preferably, the surface layer is 43 μm of span surface of steel plate of thickness range.
Preferably, the 600MPa grades of hot rolling TRIP type dual phase steel includes chemical component: by percentage to the quality, C 0.12-0.14%, Si 0.3-0.4%, Mn 1.5-1.7%, Al 0.35-0.45%, P≤0.014%, remaining is for Fe and not Evitable impurity.
Preferably, the retained austenite is film-form.Film-form retained austenite is able to ascend the elongation percentage of steel.
Preferably, the regulation plastic elongation intensity of the 600MPa grades of hot rolling TRIP type dual phase steel is 333-351MPa, tension Intensity is 602-614MPa, and the elongation after fracture under 80mm gauge length is 23-25%.
Second aspect of the present invention provides the preparation method of above-mentioned 600MPa grades of hot rolling TRIP type dual phase steel, and step includes:
S1, molten iron smelting cast to obtain the slab for meeting chemical component requirement, under inert gas protection heat slab Heat preservation;
S2, the slab after heat preservation is controlled into hot rolling, obtains hot rolled strip;
S3, hot rolled strip is controlled into cooling, batches to obtain product.
The present invention is double by the TRIP type that heat preservation, hot rolling, cooling, the process flow batched form above-mentioned specific microstructure Xiang Gang, coiling technique is conducive to the formation of film-form retained austenite after especially specific cooling.
Preferably, in step S1, the heat preservation is that slab is kept the temperature 1.5-2.5h at 1150-1250 DEG C, 99.99% High pure nitrogen protection.Heat preservation makes steel temperature uniformity.
Preferably, in step S2, the control hot rolling includes the roughing of 2-3 passage and 3-5 passage finish rolling, the roughing stagnation pressure Lower amount is 82-84%, and the finish rolling is at the uniform velocity rolled with the speed of 7-8m/s, and finish rolling overall reduction is 72-82%;The hot-rolled steel Tape thickness is 4.3-4.7mm.Heat preservation and course of hot rolling influence carbide precipitate distribution trend in steel.
Preferably, in step S3, the control cooling step includes: with the ultrafast cooling velocity of 40-55 DEG C/s by step Steel band water cooling obtained by S2 is to 690-710 DEG C, then air-cooled 20-30s, then again with the cooling velocity water cooling of 25-35 DEG C/s extremely 250-285℃;By steel strip coiling after cooling, then heap is cooled to room temperature.Cooling procedure influences steel surface layer and main body three-phase is multiple Close the formation of phase.Water cooling before air-cooled terminates the excessively high ferrite volume fraction that can be reduced in tissue of temperature, reduces prolonging for steel plate Stretch rate;Water cooling terminates the too low meeting of temperature so that ferrite volume fraction is excessive, reduces steel strength.Water cooling before batching terminates temperature It spends low, can to form a large amount of martensite in tissue, steel plate elongation percentage is greatly reduced;It is excessively high and can make that water cooling terminates temperature Deficiency is formed at martensite, reduces armor plate strength.
Compared with prior art, the invention has the following advantages that 600MPa grades of hot rolling TRIP type two-phase provided by the invention The regulation plastic elongation intensity of steel is up to 333-351MPa, and tensile strength is up to 602-614MPa, elongation after fracture (80mm mark Away from) up to 23-25%, it can be widely applied to complicated automobile structure, chassis member, not only can solve stamping process The punching press problem of middle complexity, and have certain forming advantage in bending flange, Bulging Process, and may be used also when external force TRIP effect occurs, safety coefficient is improved, there is preferable economic serviceability and application prospect.
Detailed description of the invention
Attached drawing 1 is morphology of carbides photo and power spectrum in the embodiment of the present invention 3.
Specific embodiment
To facilitate the understanding of the present invention, present invention work more comprehensively, is meticulously described below in conjunction with embodiment, but this hair Bright protection scope is not limited to embodiment in detail below.
Unless otherwise defined, all technical terms used hereinafter and the normally understood meaning of those skilled in the art It is identical.Technical term used herein is intended merely to the purpose of description specific embodiment, is not intended to the limitation present invention Protection scope.
Unless otherwise specified, various raw material, reagent, the instrument and equipment etc. used in the present invention, can pass through Market is commercially available or can be prepared by existing method.
First aspect present invention provides a kind of 600MPa grades of hot rolling TRIP type dual phase steel, including steel main body and covering steel master The surface layer of body, the surface layer with a thickness of 43 μm.The microstructure of the 600MPa grades of hot rolling TRIP type dual phase steel by ferrite, Three kinds of martensite, film-form retained austenite phase compositions;With volume percentage, the textura epidermoidea are as follows: the film-form of 4-6% Retained austenite, the martensite of 5-15%, remaining is ferrite, and has rodlike carbide in the ferrite;The steel master Body tissue are as follows: the film-form retained austenite of 2-5%, the martensite of 25-40%, remaining is ferrite, and in the ferrite Middle carbides-free is precipitated.Specifically, the rodlike carbonization within the scope of away from surface 0-22 μ m thick, in average every 1000 square micron The quantity of object is 23-27;Rodlike carbide within the scope of away from surface 22-43 μ m thick, in average every 1000 square micron Quantity be 8-10;At 43 μm away from surface to thickness of strips half, carbides-free is precipitated.The change of TRIP type dual phase steel Study point includes: C 0.12-0.14%, Si 0.3-0.4%, Mn 1.5-1.7%, Al 0.35- by percentage to the quality 0.45%, P≤0.014%, remaining is Fe and inevitable impurity.
The regulation plastic elongation intensity of above-mentioned 600MPa grades of hot rolling TRIP type dual phase steel is 333-351MPa, and tensile strength is Elongation after fracture under 602-614MPa, 80mm gauge length is 23-25%.
Second aspect of the present invention provides the preparation method of above-mentioned 600MPa grades of hot rolling TRIP type dual phase steel, and step includes:
S1, molten iron smelting cast to obtain the slab for meeting chemical component requirement, will under 99.99% high pure nitrogen protection Slab is heated to 1150-1250 DEG C and keeps the temperature 1.5-2.5h;
S2, the slab after heat preservation is controlled into hot rolling, the control hot rolling includes the roughing of 2-3 passage and 3-5 passage finish rolling, institute Stating roughing overall reduction is 82-84%, and the finish rolling is at the uniform velocity rolled with the speed of 7-8m/s, and finish rolling overall reduction is 75-82%, Obtain the hot rolled strip of thickness 4.3-4.7mm;
S3, hot rolled strip is cooled to 690-720 DEG C with the cooling velocity of 40-55 DEG C/s, then air-cooled 20-30s, then 250-280 DEG C is cooled to again with the cooling velocity of 35-35 DEG C/s;By steel strip coiling after cooling, then heap is cooled to room temperature and obtains Product.
Below in conjunction with five specific embodiments to the 600MPa grade hot rolling TRIP type dual phase steel of the application and its preparation side Method is described in detail.
Embodiment 1
A kind of preparation method of 600MPa grades of hot rolling TRIP type dual phase steel is present embodiments provided, step includes:
Slab is heated to 1200 DEG C of heat preservation 2h under 99.99% high pure nitrogen protection, with purity 99.99% when heating Nitrogen protected.The chemical component of the slab forms are as follows: it is calculated in mass percent, C:0.124%, Si:0.39%, Mn:1.67%, Alt:0.42%, P:0.014%, remaining is Fe and inevitable impurity.
By the slab after heating and thermal insulation in 1180 DEG C of beginning hot rollings, hot rolling technology is controlled are as follows: carry out 3 passage roughing, roughing Overall reduction is 83%, then carries out 4 passage finish rolling, and the finish rolling is at the uniform velocity rolled with the speed of 7.5m/s, finish rolling extreme trace time entrance Temperature is 880 DEG C, and finish rolling overall reduction is 79%, obtains the hot rolled strip of 4.5mm thickness;
Obtained hot rolled strip is subjected to control cooling, control hot rolled strip tissue is ferrite, martensite, residual austenite Body three-phase contexture.Specific Controlled cooling process are as follows: then air-cooled with the cooling velocity of 50 DEG C/s by steel band water cooling to 700 DEG C 25s, then again with the cooling velocity of 30 DEG C/s by steel band water cooling to 275 DEG C;By steel strip coiling after cooling, then heap is cooled to room Temperature obtains product.
The 600MPa grade hot rolling TRIP type dual phase steel being prepared using above-mentioned preparation method, microstructure by ferrite, Three kinds of martensite, film-form retained austenite phase compositions.Each phase percentage (percent by volume, %) of textura epidermoidea are as follows: 4.8% Retained austenite, 8.6% martensite, remaining is ferrite, there is rodlike carbide in ferrite.Outside skim-coat tissue Steel subject organization each phase percentage are as follows: 2.5% retained austenite, 31% martensite, remaining is ferrite, carbon-free Compound is precipitated;Within the scope of away from surface 0-22 μ m thick, the quantity of the rodlike carbide in average every 1000 square micron is 23 It is a;Within the scope of 22 μm -343 away from surface μ m thick, the quantity of the rodlike carbide in average every 1000 square micron is 10; At the half away from the 43 μm-whole thickness in surface, without Carbide Precipitation;Retained austenite in tissue is film Shape.
The regulation plastic elongation intensity for the hot-rolled dual-phase steel that the present embodiment obtains after measured is 351MPa, and tensile strength is 614MPa, elongation after fracture (80mm gauge length) are 23.5%.
Embodiment 2
A kind of 600MPa grades of hot rolling TRIP type dual phase steel is present embodiments provided, using system substantially the same manner as Example 1 Standby step, different is: its Chemical Composition in Cast Billet are as follows: is calculated in mass percent, C:0.131%, Si:0.36%, Mn: 1.55%, Alt:0.45%, P:0.012%, remaining is Fe and inevitable impurity.
Obtained 600MPa grade hot rolling TRIP type dual phase steel microstructure is by ferrite, martensite, film-form residual austenite Three kinds of phase compositions of body.Each phase percentage (percent by volume, %) of textura epidermoidea are as follows: 5.2% retained austenite, 11% horse Family name's body, remaining is ferrite, there is rodlike carbide in ferrite.Each phase hundred of the subject organization of steel outside skim-coat tissue Divide ratio are as follows: 3.5% retained austenite, 38% martensite, remaining is ferrite, and carbides-free is precipitated;Away from surface 0-22 μ In m thickness range, the quantity of the rodlike carbide in average every 1000 square micron is 26;In 22 μm -343 away from surface μ m-thick It spends in range, the quantity of the rodlike carbide in average every 1000 square micron is 8;Away from the 43 μm-whole thickness in surface At half, without Carbide Precipitation;Retained austenite in tissue is film-form.
The regulation plastic elongation intensity for the hot-rolled dual-phase steel that the present embodiment obtains after measured is 337MPa, and tensile strength is 613MPa, elongation after fracture (80mm gauge length) are 24.5%.
Embodiment 3
A kind of 600MPa grades of hot rolling TRIP type dual phase steel is present embodiments provided, using system substantially the same manner as Example 1 Standby step, different is: Chemical Composition in Cast Billet mass percent is C:0.136%, Si:0.34%, Mn:1.61%, Alt: 0.37%, P:0.014%, remaining is Fe and inevitable impurity.
Obtained 600MPa grade hot rolling TRIP type dual phase steel microstructure is by ferrite, martensite, film-form residual austenite Three kinds of phase compositions of body.Each phase percentage (percent by volume, %) of textura epidermoidea are as follows: 4.4% retained austenite, 9% horse Family name's body, remaining is ferrite, there is rodlike carbide in ferrite.Each phase hundred of the subject organization of steel outside skim-coat tissue Divide ratio are as follows: 2.5% retained austenite, 29% martensite, remaining is ferrite, and carbides-free is precipitated;Away from surface 0-22 μ In m thickness range, the quantity of the rodlike carbide in average every 1000 square micron is 27;In 22 μm -343 away from surface μ m-thick It spends in range, the quantity of the rodlike carbide in average every 1000 square micron is 10;Away from the 43 μm-whole thickness in surface At half, without rodlike Carbide Precipitation;Retained austenite in tissue is film-form.
The pattern photo of carbide and power spectrum are as shown in Fig. 1 in the present embodiment, and the corresponding specific data of power spectrum are such as in Fig. 1 Shown in table 1.
Carbide power spectrum in 1 embodiment 3 of table
The regulation plastic elongation intensity for the hot-rolled dual-phase steel that the present embodiment obtains after measured is 333MPa, and tensile strength is 602MPa, elongation after fracture (80mm gauge length) are 24%.
Comparative example 1
The dual phase steel Chemical Composition in Cast Billet that this comparative example provides is same as Example 3, using substantially the same manner as Example 3 Preparation step, different is: hot rolling uses+5 passage finish rolling of 2 passage roughing, and roughing overall reduction is 60%, under finish rolling stagnation pressure 77.5%, finish rolling 860 DEG C of inlet temperature of extreme trace time is air-cooled to 670 DEG C after finish rolling, then water cooling is batched to 450 DEG C, volume Rear heap is taken to be cooled to room temperature.
The institute for the dual phase steel that this comparative example provides is organized by 55% ferrite and two kinds of bainite of 45% in a organized way It constitutes, the regulation plastic elongation intensity of obtained hot-rolled dual-phase steel is 449MPa, tensile strength 592MPa, elongation after fracture (80mm gauge length) is 20%.
In conjunction with the embodiment of the present invention and the chemical component preparation process and mechanical property of comparison it follows that institute of the present invention There are embodiment better performances, the regulation plastic elongation intensity of obtained 600MPa grade hot rolling TRIP type dual phase steel is 333- 351MPa, tensile strength 602-614MPa, elongation after fracture (80mm gauge length) are 23-25%.Tissue is ferrite, geneva Body, retained austenite three-phase contexture, and contain rodlike carbide in the ferritic structure of surface layer.The chemical component of comparative example although with Embodiment is identical, but organizational controls is different, and obtained tissue is ferrite and bainite, and row's carbon is insufficient in ferrite, not formed Retained austenite does not obtain lower regulation plastic elongation intensity, higher tensile strength and higher elongation percentage, and it is even more impossible to shapes At TRIP effect.
Embodiment 4
A kind of preparation method of 600MPa grades of hot rolling TRIP type dual phase steel is present embodiments provided, step includes:
Slab is heated to 1180 DEG C of heat preservation 2.5h, when heating is protected with the nitrogen of purity 99.99%.The slab Chemical component composition are as follows: be calculated in mass percent, C:0.124%, Si:0.39%, Mn:1.67%, Alt:0.42%, P: 0.014%, remaining is Fe and inevitable impurity.
By the slab after heating and thermal insulation in 1150 DEG C of beginning hot rollings, hot rolling technology is controlled are as follows: carry out 3 passage roughing, roughing Overall reduction is 83%, then carries out 4 passage finish rolling, and the finish rolling is at the uniform velocity rolled with the speed of 7m/s, finish rolling extreme trace time entrance temperature Degree is 850 DEG C, and finish rolling overall reduction is 76%, obtains the hot rolled strip of 4.7mm thickness;
Obtained hot rolled strip is subjected to control cooling, control hot rolled strip tissue is ferrite, martensite, residual austenite Body three-phase contexture.Specific Controlled cooling process are as follows: be cooled to 690 DEG C with the cooling velocity of 52 DEG C/s, then air-cooled 20s, then 265 DEG C are cooled to again with the cooling velocity of 25 DEG C/s;By steel strip coiling after cooling, then heap is cooled to room temperature and obtains product.Institute It obtains properties of product and embodiment 1 is almost the same.
Embodiment 5
A kind of preparation method of 600MPa grades of hot rolling TRIP type dual phase steel is present embodiments provided, step includes:
Slab is heated to 1250 DEG C of heat preservation 1.5h, when heating is protected with the nitrogen of purity 99.99%.The slab Chemical component composition are as follows: be calculated in mass percent, C:0.124%, Si:0.39%, Mn:1.67%, Alt:0.42%, P: 0.014%, remaining is Fe and inevitable impurity.
By the slab after heating and thermal insulation in 1220 DEG C of beginning hot rollings, hot rolling technology is controlled are as follows: carry out 3 passage roughing, roughing Overall reduction is 83%, then carries out 4 passage finish rolling, and the finish rolling is at the uniform velocity rolled with the speed of 8m/s, finish rolling extreme trace time entrance temperature Degree is 860 DEG C, and finish rolling overall reduction is 82%, obtains the hot rolled strip of 4.3mm thickness;
Obtained hot rolled strip is subjected to control cooling, control hot rolled strip tissue is ferrite, martensite, residual austenite Body three-phase contexture.Specific Controlled cooling process are as follows: then air-cooled with the cooling velocity of 45 DEG C/s by steel band water cooling to 710 DEG C 20s, then again with the cooling velocity of 28 DEG C/s by steel band water cooling to 275 DEG C;By steel strip coiling after cooling, then heap is cooled to room Temperature obtains product.Products obtained therefrom performance and embodiment 1 are almost the same.
Although preferred embodiments of the present invention have been described, it is created once a person skilled in the art knows basic Property concept, then additional changes and modifications may be made to these embodiments.So it includes excellent that the following claims are intended to be interpreted as It selects embodiment and falls into all change and modification of the scope of the invention.
Obviously, various changes and modifications can be made to the invention without departing from essence of the invention by those skilled in the art Mind and range.In this way, if these modifications and changes of the present invention belongs to the range of the claims in the present invention and its equivalent technologies Within, then the present invention is also intended to include these modifications and variations.

Claims (10)

1. a kind of 600MPa grades of hot rolling TRIP type dual phase steel, the surface layer including steel main body and covering steel main body, it is characterised in that: institute The microstructure of 600MPa grades of hot rolling TRIP type dual phase steels is stated by three kinds of ferrite, martensite, retained austenite phase compositions;With body Product percentages, the textura epidermoidea are as follows: the retained austenite of 4-6%, the martensite of 5-15%, remaining is to have rodlike carbide The ferrite of precipitation;The steel subject organization are as follows: the retained austenite of 2-5%, the martensite of 25-40%, remaining is Non-carbonized The ferrite that object is precipitated.
2. 600MPa grades of hot rolling TRIP type dual phase steel as described in claim 1, it is characterised in that: away from the 600MPa grades of heat It rolls within the scope of TRIP type two-phase steel surface 0-22 μ m thick, the quantity of the rodlike carbide in average every 1000 square micron is 23-27;Within the scope of away from surface 22-43 μ m thick, the quantity of the rodlike carbide in average every 1000 square micron is 8- 10;At 43 μm away from surface to thickness of strips half, carbides-free is precipitated.
3. 600MPa grades of hot rolling TRIP type dual phase steel as described in claim 1, it is characterised in that: the surface layer is span steel plate The thickness range that 43 μm of surface.
4. 600MPa described in claim 1- grades of hot rolling TRIP type dual phase steel, it is characterised in that: by percentage to the quality, including Chemical component: C 0.12-0.14%, Si 0.3-0.4%, Mn 1.5-1.7%, Al0.35-0.45%, P≤0.014%, Remaining is Fe and inevitable impurity.
5. the 600MPa grade hot rolling TRIP type dual phase steel as described in any one of claim 1-4 claim, it is characterised in that: institute Stating retained austenite is film-form.
6. 600MPa grades of hot rolling TRIP type dual phase steel as described in claim 1, it is characterised in that: the 600MPa grades of hot rolling TRIP The regulation plastic elongation intensity of type dual phase steel is 333-351MPa, having no progeny under tensile strength 602-614MPa, 80mm gauge length Elongation is 23-25%.
7. the preparation method of 600MPa described in claim 1 grades of hot rolling TRIP type dual phase steel, step include:
S1, molten iron smelting cast to obtain the slab for meeting chemical component requirement, and slab is heated and protected under inert gas protection Temperature;
S2, the slab after heat preservation is controlled into hot rolling, obtains hot rolled strip;
S3, hot rolled strip is controlled into cooling, batches to obtain product.
8. the preparation method of 600MPa grades of hot rolling TRIP type dual phase steel as claimed in claim 7, it is characterised in that: in step S1, For slab is kept the temperature 1.5-2.5h at 1150-1250 DEG C, 99.99% high pure nitrogen is protected for the heat preservation.
9. the preparation method of 600MPa grades of hot rolling TRIP type dual phase steel as claimed in claim 7, it is characterised in that: step S2 In, the control hot rolling includes the roughing of 2-3 passage and 3-5 passage finish rolling, and the roughing overall reduction is 82-84%, the essence It rolls and is at the uniform velocity rolled with the speed of 9m/s, finish rolling overall reduction is 75-82%;The hot rolled strip thickness 4.3-4.7mm.
10. the preparation method of 600MPa grades of hot rolling TRIP type dual phase steel as claimed in claim 9, it is characterised in that: step S3 In, the control cooling step includes: by steel band water cooling obtained by step S2 with the cooling velocity of 40-55 DEG C/s to 690-720 DEG C, Then air-cooled 20-30s, then again with the cooling velocity water cooling of 25-35 DEG C/s to 250-285 DEG C;By steel strip coiling after cooling, Then heap is cooled to room temperature.
CN201811639349.4A 2018-12-29 2018-12-29 600 MPa-grade hot-rolled TRIP type dual-phase steel and preparation method thereof Active CN109402355B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201811639349.4A CN109402355B (en) 2018-12-29 2018-12-29 600 MPa-grade hot-rolled TRIP type dual-phase steel and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201811639349.4A CN109402355B (en) 2018-12-29 2018-12-29 600 MPa-grade hot-rolled TRIP type dual-phase steel and preparation method thereof

Publications (2)

Publication Number Publication Date
CN109402355A true CN109402355A (en) 2019-03-01
CN109402355B CN109402355B (en) 2020-12-15

Family

ID=65462162

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201811639349.4A Active CN109402355B (en) 2018-12-29 2018-12-29 600 MPa-grade hot-rolled TRIP type dual-phase steel and preparation method thereof

Country Status (1)

Country Link
CN (1) CN109402355B (en)

Citations (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5585626A (en) * 1978-11-14 1980-06-27 Nisshin Steel Co Ltd Manufacture of low alloy steel sheet or hoop for precise punching
CN102321845A (en) * 2011-09-21 2012-01-18 首钢总公司 A kind of high-strength hot-rolled dual-phase steel and method of manufacture thereof
CN102517496A (en) * 2011-12-23 2012-06-27 首钢总公司 Hot rolled ferrite/martensite double phase steel and production method thereof
CN102650017A (en) * 2012-05-25 2012-08-29 宝山钢铁股份有限公司 Hot-rolled steel plate and manufacturing method thereof
CN102719732A (en) * 2012-06-28 2012-10-10 宝山钢铁股份有限公司 Hot-rolled high-strength dual phase steel plate and manufacturing method thereof
CN103233161A (en) * 2013-04-09 2013-08-07 宝山钢铁股份有限公司 Low-yield-ratio high-strength hot-rolled Q&P steel and manufacturing method thereof
KR20140018580A (en) * 2012-08-02 2014-02-13 주식회사 포스코 Hot-rolled steel sheet for steel pipe having excellent surface integrity and method for manufacturing the same
CN104105807A (en) * 2012-02-08 2014-10-15 新日铁住金株式会社 High-strength cold-rolled steel sheet and process for manufacturing same
WO2015127523A1 (en) * 2014-02-28 2015-09-03 Vallourec Tubos Do Brasil S.A. Martensitic-ferritic stainless steel, manufactured product and processes using the same
CN106119703A (en) * 2016-06-21 2016-11-16 宝山钢铁股份有限公司 A kind of 980MPa level hot-rolled dual-phase steel and manufacture method thereof
CN108950383A (en) * 2018-06-25 2018-12-07 敬业钢铁有限公司 A kind of high-strength and high-plasticity enhancing backplate cold-rolled steel sheet and its production technology

Patent Citations (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5585626A (en) * 1978-11-14 1980-06-27 Nisshin Steel Co Ltd Manufacture of low alloy steel sheet or hoop for precise punching
CN102321845A (en) * 2011-09-21 2012-01-18 首钢总公司 A kind of high-strength hot-rolled dual-phase steel and method of manufacture thereof
CN102517496A (en) * 2011-12-23 2012-06-27 首钢总公司 Hot rolled ferrite/martensite double phase steel and production method thereof
CN104105807A (en) * 2012-02-08 2014-10-15 新日铁住金株式会社 High-strength cold-rolled steel sheet and process for manufacturing same
CN102650017A (en) * 2012-05-25 2012-08-29 宝山钢铁股份有限公司 Hot-rolled steel plate and manufacturing method thereof
CN102719732A (en) * 2012-06-28 2012-10-10 宝山钢铁股份有限公司 Hot-rolled high-strength dual phase steel plate and manufacturing method thereof
KR20140018580A (en) * 2012-08-02 2014-02-13 주식회사 포스코 Hot-rolled steel sheet for steel pipe having excellent surface integrity and method for manufacturing the same
CN103233161A (en) * 2013-04-09 2013-08-07 宝山钢铁股份有限公司 Low-yield-ratio high-strength hot-rolled Q&P steel and manufacturing method thereof
WO2015127523A1 (en) * 2014-02-28 2015-09-03 Vallourec Tubos Do Brasil S.A. Martensitic-ferritic stainless steel, manufactured product and processes using the same
CN106119703A (en) * 2016-06-21 2016-11-16 宝山钢铁股份有限公司 A kind of 980MPa level hot-rolled dual-phase steel and manufacture method thereof
CN108950383A (en) * 2018-06-25 2018-12-07 敬业钢铁有限公司 A kind of high-strength and high-plasticity enhancing backplate cold-rolled steel sheet and its production technology

Also Published As

Publication number Publication date
CN109402355B (en) 2020-12-15

Similar Documents

Publication Publication Date Title
CN103361547B (en) A kind of production method of cold formability ultrahigh-strength steel plates and steel plate
CN108486494B (en) The production method of vanadium micro-alloying 1300MPa grade high-strength hot rolled steel plate and cold-rolled biphase steel plate
CN103233161B (en) A kind of low yield strength ratio high-strength hot-rolled Q & P steel and manufacture method thereof
CN106256918B (en) A kind of the Automobile flywheel cold-strip steel and its manufacturing method of precision stamping processing
CN103805851B (en) A kind of superstrength low cost hot rolling Q & P steel and production method thereof
CN104593675A (en) Preparation method of metal material with TWIP (twinning induced plasticity) and TRIP (transformation of retained austenite induced plasticity) effects
CN103215516A (en) 700MPa high strength hot rolling Q&P steel and manufacturing method thereof
CN108018484A (en) A kind of tensile strength is in more than 1500MPa and the cold rolling high-strength steel and its manufacture method that have excellent moldability
KR20100019443A (en) Low density steel with good stamping capability
CN103805869A (en) High-strength hot-rolled Q and P steel and manufacturing method thereof
CN108707823A (en) Ultrahigh-strength steel plates and preparation method thereof and unimach slab products
CN104862597A (en) Method for improving elongation of cold-rolled dual-phase steel by utilizing retained austenite
CN108431280A (en) High yield is than type high strength cold rolled steel plate and its manufacturing method
CN103103438A (en) High-strength and high-plasticity medium manganese cold-roll steel sheet and manufacturing method thereof
CN108342655A (en) A kind of quenching and tempering type acid-resistant pipeline steel and its manufacturing method
CN109252107A (en) A kind of production method of high straightness super-high strength steel
WO2002077310A1 (en) High strength and high ductility steel plate having hyperfine crystal grain structure produced by subjecting ordinary low carbon steel to low strain working and annealing, and method for production thereof
CN105925905B (en) 780MPa grades of hot-rolled dual-phase steels of Nb-Ti systems and its production method
CN101003878A (en) Low yield ratio fire-resistant steel
CN106498297A (en) Precision stamping automotive seat actuator fluted disc cold-rolled steel sheet and its manufacture method
CN109112416A (en) A kind of cold-rolled steel sheet and its manufacturing method of the high Oxygen potential of precision stamping
CN105950970B (en) Tough automobile steel of a kind of compound bainite high-strength of Ultra-fine Grained and preparation method thereof
CN109554616A (en) A kind of 700MPa grades of hot rolling TRIP auxiliary type dual phase steel and preparation method thereof
CN108504925A (en) A kind of short route hot rolling Q&P steel plates and preparation method thereof
CN100500915C (en) Dual phase steel of ferrite and bainite

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant